Patents by Inventor Samuel Dull

Samuel Dull has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20240132347
    Abstract: The present disclosure provides a catalyst, methods of manufacturing the catalyst, and methods for using the catalyst for ammonia decomposition to produce hydrogen and nitrogen. The catalyst may comprise an electrically conductive support with a layer of one or more metal oxides adjacent to the support and at least one active metal adjacent to the layer. Methods are disclosed for deposition of metal oxide and active metal, drying and heat treatment. The method of using the catalyst may comprise bringing ammonia in contact with the catalyst in a reactor. The catalyst may be configured to be heated to a target temperature in less than about 60 minutes, by passing an electrical current through the catalyst. The method of using the catalyst may comprise bringing the catalyst in contact with ammonia at about 400 to 900° C., to generate a reformate stream with a conversion efficiency of greater than about 70%.
    Type: Application
    Filed: November 14, 2023
    Publication date: April 25, 2024
    Inventors: Boris SHELUDKO, Jongwon CHOI, Young Suk JO, Gregory Robert JOHNSON, Hyunho KIM, Samuel DULL, Tomas RICCIARDULLI
  • Publication number: 20230079048
    Abstract: A manufacturing process includes: depositing a first catalyst on a first gas diffusion layer (GDL) to form a first catalyst-coated GDL; depositing a first ionomer on the first catalyst-coated GDL to form a first gas diffusion electrode (GDE); depositing a second catalyst on a second GDL to form a second catalyst-coated GDL; depositing a second ionomer on the second catalyst-coated GDL to form a second GDE; and laminating the first GDE with the second GDE and with an electrolyte membrane disposed between the first GDE and the second GDE to form a membrane electrode assembly (MEA). A MEA includes a first GDL; a second GDL; an electrolyte membrane disposed between the first GDL and the second GDL; a first catalyst layer disposed between the first GDL and the electrolyte membrane; and a second catalyst layer disposed between the second GDL and the electrolyte membrane, wherein a thickness of the electrolyte membrane is about 15 ?m or less.
    Type: Application
    Filed: February 12, 2021
    Publication date: March 16, 2023
    Applicants: Board of Trustees of the Leland Stanford Junior University, Volkswagen Aktiengesellschaft
    Inventors: Friedrich B. Prinz, Timothy Goh, Shicheng Xu, Zhaoxuan Wang, Soonwook Hong, Yongmin Kim, Samuel Dull, Dong Un Lee, Thomas Francisco Jaramillo, Thomas Schladt, Gerold Huebner, Jonathan Müller, Glavas Vedran
  • Patent number: 11462744
    Abstract: A manufacturing process includes: depositing a first catalyst on a first gas diffusion layer (GDL) to form a first catalyst-coated GDL; depositing a first ionomer on the first catalyst-coated GDL to form a first gas diffusion electrode (GDE); depositing a second catalyst on a second GDL to form a second catalyst-coated GDL; depositing a second ionomer on the second catalyst-coated GDL to form a second GDE; and laminating the first GDE with the second GDE and with an electrolyte membrane disposed between the first GDE and the second GDE to form a membrane electrode assembly (MEA). A MEA includes a first GDL; a second GDL; an electrolyte membrane disposed between the first GDL and the second GDL; a first catalyst layer disposed between the first GDL and the electrolyte membrane; and a second catalyst layer disposed between the second GDL and the electrolyte membrane, wherein a thickness of the electrolyte membrane is about 15 ?m or less.
    Type: Grant
    Filed: February 14, 2020
    Date of Patent: October 4, 2022
    Assignees: The Board of Trustees of the Leland Stanford Junior University, Volkswagen Aktiengesellschaft
    Inventors: Friedrich B. Prinz, Timothy Goh, Shicheng Xu, Zhaoxuan Wang, Soonwook Hong, Yongmin Kim, Samuel Dull, Dong Un Lee, Thomas Francisco Jaramillo, Thomas Schladt, Gerold Huebner, Jonathan Müller, Glavas Vedran
  • Publication number: 20210257629
    Abstract: A manufacturing process includes: depositing a first catalyst on a first gas diffusion layer (GDL) to form a first catalyst-coated GDL; depositing a first ionomer on the first catalyst-coated GDL to form a first gas diffusion electrode (GDE); depositing a second catalyst on a second GDL to form a second catalyst-coated GDL; depositing a second ionomer on the second catalyst-coated GDL to form a second GDE; and laminating the first GDE with the second GDE and with an electrolyte membrane disposed between the first GDE and the second GDE to form a membrane electrode assembly (MEA). A MEA includes a first GDL; a second GDL; an electrolyte membrane disposed between the first GDL and the second GDL; a first catalyst layer disposed between the first GDL and the electrolyte membrane; and a second catalyst layer disposed between the second GDL and the electrolyte membrane, wherein a thickness of the electrolyte membrane is about 15 ?m or less.
    Type: Application
    Filed: February 14, 2020
    Publication date: August 19, 2021
    Inventors: Friedrich B. Prinz, Timothy Goh, Shicheng Xu, Zhaoxuan Wang, Soonwook Hong, Yongmin Kim, Samuel Dull, Dong Un Lee, Thomas Francisco Jaramillo, Thomas Schladt, Gerold Huebner, Jonathan Muller, Glavas Vedran
  • Patent number: 9975804
    Abstract: The invention provides a method for producing composite nanoparticles, the method using a first compound capable of transitioning from a monoclinic to a tetragonal rutile crystal state upon heating, and having the steps of subjecting the first compound to a hydrothermal synthesis to create anisotropic crystals of the compound; encapsulating the first compound with a second compound to create a core-shell construct; and annealing the construct as needed. Also provided is a device for continuously synthesizing composite nanoparticles, the device having a first precursor supply and a second precursor supply; a mixer to homogeneously combine the first precursor and second precursor to create a liquor; a first microreactor to subject the liquor to hydrothermic conditions to create an\isotropic particles in a continuous operation mode; and a second microreactor for coating the particles with a third precursor to create a core-shell construct.
    Type: Grant
    Filed: April 13, 2017
    Date of Patent: May 22, 2018
    Assignee: UCHICAGO ARGONNE, LLC
    Inventors: Jie Li, Yugang Sun, Ralph T. Muehleisen, Leah B. Guzowski, Xiaojie Yan, Samuel Dull, Ioannina Castano
  • Publication number: 20170297949
    Abstract: The invention provides a method for producing composite nanoparticles, the method using a first compound capable of transitioning from a monoclinic to a tetragonal rutile crystal state upon heating, and having the steps of subjecting the first compound to a hydrothermal synthesis to create anisotropic crystals of the compound; encapsulating the first compound with a second compound to create a core-shell construct; and annealing the construct as needed. Also provided is a device for continuously synthesizing composite nanoparticles, the device having a first precursor supply and a second precursor supply; a mixer to homogeneously combine the first precursor and second precursor to create a liquor; a first microreactor to subject the liquor to hydrothermic conditions to create an\isotropic particles in a continuous operation mode; and a second microreactor for coating the particles with a third precursor to create a core-shell construct.
    Type: Application
    Filed: April 13, 2017
    Publication date: October 19, 2017
    Applicant: UCHICAGO ARGONNE, LLC
    Inventors: Jie LI, Yugang SUN, Ralph T. MUEHLEISEN, Leah B. GUZOWSKI, Xiaojie YAN, Samuel Dull, Ioannina CASTANO