Abstract: An inlet liner is provided for use in an inlet assembly of a chromatograph system. The inlet liner has an elongate tube that extends along a longitudinal axis and defines a bore that extends along the longitudinal axis and has an inner bore surface. At least one projection extends from the inner bore surface into the bore. Chromatograph systems are provided including the exemplary inlet liner(s). Methods are also provided for analyzing a sample containing a matrix in a chromatograph system having an inlet assembly connected to a chromatograph column. The method includes positioning an exemplary inlet liner in the inlet assembly, flowing the sample through the inlet liner, and adhering a portion of the matrix to a projection surface of at least one projection of the inlet liner.

Abstract: A luggage conveyor system includes a frame, a plurality of pallets movably supported by the frame each having a load carrying surface configured to convey luggage thereon, and a drive assembly. The drive assembly includes a chain formed by a plurality of chain links connected to each other. At least one chain link of the plurality of chain links is coupled to one of the plurality of pallets. The drive assembly further includes a motor-driven drive wheel, and a plurality of driven wheels coupled to and driven by the drive wheel. The plurality of driven wheels are arranged such that at least two of the driven wheels simultaneously contact the same one of the plurality of chain links to frictionally drive the chain.

Abstract: An adjustable surfboard transporter that protects the most fragile parts of a surfboard whether in transit or for storage. The surfboard protector or transporter can be adjusted in size to accommodate several different surfboard lengths. The transporter may focus on the most vulnerable parts of the surfboard protecting the nose, tail, and rails. In particular, an adjustable protective cover for the fragile outer perimeter of a surfboard is described. The light and durable form of protection cushions the surfboard to prevent damage from impacts. The system may be easy to use, quick to assemble, and may be broken down to an easily-transportable or storable size.

Abstract: The present invention relates to methods and systems for controlling depressurization of a vial containing a gas sample. The disclosed systems and methods are employed during sampling and/or analysis of the gas sample. One exemplary method for controlling depressurization of a vial containing a gas sample includes establishing fluid communication between a sample loop of a head space sampling device and the head space of the vial. A sample gas pressure is established within the head space of the vial. The sample loop is connected in fluid communication with a lower pressure environment through a ventilation pathway. A ventilation valve within the ventilation pathway is used to vent gas from the vial through the sample loop to the lower pressure environment at a predetermined rate. Devices and systems for depressurizing a vial containing a gas sample at a predetermined rate are also disclosed.

Abstract: An apparatus is provided to facilitate the transfer of baggage on conveyor systems at the junction between a sort conveyor and a take-away conveyor. The transfer apparatus includes a sweeper arm that rotates across the sort conveyor to sweep a baggage article thereon toward the take-away conveyor. The sweeper arm translates linearly relative to the sort conveyor so that the baggage remains in continuous contact with the sweeper arm. The rotation of the arm is coordinated with the translation so that the baggage will be fully diverted from the sort conveyor by the time the sweeper arm reaches the end of its translation.

Abstract: A bed pad wedge system for inhibiting a person from falling out of bed. The system includes a fitted mattress pad fastened to a mattress. Each lateral edge of the fitted pad has pockets located therein that contain foam rubber wedges having the shape of an obtuse triangle. The pockets are installed on an underside of the fitted pad and are facing an outer edge of the mattress. The triangular foam rubber wedges are each encased in a slippery material to aid in installing the wedges in the pockets. A third wedge or triangle may be installed in the middle of a mattress between the outer wedges that are located at each edge of the mattress. The wedge system may be covered by standard sheets and bedding.

Abstract: Systems and methods of chemical sensing in fuel cell systems are described. In one aspect, a replaceable sacrificial sensor system includes an input that is configured to be coupled to a fuel stream delivery system, two or more sacrificial chemical sensor fuel cells, and a manifold that is configured to selectively couple the sacrificial chemical sensor fuel cells to the input. In another aspect, a fuel cell system includes a main fuel cell, a fuel stream delivery system that is configured to direct a fuel stream to the main fuel cell, an oxidant stream delivery system that is configured to direct an oxidant stream to the main fuel cell, and a sensor system. The sensor system is coupled to the fuel stream delivery system at a location upstream of the main fuel cell and includes two or more sacrificial chemical sensors and a manifold that is configured to selectively couple the sacrificial chemical sensors to the fuel stream delivery system. A fuel cell monitoring method also is described.

Abstract: A method for desensitizing explosives illicitly manufactured from commercial fertilizers, preferably ammonium nitrate. Ammonium nitrate prills are impregnated with microballoons which carry a desensitizing agent, preferably water. The microballoons are sufficiently small that they can be incorporated into the prills where they are not easily separated. Should the modified ammonium nitrate be used as a starting material for the manufacture of ANFO, the resulting ANFO exhibits a diminished explosive potential. The microballoons release their contents in response to a prompt shock wave which passes through the ANFO. The released water quenches the explosive reactions in AN/fuel compositions and curtails the explosive performance of the ANFO. Further, the microballoons are a benign additive having no adverse impact on the fertilizer itself, the plant material or the environment if it is instead used for its intended purpose as a fertilizer.

Abstract: A sample inlet liner includes a novel matrix that serves to retain an injected sample. The preferred inert matrix is polytetrafluoroethylene (PTFE) that serves to retain an injected sample and is provided in lieu of a conventional packing material. The contemplated inert matrix may be selected from a range of configurations of PTFE so as to provide a supporting material capable of retaining an ample quantity of injected sample in the sample inlet liner. The contemplated matrix nonetheless provides a tortuous path for the retained quantity of injected sample so as to facilitate known injection techniques such as split/splitless injection and large volume injections.

Abstract: A chromatograph includes an inlet for receiving a sample and a pressurized hydrogen gas flow and in response providing a sample/fluid mixture; a separation column located in a temperature-controlled zone for receiving the sample/fluid mixture and for providing a column effluent stream; a detector for receiving the effluent stream and for providing a detector output stream; and a gas storage system for receiving the detector output stream (and optionally a split flow and a septum purge flow in the instance of a split/splitless inlet) and for storing the received gas stream for subsequent reuse. In the preferred embodiments of the gas storage system, a plurality of metal hydride storage (MHS) systems are used.

Abstract: A chromatograph includes an inlet for receiving a sample and a pressurized hydrogen gas flow and in response providing a sample/fluid mixture; a separation column located in a temperature-controlled zone for receiving the sample/fluid mixture and for providing a column effluent stream; a detector for receiving the effluent stream and for providing a detector output stream; and a gas storage system for receiving the detector output stream (and optionally a split flow and a septum purge flow in the instance of a split/splitless inlet) and for storing the received gas stream for subsequent reuse. In the preferred embodiment of the gas storage system, a plurality of metal hydride storage (MHS) systems are used.

Abstract: An airflow director constructed for use with a separation column in a temperature-controlled air bath in a chromatographic oven cavity, wherein the airflow director includes at least a first baffle locatable with respect to the separation column and to the low pressure and high-pressure regions of the air bath, wherein the baffle is configured to direct air flow away from the high-pressure region before passing over the separation column. The temperature-controlled air thereby mixes with oven cavity air before passing over the separation column, which is thereby less subject to thermal gradients.

Abstract: A sample inlet liner includes a novel matrix that serves to retain an injected sample. The preferred inert matrix is polytetrafluoroethylene (PTFE) that serves to retain an injected sample and is provided in lieu of a conventional packing material. The contemplated inert matrix may be selected from a range of configurations of PTFE so as to provide a supporting material capable of retaining an ample quantity of injected sample in the sample inlet liner. The contemplated matrix nonetheless provides a tortuous path for the retained quantity of injected sample so as to facilitate known injection techniques such as split/splitless injection and large volume injections.

Abstract: A chromatograph includes an inlet for receiving a sample and a pressurized carrier fluid flow and in response providing a sample/fluid mixture; a separation column located in a temperature-controlled zone for receiving the sample/fluid mixture and for providing a column effluent stream; a detector for receiving the effluent stream and for providing a detector output stream; and a gas recycling system for receiving the detector output stream, and optionally a split flow and a septum purge line flow, and for providing therefrom a recycled carrier gas stream suitable for reuse as the pressurized carrier fluid flow.

Abstract: A chromatograph includes an inlet for receiving a sample and a pressurized hydrogen gas flow and in response providing a sample/fluid mixture; a separation column located in a temperature-controlled zone for receiving the sample/fluid mixture and for providing a column effluent stream; a detector for receiving the effluent stream and for providing a detector output stream; and a gas storage system for receiving the detector output stream (and optionally a split flow and a septum purge flow in the instance of a split/splitless inlet) and for storing the received gas stream for subsequent reuse. In the preferred embodiments of the gas storage system, a plurality of metal hydride storage (MHS) systems are used.

Abstract: A sample inlet liner includes an internal surface barrier wherein the surface barrier is situated so as to circumvent undesirable reactions between the sample and the liner. The barrier surface composition includes PTFE to an extent sufficient to reduce or eliminate such undesirable reactions, and the surface barrier is situated so as to receive substantially all of the wetting of the liner by an injected sample, such that little or no contact is made by the sample with a surface that lacks sufficient PTFE. As a result, decomposition or adsorption of the sample is reduced.

Abstract: Energy efficiency of a thermal zone in an analytical instrument is improved by use of an oven cavity insert that may be removably positioned in an insulated enclosure in an oven cavity housing, whereby the combination of the oven cavity insert and one or more of the enclosure walls completely encloses a first space suitable for effecting the thermal zone. The oven cavity insert is positionable so as to separate the first space from at least a portion of the unused volume of the oven cavity, thus reducing the volume of the thermal zone, so as to reduce the amount of heating or cooling required for temperature control of a component positioned therein. When present in the oven cavity, the contemplated oven cavity insert effectively conceals a portion of the housing from the thermal zone, thus reducing the effective thermal mass of the oven cavity housing.

Abstract: In a discharge ionization detector, a method and apparatus are disclosed for increasing the transfer of photons and metastables from a discharge chamber to a ionization chamber, while effecting ion discrimination of the ionic current with respect to a signal cathode, thereby reducing the effect of ionic current in the signal output. Preferred embodiments of the invention include a discharge source located in a discharge chamber, means for introducing discharge gas flow into the discharge chamber, a flow guide that directs discharge gas flow between the discharge chamber and an adjacent ionization chamber, and inlet port for introducing a flow of sample gas containing an analyte into the ionization chamber and an outlet port for exhausting the sample gas and the discharge gas. A plurality of apertures in the flow guide are situated proximate the discharge source so as to promote the rapid and efficient transfer of photons and metastables from the discharge source into the ionization chamber.

Abstract: A method and device are disclosed for performing supercritical fluid chromatography in packed columns of at least about 0.5 mm inside diameter. The column provides at least 50,000, preferably at least 100,000, theoretical plates with pressure drop across the column of at least 25 bar. The outlet pressure is controlled by the back pressure regulator. The column may comprise a plurality of individual columns in series. Separation is performed at a rate of at least 25 plates/min, preferably at least 100 plates/min.