Patents by Inventor Rupert Spence

Rupert Spence has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 9828328
    Abstract: A method for preparing 3-methyl-2-nitrobenzoic acid is disclosed wherein 1,3-dimethyl-2-nitrobenzene is combined with an oxidation catalyst in the presence of an oxygen source and an initiator, provided that less than 99% of the 1,3-dimethyl-2-nitrobenzene is oxidized. A method for preparing compounds of Formula 7 and Formula 11 is also disclosed wherein the method is characterized by using 3-methyl-2-nitrobenzoic acid as prepared by the method disclosed above. wherein R1 is C1-C7 alkyl, C3-C6 cycloalkyl or C4-C7 alkylcycloalkyl.
    Type: Grant
    Filed: May 29, 2015
    Date of Patent: November 28, 2017
    Assignee: E I DU PONT DE NEMOURS AND COMPANY
    Inventors: Stephen Ernest Jacobson, Donald J. Dumas, Rupert Spence, Sarah May Crawford, Venkateswara Rao Surisetty
  • Publication number: 20170197907
    Abstract: A method for preparing 3-methyl-2-nitrobenzoic acid is disclosed wherein 1,3-dimethyl-2-nitrobenzene is combined with an oxidation catalyst in the presence of an oxygen source and an initiator, provided that less than 99% of the 1,3-dimethyl-2-nitrobenzene is oxidized. A method for preparing compounds of Formula 7 and Formula 11 is also disclosed wherein the method is characterized by using 3-methyl-2-nitrobenzoic acid as prepared by the method disclosed above.
    Type: Application
    Filed: May 29, 2015
    Publication date: July 13, 2017
    Inventors: Stephen Ernest Jacobson, Donald J. Dumas, Rupert Spence, Sarah May Crawford, Venkateswara Rao Surisetty
  • Patent number: 8598391
    Abstract: Processes for reducing the color of polytrimethylene ether glycol or copolymers thereof are provided. The processes include polycondensing diols in the presence of an acid catalyst and adding base continuously over a period of the polycondensation reaction. The invention also relates to the polytrimethylene ether glycol thereof produced by these processes.
    Type: Grant
    Filed: September 29, 2010
    Date of Patent: December 3, 2013
    Assignee: E I du Pont de Nemours and Company
    Inventors: Aaron Minter, Edward R. Murphy, Howard C. Ng, Rupert Spence, Tuyu Xie
  • Patent number: 8148491
    Abstract: This invention relates to a process for preparing polytrimethylene ether glycols or copolymers thereof by a polycondensation reaction using at least one acid catalyst, wherein the temperature of the reaction is controlled such that the average temperature during the first half of the reaction is higher than the average temperature during the second half of the reaction.
    Type: Grant
    Filed: October 31, 2008
    Date of Patent: April 3, 2012
    Assignee: E I du Pont de Nemours and Company
    Inventors: David C. Confer, Mark Andrew Harmer, Christian Hoffmann, Scott Christopher Jackson, Sigridur Soley Kristjansdottir, Rupert Spence
  • Patent number: 8143371
    Abstract: This invention relates to a process for preparing polytrimethylene ether glycols or copolymers thereof having a number-average molecular weight of at least about 250 g/mole by a polycondensation reaction using at least one acid catalyst.
    Type: Grant
    Filed: October 31, 2008
    Date of Patent: March 27, 2012
    Assignee: E I du Pont de Nemours and Company
    Inventors: Mark Andrew Harmer, Christian Hoffmann, Scott Christopher Jackson, Edward R. Murphy, Rupert Spence
  • Publication number: 20110077433
    Abstract: Processes for reducing the color of polytrimethylene ether glycol or copolymers thereof are provided. The processes include polycondensing diols in the presence of an acid catalyst and adding base continuously over a period of the polycondensation reaction. The invention also relates to the polytrimethylene ether glycol thereof produced by these processes.
    Type: Application
    Filed: September 29, 2010
    Publication date: March 31, 2011
    Applicant: E.I. DU PONT DE NEMOURS AND COMPANY
    Inventors: Aaron Minter, Edward R. Murphy, Howard C. Ng, Rupert Spence, Tuyu Xie
  • Publication number: 20100267994
    Abstract: Processes for preparing polytrimethylene ether glycol or copolymers thereof using an acid polycondensation catalyst and ion exchange resins are provided.
    Type: Application
    Filed: April 14, 2010
    Publication date: October 21, 2010
    Applicant: E. I. DU PONT DE NEMOURS AND COMPANY
    Inventor: Rupert SPENCE
  • Publication number: 20090118465
    Abstract: This invention relates to a process for preparing polytrimethylene ether glycols or copolymers thereof by a polycondensation reaction using at least one acid catalyst, wherein the temperature of the reaction is controlled such that the average temperature during the first half of the reaction is higher than the average temperature during the second half of the reaction.
    Type: Application
    Filed: October 31, 2008
    Publication date: May 7, 2009
    Applicant: E. I. DU PONT DE NEMOURS AND COMPANY
    Inventors: David C. Confer, Mark Andrew Harmer, Christian Hoffmann, Scott Christopher Jackson, Sigridur Soley Kristjansdottir, Rupert Spence
  • Publication number: 20090118464
    Abstract: This invention relates to a process for preparing polytrimethylene ether glycols or copolymers thereof having a number-average molecular weight of at least about 250 g/mole by a polycondensation reaction using at least one acid catalyst.
    Type: Application
    Filed: October 31, 2008
    Publication date: May 7, 2009
    Applicant: E. I. DU PONT DE NEMOURS AND COMPANY
    Inventors: Mark Andrew Harmer, Christian Hoffmann, Scott Christopher Jackson, Edward R. Murphy, Rupert Spence
  • Patent number: 7022787
    Abstract: Improved suspensions of transition metal complexes of 2,6-diacylpyridine(bisimines) or 2,6-pyridinedicarboxaldehyde(bisimines), which are useful in catalysts for the polymerization or oligomerization of olefins, are prepared by sonicating a mixture of one or more of these complexes and an inert liquid. The resulting suspensions can be directly used as olefin polymerization or oligomerization catalyst components in oligomerization or polymerization processes. These processes may produce, for example, polyolefins useful for molding resins or films, or linear ?-olefins.
    Type: Grant
    Filed: September 23, 2004
    Date of Patent: April 4, 2006
    Assignee: E. I. du Pont de Nemours and Company
    Inventors: Rupert Spence, Robert Louis Stevens
  • Publication number: 20050113248
    Abstract: Improved suspensions of transition metal complexes of 2,6-diacylpyridine(bisimines) or 2,6-pyridinedicarboxaldehyde(bisimines), which are useful in catalysts for the polymerization or oligomerization of olefins, are prepared by sonicating a mixture of one or more of these complexes and an inert liquid. The resulting suspensions can be directly used as olefin polymerization or oligomerization catalyst components in oligomerization or polymerization processes. These processes may produce, for example, polyolefins useful for molding resins or films, or linear ?-olefins.
    Type: Application
    Filed: September 23, 2004
    Publication date: May 26, 2005
    Inventors: Rupert Spence, Robert Stevens