Abstract: A process for the salt-free coagulation of polymer dispersions in a rotor/stator assembly is disclosed. The rotor/stator assembly includes a casing, a rotor shaft rotatably mounted within the casing, a rotor having a conical surface affixed to the rotor shaft, and a stator affixed to the casing and concentrically associated with the rotor. The conical surface faces a surface of the stator to form an adjustable shear gap, which is surrounded by an annular space. A polymer dispersion is fed into the assembly and conveyed through the shear gap. During this conveyance, the polymer dispersion is precipitated at a predetermined shear rate and a predetermined shear deformation. The polymer dispersion is discharged from the assembly through an outlet neck, and the assembly is flushed with water using one or more ports formed in at least one of a pipeline coupled to the axial feed neck, the stator, and the casing.

Abstract: A rotor/stator apparatus is proposed, with a bearing block, a casing (1), a rotor shaft mounted therein, on whose end directed toward the casing a rotor designed with a conical surface has been secured, there being a stator (2) secured within the casing and concentrically associated with the rotor, where those surfaces that face toward one another of the rotor (2) and of the stator (3) form a gap upstream of which there is an axial feed neck and downstream of which there is a radial outlet neck, where rotor and stator have been mounted so as to be capable of axial shift in order to form a gap with adjustable gap width, wherein one or more holes extending to the exterior has/have been provided in the region of the feed aperture of the rotor/stator apparatus in the feed line prior to and very close to the rotor/stator apparatus and/or in the casing (1) and/or in the stator (2), and alongside the outlet aperture at least one further hole has been provided in the annular space around the shear gap.