Patents by Inventor James M. Tour

James M. Tour has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11958006
    Abstract: Virus and microbe-killing, self-sterilizing resistive heated air filters and methods of making and using same methods. The air filter is includes laser-induced graphene (LIG), a porous conductive graphene foam formed through photothermal conversion of a polyimide film (or another source or source of polymer or other LIG precursor material) by a laser source. The LIG in the air filter can capture particulates and bacteria. The bacteria cannot proliferate even when submerged in culture medium. Through a periodic Joule-heating mechanism, the filter easily reaches greater than 300° C. This destroys any microorganisms including bacteria, along with molecules that can cause adverse biological reactions and diseases such as viruses, pyrogens, allergens, exotoxins, endotoxins, teichoic acids, mycotoxins, nucleic acids, and prions.
    Type: Grant
    Filed: August 10, 2020
    Date of Patent: April 16, 2024
    Assignees: William Marsh Rice University, B.G. Negev Technologies and Applications Ltd., at Ben-Gurion University
    Inventors: James M. Tour, Michael G. Stanford, John Li, Yieu Chyan, Christopher John Arnusch, Steven E. Presutti
  • Publication number: 20240116094
    Abstract: Method and system for soil remediation by flash Joule heating. A contaminated soil that includes organic pollutants and/or one or more metal pollutants can be mixed with carbon black or other conductive additive to form a mixture. The mixture then undergoes flash Joule heating to clean the soil (by the decomposing of the organic pollutants and/or removing of the one or more toxic metals, such as by vaporization).
    Type: Application
    Filed: February 2, 2022
    Publication date: April 11, 2024
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Bing Deng
  • Publication number: 20240100502
    Abstract: Rigid porous polymeric carbon sorbents, including particularly polymeric carbon sorbents for CO2 capture for flue gas from power plants and for gases from other post combustion CO2 emission outlets, and methods of making and using same. The porous carbon material can be prepared by heating plastic with an additive. The additive can be selected from metal hydroxide, metal oxalate, metal acetate, metal acetylacetonoate or mixtures thereof. By controlling the preparation, such as the temperature of preparation, the porous carbon sorbent can be controlled to be rigid.
    Type: Application
    Filed: October 14, 2020
    Publication date: March 28, 2024
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Wala Algozeeb, Paul E. Savas, Jr., Wilbur Carter Kittrell
  • Publication number: 20230374623
    Abstract: Ultrafast flash Joule heating synthesis methods and systems, and more particularly, ultrafast synthesis methods to recover metal from ores, fly ash, and bauxite residue (red mud).
    Type: Application
    Filed: September 24, 2021
    Publication date: November 23, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Bing Deng
  • Publication number: 20230357885
    Abstract: Ultrafast flash Joule heating synthesis methods and systems, and more particularly, ultrafast synthesis methods to recover precious metals recovery and other metals from electronic waste (e-waste).
    Type: Application
    Filed: September 24, 2021
    Publication date: November 9, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Bing Deng
  • Patent number: 11807533
    Abstract: Laser-induced graphene (LIG) and laser-induced graphene scrolls (LIGS) materials and, more particularly to LIGS, methods of making LIGS (such as from polyimide (PI)), laser-induced removal of LIG and LIGS, and 3D printing of LIG and LIGS using a laminated object manufacturing (LOM) process.
    Type: Grant
    Filed: November 23, 2020
    Date of Patent: November 7, 2023
    Assignee: William Marsh Rice University
    Inventors: James M. Tour, Duy X. Luong, Ajay Subramanian
  • Publication number: 20230327113
    Abstract: Embodiments of the present disclosure pertain to electrodes for energy storage devices. The electrodes include a substrate from which extends bundles of carbon nanotubes. A metal, such as lithium, infiltrates the bundles, between the carbon nanotubes, to coat the surfaces of the carbon nanotubes. The bundled, metal-coated carbon nanotubes are covered with a layer of solid-electrolyte interphase that can be formed before the metal is inserted into the bundles by pretreating the bundles with an electrolyte bearing ions of the metal.
    Type: Application
    Filed: February 10, 2023
    Publication date: October 12, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Abdul-Rahman O. Raji, Rodrigo V. Salvatierra
  • Publication number: 20230299291
    Abstract: Energy-storage devices in which the energy storage device has an electrode that includes graphitic carbon, carbon nanotubes, and a metallic-lithium layer between the carbon nanotubes and the energy-storage device further has an electrolyte that is in contact with the metallic lithium layer. The methods of manufacturing the energy-storage devices include that the energy storage device is made by providing electrodes that have a layer of carbon nanotubes adjacent additional carbon, applying a layer of lithium between the carbon nanotubes in the layer of carbon nanotubes of at least one of the electrodes, and providing an electrolyte between the electrodes.
    Type: Application
    Filed: April 21, 2023
    Publication date: September 21, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M Tour, Abdul-Rahman O Raji, Rodrigo V Salvatierra
  • Publication number: 20230253545
    Abstract: Anodes, cathodes, and separators for batteries (electrochemical energy storage devices). The anodes are Li metal anodes having lithiated carbon films (Li-MWCNT) (as dendrite suppressors and protective coatings for the Li metal anodes). The cathodes are sulfurized carbon cathodes. The separators are GNR-coated (or modified) separators. The invention includes each of these separately (as well as in combination both with each other and with other anodes, cathodes, and separators) and the methods of making each of these separately (and in combination). The invention further includes a battery that uses at least one of (a) the anode having a lithiated carbon film, (b) the sulfurized carbon cathode, and (c) the GNR-modified separator in the anode/cathode/separator arrangement. For instance, a full battery can include the sulfurized carbon cathode in combination with the Li-MWCNT anode or a full battery can include the sulfurized carbon cathode in combination with other anodes (such as a GCNT-Li anode).
    Type: Application
    Filed: March 8, 2023
    Publication date: August 10, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Rodrigo Villegas Salvatierra, Gladys Anahi Lopez Silva
  • Publication number: 20230241245
    Abstract: A therapeutic method for catalytically forming persulfide and/or polysulfide from hydrogen sulfide in vitro and in vivo using endogenously or exogenously released hydrogen sulfide is disclosed. That method comprises contacting cells in need including those under oxidative stress, traumatic brain injury (TBI) and hypoxia, or have an excess of hydrogen sulfide or deficiency of protein persulfidation with oxidized carbon nanoparticulate material in which the particles contain a plurality of carbonyl, hydroxyl and carboxyl substituents. Oxidized carbon nanoparticulate (OCN) material can be prepared from any of a variety of sources of which activated charcoal is preferred. A water-dispersible OCN material is described that does not need added hydrophilic polymers to provide dispersibility for at least 7 days at a concentration of about 1-5 mg/mL. These OCN materials also have a UV absorbance maximum in water of about 220 nm and pass through a 0.22 µm pore PES membrane.
    Type: Application
    Filed: June 7, 2021
    Publication date: August 3, 2023
    Applicants: The Texas A&M University System, William Marsh Rice University, The Trustees of Indiana University
    Inventors: Thomas A. KENT, Paul J. DERRY, David P. HUSTON, Anton V. LIOPO, James M. TOUR, Emily M. McHUGH, Kimberly MENDOZA, Kenneth R. OLSON, Mansoor KAHN
  • Publication number: 20230173419
    Abstract: Virus and microbe-killing, self-sterilizing resistive heated air filters and methods of making and using same methods. The air filter is includes laser-induced graphene (LIG), a porous conductive graphene foam formed through photothermal conversion of a polyimide film (or another source or source of polymer or other LIG precursor material) by a laser source. The LIG in the air filter can capture particulates and bacteria. The bacteria cannot proliferate even when submerged in culture medium. Through a periodic Joule-heating mechanism, the filter easily reaches greater than 300° C.
    Type: Application
    Filed: August 10, 2020
    Publication date: June 8, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Michael G. Stanford, John Li, Yieu Chyan, Christopher John Arnusch, Steven E. Presutti
  • Publication number: 20230149567
    Abstract: Embodiments of the present disclosure pertain to methods of opening a lipid bilayer by associating the lipid bilayer with a molecule that includes a moving component capable of moving (e.g., rotating) in response to an external stimulus; and exposing the molecule to an external stimulus before, during or after associating the molecule with the lipid bilayer. The exposing causes the moving component of the molecule to move and thereby open the lipid bilayer (e.g., by pore formation). The external stimuli may include an energy source, such as ultraviolet light. The opened lipid bilayer may be a component of cell membranes in vitro or in vivo. The opening of the lipid bilayer may allow for the passage of various materials (e.g., active agents, such as peptide-based drugs) through the lipid bilayer and into cells. Additional embodiments of the present disclosure pertain to the aforementioned molecules for opening lipid bilayers.
    Type: Application
    Filed: January 4, 2023
    Publication date: May 18, 2023
    Applicants: William Marsh Rice University, Durham University
    Inventors: James M. TOUR, Robert PAL, Victor GARCÍA LÓPEZ, Lizanne NILEWSKI
  • Publication number: 20230113503
    Abstract: Alkali metal-sulfur cells and batteries with cathode layers that store alkali metal charge carriers (e.g., lithium ions) in agglomerates of sulfurized carbon. The cathode layers lack costly and environmentally unfriendly nickel and cobalt. The cathode layers are composites that include agglomerates of sulfurized-carbon particles in a conductive binder and interconnected by sp2-bonded carbon materials, such as carbon nanotubes or nanoribbons, that extend within the agglomerates and between the sulfurized-carbon particles.
    Type: Application
    Filed: October 7, 2022
    Publication date: April 13, 2023
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: James M. Tour, Rodrigo Villegas Salvatierra, Gladys Anahi Lopez Silva, Abdul-Ramahn O. Raji
  • Patent number: 11605817
    Abstract: Alkali metal-sulfur cells and batteries with cathode layers that store alkali metal charge carriers (e.g., lithium ions) in agglomerates of sulfurized carbon. The cathode layers lack costly and environmentally unfriendly nickel and cobalt. The cathode layers are composites that include agglomerates of sulfurized-carbon particles in a conductive binder and interconnected by sp2-bonded carbon materials, such as carbon nanotubes or nanoribbons, that extend within the agglomerates and between the sulfurized-carbon particles.
    Type: Grant
    Filed: September 1, 2020
    Date of Patent: March 14, 2023
    Assignee: William Marsh Rice University
    Inventors: James M. Tour, Rodrigo Villegas Salvatierra, Gladys Anahi Lopez Silva, Abdul-Rahman O. Raji
  • Patent number: 11565003
    Abstract: Embodiments of the present disclosure pertain to methods of opening a lipid bilayer by associating the lipid bilayer with a molecule that includes a moving component capable of moving (e.g., rotating) in response to an external stimulus; and exposing the molecule to an external stimulus before, during or after associating the molecule with the lipid bilayer. The exposing causes the moving component of the molecule to move and thereby open the lipid bilayer (e.g., by pore formation). The external stimuli may include an energy source, such as ultraviolet light. The opened lipid bilayer may be a component of cell membranes in vitro or in vivo. The opening of the lipid bilayer may allow for the passage of various materials (e.g., active agents, such as peptide-based drugs) through the lipid bilayer and into cells. Additional embodiments of the present disclosure pertain to the aforementioned molecules for opening lipid bilayers.
    Type: Grant
    Filed: April 16, 2021
    Date of Patent: January 31, 2023
    Assignees: William Marsh Rice University, Durham University
    Inventors: James M. Tour, Robert Pal, Victor García López, Lizanne Nilewski
  • Patent number: 11437620
    Abstract: In some embodiments, the present disclosure pertains to methods of producing a graphene material by exposing a polymer to a laser source. In some embodiments, the exposing results in formation of a graphene from the polymer. In some embodiments, the methods of the present disclosure also include a step of separating the formed graphene from the polymer to form an isolated graphene. In some embodiments, the methods of the present disclosure also include a step of incorporating the graphene material or the isolated graphene into an electronic device, such as an energy storage device. In some embodiments, the graphene is utilized as at least one of an electrode, current collector or additive in the electronic device. Additional embodiments of the present disclosure pertain to the graphene materials, isolated graphenes, and electronic devices that are formed by the methods of the present disclosure.
    Type: Grant
    Filed: December 3, 2019
    Date of Patent: September 6, 2022
    Assignee: William Marsh Rice University
    Inventors: James M. Tour, Jian Lin, Zhiwei Peng, Wilbur Carter Kittrell
  • Publication number: 20220267153
    Abstract: Methods that expand the properties of laser-induced graphene (LIG) and the resulting LIG having the expanded properties. Methods of fabricating laser-induced graphene from materials, which range from natural, renewable precursors (such as cloth or paper) to high performance polymers (like Kevlar). With multiple lasing, however, highly conductive PEI-based LIG could be obtained using both multiple pass and defocus methods. The resulting laser-induced graphene can be used, inter alia, in electronic devices, as antifouling surfaces, in water treatment technology, in membranes, and in electronics on paper and food Such methods include fabrication of LIG in controlled atmospheres, such that, for example, superhydrophobic and superhydrophilic LIG surfaces can be obtained. Such methods further include fabricating laser-induced graphene by multiple lasing of carbon precursors. Such methods further include direct 3D printing of graphene materials from carbon precurors.
    Type: Application
    Filed: November 1, 2021
    Publication date: August 25, 2022
    Applicants: WILLIAM MARSH RICE UNIVERSITY, B.G. NEGEV TECHNOLOGIES AND APPLICATIONS LTD. AT BEN-GURION UNIVERSITY
    Inventors: James M. Tour, Yieu Chyan, Christopher John Arnusch, Swatantra Pratap Singh, Yilun Li, Duy X. Luong, Carter Kittrell, Ruquan Ye, Jordan Miller, Ian Kinstlinger, Savannah Cofer
  • Patent number: 11246962
    Abstract: Graphene compositions used for neuronal repair and treatments, and, in particular neuronal scaffold-water soluble graphene for treatment of severed spinal cords and other neuronal repairs. The neuronal scaffold-water soluble graphene can be PEGylated GNR used in combination with a fusogen agent, such as PEG600.
    Type: Grant
    Filed: August 22, 2017
    Date of Patent: February 15, 2022
    Assignee: William Marsh Rice University
    Inventors: James M. Tour, William Sikkema
  • Patent number: 11161744
    Abstract: Methods that expand the properties of laser-induced graphene (LIG) and the resulting LIG having the expanded properties. Methods of fabricating laser-induced graphene from materials, which range from natural, renewable precursors (such as cloth or paper) to high performance polymers (like Kevlar). With multiple lasing, however, highly conductive PEI-based LIG could be obtained using both multiple pass and defocus methods. The resulting laser-induced graphene can be used, inter alia, in electronic devices, as antifouling surfaces, in water treatment technology, in membranes, and in electronics on paper and food Such methods include fabrication of LIG in controlled atmospheres, such that, for example, superhydrophobic and superhydrophilic LIG surfaces can be obtained. Such methods further include fabricating laser-induced graphene by multiple lasing of carbon precursors. Such methods further include direct 3D printing of graphene materials from carbon precursors.
    Type: Grant
    Filed: November 6, 2017
    Date of Patent: November 2, 2021
    Assignees: William Marsh Rice University, B.G. Negev Technologies and Applications, Ltd., at Ben-Gurion University
    Inventors: James M. Tour, Yieu Chyan, Christopher John Arnusch, Swatantra Pratap Singh, Yilun Li, Duy X. Luong, Carter Kittrell, Ruquan Ye, Jordan Miller, Ian Kinstlinger, Savannah Cofer
  • Patent number: 11154623
    Abstract: Embodiments of the present disclosure pertain to methods of opening a lipid bilayer by associating the lipid bilayer with a molecule that includes a moving component capable of moving (e.g., rotating) in response to an external stimulus; and exposing the molecule to an external stimulus before, during or after associating the molecule with the lipid bilayer. The exposing causes the moving component of the molecule to move and thereby open the lipid bilayer (e.g., by pore formation). The external stimuli may include an energy source, such as ultraviolet light. The opened lipid bilayer may be a component of cell membranes in vitro or in vivo. The opening of the lipid bilayer may allow for the passage of various materials (e.g., active agents, such as peptide-based drugs) through the lipid bilayer and into cells. Additional embodiments of the present disclosure pertain to the aforementioned molecules for opening lipid bilayers.
    Type: Grant
    Filed: July 14, 2017
    Date of Patent: October 26, 2021
    Assignees: WILLIAM MARSH RICE UNIVERSITY, DURHAM UNIVERSITY
    Inventors: James M. Tour, Robert Pal, Victor García-López, Lizanne Nilewski