Patents by Inventor Salkod Parameshwar Mallika
Salkod Parameshwar Mallika has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Publication number: 20230048457Abstract: A catalyst precursor composition for forming a phenol alkylation catalyst, the composition comprising: 70 to 98 weight percent of abase oxide comprising: magnesium oxide with a Brunauer-Emmett-Teller surface area from 75 meter2/gram to 220 meter2/gram, preferably from 75 meter2/gram to 140 meter2/gram, more preferably from 90 meter2/gram to 130 meter2/gram; or magnesium carbonate with a Brunauer-Emmett-Teller surface area of from 100 meter2/gram to 220 meter2/gram, preferably from 120 meter2/gram to 200 meter2/gram; or a combination thereof; at least one metal promoter precursor comprising an iron precursor, a manganese, a vanadium precursor, or a copper precursor; and a pore former, a lubricant, a coke inhibitor; and optionally, a strength additive; and optionally a binder, and a method of alkylating phenol using a catalyst derived from the catalyst precursor.Type: ApplicationFiled: December 24, 2020Publication date: February 16, 2023Inventors: Douglas Henry Lenz, Lawrence D'Souza, Lohith Kenchaiah, Salkod Parameshwar Mallika, Bedour Al-Sabban
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Patent number: 10737994Abstract: A method for purifying acetone includes contacting an initial solution with a basic ion-exchange resin at a temperature of 15° C. to 30° C., wherein the initial solution comprises acetone and acetone impurities; and removing the acetone impurities from the initial solution with the basic ion-exchange resin to produce a purified solution.Type: GrantFiled: July 12, 2017Date of Patent: August 11, 2020Assignee: SABIC GLOBAL TECHNOLOGIES B.V.Inventors: Syed Azhar Hashmi, Salkod Parameshwar Mallika, Flaiyh Al-Anazi
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Publication number: 20200181054Abstract: A method for purifying acetone includes contacting an initial solution with a basic ion-exchange resin at a temperature of 15° C. to 30° C., wherein the initial solution comprises acetone and acetone impurities; and removing the acetone impurities from the initial solution with the basic ion-exchange resin to produce a purified solution.Type: ApplicationFiled: July 12, 2017Publication date: June 11, 2020Applicant: SABIC Global Technologies B.V.Inventors: Syed Azhar Hashmi, Salkod Parameshwar Mallika, Flaiyh Al-Anazi
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Patent number: 10005884Abstract: Methods for synthesizing and purifying 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine compounds are provided. The method includes heating a reaction mixture including a phenolphthalein, a primary aryl amine, and an acid catalyst to form a phthalimidine; precipitating the phthalimidine from the reaction mixture to provide a crude phthalimidine; providing a solution including the crude phthalimidine, an additive, and at least one solvent; contacting the solution with one or more purification agents to provide a treated solution; precipitating and recovering a phthalimidine adduct from the treated solution; and recovering a purified phthalimidine compound from the adduct.Type: GrantFiled: April 22, 2015Date of Patent: June 26, 2018Assignee: SABIC GLOBAL TECHNOLOGIES B.V.Inventors: Anup Krishnnan Appukuttan Pillai, Shivakumar Konda, Gaurav Mediratta, Venkata Rama Narayanan Ganapathy Bhotla, Salkod Parameshwar Mallika, Pradeep Jeevaji Nadkarni
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Publication number: 20170029562Abstract: Methods for synthesizing and purifying 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine compounds are provided. The method includes heating a reaction mixture including a phenolphthalein, a primary aryl amine, and an acid catalyst to form a phthalimidine; precipitating the phthalimidine from the reaction mixture to provide a crude phthalimidine; providing a solution including the crude phthalimidine, an additive, and at least one solvent; contacting the solution with one or more purification agents to provide a treated solution; precipitating and recovering a phthalimidine adduct from the treated solution; and recovering a purified phthalimidine compound from the adduct.Type: ApplicationFiled: April 22, 2015Publication date: February 2, 2017Inventors: Anup Krishnnan Appukuttan Pillai, Shivakumar Konda, Gaurav Mediratta, Venkata Rama Narayanan Ganapathy Bhotla, Salkod Parameshwar Mallika, Pradeep Jeevaji Nadkarni
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Patent number: 9340502Abstract: Disclosed herein is a method for producing a purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I) wherein R1 is hydrogen or a C1-25 hydrocarbyl group and R2 is a hydrogen, a C1-25 hydrocarbyl group, or a halogen, and wherein the method comprises dissolving a crude phthalimidine compound in an aqueous base solution; precipitating the dissolved, crude phthalimidine compound from the aqueous base solution by adding an acid in an amount effective to lower the pH of the solution to 9.0 to 12.0, to provide a semicrude phthalimidine compound; and isolating the semicrude phthalimidine compound from the aqueous base solution, to provide the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I), and having a phenolphthalein compound content of less than 2,500 ppm, based on the weight of the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine.Type: GrantFiled: August 18, 2014Date of Patent: May 17, 2016Assignee: SABIC GLOBAL TECHNOLOGIES B.V.Inventors: Venkata Rama Narayanan Ganapathy Bhotla, Balakrishnan Ganesan, Kishan Gurram, Salkod Parameshwar Mallika, Arun Satyanarayana Kumar, Shubashree Swaminathan
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Publication number: 20140357830Abstract: Disclosed herein is a method for producing a purified 2-aryl-3,3-bis(4-hydroxyaryl) phthalimidine of formula (I) wherein R1 is hydrogen or a C1-25 hydrocarbyl group and R2 is a hydrogen, a C1-25 hydrocarbyl group, or a halogen, and wherein the method comprises dissolving a crude phthalimidine compound in an aqueous base solution; precipitating the dissolved, crude phthalimidine compound from the aqueous base solution by adding an acid in an amount effective to lower the pH of the solution to 9.0 to 12.0, to provide a semicrude phthalimidine compound; and isolating the semicrude phthalimidine compound from the aqueous base solution, to provide the purified 2-aryl-3,3-bis(4-hydroxyaryl) phthalimidine of formula (I), and having a phenolphthalein compound content of less than 2,500 ppm, based on the weight of the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine.Type: ApplicationFiled: August 18, 2014Publication date: December 4, 2014Inventors: Venkata Rama Narayanan Ganapathy BHOTLA, Balakrishnan GANESAN, Kishan GURRAM, Salkod Parameshwar MALLIKA, Kumar Arun SATYANARAYANA, Swaminathan SHUBASHREE
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Patent number: 8809486Abstract: Disclosed is a method for producing a purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I) wherein R1 is hydrogen or a C1-25 hydrocarbyl group and R2 is a hydrogen, a C1-25 hydrocarbyl group, or a halogen, and wherein the method comprises dissolving a crude phthalimidine compound in an aqueous base solution; precipitating the dissolved, crude phthalimidine compound from the aqueous base solution by adding an acid in an amount effective to lower the pH of the solution to 9.0 to 12.0, to provide a semicrude phthalimidine compound; and isolating the semicrude phthalimidine compound from the aqueous base solution, to provide the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I), and having a phenolphthalein compound content of less than 2,500 ppm, based on the weight of the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine.Type: GrantFiled: July 13, 2012Date of Patent: August 19, 2014Assignee: Sabic Innovative Plastics IP B.V.Inventors: Venkata Rama Narayanan Ganapathy Bhotla, Balakrishnan Ganesan, Kishan Gurram, Salkod Parameshwar Mallika, Kumar Arun Satyanarayana, Swaminathan Shubashree
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Publication number: 20120309926Abstract: Disclosed is a method for producing a purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I) wherein R1 is hydrogen or a C1-25 hydrocarbyl group and R2 is a hydrogen, a C1-25 hydrocarbyl group, or a halogen, and wherein the method comprises dissolving a crude phthalimidine compound in an aqueous base solution; precipitating the dissolved, crude phthalimidine compound from the aqueous base solution by adding an acid in an amount effective to lower the pH of the solution to 9.0 to 12.0, to provide a semicrude phthalimidine compound; and isolating the semicrude phthalimidine compound from the aqueous base solution, to provide the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I), and having a phenolphthalein compound content of less than 2,500 ppm, based on the weight of the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine.Type: ApplicationFiled: July 13, 2012Publication date: December 6, 2012Applicant: SABIC INNOVATIVE PLASTICS IP B.V.Inventors: Venkata Rama Narayanan Ganapathy BHOTLA, Balakrishnan GANESAN, Kishan GURRAM, Salkod Parameshwar MALLIKA, Kumar Arun SATYANARAYANA, Swaminathan SHUBASHREE
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Patent number: 8247523Abstract: Disclosed herein is a method for producing a purified 2-aryl-3,3-bis(4-hydroxyaryl) phthalimidine of formula (I) wherein R1 is hydrogen or a C1-25 hydrocarbyl group and R2 is a hydrogen, a C1-25 hydrocarbyl group, or a halogen, and wherein the method comprises dissolving a crude phthalimidine compound in an aqueous base solution; precipitating the dissolved, crude phthalimidine compound from the aqueous base solution by adding an acid in an amount effective to lower the pH of the solution to 9.0 to 12.0, to provide a semicrude phthalimidine compound; and isolating the semicrude phthalimidine compound from the aqueous base solution, to provide the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I), and having a phenolphthalein compound content of less than 2,500 ppm, based on the weight of the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine.Type: GrantFiled: December 12, 2008Date of Patent: August 21, 2012Assignee: Sabic Innovative Plastics IP B.V.Inventors: Venkata Rama Narayanan Ganapathy Bhotla, Balakrishnan Ganesan, Kishan Gurram, Salkod Parameshwar Mallika, Kumar Arun Satyanarayana, Swaminathan Shubashree
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Patent number: 7915430Abstract: A method of producing a phenolphthalein comprises reacting a phenolic compound of the formula: wherein R1 is a hydrogen or a C1-C12 hydrocarbyl group, with a phthalic anhydride compound of the formula: wherein R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen, in the presence of a heterogeneous catalyst and a promoter to form a reaction mixture comprising a phenolphthalein compound of the formula: wherein each R1 is independently a hydrogen or a C1-C12 hydrocarbyl group, and R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen; wherein the heterogeneous catalyst comprises a metal oxide composition in combination with a porous support, wherein the metal is molybdenum, tungsten, or a combination comprising at least one of the foregoing metals.Type: GrantFiled: September 29, 2008Date of Patent: March 29, 2011Assignee: Sabic Innovative Plastics IP B.V.Inventors: Venkata Rama Narayanan Ganapathy Bhotla, Shivappa Basappa Halligudi, Gurram Kishan, Salkod Parameshwar Mallika, Bhaskar Veldurthy
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Patent number: 7868190Abstract: A method for producing a phenolphthalein compound comprises: reacting a phenolic compound of the formula: wherein R1 is a hydrogen or a C1-C12 hydrocarbyl group, with a phthalic anhydride compound of the formula: wherein R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen, in the presence of a heterogeneous catalyst and a promoter to form a reaction mixture comprising a phenolphthalein compound of the formula: wherein each R1 is independently a hydrogen or a C1-C12 hydrocarbyl group; and R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen; wherein the heterogeneous catalyst comprises, on a porous support, a calcination product of a heteropolyacid composition.Type: GrantFiled: September 29, 2008Date of Patent: January 11, 2011Assignee: Sabic Innovative Plastics IP B.V.Inventors: Venkata Rama Narayanan Ganapathy Bhotla, Shivappa Basappa Halligudi, Gurram Kishan, Salkod Parameshwar Mallika, Bhaskar Veldurthy
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Patent number: 7838689Abstract: A method for producing a phenolphthalein compound is disclosed, comprising: reacting a phenolic compound of the formula: wherein Ra is a hydrogen or a C1-C12 hydrocarbyl group, with a phthalic anhydride compound of the formula: wherein Rb is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen, in the presence of an ionic liquid catalyst composition and a promoter to form a reaction mixture comprising a phenolphthalein compound of the formula: wherein each Ra is independently a hydrogen or a C1-C12 hydrocarbyl group, and Rb is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen; wherein the ionic liquid catalyst composition comprises a combination of an ionic liquid and a metal halide wherein the metal is selected from the group consisting of a Group IIB, IIIA, VIII, or IVA metal, and a combination thereof.Type: GrantFiled: September 29, 2008Date of Patent: November 23, 2010Assignee: Sabic Innovative Plastics IP B.V.Inventors: Venkata Rama Narayanan Ganapathy Bhotla, Dwairath Dhar, Gurram Kishan, Salkod Parameshwar Mallika
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Publication number: 20100152416Abstract: Disclosed herein is a method for producing a purified 2-aryl-3,3-bis(4-hydroxyaryl) phthalimidine of formula (I) wherein R1 is hydrogen or a C1-25 hydrocarbyl group and R2 is a hydrogen, a C1-25 hydrocarbyl group, or a halogen, and wherein the method comprises dissolving a crude phthalimidine compound in an aqueous base solution; precipitating the dissolved, crude phthalimidine compound from the aqueous base solution by adding an acid in an amount effective to lower the pH of the solution to 9.0 to 12.0, to provide a semicrude phthalimidine compound; and isolating the semicrude phthalimidine compound from the aqueous base solution, to provide the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine of formula (I), and having a phenolphthalein compound content of less than 2,500 ppm, based on the weight of the purified 2-aryl-3,3-bis(4-hydroxyaryl)phthalimidine.Type: ApplicationFiled: December 12, 2008Publication date: June 17, 2010Inventors: Venkata Rama Narayanan Ganapathy BHOTLA, Balakrishnan GANESAN, Kishan Gurram, Salkod Parameshwar MALLIKA, Kumar Arun Satyanarayana, Swaminathan SHUBASHREE
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Publication number: 20100081828Abstract: A method of producing a phenolphthalein comprises reacting a phenolic compound of the formula: wherein R1 is a hydrogen or a C1-C12 hydrocarbyl group, with a phthalic anhydride compound of the formula: wherein R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen, in the presence of a heterogeneous catalyst and a promoter to form a reaction mixture comprising a phenolphthalein compound of the formula: wherein each R1 is independently a hydrogen or a C1-C12 hydrocarbyl group, and R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen; wherein the heterogeneous catalyst comprises a metal oxide composition in combination with a porous support, wherein the metal is molybdenum, tungsten, or a combination comprising at least one of the foregoing metals.Type: ApplicationFiled: September 29, 2008Publication date: April 1, 2010Inventors: Venkata Rama Narayanan Ganapathy BHOTLA, Shivappa Basappa HALLIGUDI, Gurram KISHAN, Salkod Parameshwar MALLIKA, Bhaskar VELDURTHY
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Publication number: 20100081829Abstract: A method for producing a phenolphthalein compound comprises: reacting a phenolic compound of the formula: wherein R1 is a hydrogen or a C1-C12 hydrocarbyl group, with a phthalic anhydride compound of the formula: wherein R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen, in the presence of a heterogeneous catalyst and a promoter to form a reaction mixture comprising a phenolphthalein compound of the formula: wherein each R1 is independently a hydrogen or a C1-C12 hydrocarbyl group; and R2 is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen; wherein the heterogeneous catalyst comprises, on a porous support, a calcination product of a heteropolyacid composition.Type: ApplicationFiled: September 29, 2008Publication date: April 1, 2010Inventors: Venkata Rama Narayanan Ganapathy BHOTLA, Shivappa Basappa HALLIGUDI, Gurram KISHAN, Salkod Parameshwar MALLIKA, Bhaskar VELDURTHY
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Publication number: 20100081831Abstract: A method for producing a phenolphthalein compound is disclosed, comprising: reacting a phenolic compound of the formula: wherein Ra is a hydrogen or a C1-C12 hydrocarbyl group, with a phthalic anhydride compound of the formula: wherein Rb is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen, in the presence of an ionic liquid catalyst composition and a promoter to form a reaction mixture comprising a phenolphthalein compound of the formula: wherein each Ra is independently a hydrogen or a C1-C12 hydrocarbyl group, and Rb is a hydrogen, a C1-C12 hydrocarbyl group, or a halogen; wherein the ionic liquid catalyst composition comprises a combination of an ionic liquid and a metal halide wherein the metal is selected from the group consisting of a Group IIB, IIIA, VIII, or IVA metal, and a combination thereofType: ApplicationFiled: September 29, 2008Publication date: April 1, 2010Inventors: Venkata Rama Narayanan Ganapathy BHOTLA, Dwairath DHAR, Gurram KISHAN, Salkod Parameshwar MALLIKA