Abstract: A multi-layer tile material produced from layers of alumina enhanced thermal barrier material having different densities. The insulation layers are bound together by a high strength, high temperature alumina or silica binder having a coefficient of thermal expansion similar to that of the insulation layers. Use of the multi-layered tile allows the problems of tile slumping and of insufficient heat management associated with low density alumina enhanced thermal barrier tile to be overcome.

Abstract: A porous ceramic body protected by a damage resistant hardened surface, and a method for preparing the surface hardened ceramic body. The ceramic body is protected by applying to the surface a slurry composition containing a binding agent, particles of a ceramic material, at least one boron containing compound, and a solvent. The inclusion of at least one boron containing compound in the slurry provides for hardened surfaces that are stable to higher temperatures as compared to those of the prior art.

Abstract: Oxide based ceramic matrix composites (CMC) having superior properties at high temperatures exhibit a sol gel matrix with mixed or blended metal oxide particles. The sol-gel matrix is an aqueous colloidal suspension of a metal oxide, preferably from about 10 wt % to about 25 wt % of the metal oxide, and preferably containing a metal oxide such as alumina (Al2O3), silica (SiO2) or alumina-coated silica.The mixture is then infiltrated into a ceramic fabric, gelled, dried and sintered to form the CMC of the present invention. Methods for making the CMC of the present invention are also provided.

Abstract: An article is fabricated with a ceramic surface having a controllable surface finish. In one form, the ceramic is applied as a coating to a substrate article. Preferably, an aqueous coating mixture of phosphoric acid, alumina powder, and cordierite powder is prepared. The mixture is contacted to the surface of the article, and a mechanical overpressure is applied to the external surface of the mixture using a pressing tool. The surface character of the pressing tool, such as a smooth surface or an intentionally patterned surface, is reproduced on the surface of the final ceramic coating. The coating is heated to a moderate temperature to set the ceramic of the coating, and thereafter the coating is heated to a higher, but still intermediate temperature, to cure the coating.

Abstract: An insulative body having first and second porous insulation members and a ceramic binder. Each of the first and second porous insulation members is formed of a fibrous, low-density silica-based material and cooperatively defines a joint. The ceramic binder is disposed between a pair of mating surfaces that form the joint. The ceramic binder couples the first and second porous insulation members together. A method for bonding insulative bodies to one another through the use of an ceramic/organic thermal setting binder is also provided.

Abstract: An article is fabricated with a ceramic surface having a controllable surface finish. In one form, the ceramic is applied as a coating to a substrate article. Preferably, an aqueous coating mixture of phosphoric acid, alumina powder, and cordierite powder is prepared. The mixture is contacted to the surface of the article, and a mechanical overpressure is applied to the external surface of the mixture using a pressing tool. The surface character of the pressing tool, such as a smooth surface or an intentionally patterned surface, is reproduced on the surface of the final ceramic coating. The coating is heated to a moderate temperature to set the ceramic of the coating, and thereafter the coating Is heated to a higher, but still intermediate temperature, to cure the coating.

Abstract: A method of making a permeable fiber-reinforced ceramic body comprising mixing an organic particulate with silica fiber, alumina fiber, alumina borosilicate fiber, a dispersant, and water to produce a slurry of fibrous ceramic material. The slurry is then placed within a mold and vaccuum pressure is applied thereto to substantially remove the water to form a fibrous ceramic body. The fibrous ceramic body is then dried and sintered to a temperature sufficient to bond the ceramic material together to form a porous ceramic article. Simultaneously, the fibrous ceramic body is heated to a temperature sufficient to generally burn off the organic particulate to create voids interconnecting the pores to form a permeable fiber reinforced porous ceramic article.

Abstract: A ruddervator for an aerospacecraft. The ruddervator is formed by a plurality of airfoil sections nestably disposed in side by side fashion and supported by a pair of titanium box beam frame elements extending through central openings in each of the airfoil sections. Each airfoil section includes an oxide fiber/oxide matrix-based ceramic matrix composite (oxide-CMC) panel made up of multiple plies of oxide-CMC fabric which are fused over a rigid ceramic foam insulation member. The lower ends of the frame elements are secured to a transition component comprising a conventional torque box. The ruddervator can be manufactured with less cost and lower weight over previous ruddervator designs which require one or more large skin sections which are mechanically fastened to a substructure. The ruddervator of the present invention further minimizes fabrication costs by using a common design for the nesting airfoil sections so that a common female lay-up mold can be used for fabricating all of the airfoil sections.

Abstract: An article has at its surface a nonmetallic ceramic form of a cation reactive with phosphate ion to form a ceramic phosphate, such as an oxide of a cation selected from the group consisting of beryllium, aluminum, iron, magnesium, calcium, thorium, barium, zirconium, zinc, silicon, and mixtures thereof. A source of reactive phosphate ions, such as concentrated phosphoric acid or monoaluminum phosphate, is applied to the surface of the article. The surface of the article is thereafter heated to cause the nonmetallic ceramic form of the cation and the source of the reactive phosphate ions to react together, producing a phosphate-bonded hard layer at the surface of the article.

Abstract: A ceramic composition for the repair of porous ceramic bodies comprises a ceramic material having cations which are reactive with phosphate ions, a source of reactive phosphate ions, and filler. An aqueous slurry of the ceramic composition is prepared and applied to the damaged region of a porous ceramic body. The slurry mixture is dried within the damaged region of the porous ceramic body and heated to bind the mixture together and to bond the mixture to the porous ceramic body within the damaged region. The method of the invention allows for the in situ repair of ceramic materials without removing them from their supporting structure and can be used in the repair of ceramic tiles for spacecraft and aircraft.

Abstract: A surface of a porous ceramic body is protected by binding ceramic particles entirely within the subsurface porosity of the body adjacent to the surface but not present as a separately identifiable surface layer. To produce such a protective layer, a slurry of a mixture of a ceramic powder and a silica-containing binding agent is first prepared. The slurry is impregnated into the surface of the body so that all of the slurry enters the porosity of the body and substantially none of the slurry resides on the surface. The slurry is dried in place, and the residual solids are fired to bind the ceramic powder to the interior walls of the porosity. Drying and firing can be accomplished at intermediate temperatures of about 700-1000.degree. F. using heat lamps, so that the surface protection can be accomplished without removing the ceramic body from a larger structure.

Abstract: A surface of a porous ceramic body is protected by binding ceramic particles entirely within the subsurface porosity of the body adjacent to the surface but not present as a separately identifiable surface layer. To produce such a protective layer, a slurry of a mixture of a ceramic powder and a silica-containing binding agent is first prepared. The slurry is impregnated into the surface of the body so that all of the slurry enters the porosity of the body and substantially none of the slurry resides on the surface. The slurry is dried in place, and the residual solids are fired to bind the ceramic powder to the interior walls of the porosity. Drying and firing can be accomplished at intermediate temperatures of about 700.degree.-1000.degree. F. using heat lamps, so that the surface protection can be accomplished without removing the ceramic body from a larger structure.