Abstract: The invention discloses a method for detecting the release performance of flavors and fragrances microcapsule, comprising the following steps: Using SPME to adsorb the gas sample released by the perfume microcapsules in different time periods under constant temperature and humidity conditions. The SPME adsorption time was 10 s˜30 min and the analytical time in GC/MS was is 1 s˜100 min, and the compounds detected by GC-MS were quantified by area normalization method. The method of the invention is simple and rapid, and is suitable for analyzing and detecting the sustained release of the perfume microcapsules. Using SPME technology, the detection process was without the use of organic solvents and green pollution. The invention can be directly used for the detection of the release of gas components of various perfume microcapsule products without destroying the sample morphology and structure, and more truly reflecting the release performance of the flavors and fragrances microcapsule in real life.