Patents by Inventor Masashi Nakabayashi

Masashi Nakabayashi has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20220046968
    Abstract: An emulsion composition includes dry powder of dicotyledonous plant seeds in a range between 1 mass % or more and 20 mass % or less, the dry powder having an average particle size in a range between 0.2 ?m or larger and 150 ?m or smaller, water in a range between 20 mass % or more and 69 mass % or less, and fat and oil in a range between 21 mass % or more and 70 mass % or less.
    Type: Application
    Filed: October 26, 2021
    Publication date: February 17, 2022
    Applicant: MIZKAN HOLDINGS CO., LTD.
    Inventors: Tomoya Takemura, Masashi Nakabayashi, Yasuki Matsumura, Kentaro Matsumiya
  • Patent number: 11078596
    Abstract: A method for evaluating the quality of a SiC single crystal by a non-destructive and simple method; and a method for producing a SiC single crystal ingot with less dislocation and high quality with good reproducibility utilizing the same. The method for evaluating the quality of a SiC single crystal body is based on the graph of a second polynomial equation obtained by differentiating a first polynomial equation, the first polynomial equation approximating the relation between a peak shift value and a position of the measurement point and the peak shift value being obtained by an X-ray rocking curve measurement. The method for producing a SiC single crystal ingot manufactures a SiC single crystal ingot by a sublimation recrystallization method using, as a seed crystal, the SiC single crystal body evaluated by the evaluation method.
    Type: Grant
    Filed: March 29, 2018
    Date of Patent: August 3, 2021
    Assignee: SHOWA DENKO K.K.
    Inventors: Masashi Nakabayashi, Shoji Ushio
  • Patent number: 10711369
    Abstract: The present invention provides a method for producing an SiC single crystal, enabling obtaining an SiC single crystal substrate in which a screw dislocation-reduced region is ensured in a wide range, and an SiC single crystal substrate. The SiC single crystal substrate is produced using a seed crystal having an off angle in the off orientation from a {0001} plane by a production method wherein in advance of a growth main step of performing crystal growth to form a facet {0001} plane in the crystal peripheral part on the crystal end face having grown thereon the bulk silicon carbide single crystal and obtain more than 50% of the thickness of the obtained SiC single crystal, a growth sub-step of growing the crystal at a higher nitrogen concentration than in the growth main step and at a growth atmosphere pressure of 3.9 to 39.9 kPa and a seed crystal temperature of 2,100° C. to less than 2,300° C. is included.
    Type: Grant
    Filed: December 4, 2015
    Date of Patent: July 14, 2020
    Assignee: SHOWA DENKO K.K.
    Inventors: Shinya Sato, Tatsuo Fujimoto, Masakazu Katsuno, Hiroshi Tsuge, Masashi Nakabayashi
  • Publication number: 20200010974
    Abstract: A method for evaluating the quality of a SiC single crystal by a non-destructive and simple method; and a method for producing a SiC single crystal ingot with less dislocation and high quality with good reproducibility utilizing the same. The method for evaluating the quality of a SiC single crystal body is based on the graph of a second polynomial equation obtained by differentiating a first polynomial equation, the first polynomial equation approximating the relation between a peak shift value and a position of the measurement point and the peak shift value being obtained by an X-ray rocking curve measurement. The method for producing a SiC single crystal ingot manufactures a SiC single crystal ingot by a sublimation recrystallization method using, as a seed crystal, the SiC single crystal body evaluated by the evaluation method.
    Type: Application
    Filed: March 29, 2018
    Publication date: January 9, 2020
    Applicant: SHOWA DENKO K.K.
    Inventors: Masashi NAKABAYASHI, Shoji USHIO
  • Patent number: 10526722
    Abstract: The present invention provides a method of manufacturing by the sublimation-recrystallization method more accurately detecting a thermal state of a starting material in a crucible and enabling control of the growth conditions while manufacturing an SiC single crystal.
    Type: Grant
    Filed: March 18, 2016
    Date of Patent: January 7, 2020
    Assignee: SHOWA DENKO K.K.
    Inventors: Masashi Nakabayashi, Kiyoshi Kojima, Hiroyuki Deai, Kota Shimomura, Yukio Nagahata
  • Patent number: 10202706
    Abstract: Provided is a SiC single crystal wafer, which is manufactured from a SiC single crystal ingot grown by the sublimation-recrystallization method, and which brings about high device performance and high device manufacture yield when used as a wafer for manufacturing a device. The SiC single crystal wafer has, in a surface thereof, a basal plane dislocation density of 1,000 dislocations per cm2 or less, a threading screw dislocation density of 500 dislocations per cm2 or less, and a Raman index of 0.2 or less. Further provided is a method of manufacturing a SiC single crystal ingot, including controlling heat input from a side surface of the single crystal ingot during growth of a single crystal, to thereby grow the crystal while changes in the temperature distribution of the single crystal ingot are reduced.
    Type: Grant
    Filed: September 30, 2014
    Date of Patent: February 12, 2019
    Assignee: SHOWA DENKO K.K.
    Inventors: Masashi Nakabayashi, Kota Shimomura, Yukio Nagahata, Kiyoshi Kojima
  • Publication number: 20180282902
    Abstract: An SiC single crystal ingot including a silicon carbide (SiC) single crystal formed on a seed crystal, a crystal growth end of a front end of the ingot having a convex shape. An SiC single crystal substrate cut out from a part of a relative height in a height direction of the ingot of at least 0.2 to 0.8 in range has a basal plane dislocation density and threading screw dislocation density observed at the surface of the substrate that are respectively predetermined values or less. Further, the Raman index of the difference (A/B) of the Raman Shift value (A) measured at the center part of the substrate and the Raman Shift value (B) measured at the peripheral parts is a predetermined value or less.
    Type: Application
    Filed: September 30, 2016
    Publication date: October 4, 2018
    Applicant: SHOWA DENKO K. K.
    Inventor: Masashi NAKABAYASHI
  • Publication number: 20180251909
    Abstract: The present invention provides a method of manufacturing by the sublimation-recrystallization method more accurately detecting a thermal state of a starting material in a crucible and enabling control of the growth conditions while manufacturing an SiC single crystal.
    Type: Application
    Filed: March 18, 2016
    Publication date: September 6, 2018
    Applicants: NIPPON STEEL & SUMITOMO METAL CORPORATION, NIPPON STEEL & SUMIKIN MATERIALS CO., LTD.
    Inventors: Masashi NAKABAYASHI, Kiyoshi KOJIMA, Hiroyuki DEAI, Kota SHIMOMURA, Yukio NAGAHATA
  • Patent number: 10048142
    Abstract: Provided are a method by which the degrees of the strains of lattices in a plurality of bulk SiC single crystals can be relatively evaluated, and a reference SiC single crystal to be used in the method.
    Type: Grant
    Filed: May 30, 2014
    Date of Patent: August 14, 2018
    Assignee: SHOWA DENKO K.K.
    Inventors: Kiyoshi Kojima, Masashi Nakabayashi
  • Patent number: 10031089
    Abstract: Provided are a method of evaluating an internal stress of a silicon carbide (SiC) single crystal wafer and a method of predicting warpage of the SiC single crystal wafer after completion of polishing by evaluating the internal stress of the wafer. Wavenumber shift amounts of Raman-scattered light are measured at two points within a surface of the SiC single crystal wafer, and the internal stress is evaluated through use of a difference between the wavenumber shift amounts. Also provided is a method of predicting warpage of a silicon carbide single crystal wafer in advance, the silicon carbide single crystal wafer being produced by sublimation-recrystallization method, the method including predicting warpage of a SiC single crystal wafer through use of the evaluation indicator.
    Type: Grant
    Filed: May 30, 2014
    Date of Patent: July 24, 2018
    Assignee: SHOWA DENKO K.K.
    Inventors: Kiyoshi Kojima, Masashi Nakabayashi, Kota Shimomura, Yukio Nagahata
  • Patent number: 9915011
    Abstract: The invention provides a low resistivity silicon carbide single crystal wafer for fabricating semiconductor devices having excellent characteristics. The low resistivity silicon carbide single crystal wafer has a specific volume resistance of 0.001 ?cm to 0.012 ?cm and 90% or greater of the entire wafer surface area is covered by an SiC single crystal surface of a roughness (Ra) of 1.0 nm or less.
    Type: Grant
    Filed: December 1, 2009
    Date of Patent: March 13, 2018
    Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATION
    Inventors: Tatsuo Fujimoto, Noboru Ohtani, Masakazu Katsuno, Masashi Nakabayashi, Hirokatsu Yashiro
  • Publication number: 20170342593
    Abstract: The present invention provides a method for producing an SiC single crystal, enabling obtaining an SiC single crystal substrate in which a screw dislocation-reduced region is ensured in a wide range, and an SiC single crystal substrate. The SiC single crystal substrate is produced using a seed crystal having an off angle in the off orientation from a {0001} plane by a production method wherein in advance of a growth main step of performing crystal growth to form a facet {0001} plane in the crystal peripheral part on the crystal end face having grown thereon the bulk silicon carbide single crystal and obtain more than 50% of the thickness of the obtained SiC single crystal, a growth sub-step of growing the crystal at a higher nitrogen concentration than in the growth main step and at a growth atmosphere pressure of 3.9 to 39.9 kPa and a seed crystal temperature of 2,100° C. to less than 2,300° C. is included.
    Type: Application
    Filed: December 4, 2015
    Publication date: November 30, 2017
    Applicant: NIPPON STEEL & SUMITOMO METAL CORPORATION
    Inventors: Shinya SATO, Tatsuo FUJIMOTO, Masakazu KATSUNO, Hiroshi TSUGE, Masashi NAKABAYASHI
  • Patent number: 9777403
    Abstract: A single-crystal silicon carbide and a single-crystal silicon carbide wafer of good-quality are disclosed that are low in dislocations, micropipes and other crystal defects and enable high yield and high performance when applied to a device, wherein the ratio of doping element concentrations on opposite sides in the direction of crystal growth of the interface between the seed crystal and the grown crystal is 5 or less and the doping element concentration of the grown crystal in the vicinity of the seed crystal is 2×1019 cm?3 to 6×1020 cm?3.
    Type: Grant
    Filed: October 14, 2009
    Date of Patent: October 3, 2017
    Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATION
    Inventors: Masashi Nakabayashi, Tatsuo Fujimoto, Masakazu Katsuno, Hiroshi Tsuge
  • Publication number: 20170199092
    Abstract: Provided are a method by which the degrees of the strains of lattices in a plurality of bulk SiC single crystals can be relatively evaluated, and a reference SiC single crystal to be used in the method.
    Type: Application
    Filed: May 30, 2014
    Publication date: July 13, 2017
    Applicant: NIPPON STEEL & SUMIKIN MATERIALS CO., LTD.
    Inventors: Kiyoshi KOJIMA, Masashi NAKABAYASHI
  • Patent number: 9691607
    Abstract: Disclosed is a process for producing an epitaxial single-crystal silicon carbide substrate by epitaxially growing a silicon carbide film on a single-crystal silicon carbide substrate by chemical vapor deposition. The step of crystal growth in the process comprises a main crystal growth step, which mainly occupies the period of epitaxial growth, and a secondary crystal growth step, in which the growth temperature is switched between a set growth temperature (T0) and a set growth temperature (T2) which are respectively lower and higher than a growth temperature (T1) used in the main crystal growth step. The basal plane dislocations of the single-crystal silicon carbide substrate are inhibited from being transferred to the epitaxial film. Thus, a high-quality epitaxial film is formed.
    Type: Grant
    Filed: April 7, 2011
    Date of Patent: June 27, 2017
    Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATION
    Inventors: Takashi Aigo, Hiroshi Tsuge, Taizo Hoshino, Tatsuo Fujimoto, Masakazu Katsuno, Masashi Nakabayashi, Hirokatsu Yashiro
  • Publication number: 20160231256
    Abstract: Provided are a method of evaluating an internal stress of a silicon carbide (SiC) single crystal wafer and a method of predicting warpage of the SiC single crystal wafer after completion of polishing by evaluating the internal stress of the wafer. Wavenumber shift amounts of Raman-scattered light are measured at two points within a surface of the SiC single crystal wafer, and the internal stress is evaluated through use of a difference between the wavenumber shift amounts. Also provided is a method of predicting warpage of a silicon carbide single crystal wafer in advance, the silicon carbide single crystal wafer being produced by sublimation-recrystallization method, the method including predicting warpage of a SiC single crystal wafer through use of the evaluation indicator.
    Type: Application
    Filed: May 30, 2014
    Publication date: August 11, 2016
    Inventors: Kiyoshi Kojima, Masashi Nakabayashi, Kota Shimomura, Yukio Nagahata
  • Publication number: 20160215414
    Abstract: Provided is a SiC single crystal wafer, which is manufactured from a SiC single crystal ingot grown by the sublimation-recrystallization method, and which brings about high device performance and high device manufacture yield when used as a wafer for manufacturing a device. The SiC single crystal wafer has, in a surface thereof, a basal plane dislocation density of 1,000 dislocations per cm2 or less, a threading screw dislocation density of 500 dislocations per cm2 or less, and a Raman index of 0.2 or less. Further provided is a method of manufacturing a SiC single crystal ingot, including controlling heat input from a side surface of the single crystal ingot during growth of a single crystal, to thereby grow the crystal while changes in the temperature distribution of the single crystal ingot are reduced.
    Type: Application
    Filed: September 30, 2014
    Publication date: July 28, 2016
    Inventors: Masashi NAKABAYASHI, Kota SHIMOMURA, Yukio NAGAHATA, Kiyoshi KOJIMA
  • Patent number: 9068277
    Abstract: The invention provides an apparatus for manufacturing good quality single-crystal silicon carbide stably without formation of cracks and the like, which apparatus comprises: at least a crucible for accommodating silicon carbide feedstock powder and seed crystal; heat insulation material installed around the crucible; and a heating device for heating the crucible, wherein the outer profile of the crucible includes at least one region of narrower diameter than a vertically adjacent region, insulation material is also installed in the space left by the diameter difference, and thickness of the insulation material at the narrower diameter region is greater than that of the insulation material at the vertically adjacent region. The apparatus for manufacturing single-crystal silicon carbide enables precise control of the temperature gradient inside the crucible, thereby enabling manufacture of good quality single-crystal silicon carbide.
    Type: Grant
    Filed: April 1, 2009
    Date of Patent: June 30, 2015
    Assignee: NIPPON STEEL & SUMITOMO METAL CORPORATION
    Inventors: Masashi Nakabayashi, Tatsuo Fujimoto, Hiroshi Tsuge, Masakazu Katsuno, Noboru Ohtani
  • Publication number: 20150075422
    Abstract: The present invention provides an epitaxial SiC monocrystalline substrate having a high quality epitaxial film suppressed in occurrence of step bunching in epitaxial growth using a substrate with an off angle of 6° or less and a method of production of the same, that is, an epitaxial silicon carbide monocrystalline substrate comprised of a silicon carbide monocrystalline substrate with an off angle of 6° or less on which a silicon carbide monocrystalline thin film is formed, the epitaxial silicon carbide monocrystalline substrate characterized in that the silicon carbide monocrystalline thin film has a surface with a surface roughness (Ra value) of 0.5 nm or less and a method of production of the same.
    Type: Application
    Filed: November 19, 2014
    Publication date: March 19, 2015
    Inventors: Takashi Aigo, Hiroshi Tsuge, Taizo Hoshino, Tatsuo Fujimoto, Masakasu Katsuno, Masashi Nakabayashi, Hirokatsu Yashiro
  • Patent number: 8936680
    Abstract: The present invention, which provides a crucible for producing single-crystal silicon carbide, and a production apparatus and a production method for single-crystal silicon carbide, which are capable of stably growing a single-crystal silicon carbide ingot good in crystallinity at high yield, is a crucible for producing single-crystal silicon carbide having a crucible vessel for holding silicon carbide raw material and a crucible cover for attaching a seed crystal and is adapted to sublimate a silicon carbide raw material in the crucible vessel to supply silicon carbide sublimation gas onto a seed crystal attached to the crucible cover and grow single-crystal silicon carbide on the seed crystal, which crucible for producing single-crystal silicon carbide is provided in the crucible vessel and the crucible cover with threaded portions to be screwed together and is provided with a sublimation gas discharge groove or grooves capable of regulating flow rate by relative rotation of the threaded portions; and is a
    Type: Grant
    Filed: February 25, 2010
    Date of Patent: January 20, 2015
    Assignee: Nippon Steel & Sumitomo Metal Corporation
    Inventors: Masakazu Katsuno, Tatsuo Fujimoto, Hiroshi Tsuge, Masashi Nakabayashi