Patent number: 11981616
Abstract: A method for preparing 3,3?-diaminobenzidine, the method comprising the following steps: subjecting 4,4?-biphenol and N,N-dimethylsulfamoyl chloride to an esterification reaction in a specified solvent at 40-70° C. to obtain 4,4?-biphenyl bis(N,N-dimethylaminosulfonate) as a first intermediate; subjecting the 4,4?-biphenyl bis(N,N-dimethylaminosulfonate) to a chlorination reaction with a chlorinating reagent under acidic conditions to obtain 3,3?-dichloro-4,4?-biphenyl bis(N,N-dimethylaminosulfonate) as a second intermediate; subjecting the second intermediate 3,3?-dichloro-4,4?-biphenyl bis(N,N-dimethylaminosulfonate) to an ammonolysis reaction with anammoniation reagent in the presence of a combined catalyst to obtain a crude product of 3,3?,4,4?-tetraaminobiphenyl, wherein the combined catalyst is a mixture of proline, a cuprous salt and a phase transfer catalyst; and subjecting the crude product of 3,3?,4,4?-tetraaminobiphenyl to a post-treatment to obtain a purified 3,3?,4,4?-tetraaminobiphenyl product.
Type:
Grant
Filed:
January 12, 2022
Date of Patent:
May 14, 2024
Assignees:
Hubei Huida High-Tech Co., Ltd, Borun High-Tech Co., Ltd.
Inventors:
Yun Ling, Yongfang Li, Kun Wang, Lizhu Chen, Wei Yin, Jinying Zhang
Publication number: 20240153257
Abstract: A monitoring system based on a digital converter station includes a first monitoring terminal deployed at a first-level monitoring side, a second monitoring terminal deployed at a second-level monitoring side, and a third monitoring terminal deployed at a third-level monitoring side; the monitoring terminal at each level includes a communication module, a human-machine interaction module, a device status monitoring module, a device alarm management module, a video fusion processing module, and a data transmission adjustment and control module.
Type:
Application
Filed:
January 11, 2024
Publication date:
May 9, 2024
Applicants:
STATE GRID CORPORATION OF CHINA, STATE GRID ECONOMIC AND TECHNOLOGICAL RESEARCH INSTITUTE CO., LTD, NR ELECTRIC CO., LTD., XJ GROUP CORPORATION, NARI TECHNOLOGY CO., LTD, BEIJING SGITG ACCENTURE INFORMATION TECHNOLOGY CENTER CO., LTD., HUAWEI TECHNOLOGY CO., LTD
Inventors:
Wei JIN, Qing WANG, Xianshan GUO, Jun LYU, Siyuan LIU, Xiang ZHANG, Yanguo WANG, Zhanguo ZHANG, Haifeng WANG, Chong TONG, Ming LI, Wei CHENG, Ning ZHAO, Zhou CHEN, Xiaojun HOU, Hanqing ZHAO