Abstract: An electrochemical battery is disclosed. The electrochemical battery has an electrode plate comprising a frame and a generally flat grid connected to the frame, the frame comprising at least a top frame member having a contact lug, wherein the grid comprises a plurality of grid wires and a plurality of window-like open areas between the grid wires, further comprising an active mass within the open areas and/or on the grid wires, wherein the electrode plate comprises on one outer surface or on both opposing outer surfaces of the active mass a pattern of grooves, wherein the grooves extend diagonally from a position closer to the top frame member to a position further away from the top frame member. A method for producing an electrode plate is also disclosed.

Abstract: An electrochemical battery is disclosed. The electrochemical battery has an electrode plate comprising a frame and a generally flat grid connected to the frame, the frame comprising at least a top frame member having a contact lug, wherein the grid comprises a plurality of grid wires and a plurality of window-like open areas between the grid wires, further comprising an active mass within the open areas and/or on the grid wires, wherein the electrode plate comprises on one outer surface or on both opposing outer surfaces of the active mass a pattern of grooves, wherein the grooves extend diagonally from a position closer to the top frame member to a position further away from the top frame member. A method for producing an electrode plate is also disclosed.

Abstract: An electrochemical battery is disclosed. The electrochemical battery has an electrode plate comprising a frame and a generally flat grid connected to the frame, the frame comprising at least a top frame member having a contact lug, wherein the grid comprises a plurality of grid wires and a plurality of window-like open areas between the grid wires, further comprising an active mass within the open areas and/or on the grid wires, wherein the electrode plate comprises on one outer surface or on both opposing outer surfaces of the active mass a pattern of grooves, wherein the grooves extend diagonally from a position closer to the top frame member to a position further away from the top frame member. A method for producing an electrode plate is also disclosed.

Abstract: Propene is continuously reacted with hydrogen peroxide in a tube bundle reactor comprising a multitude of parallel reaction tubes in the presence of a titanium silicalite catalyst arranged as a fixed bed in the reaction tubes. A cooling jacket encloses the reaction tubes, which has a feed point for cooling medium near the entry of the reaction tubes, a withdrawal point for cooling medium near the end of the reaction tubes and at least one additional withdrawal point upstream of the withdrawal point near the end of the reaction tubes. Cooling medium is fed to the feed point for cooling medium, a part of the cooling medium is withdrawn at the at least one additional withdrawal point and the remainder exits at the withdrawal point near the end of the reaction tubes.

Abstract: Propene is continuously reacted with hydrogen peroxide in a tube bundle reactor comprising a multitude of parallel reaction tubes in the presence of a titanium silicalite catalyst arranged as a fixed bed in the reaction tubes. A cooling jacket encloses the reaction tubes, which has a feed point for cooling medium near the entry of the reaction tubes, a withdrawal point for cooling medium near the end of the reaction tubes and at least one additional withdrawal point upstream of the withdrawal point near the end of the reaction tubes. Cooling medium is fed to the feed point for cooling medium, a part of the cooling medium is withdrawn at the at least one additional withdrawal point and the remainder exits at the withdrawal point near the end of the reaction tubes.

Abstract: An electrochemical battery is disclosed. The electrochemical battery has an electrode plate comprising a frame and a generally flat grid connected to the frame, the frame comprising at least a top frame member having a contact lug, wherein the grid comprises a plurality of grid wires and a plurality of window-like open areas between the grid wires, further comprising an active mass within the open areas and/or on the grid wires, wherein the electrode plate comprises on one outer surface or on both opposing outer surfaces of the active mass a pattern of grooves, wherein the grooves extend diagonally from a position closer to the top frame member to a position further away from the top frame member. A method for producing an electrode plate is also disclosed.

Abstract: The invention relates to a falling film evaporator, which is fitted with a liquid distributor which is divided into segments, such that it is possible to charge only a limited number of evaporator tubes with liquid and the evaporator can be operated in an optimum manner even with a partial load. The invention also relates to a method for operating said falling film evaporator, the aim of which is to transfer heat, which is released when a gas-vapor mixture is condensed, to a liquid which is to be evaporated at least partially. It would be useful to use said falling film evaporator thus fitted in heat recuperation systems such as those used in the production of 1,2 dichloroethane.

Abstract: A distributor includes first and second liquid distribution systems for two liquid phases for an upright tube-bundle reactor. The first system is arranged directly above or on a tubesheet and is connected to at least one outer feed device and contains an annular weir. The second system is connected to at least one other outer feed device and contains one upper and one lower distribution tray which contains a plurality of openings which are arranged flush above the inlet sleeves of the first system, and has at least one device for setting a uniform liquid level above the openings. The upper distribution tray is connected to the feed device for liquid, and contains a plurality of overflow weirs from which the liquid is able to discharge into the lower distribution tray. Each of the overflow weirs is assigned to a plurality of openings of the lower distribution tray.

Abstract: The invention relates to a falling film evaporator, which is fitted with a liquid distributor which is divided into segments, such that it is possible to charge only a limited number of evaporator tubes with liquid and the evaporator can be operated in an optimum manner even with a partial load. The invention also relates to a method for operating said falling film evaporator, the aim of which is to transfer heat, which is released when a gas-vapor mixture is condensed, to a liquid which is to be evaporated at least partially. It would be useful to use said falling film evaporator thus fitted in heat recuperation systems such as those used in the production of 1,2 dichloroethane.

Abstract: A liquid distributor for two liquid phases to be uniformly distributed into a plurality of tubes of an upright tube-bundle reactor for carrying out chemical reactions, wherein the inside of the tubes forming the tube bundle are provided for a trickle-bed operation, the tubes are retained at the top and bottom by tubesheets and are closed against the outside of the tube, a distribution chamber is arranged above the upper tubesheet, which chamber contains feed pipes for two different liquids and at least one gas phase, wherein a first liquid distribution system is arranged directly above the tubesheet or on it, which system is connected to at least one outer feed device and contains an annular weir installed outside the tubed area, with openings at the bottom and a plurality of inlet sleeves, wherein one inlet sleeve is assigned at the top to each of the tubes of the tube bundle, the inlet sleeves are of tubular design and are vertically aligned, and the said sleeves have at least one lateral and one further op

Abstract: The invention relates to a method and a device for the optimal use of reaction heat resulting from the production of 1,2-dichloroethane from ethene and chlorine. The aim of the invention is achieved by extracting reaction heat liberated during the reaction of chlorine with ethene and the reaction heat contained in 1,2-dichloroethane. Extraction of said reaction heat from the reaction chamber occurs using at least one part of gaseous 1,2-dichloroethane (latent heat) and at least one part of liquid 1,2-dichloroethane (feelable heat) removed from the reaction chamber. Said reaction heat is used to heat two fractioning columns in order to purify 1,2-dichloroethane of impurities having a boiling point higher than 1,2-dichloroethane.

Abstract: By a process for the production of 1,2-dichloroethane (EDC) by reaction of ethylene with chlorine in the liquid phase (direct chlorination), the heavy ends being separated from the obtained 1,2-dichloroethane in a heavy-ends column and in a downstream vacuum column and, for the purpose of heat recovery and heating of the column bottoms, a 1,2-dichloroethane part-stream from the direct chlorination passing through a heat exchanger (one attributed to each column) for indirect heat exchange with the bottom product of each column, the aim of the invention is to provide a solution in which the reaction enthalpy of the direct chlorination can be used in a variable manner, thus precluding the above-described disadvantages. This is achieved by using at least one falling-film evaporator for heating the column bottoms, the bottom product of the respective column being routed to the distributor at the head of the column.