Abstract: A machinable, high strength epoxy tool which is the polymeric reaction product of a mixture containing 5 to 12 weight percent of a bisphenol A epoxy, 3 to 8 weight percent of at least one polyoxypropylene amine catalyst, 60 to 85 weight percent of a mixture of no less than three different sized particulate fillers, the major portion of which is iron powder, 5 to 15 weight percent of short (<250 .mu.m) glass fibers, and 0.02 to 1 weight percent of a surface active agent.

Abstract: A tough, durable, high temperature epoxy tooling composition for making cast-to-size forming tools. The composition comprises a bisphenol-A epoxy, a trifunctional aromatic epoxy, an anhydride catalyst, and an imidazole catalyst. The composition may optionally contain a filler system comprising filler particles having different diameters that are interstitially-matched.

Abstract: A high strength, room temperature curable epoxy tooling compositions containing interstitially-matched filler systems for making cast-to-size forming tools for metal sheet stamping. The composition can be fully cured by at least one aliphatic amine catalyst in twelve hours producing a rigid article having a tensile strength of at least 40 MPa and a compressive strength of at least 100 MPa.

Abstract: A one-part epoxy adhesive has been developed that cures rapidly at relatively low elevated temperatures and is based on a diglycidyl ether of bisphenol A (DGEBA), DGBE reacted with glycerol and natural oils, and a unique triple catalyst system of metal imidazole salt, dicyandiamide and a cyclic latent curing agent that liberates diethylenetriamine when heated.

Abstract: A method and composition have been developed for providing wear resistant surfaces on tools used to stamp sheet metal. The composition is based on liquid epoxy novolac resin having a functionality greater than two filled with an inorganic powder having very high hardness. The epoxy constituent is cross linked and cured in two stages: it is first cured at room temperature with an aliphatic amine curing agent until it is hardened and is then toughened by an elevated temperature cure initiated by an imidazole curing agent. The composition may be used to cast an entire tool or as a surface coating layer for a less durable base.

Abstract: A novel adhesive has been developed that is particularly adapted for use in bonding automotive components made of sheet molding compound. It is comprised of suitable amounts of cross-linkable epoxy novolac resin; an epoxy flexibilizer; natural and colloidal silica; and an imidazole curing agent substituted in the one position with a short chain hydroxyalkyl group. The adhesive cures to a high bond strength in three minutes at 150.degree. C. It is resistant to degradation due to temperatures up to 200.degree. C., salt spray, humidity and water soak.

Abstract: In a preferred embodiment, a spreadable, thermosetting automotive body solder is comprised of 100 parts of an epoxy resin adduct of epichlorohydrin and bisphenol A, 25 to 40 parts liquid polysulfide rubber, 0.02 to 0.06 moles of an imidazole curing agent substituted in the 2-position with a hydrocarbon group, and a filler system consisting of 5 to 20 parts aluminum powder, 10 to 20 parts ion-exchanged clay, 3 to 6 parts wetting agent for the clay, and 70 to 130 parts fibrous or plate talc average particle size 3 microns or less. The composition is workable for several hours at room temperatures but cures in a few minutes at temperatures over 100.degree. C. The filler system provides the body solder with thixotropic properties at room temperatures, and sag resistance in both the cured and uncured states at temperatures up to 200.degree. C. The solder is corrosion resistant without other additives.

Abstract: In accordance with a preferred embodiment of this invention, a polyether-type, isocyanate-terminated, polyurethane prepolymer is formed by (1) blending about one equivalent of diphenylmethane diisocyanate (hereinafter "MDI") and a mixture of from about 0.5 to about 0.55 equivalent of a polyoxypropylene diol having a molecular weight (Mn) within the range of about 1,000 to about 2,000, from about 0.08 to about 0.13 equivalent of a polyoxypropylene trio, having a molecular weight (Mn) in the range of from about 4,000 to about 4,500, and from about 10 to about 15 parts by weight of a hydrogenated terphenyl plasticizer per 100 parts by weight of the mixture of MDI and the polyols, (2) initiating the polymerization reaction by adding from about 0.08 to about 0.