Abstract: To measure the phase behavior of a fluid in a porous medium such as a tight gas shale, one illustrative method involves: (a) loading the fluid into a sample cell containing the porous medium; (b) setting a pressure and a temperature for the fluid in the sample cell; (c) applying an RF pulse sequence to the fluid in the sample cell to acquire an NMR signal; (d) deriving from the NMR signal an NMR parameter distribution that depends on the pressure and the temperature; (e) determining whether a fluid phase is present based on the NMR parameter distribution; (f) repeating operations (c) through (f) to determine the presence or absence of the fluid phase at multiple points along a pressure-temperature path that crosses a phase boundary; and (g) providing an estimated location of the phase boundary based on the presence or absence of the fluid phase at said points.

Abstract: An NMR sensor and method is disclosed for analyzing a core sample from a subsurface formation. Embodiments of the method utilize two or more magnets disposed proximate to each other. The configuration of the magnets allows for increased detection frequency, and creates a strong field with much finer resolution than existing designs. In addition, embodiments of the sensor may be used at the well site due to its small size and simple hardware. Further details and advantages of various embodiments of the method are described in more detail herein.

Abstract: To measure the phase behavior of a fluid in a porous medium such as a tight gas shale, one illustrative method involves: (a) loading the fluid into a sample cell containing the porous medium; (b) setting a pressure and a temperature for the fluid in the sample cell; (c) applying an RF pulse sequence to the fluid in the sample cell to acquire an NMR signal; (d) deriving from the NMR signal an NMR parameter distribution that depends on the pressure and the temperature; (e) determining whether a fluid phase is present based on the NMR parameter distribution; (f) repeating operations (c) through (f) to determine the presence or absence of the fluid phase at multiple points along a pressure-temperature path that crosses a phase boundary; and (g) providing an estimated location of the phase boundary based on the presence or absence of the fluid phase at said points.

Abstract: An NMR sensor and method is disclosed for analyzing a core sample from a subsurface formation. Embodiments of the method utilize two or more magnets disposed proximate to each other. The configuration of the magnets allows for increased detection frequency, and creates a strong field with much finer resolution than existing designs. In addition, embodiments of the sensor may be used at the well site due to its small size and simple hardware. Further details and advantages of various embodiments of the method are described in more detail herein.

Abstract: This disclosure provides systems, methods, and apparatus related to depth well logging. In one aspect, an apparatus includes a radio frequency (RF) coil and a magnetic field sensing device. The apparatus is configured to be positioned in a first magnetic field. The first magnetic field polarizes nuclear spins of species in a detection region proximate the apparatus. The apparatus generates a second magnetic field for a time period with the RF coil to excite the nuclear spins of the species in the detection region. Then, the apparatus measures electromagnetic radiation, using the magnetic field sensing device, generated by the species as a result of the excitation of the nuclear spins.

Abstract: A radio-frequency tunable atomic magnetometer for detection of nuclear quadrupole resonance (NQR) from room temperature solids, including detection of nitrogen-containing explosives placed external to a sensor unit. A potassium radio-frequency magnetometer with sensitivity of 0.24 fT/Hz1/2 operating at 423 kHz is provided. The magnetometer detected a 14N NQR signal from room temperature ammonium nitrate (NH4NO3) in the zero-applied field limit. Results demonstrate first time detection of NQR with an atomic magnetometer, providing that a cryogen-free atomic magnetometer, with intrinsically frequency-independent sensitivity and easy tuning capabilities, can be an attractive new tool for detecting magnetic resonance signals in the kHz to MHz range.

Abstract: A radio-frequency tunable atomic magnetometer for detection of nuclear quadrupole resonance (NQR) from room temperature solids, including detection of nitrogen-containing explosives placed external to a sensor unit. A potassium radio-frequency magnetometer with sensitivity of 0.24 fT/Hz1/2 operating at 423 kHz is provided. The magnetometer detected a 14N NQR signal from room temperature ammonium nitrate (NH4NO3) in the zero-applied field limit. Results demonstrate first time detection of NQR with an atomic magnetometer, providing that a cryogen-free atomic magnetometer, with intrinsically frequency-independent sensitivity and easy tuning capabilities, can be an attractive new tool for detecting magnetic resonance signals in the kHz to MHz range.