Patents by Inventor Milton E. Winyall

Milton E. Winyall has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 4631184
    Abstract: A dentifrice composition which contains a particulate, dialytic silica abrasive/thickening agent.
    Type: Grant
    Filed: January 10, 1984
    Date of Patent: December 23, 1986
    Assignee: W. R. Grace & Co.
    Inventors: Milton E. Winyall, Cathy L. Harville
  • Patent number: 4508607
    Abstract: Finely divided particulate silica is prepared by the electrodialysis of sodium silicate solution in the presence of silica-containing nucleation particles (seeds). The novel particulate silica product, herein referred to as dialytic silica, may be used in the preparation of catalysts, sorbents, abrasives, fillers and thickeners.
    Type: Grant
    Filed: September 20, 1983
    Date of Patent: April 2, 1985
    Assignee: W. R. Grace & Co.
    Inventor: Milton E. Winyall
  • Patent number: 4387008
    Abstract: Silica hydrogel is prepared by electrolysis of an aqueous anolyte solution containing an alkali metal silicate and a salt of a non-siliceous anion, such as sodium nitrate or sodium sulfate, in a cell with a cation permselective membrane separating the anolyte and an aqueous catholyte. The electrolysis is effected in the presence of the salt to deposit silica hydrogel on the anode. The hydrogel can be easily recovered from the anode and dried to produce regular and intermediate density silica xerogels having narrow pore size distributions.
    Type: Grant
    Filed: December 12, 1980
    Date of Patent: June 7, 1983
    Assignee: W. R. Grace & Co.
    Inventors: Milton E. Winyall, Charles Davidoff
  • Patent number: 4279879
    Abstract: Silica hydrogel is prepared by electrolysis of an aqueous anolyte solution containing an alkali metal silicate and a salt of a non-siliceous anion, such as sodium nitrate or sodium sulfate, in a cell with a cation permselective membrane separating the anolyte and an aqueous catholyte. The electrolysis is effected in the presence of the salt to deposit silica hydrogel on the anode. The hydrogel can be easily recovered from the anode and dried to produce regular and intermediate density silica xerogels having narrow pore size distributions.
    Type: Grant
    Filed: October 1, 1979
    Date of Patent: July 21, 1981
    Assignee: W. R. Grace & Co.
    Inventors: Milton E. Winyall, Charles Davidoff
  • Patent number: 4216113
    Abstract: This invention consists in the exchanging of the water of a silica hydrogel with a water miscible organic solvent to a water content of less than 10 percent by weight, and then feeding this organogel to a fluid energy mill for concurrent drying and deagglomerating.
    Type: Grant
    Filed: January 18, 1973
    Date of Patent: August 5, 1980
    Assignee: W. R. Grace & Co.
    Inventor: Milton E. Winyall
  • Patent number: 4180566
    Abstract: A method of reducing the lipid concentration in the blood of a patient comprises administering to the patient a lipid-lowering effective amount of silica gel.
    Type: Grant
    Filed: May 15, 1978
    Date of Patent: December 25, 1979
    Assignee: W. R. Grace & Co.
    Inventors: Milton E. Winyall, Kamal M. Abdo
  • Patent number: 3959174
    Abstract: High pore volume silica materials are useful as thickening, reinforcing and flatting agents. This invention comprises selectively forming silica gels having pore volumes in the range of 1.2 to 3.0 cc/g. These high pore volume silica gels can be produced by the alkaline gelation of a mixture of silicate and ammonium hydroxide at a pH of from 10.6 to 11.2, using a water soluble silica desolubilizing agent selected from the group consisting of ammonia, monohydric alcohols, glycols, ketones and salts. The silica is then aged, neutralized, optionally aged a second time, filtered and washed. This silica may then be dried and directly used, or it may be milled to a smaller size. For use as a thickening agent, the silica is milled in a fluid energy mill to an average particle size of less than about 1 micron, and preferably to less than 0.5 micron.
    Type: Grant
    Filed: January 10, 1973
    Date of Patent: May 25, 1976
    Assignee: W. R. Grace & Co.
    Inventors: Milton E. Winyall, Ellsworth G. Acker