Abstract: A photocatalytic method of colored discharge printing for producing colorized patterns on textiles includes over dyeing textiles with illuminant dyes and ground shade dyes respectively, manufacturing patterned printing plates with hollow-out decorative patterns, applying a photocatalyst on the over-dyed textiles through the hollow-outs, using a photocatalytic method of colored discharge printing to produce localized discoloration of the ground shade while leaving the illuminant dyes on the textile which produces an effect of colorized patterns on the textiles. The method has the characteristics of being a simple process with a simple apparatus and has short processing, easy control and wide adaptability. The method eliminates the needs for printing pastes and expensive printing apparatus used in the complicated process in a conventional printing method.

Abstract: A method for photocatalytic white discharge printing for achieving patterns on textiles includes closely integrating substrates with patterned printing plates or fixing patterned printing plates on one or both sides of a substrate, placing them in a reactor equipped with a light source and containing the photocatalytic white discharging formulation. The method has the characteristics of a simple process, short processing, easy controlling and wide adaptability. The process eliminates the need for printing plates and expensive printing apparatus used in complicated conventional printing methods. Additionally, the photocatalytic solution can be reused which avoids generous application of chemical agents and waste discharges that are present in conventional printing methods. The method is beneficial for cutting costs, saving energy, reducing emissions and has cleaner production.

Abstract: A phase-transfer catalytic color fixation processing method for textile includes the following steps: (1) dry-dyeing a textile with disperse reactive dyes in supercritical carbon dioxide fluid under waterless condition; (2) putting the textile in a phase-transfer catalytic fixation device, taking phase-transfer catalyst as the carrier of circulated supercritical carbon dioxide fluid, transporting the ionized fixing catalytic alkaline substance from aqueous phase to hydrophobic supercritical carbon dioxide fluid phase, getting full contact with functional groups on fibers, resulting in the fixing catalytic reaction with disperse reactive dyes.

Abstract: A solvent medium for diazotization reaction includes a mixed solution of polyethylene glycol and water. The molecular weight of polyethylene glycol is 200-600, and the volume ratio of polyethylene glycol and water is 1:0.4-1.5. The mixed solution also includes hydrochloric acid or sulfuric acid, and the concentration of H+ in the mixed solution is 0.32-1.72 mol L?1.

Abstract: The invention provides a method for measuring the diffusion performance of an acid dye in a color paste, comprising preparing a primary paste and placing the primary paste into a transparent cylindrical container; adding a dye to the primary paste formulate a color paste, and flatly and uniformly paving a layer of the color paste on an upper surface of the primary paste; performing constant-temperature treatment at 60-95° C. on the cylindrical container, so that the dye in the color paste on the top of the blank primary paste in the cylindrical container diffuses downwards to the bottom of the cylinder; and sampling the primary paste from a sampling hole, and diluting the sampled primary paste with deionized water. The method of the invention has simple operation steps, reliable and safe experiments, highly stable test data and good reproducibility of results, and high temperature and high pressure are not required herein.

Abstract: The present invention relates to a phase-transfer catalytic colour fixation processing method for a textile. The processing method comprises the following steps: dyeing a natural fibre textile in a supercritical carbon dioxide fluid waterless dyeing system using a disperse reactive dye, and then realizing a reaction fixation of the dye on the fibres using a phase transfer catalyst in the supercritical carbon dioxide fluid. Since the method utilizes the action of the phase-transfer catalyst in the colour fixation stage, an ionized colour fixation reaction accelerator and the like is effectively transferred to the supercritical carbon dioxide colour fixation fluid and solid-phase fibres, thus improving the nucleophilic reactivity of the functional group on the fibres, achieving the colour fixation reaction between the fibres and the dye in the supercritical carbon dioxide fluid conditions, and improving the colour fixation efficiency of the dye on the fibres.

Abstract: A device for colour-fixing processing on textiles includes a system of supercritical carbon dioxide fluid, a fixing liquid storage tank (2) and a fixing reactor (9). The fixing liquid storage tank (2) is below the fixing reactor (9) and sealed connected by a connecting device (6). The fixing liquid storage tank (2) has a cylindrical cavity in which a fluid distributor (4) is mounted. The fluid distributor (4) is composed of several interconnected pipes which bending down with the nozzles downward, and one of the pipes is used as circulated fluid inlet (1) connected with the supercritical carbon dioxide fluid system, and the rest pipes are used as circulated fluid outlets.

Abstract: A photocatalytic method of colored discharge printing for producing colorized patterns on textiles includes: textiles are over dyed with illuminant dyes and ground shade dyes respectively; then the patterned printing plates with hollow-outs decorative patterns are manufactured, and the photocatalyst is applied on the over-dyeing textiles through the hollow-outs; finally, with the photocatalytic method of colored discharge printing, the ground shade dyes are localized discolored, while the illuminant dyes are left on the substrates, having an effect of colorized patterns on textiles. The method has the characteristics of simple process and apparatuses, short processing, easy controlling and wide adaptability, along with eliminations of the needs for printing pastes and expensive printing apparatuses, so as the complicated process in the conventional printing method.

Abstract: A method of photocatalytic white discharge printing for achieving patterns on textiles includes: substrates are closely integrated with patterned printing plates, or patterned printing plates are fixed in one side or both sides of the substrates; then put them in a reactor equipped with a light source and occupied by the photocatalytic white discharging formulation. The method has the characteristics of simple process, short processing, easy controlling and wide adaptability, along with eliminations of the need for printing pastes and expensive printing apparatuses, so as the complicated process in the conventional printing method. Additionally, photocatalytic solution can be reused, avoiding generous applications of chemical agents and waste discharges in the conventional printing method. It is also beneficial to cutting costs, along with significant advantages of energy saving, emission reduction and cleaner production.