Abstract: Disclosed is a method for preparing a compound of Formula 1 by contacting compound of Formula 2 with R1—NH2 in the presence of a carboxylic acid and a method for preparing a compound of Formula 2 by contacting a compound of Formula 4 with phosphorus tribromide. wherein R1 is H, C1-C4 alkyl, cyclopropyl, cyclopropylmethyl or methylcyclopropyl; R2 is CH3 or Cl; R3 is C1-C6 alkyl or C3-C6 alkenyl, each optionally substituted with up to 3 halogen and up to 1 phenyl; and X is Cl or Br. Also disclosed is a method for preparing a compound of Formula 5 wherein R4, R5, R6 and Z are as defined in the disclosure, using a compound of Formula 1 that is characterized by preparing the compound of Formula 1 by the method above.

Abstract: Disclosed is a method for preparing a compound of Formula 1 by contacting compound of Formula 2 with R1—NH2 in the presence of a carboxylic acid and a method for preparing a compound of Formula 2 by contacting a compound of Formula 4 with phosphorus tribromide. wherein R1 is H, C1-C4 alkyl, cyclopropyl, cyclopropylmethyl or methylcyclopropyl; R2 is CH3 or Cl; R3 is C1-C6 alkyl or C3-C6 alkenyl, each optionally substituted with up to 3 halogen and up to 1 phenyl; and X is Cl or Br. Also disclosed is a method for preparing a compound of Formula 5 wherein R4, R5, R6 and Z are as defined in the disclosure, using a compound of Formula 1 that is characterized by preparing the compound of Formula 1 by the method above.

Abstract: Methods and apparatus are provided for an interconnect system for coupling radio frequency signals from one component to another in a RF system. The interconnect system acts as a coaxial connection. The apparatus comprises an interconnect, a dielectric sleeve, and a conductive elastomeric gasket. The interconnect has a first major surface and second major surface for providing an electrical connection. A through hole is formed in a first component. The dielectric sleeve is placed in the through hole. The interconnect is placed in the dielectric sleeve. The conductive elastomeric gasket is placed in proximity to the through hole contacting the first component and a second component. The RF system is assembled compressing the elastomeric gasket to have intimate contact with the first and second component. The intimate contact electrically connects the first and second component and an electric shield is formed around the interconnect thereby suppressing the reception and transmission of RF signals.

Abstract: Methods and apparatus are provided for an interconnect system for coupling radio frequency signals from one component to another in a RF system. The interconnect system acts as a coaxial connection. The apparatus comprises an interconnect, a dielectric sleeve, and a conductive elastomeric gasket. The interconnect has a first major surface and second major surface for providing an electrical connection. A through hole is formed in a first component. The dielectric sleeve is placed in the through hole. The interconnect is placed in the dielectric sleeve. The conductive elastomeric gasket is placed in proximity to the through hole contacting the first component and a second component. The RF system is assembled compressing the elastomeric gasket to have intimate contact with the first and second component. The intimate contact electrically connects the first and second component and an electric shield is formed around the interconnect thereby suppressing the reception and transmission of RF signals.

Abstract: A radiographic silver halide film has reduced yellow dye stain by including a blend of tabular silver halide grains in the emulsion layers. The blend of grains includes blue-sensitive tabular silver halide grains that have an aspect ratio of at least 15, a grain thickness of at least 0.1 &mgr;m, and comprise at least 90 mol % bromide and up to 4 mol % iodide, based on total silver halide. Substantially all of the iodide is present in an internal localized portion of the tabular silver halide grains that excludes the surface of the grains. The blend also includes green-sensitive tabular silver halide grains that have an aspect ratio of at least 20, a grain thickness of at least 0.07 &mgr;m, and comprise at least 90 mol % bromide, up to 1.5 mol % chloride, and up to 1.5 mol % iodide, based on total silver halide. The molar ratio of silver in the blue-sensitive silver halide grains to the silver in the green-sensitive silver halide grains is from about 2:1 to about 6:1.

Abstract: A blue-sensitive, radiographic silver halide film comprises a silver halide emulsion layer comprising predominantly tabular silver halide grains that have an aspect ratio of at least 15, a grain thickness of at least 0.1 &mgr;m, and comprise at least 90 mol % bromide and up to 4 mol % iodide, based on total silver halide. Substantially all of the iodide is present in an internal localized portion of the tabular silver halide grains that excludes the surface of the grains. The tabular silver halide grains are dispersed in a hydrophilic polymeric vehicle mixture comprising at least 0.5% of oxidized gelatin, based on the total dry weight of the polymeric vehicle mixture in the emulsion layer.

Abstract: A blue-sensitive, radiographic silver halide film comprises a silver halide emulsion layer comprising predominantly tabular silver halide grains that have an aspect ratio of at least 15, a grain thickness of at least 0.1 &mgr;M, and comprise at least 90 mol % bromide and from about 0.5 to about 2.75 mol % iodide, based on total silver halide. Substantially all of the iodide is present in an internal localized portion of the tabular silver halide grains that excludes the surface of the grains. The tabular silver halide grains are dispersed in a hydrophilic polymeric vehicle mixture comprising at least 0.5% of oxidized gelatin, based on the total dry weight of the polymeric vehicle mixture in the emulsion layer. In addition, the tabular grain emulsion includes a mercapto-substituted benzothiazole, benzoxazole, or benzimidazole to provide desired image tone and processability.

Abstract: A blue-sensitive radiographic silver halide film comprises a silver halide emulsion layer comprising predominantly tabular silver halide grains that have an aspect ratio of at least 15, a grain thickness of at least 0.1 &mgr;m, and comprise at least 90 mol % bromide and up to 4 mol % iodide, based on total silver halide. Substantially all of the iodide is present in an internal localized portion of the tabular silver halide grains that excludes the surface of the grains. The tabular silver halide grains are dispersed in a hydrophilic polymeric vehicle mixture comprising at least 0.5% of oxidized gelatin, based on the total dry weight of the polymeric vehicle mixture in the emulsion layer. The tabular silver halide grains are spectrally sensitized using a combination of spectral sensitizing dyes to provide increased speed and reduced dye stain.

Abstract: An imaging assembly includes a blue-sensitive, radiographic silver halide film comprises a silver halide emulsion layer comprising predominantly tabular silver halide grains that have an aspect ratio of at least 15, a grain thickness of at least 0.1 &mgr;m, and comprise at least 90 mol % bromide and up to 4 mol % iodide, based on total silver halide. The tabular silver halide grains are dispersed in a hydrophilic polymeric vehicle mixture comprising at least 0.5% of oxidized gelatin. The film is used in combination with one or more intensifying screens that absorb X-radiation and emit radiation having a wavelength of from about 300 to about 500 nm. In many embodiments, the intensifying screens include a “blue-light” emitting alkaline earth fluorohalide phosphor dispersed in a binder on a support.

Abstract: A method and device for detecting and/or photographing unregulated light flash events such as lighting strikes and muzzle flashes during both daylight and night time conditions is disclosed. The present device utilizes a photodiode sensor in conjunction with a photoresistor to control feedback gain of a transimpedance amplifier thereby providing non-linear amplification and therein constant sensitivity to detect an unregulated, omni-directional flash of light and produce an output signal that is input to an analog comparator circuit whereat a predetermined threshold level is set to prevent false triggering of the isolation relays and/or camera shutter. The output from the comparator circuit is input to a timer circuit to produce a signal of sufficient duration to trigger the isolation relay(s) and/or camera shutter.

Abstract: A method and device for detecting and photographing unregulated light flash events such as lighting strikes during both daylight and night time conditions is disclosed by detecting the initiation of the lightning stepped leader event of the immediate lightning flash for photographic and detecting activities. The present device utilizes a photodiode sensor in conjunction with a photoresistor to control feedback gain of a transimpedance amplifier to detect an unregulated, omni-directional flash of light and produces an output signal that is input to an analog comparator circuit where a predetermined threshold level is set to prevent false triggering of the isolation relay(s) and/or camera shutter. The output from the comparator circuit is input to a timer circuit to produce a signal of sufficient duration to trigger the isolation relay(s) and/or camera shutter.

Abstract: An adhesive and method for attaching a heat sink to a printing wiring assembly that provides a thermal path from electronic components on the printing wiring assembly to the heat sink. The adhesive is flexible and accommodates thermal expansion stresses and is readily reworkable. The adhesive comprises a filler material that is disposed between the heat sink and the printing wiring assembly, and an impregnant that impregnates the filler material, which impregnated filler material is cured. The filler material may comprise alumina particles that have a spherical shape. The impregnant comprises a polymer, typically selected from a group of epoxy resins and their curatives that form a flexible material when cured. In practicing the method, a heat sink is positioned adjacent to and spaced apart from a printing wiring assembly to provide an appropriate spacing between them. The periphery of the printing wiring assembly is sealed.

Abstract: A thermally conductive wedgelock having improved thermal conductivity is used to secure a circuit card assembly in a card guide slot formed in a housing of an electronics package. The circuit card assembly has a thermal mounting plate that is used to secure the assembly in the slot. The thermally conductive wedgelock secures the circuit card assembly in the housing and conductively couples heat from the circuit card assembly to the housing by way of the card guide slot. The wedgelock provides a secondary heat path to the card guide slot to housing in addition to the primary heat path through the thermal mounting plate. Apparatus is provide for expanding the wedgelock in the card guide slot to secure the circuit card assembly therein. The thermally conductive wedgelock may be made of copper or other metal having high thermal conductivity. The wedgelock preferably comprises two tapered wedges, and has a guide that prevents rotation between the adjacent wedges.

Abstract: This invention relates to a process for preparing sulfonylureas comprising reacting a sulfonyl chloride with a cyanate salt and an amine base in the presence of an inert aprotic solvent to give an isocyanate complex which is then reacted with an amino heterocycle to form the sulfonylurea product and a process for converting the crystal form of the prepared sulfonylurea product to a more stable crystal product form.

Abstract: A process for the preparation of 2-chloro-6-haloquinoxaline compounds from the corresponding 4-halo-2-nitroaniline utilizing four reaction steps with generally compatible solvents and reagents with volatile by-products to minimize the isolation and purification of intermediates has been developed.

Abstract: A curved mandrel, method of making same, and method of curing an uncured polymeric hose employing such curved mandrel are provided and the curved mandrel comprises a plurality of members disposed in end-to-end relation to define the configuration of the mandrel including a predetermined curvature therein, interlocking portions for interlocking the members in only one position to define the configuration and curvature, and a readily attachable and detachable device for holding the members axially against each other after interlocking wherein the members with the interlocking portions and holding device are adapted to provide a substantially straight mandrel for installation of an uncured straight hose therearound, define the configuration and curvature in the mandrel and uncured hose, and provide looseness and axial spacing between members to enable easy withdrawal of the cured curved hose from around the members.

Abstract: A curved mandrel, method of making same, and method of curing an uncured polymeric hose employing such curved mandrel are provided and the curved mandrel comprises a plurality of members disposed in end-to-end relation to define the configuration of the mandrel including a predetermined curvature therein, interlocking portions for interlocking the members in only one position to define the configuration and curvature, and a readily attachable and detachable device for holding the members axially against each other after interlocking wherein the members with the interlocking portions and holding device are adapted to provide a substantially straight mandrel for installation of an uncured straight hose therearound, define the configuration and curvature in the mandrel and uncured hose, and provide looseness and axial spacing between members to enable easy withdrawal of the cured curved hose from around the members.

Abstract: A tool for and method of removing a die-cutting mat from a rotary anvil is provided wherein such anvil has a groove therein provided with an immobile locking wedge disposed centrally therewithin and the die-cutting mat has flanges at opposite end portions thereof which are snap locked in position utilizing the locking wedge.