Abstract: Lubricating grease compositions have a titanium complex grease component along with a mineral/synthetic oil-based component and a conventional soap or grease. The conventional soaps and greases may be lithium complex, calcium sulfonate, or aluminum complex-based, among others, with and without additives. The compositions are high performance geases, exhibiting improved drop point, extreme pressure, antiwear, oil separation, and shelf life properties.

Abstract: An organic solvent free process for the preparation of a grease thickener which is at least one of an imide-diurea and an imide-urethane urea includes (a) providing approximately equimolar amounts of reagents including dibasic acid selected from the group consisting of succinic acid, glutaric acid, phthalic acid, and anhydrides thereof, reactant selected from the group consisting of a primary diamine and a primary amino hydroxy compound, and having 2 to 10 carbon atoms, toluene diisocyanate, and primary monoamine having 8 to 22 carbon atoms; (b) reacting the dibasic acid with the reactant to provide a first reaction mixture; (c) reacting the first reaction mixture with the toluene diisocyanate to provide a second reaction mixture; and (d) reacting the second reaction mixture with the primary monoamine to provide said grease thickener.

Abstract: A lubricating grease composition includes from 2 to 20% by weight of titanium alkoxide; from 2 to 20% by weight of carboxylic acid other than fatty acid; from 5.0 to 35.0% by weight of fatty acids; from 0.0 to 5.0% by weight of water; from 20 to 90% by weight of oil selected from the group consisting of mineral and synthetic oil; and from 0.01 to 50% of performance additives.