Patents by Inventor Othman Charles Sadeq Al-Hamouz

Othman Charles Sadeq Al-Hamouz has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11897789
    Abstract: Polymer/carbon nanotube composites made up of melamine, aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these composites is introduced. A process of synthesizing the polymer/carbon nanotube composites is also described.
    Type: Grant
    Filed: February 2, 2018
    Date of Patent: February 13, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Isaiah Olabisi Adelabu, Tawfik Abdo Saleh Awadh
  • Publication number: 20240001337
    Abstract: The method includes mixing an aldehyde and a first solvent to form a mixture. The method further includes mixing an organosulfur phenol and an aromatic compound to the mixture to form a phenol mixture and heating the phenol mixture in the presence of an acid to form a solid. The solid is dried to obtain the cross-linked porous polymer. The obtained cross-linked porous polymer has repeat pyrrole units bonded to one another, and the cross-linked porous polymer has a thiol group which separates non-adjacent pyrrole units. The cross-linked porous polymer obtained after drying is in a form of solid particles having a spherical particle structure.
    Type: Application
    Filed: June 29, 2022
    Publication date: January 4, 2024
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq AL HAMOUZ, Mahmoud Mohamed ABDELNABY
  • Publication number: 20230348796
    Abstract: A composition and method for the removal of water from a water-containing hydrocarbon stream, and a method for the production of a metal/water-soluble polymer composite are provided. The composite includes a water-soluble polymer, such as guar gum, and a metal salt, such as aluminum nitrate or copper sulfate. The ratio of the metal salt to the water-soluble polymer is in the range from about 1:1 to about 5:1 by mass. The water-soluble polymer and the metal salt form a crosslinked material. The method for producing the metal/water-soluble polymer composite includes mixing a non-crosslinked water-soluble polymer with a metal salt and water to form a paste. The paste is then dried.
    Type: Application
    Filed: April 28, 2022
    Publication date: November 2, 2023
    Applicants: SAUDI ARABIAN OIL COMPANY, KING FAHD UNIVERSITY OF PETROLEUM & MINERALS
    Inventors: Youcef Mankour, Othman Charles Sadeq Al Hamouz
  • Patent number: 11772990
    Abstract: A method for removing cadmium ions from contaminated water sources and systems via contacting and treatment with composites formed from reaction between melamine, an aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups.
    Type: Grant
    Filed: April 19, 2018
    Date of Patent: October 3, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Othman Charles Sadeq Al Hamouz, Isaiah Olabisi Adelabu, Tawfik Abdo Saleh Awadh
  • Patent number: 11773201
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Grant
    Filed: December 8, 2022
    Date of Patent: October 3, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Patent number: 11760827
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Grant
    Filed: December 8, 2022
    Date of Patent: September 19, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Publication number: 20230140110
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Application
    Filed: December 8, 2022
    Publication date: May 4, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq AL HAMOUZ, Mohammed ESTATIE, Tawfik Abdo Saleh AWADH, Mohamed A. MORSY
  • Publication number: 20230116824
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Application
    Filed: December 8, 2022
    Publication date: April 13, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq AL HAMOUZ, Mohammed ESTATIE, Tawfik Abdo Saleh AWADH, Mohamed A. MORSY
  • Patent number: 11530289
    Abstract: A crosslinked polymer that is in the form of a Mannich polycondensation product including reacted units of a cyclic diaminoalkane, an aldehyde, and bisphenol-S or melamine. Also disclosed is a method for removing heavy metals from an aqueous solution by contacting the aqueous solution having an initial concentration of the heavy metal with the crosslinked polymer to form a mixture, and filtering the mixture to obtain an aqueous solution having a reduced concentration of the heavy metal compared to the initial concentration.
    Type: Grant
    Filed: March 16, 2018
    Date of Patent: December 20, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Patent number: 11235306
    Abstract: Crosslinked polymers made up of polymerized units of phenothiazine, pyrrole, and aldehyde. The crosslinked polymers are porous with a BET surface area in the range of 300-600 m2/g. A method of synthesizing the crosslinked polymers is described. Processes for using the crosslinked polymers as adsorbent materials for adsorbing gases (e.g. CO2 capturing), and separating fluid mixtures under dry and wet conditions are also introduced.
    Type: Grant
    Filed: May 1, 2019
    Date of Patent: February 1, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mahmoud Mohamed Abdelnaby
  • Patent number: 10844156
    Abstract: A method for producing a cross-linked polymeric resin, whereby (i) a phenol compound, or an oligomer or polymer thereof, (ii) a diol, or an oligomer or polymer thereof, (iii) an aldehyde, (iv) an acid, and (v) an organic solvent are mixed together to produce a reaction mixture, the reaction mixture is heated at 70-200° C. to produce a precipitate, and the precipitate is washed and dried to form the cross-linked polymeric resin, wherein the phenol compound is of formula I: and wherein the diol is of formula II: wherein R1, R2, R4 and R5 are independently H, an optionally substituted alkyl, an optionally substituted cycloalkyl, or an optionally substituted aryl; X is absent, HC?CH, or C?C; and n=1, 2, 3, 4, 5, or 6.
    Type: Grant
    Filed: March 16, 2018
    Date of Patent: November 24, 2020
    Assignee: King Fahd University of Petroleum and Minerals
    Inventor: Othman Charles Sadeq Al Hamouz
  • Publication number: 20200346185
    Abstract: Crosslinked polymers made up of polymerized units of phenothiazine, pyrrole, and aldehyde. The crosslinked polymers are porous with a BET surface area in the range of 300-600 m2/g. A method of synthesizing the crosslinked polymers is described. Processes for using the crosslinked polymers as adsorbent materials for adsorbing gases (e.g. CO2 capturing), and separating fluid mixtures under dry and wet conditions are also introduced.
    Type: Application
    Filed: May 1, 2019
    Publication date: November 5, 2020
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mahmoud Mohamed Abdelnaby
  • Patent number: 10501341
    Abstract: Cross-linked polymeric resins from anilines linked together with polyamine alkyl chains. A process for producing the cross-linked polymeric resins by Mannich-type polycondensation of anilines and diaminoalkanes linked together by an aldehyde and subsequent basification. In addition, a method for removing heavy metals, such as Pb (II) and As (V) from aqueous solution via contacting and treatment with the cross-linked polymeric resins.
    Type: Grant
    Filed: May 30, 2019
    Date of Patent: December 10, 2019
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Othman Charles Sadeq Al Hamouz, Oluwafemi S. Akintola, Tawfik Abdo Saleh Awadh
  • Patent number: 10494472
    Abstract: Crosslinked polydithiocarbamates based on 1,3,5-triazinane cores linked to pyrrole-dithiocarbamates via alkyl chains. A process for preparing these crosslinked polydithiocarbamates via a Mannich-type polycondensation of diaminoalkane, paraformaldehyde and a pyrrole compound, which is followed by additional modification of the pyrrole moiety to a pyrrole-dithiocarbamate. A method for removing heavy metals, such as Cd(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polydithiocarbamates is also described.
    Type: Grant
    Filed: December 28, 2017
    Date of Patent: December 3, 2019
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh
  • Publication number: 20190322545
    Abstract: A method for removing cadmium ions from contaminated water sources and systems via contacting and treatment with composites formed from reaction between melamine, an aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups.
    Type: Application
    Filed: April 19, 2018
    Publication date: October 24, 2019
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Othman Charles Sadeq AL HAMOUZ, Isaiah Olabisi ADELABU, Tawfik Abdo Saleh AWADH
  • Publication number: 20190300390
    Abstract: A cross-linked polymeric resin which contains reacted monomer units of an aniline, a diaminoalkane, and an aldehyde, and which is functionalized with at least one dithiocarbamate moiety. A process for producing the cross-linked polymeric resin whereby an aniline and a diaminoalkane are linked together by Mannich-type polycondensation reactions with an aldehyde. The resulting Mannich-type polycondensation product is converted into the cross-linked polymeric resin through functionalization of one or more amine functional groups with dithiocarbamate moieties. A method for removing heavy metals, such as Hg(II), from an aqueous solution, whereby the cross-linked polymeric resin is contacted with the aqueous solution, and the heavy metal is thus adsorbed onto the cross-linked polymeric resin.
    Type: Application
    Filed: June 17, 2019
    Publication date: October 3, 2019
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Oluwafemi S. AKINTOLA, Tawfik Abdo Saleh Awadh, Mazen Mohammad Khaled, Othman Charles Sadeq Al Hamouz
  • Publication number: 20190300389
    Abstract: A cross-linked polymeric resin which contains reacted monomer units of an aniline, a diaminoalkane, and an aldehyde, and which is functionalized with at least one dithiocarbamate moiety. A process for producing the cross-linked polymeric resin whereby an aniline and a diaminoalkane are linked together by Mannich-type polycondensation reactions with an aldehyde. The resulting Mannich-type polycondensation product is converted into the cross-linked polymeric resin through functionalization of one or more amine functional groups with dithiocarbamate moieties. A method for removing heavy metals, such as Hg(II), from an aqueous solution, whereby the cross-linked polymeric resin is contacted with the aqueous solution, and the heavy metal is thus adsorbed onto the cross-linked polymeric resin.
    Type: Application
    Filed: June 17, 2019
    Publication date: October 3, 2019
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Oluwafemi S. AKINTOLA, Tawfik Abdo Saleh Awadh, Mazen Mohammad Khaled, Othman Charles Sadeq Al Hamouz
  • Patent number: 10427953
    Abstract: A cross-linked polymeric resin which contains reacted monomer units of an aniline, a diaminoalkane, and an aldehyde, and which is functionalized with at least one dithiocarbamate moiety. A process for producing the cross-linked polymeric resin whereby an aniline and a diaminoalkane are linked together by Mannich-type polycondensation reactions with an aldehyde. The resulting Mannich-type polycondensation product is converted into the cross-linked polymeric resin through functionalization of one or more amine functional groups with dithiocarbamate moieties. A method for removing heavy metals, such as Hg(II), from an aqueous solution, whereby the cross-linked polymeric resin is contacted with the aqueous solution, and the heavy metal is thus adsorbed onto the cross-linked polymeric resin.
    Type: Grant
    Filed: June 17, 2019
    Date of Patent: October 1, 2019
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Oluwafemi S. Akintola, Tawfik Abdo Saleh Awadh, Mazen Mohammad Khaled, Othman Charles Sadeq Al Hamouz
  • Publication number: 20190284323
    Abstract: The synthesis and characterization of phenol-glycol cross-linked polymers are reported. The polymers have high affinity for toxic metal ions such as mercury (II) and can be utilized in methods of analyzing the content of toxic metal ions in a sample and the removal of toxic metal ions from aqueous solutions.
    Type: Application
    Filed: March 16, 2018
    Publication date: September 19, 2019
    Applicant: King Fahd University of Petroleum and Minerals
    Inventor: Othman Charles Sadeq AL Hamouz
  • Publication number: 20190284063
    Abstract: Cross-linked polymeric resins from anilines linked together with polyamine alkyl chains. A process for producing the cross-linked polymeric resins by Mannich-type polycondensation of anilines and diaminoalkanes linked together by an aldehyde and subsequent basification. In addition, a method for removing heavy metals, such as Pb (II) and As (V) from aqueous solution via contacting and treatment with the cross-linked polymeric resins.
    Type: Application
    Filed: May 30, 2019
    Publication date: September 19, 2019
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq AL HAMOUZ, Oluwafemi S. AKINTOLA, Tawfik Abdo Saleh AWADH