Abstract: A method of TEM sample preparation from a circuit layer structure, the method comprising electron-beam assisted deposition of a first protective layer over a site of interest of the circuit layer structure; ion-beam assisted deposition of a second protective layer over the first protective layer; and ion-beam milling at the site of interest through the first and second protective layers.

Abstract: A method of preparing a planar view TEM sample of a planar portion of a circuit layer structure formed on a substrate. The method includes polishing the substrate circuit layer structure until a cross-sectional polishing face has substantially reached a first side face of the planar portion of the circuit layer structure; forming a trench structure in the cross-sectional polishing face. The trench structure extends into the cross-sectional polishing face substantially in the direction parallel to the substrate such that top and bottom faces of the planar portion of the circuit layer structure are exposed, wherein the planar portion of the circuit layer structure extends substantially parallel to the substrate from the first side face. The method further includes performing a cut around the first side face to free the planar portion of the circuit layer structure.