Abstract: Method and apparatus of charge distribution analysis insulating and semiconducting dielectric materials to measure by using a Coulomb Balance surface/subsurface space charge layers and the sign, mobility and polarizability of charge carriers. The technique includes measuring the force, attractive or repellent, between a bias electrode to which a voltage is applied and a dielectric material in a condensor half cell arrangement. An apparatus is provided for heating a sample for causing the generation of surface/subsurface charges, and then for applying an external potential while the sample is maintained at a high temperature. The effective mass of the sample is detected by determining the amount of force necessary to restore a balance arm, by which the sample is supported, to its original position, the alteration in position being due to attractive or repulsive electrostatic forces between the sample and the electrodes.