Abstract: A method for calibrating an analysis instrument, e.g., a gas chromatograph, for water analysis that includes four steps. The first step is to continuously remove water from a liquid that contains water to produce a liquid containing a reduced amount of water such as by membrane pervaporation. The second step is to analyze the liquid containing a reduced amount of water for water by a reference water analysis method such as by Karl Fischer titration. The third step is to analyze the stream of liquid containing a reduced amount of water using the instrument to be calibrated, e.g., a gas chromatograph having a helium photoionization pulse discharge detector. The fourth step is to calibrate the instrument using the analysis of the second step. In a related embodiment, a system for normal phase chromatography.

Abstract: The invention provides a method for measuring an acyl coenzyme A (acyl CoA) ester or esters in a sample, comprising the steps of: a) forming a reaction mixture comprising the sample to be tested and a derivatizing agent; b) allowing the sample and said derivatizing agent to react, so as to form a fluorescent derivative(s) of any acyl CoA ester(s) present in the sample; and c) determining a level of said fluorescent derivative(s).

Abstract: A binder composition for aqueous coatings that exhibit high gloss and superior corrosion resistance when applied to metal substrates comprising an aqueous emulsion copolymer, the copolymer including as polymerized units, at least one ethylenically unsaturated monomer and an ethylenically unsaturated strong acid monomer, such as phosphorus containing monomers, particularly phosphoethylmethacrylate; or salts thereof. Also provided is a method for achieving high gloss and superior corrosion resistance of metal substrates by coating a substrate with an aqueous coating composition comprising the binders of the present invention and drying, or allowing to dry, the aqueous composition.

Abstract: A polymer composition is provided including copolymer particles bearing phosphorus acid groups dispersed in an aqueous medium, wherein the polymer composition is substantially-free of water soluble phosphorus acid compounds. Also provided is a monomer composition containing at least one phosphorus acid monomer and a method of preparing the polymer composition from the monomer composition. The monomer composition is substantially-free of inorganic phosphorus acid compounds. A method is provided for applying the polymer composition to a substrate. The polymer composition is useful as a coating composition to prepare coatings for metal substrates, which have improved solvent resistance.

Abstract: An apparatus having a foot, a reciprocating saw and a housing. Between the foot and the housing there are means for releasable mounting the foot on the housing, characterized in that the releasable mounting means have a first coupling member connected to the foot and, co-acting therewith, a second coupling member connected to the housing. The coupling members can be carried from a disconnected to a connected position by a relative displacement between the foot and housing.

Abstract: A polymer composition is provided including copolymer particles bearing phosphorus acid groups dispersed in an aqueous medium, wherein the polymer composition is substantially-free of water soluble phosphorus acid compounds. Also provided is a monomer composition containing at least one phosphorus acid monomer and a method of preparing the polymer composition from the monomer composition. The monomer composition is substantially-free of inorganic phosphorus acid compounds. A method is provided for applying the polymer composition to a substrate. The polymer composition is useful as a coating composition to prepare coatings for metal substrates, which have improved solvent resistance.

Abstract: The invention is an automated lap washer and rack system for washing and drying aluminum laps used in the processing of opthalmic lenses and consists of an enclosure containing a washing and a drying chamber through which special mounting trays, removably attached to a table top conveyor, carry aluminum laps first through the washing stage and then through the drying chamber.

Abstract: A continuous process for oligomers which do not contain, as polymerized units, carboxylic acid-containing monomers and their salts, including the steps of: (1) forming a reaction mixture, substantially free of carboxylic acid-containing monomers and their salts, containing: (i) 0.5 to 99.95% by weight of the reaction mixture of at least one ethylenically unsaturated monomer; and (ii) 0.05 to 25% by weight, based on the weight of the ethylenically unsaturated monomer, of at least one free-radical initiator; and (2) continuously passing the reaction mixture through a heated zone wherein the reaction mixture is maintained at a temperature of at least 150° C. and a pressure of at least 30 bars for from 0.1 seconds to 4 minutes to form terminally-unsaturated oligomers. In addition, processes for forming oligomers of vinyl acetate and oligomers of vinyl alcohol are disclosed. Mixtures of fully saturated and terminally unsaturated oligomers are also disclosed.

Abstract: An aqueous composite particle composition containing composite particles and polyvalent metal ion is provided. The composite particles contain pigment particle with adsorbed polymer particles. The polymer particles contain pendant acid functional groups and has a molecular weight in a select range. Also provided are methods of preparing the aqueous composite particle composition. The aqueous composite particle composition is useful for preparing coating with high gloss and improved solvent resistance.

Abstract: A continuous process for oligomers which do not contain, as polymerized units, carboxylic acid-containing monomers and their salts, including the steps of:

Abstract: An apparatus having a foot, a reciprocating saw and a housing. Between the foot and the housing there are means for releasable mounting the foot on the housing, characterized in that the releasable mounting means have a first coupling member connected to the foot and, co-acting therewith, a second coupling member connected to the housing. The coupling members can be carried from a disconnected to a connected position by a relative displacement between the foot and housing.

Abstract: A continuous process for oligomers which do not contain, as polymerized units, carboxylic acid-containing monomers and their salts, including the steps of:

Abstract: A binder composition for aqueous coatings that exhibit high gloss and superior corrosion resistance when applied to metal substrates comprising an aqueous emulsion copolymer, the copolymer including as polymerized units, at least one ethylenically unsaturated monomer and an ethylenically unsaturated strong acid monomer, such as phosphorus containing monomers, particularly phosphoethylmethacrylate; or salts thereof Also provided is a method for achieving high gloss and superior corrosion resistance of metal substrates by coating a substrate with an aqueous coating composition comprising the binders of the present invention and drying, or allowing to dry, the aqueous composition.

Abstract: Aqueous dispersion of copolymers formed by the polymerization of a monomer mixture containing 0.05% to less than 4.5% by weight of certain terminally unsaturated oligomers are useful for improving the scrub resistance, corrosion resistance, opacifying capacity and/or efflorescence resistance of a coating.

Abstract: A method of crosslinking an oxidative polymer having oxidatively crosslinkable functional groups and a two-pack composition used therein. The oxidatively crosslinkable functional groups on the oxidative polymer are crosslinked by contacting the oxidative polymer with a catalytic amount of an oxidizing enzyme, such as horseradish peroxidase. The present invention is further directed to a two-pack coating composition which includes a polymeric component and a catalytic component, which are mixed together prior to use.

Abstract: The present invention is directed to a method of producing a waterborne isocyanate-modified acrylic polymer. The method provides for reacting a compound having at least two-isocyanate functionalities with an isocyanate-reactive polymer to produce the isocyanate-modified acrylic polymer of the present invention having extended shelf stability and solvent resistance.

Abstract: A method of crosslinking an oxidative polymer having oxidatively crosslinkable functional groups and a two-pack composition used therein is provided. The oxidatively crosslinkable functional groups on the oxidative polymer are crosslinked by contacting the oxidative polymer with a catalytic amount of an oxidizing enzyme, such as horseradish peroxidase. The present invention is further directed to a two-pack coating composition which includes a polymeric component and a catalytic component, which are mixed together prior to use.

Abstract: High temperature polymerization process and products obtained therefrom are provided. The polymerization is conducted at above 225.degree. C. to produce polymers having a degree of polymerization below 50. The products are useful as detergent additives and for subsequent polymerization.

Abstract: The present invention is directed to producing a luminescent screen used in a cathode ray tube (CRT) suitable for monochromatic or chromatic images, such as, those utilized in televisions, computers or data monitoring equipment, which require CRTs. The method of the present invention produces an ablative layer of the luminescent screen having a smooth surface with reduced surface distortions, such as, streaks and waviness, which are typically produced by conventional coating processes. When a reflective aluminum film is deposited on such a smooth ablative layer, the reflective aluminum film is also provided with a smooth surface, since it typically conforms to the underlying smooth surface of the ablative layer. As a result, CRT images having reduced distortions are produced.

Abstract: High temperature polymerization process and products obtained therefrom are provided. The polymerization is conducted at above 225.degree. C. to produce polymers having a degree of polymerization below 50. The products are useful as detergent additives and for subsequent polymerization.