Mg BASE ALLOY

An Mg base alloy of this invention is characterized in that Ag is contained in an amount of not more than 1.98 at % as an additive material other than Zn. There is provided an Mg base alloy having not only a practically sufficient strength but good ductility at room temperature to an extent that it has hitherto been unable to be desired and having small anisotropy in strength characteristics.

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Description
TECHNICAL FIELD

This invention relates to an Mg base alloy containing Mg as a main material, realization of which is desired as a lightweight material which is a replacement for Al.

BACKGROUND ART

With respect to this Mg base alloy, there have hitherto been developed various alloys disclosed in the following Patent Documents 1 to 8.

In Patent Documents 2, 3, 4, 6 and 8, in order to contrive to improve strength, a rare earth element, scandium or lithium is added. However, since such a rare earth element is a rare element which is hardly obtainable on the earth, alloys thereof are high in the price and low in the multiplicity of use.

Patent Document 1 is concerned with a quinary alloy containing from 0.3 to 3% by mass of Ca and simultaneously containing Al, Sr and Mn. In such an alloy, a precipitate (crystal) is formed on the grain boundary of Mg.

Patent Document 2 is concerned with an Mg alloy which contains 0.3% or more and not more than 1.0% of Zr and which in the case of containing Ca, contains 0.2% or more and not more than 2.0% of Ca (% means % by mass).

Patent Document 8 discloses an Mg alloy developed as a casting material, which contains from 3 to 8% by weight of Zn and from 0.8 to 5% by weight of Ca.

During the process of experiments of this invention, it has become clear that a grain boundary precipitate is formed because of an excess of the content of Ca, whereby ductility at room temperature is lowered. From this fact, in all of the foregoing Patent Documents 1, 2 and 8, the ductility at room temperature is poor, too.

An alloy of Patent Document 7 is an alloy developed as a casting material. Specifically, it is disclosed that Ca is zero or 0.5% by weight, and Zn is from 1% by weight to 7% by weight; and in combinations of zero, in the case where Ca is zero or 0.5% by weight, when Zn is zero, then the alloy has a 0.2% proof stress of less than 75 MPa, whereas when Zn is from 1% by weight to 7% by weight, then the alloy has a 0.2% proof stress of 75 MPa or more and less than 100 MPa. Thus, it is demonstrated that when such an alloy is used as a structural material, its strength is insufficient. Also, according to the foregoing knowledge obtained in the experiments of this invention made by the present inventors, there is nothing other than estimation that an alloy containing Ca in a high concentration is low in the ductility.

Patent Document 5 discloses an Mg base alloy containing Mn and Zn as main components of additive materials, and in order to obtain a high strength, it is described to perform a solution heat treatment. However, there is involved such a problem that the process is complicated because, for example, an additional heat treatment of two-stage aging is required.

In Patent Document 8, an alloy in which not more than 10% by weight of Cu is added is developed. However, the addition of Cu encounters a defect that the corrosion resistance of the Mg alloy is remarkably lowered.

In summary, most of members in which an Mg alloy is used are currently manufactured by a casting or die casting method. In the future, though applications of an Mg alloy to transportation equipment such as automobiles, aircrafts, etc. are expected, the casting method involves such defects that the structure of the material is coarse; the ductility is low; and the size is limited so that the Mg alloy is not applicable to plate materials, rod materials, pipe materials, etc. On the other hand, a wrought Mg alloy which is practically useful includes Mg—Al—Zn (AZ based alloy) and Mg—Zn—Zr (ZK based alloy). However, the strength of such a wrought Mg alloy is insufficient, and a proof stress to be used for strength design is largely different between the case where a tensile load is applied and the case where a compression load is applied due to influences of the texture to be formed at the time of hot working (in commercially available AZ31 alloy rolled materials, the compression proof stress is about 50% of the tensile proof stress). Therefore, it is difficult to use such a wrought Mg alloy as it is. Up to date, in order to realize a high strength of an Mg alloy, there have been adopted methods for adding a rare earth element or adding large amounts of alloying elements.

However, since the rare earth element is expensive, its multiplicity of use is low; and furthermore, the addition of large amounts of alloying elements is accompanied with the formation of a coarse compound phase and involves such a defect that though a high strength is obtained, the ductility is impaired. Then, the development of a new wrought Mg alloy which is free from a rare earth element and which is excellent in strength and ductility by the addition of inexpensive alloying elements is being demanded.

Patent Document 1: JP-A-2007-70688 Patent Document 2: JP-A-2006-28548 Patent Document 3: JP-A-2006-16658 Patent Document 4: JP-A-2005-113235 Patent Document 5: JP-T-2004-510057 Patent Document 6: JP-A-2003-226929 Patent Document 7: JP-A-2002-212662 Patent Document 8: JP-A-6-25791 DISCLOSURE OF INVENTION Problems That the Invention is to Solve

In view of such circumstances, an object of this invention is to provide an Mg base alloy having not only a practically sufficient strength but good ductility at room temperature to an extent that it has hitherto been unable to be desired and having small anisotropy in strength characteristics.

Means for Solving the Problems

An Mg base alloy of Invention 1 is characterized in that Ag is contained in an amount of not more than 1.98 at % as an additive material other than Zn.

Invention 2 is characterized in that in the Mg base alloy as set forth in Invention 1, Ca is further contained in an amount of not more than 0.61 at % as an additive material other than Zn and Ag.

Invention 3 is characterized in that in the Mg base alloy as set forth in Invention 2, Zr is further contained in an amount of not more than 0.17 at % as an additive material other than Zn, Ag and Ca.

Invention 4 is characterized in that in the Mg base alloy as set forth in any one of Inventions 1 to 3, a crystal grain size thereof is from 0.1 μm to 25 μm.

ADVANTAGES OF INVENTION

According to Inventions 1 to 4, it has become possible to provide an Mg base alloy having excellent strength and ductility to an extent that both of them have hitherto been unable to be desired and having small anisotropy in strength, by the addition of inexpensive alloying elements.

Furthermore, since alloying elements which impair corrosion resistance, such as Cu, etc., are not used, excellent durability can also be expected.

The alloy of this invention has an average Schmid factor in the bottom slip direction against the load application direction of 0.2 or more and has uniform distribution of the Schmid factor as compared with extruded materials of the existing AZ91 alloy (Mg-9 mass % Al-1 mass % Zn alloy) which is a practical Mg alloy. Namely, the alloy of this invention is characterized in that a degree of integration of the bottom parallel to the extrusion direction is weak.

The alloy of this invention has such excellent mechanical properties that the compression proof stress is 75% or more of the tensile proof stress and that anisotropy in strength is small.

BRIEF DESCRIPTION OF DRAWINGS

FIG. 1 is a flow showing experimental procedures of Example 1.

FIG. 2 is a graph showing an age hardening curve of each of alloys of Example 1 at 160° C.

FIG. 3 is a graph showing an age hardening curve of each of alloys of Example 1 at 200° C.

FIG. 4 is a TEM micrograph of an Mg-2.3% Zn alloy of Example 1 at the peak aging stage when aged at 160° C.

FIG. 5 is a TEM micrograph of an Mg-2.3% Zn-0.1% Ag alloy of Example 1 at the peak aging stage when aged at 160° C.

FIG. 6 is a TEM micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy of Example 1 at the peak aging stage when aged at 160° C.

FIG. 7 is a TEM micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy of Example 1 at the peak aging stage when aged at 160° C. and is a high-magnification photograph of FIG. 6.

FIG. 8 is a TEM micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 1 at the peak aging stage when aged at 160° C.

FIG. 9 is a TEM micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 1 at the peak aging stage when aged at 160° C. and is a high-magnification micrograph of FIG. 8.

FIG. 10 is a flow showing experimental procedures of Example 2.

FIG. 11 is an aging curve of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy of Example 2 at 160° C. and is a graph showing the comparison between a material having been subjected to a solution heat treatment after casting and a material having been subjected to a solution heat treatment for one hour after hot extrusion.

FIG. 12 is an aging curve of an Mg-2.3% Zn-0.1%Ag-0.1% Ca alloy of Example 2 at 200° C. and is a graph showing the comparison between a material having been subjected to a solution heat treatment after casting and materials having been subjected to a solution heat treatment for 0.5 hours and one hour, respectively after hot extrusion.

FIG. 13 is an aging curve of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 2 at 160° C. and is a graph showing the comparison between a material having been subjected to a solution heat treatment after casting and a material having been subjected to a solution heat treatment for one hour after hot extrusion.

FIG. 14 is an aging curve of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 2 at 200° C. and is a graph showing the comparison between a material having been subjected to a solution heat treatment after casting and materials having been subjected to a solution heat treatment for one hour and 4 hours, respectively after hot extrusion.

FIG. 15 is an optical micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy of Example 2 as extruded at 350° C.

FIG. 16 is an optical micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 2 as extruded at 350° C.

FIG. 17 is a TEM micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 2 as extruded at 350° C.

FIG. 18 is a high-magnification micrograph of FIG. 17.

FIG. 19 is a graph showing distribution of a Schmid factor in the bottom slip direction against the tensile load application direction of each of samples of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy and an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 2 as extruded at 300° C. and 350° C., respectively and showing that the distribution is more uniform than that of an extruded material of an existing AZ91 alloy at 400° C. and that a degree of the bottom texture is small.

FIG. 20 is a graph showing a stress-strain curve obtained by each of a tensile test and a compression test at room temperature of an extruded material of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy of Example 2 at 350° C.

BEST MODE FOR CARRYING OUT THE INVENTION

It is noted from the following Examples that according to the invention of this application, age hardening properties are enhanced by adding trace amounts of Ag, Ca and Zr, each of which is free from a rare earth element and is relatively easily available. Also, it is noted that even by merely hot extruding the alloy, a fine grain structure having a fine precipitate dispersed therein is formed and that the subject alloy is an Mg base alloy which is excellent in not only strength but ductility and which has small anisotropy in strength as compared with the conventional alloys. Also, in view of the Examples and the technical common knowledge, it can be expected that the foregoing effects are displayed within the following ranges.

With respect to Zn, the maximum solubility of Zn in Mg is 2.4 at %.

So far as the composition range of Zn is 0.75 at % or more, age hardening is achieved. However, in order to contrive to realize a high strength by dispersing a rod-like β′-precipitate which works as a strengthening phase of an Mg—Zn based alloy, it is necessary that the Zn content is as high as possible, and the Zn content is preferably 1.52 at % or more.

In order to disperse this rod-like β′-precipitate in a larger amount and finely, the Zn content is preferably 1.92 at % or more.

With respect to Ag, the solubility of Ag in Mg is large, and its maximum solid solution amount is 3.82 at %.

In the case where a solution heat treatment after casting is performed at 400° C., when the Ag content exceeds 1.98 at %, there is a concern that a coarse precipitate is formed, thereby deteriorating mechanical properties.

When the Ag content exceeds 0.2 at %, even by increasing the addition amount, age hardening properties do not change too much. Therefore, in order to inhibit the formation of a compound phase with Zn or Ca or Zr as a constituent element, in a sense of suppressing the Ag content, an upper limit thereof is preferably 0.2 at %.

Also, when the Ag content Is 0.08 at % or more, a work for promoting the formation of a nucleus of the precipitate is revealed, and therefore, a lower limit value thereof is preferably 0.08 at % or more.

With respect to Ca, the maximum solubility of Ca in Mg is 0.82 at %.

In the case where a solution heat treatment after casting is performed at 400° C., when the Ca content exceeds 0.61 at %, a grain boundary precipitate is formed, thereby impairing mechanical properties.

Therefore, its upper limit was specified to be not more than 0.61 at %.

Also, as shown in FIGS. 2 and 3 of Example 1, even by doubling the addition amount of Ca, changes in age hardening characteristics are not noticed. Therefore, in order to inhibit the formation of a compound phase with Zn or Ag or Zr as a constituent element, in a sense of suppressing the Ca content, an upper limit thereof is preferably 0.2 at %.

Also, when the Ca content is 0.08 at % or more, a work for promoting the formation of a nucleus of the precipitate is revealed, and therefore, a lower limit value thereof is preferably 0.08 at % or more.

With respect to Zr, the maximum solubility of Zr in Mg is 1.04 at %.

However, when the Zr content exceeds 0.17 at %, a peritectic reaction exists in the vicinity of 650° C., and a coarse precipitate is formed. Therefore, the Zr content was specified to be not more than 0.17 at %.

When the Zr content is 0.08 at % or more, an effect for inhibiting grain coarsening in the solution heat treatment and hot extrusion is expected due to a fine precipitate or the Zr atom itself. Therefore, a lower limit of the Zr content is preferably 0.08 at % or more.

The foregoing specific addition amount of each of the elements is distributed on the basis of results of the following Examples such that an average grain size of the fine grain structure is as small as possible and that orientation properties of the crystal grain are weakened.

Example 1

Respective elements were blended so as to have an alloy composition shown in Table 1 and smelted in a high-frequency melting furnace using an iron-made crucible in an argon atmosphere.

TABLE 1 Alloy composition Composition (at %) Composition (wt %) Alloy Zn Ag Ca Zr Mg Zn Ag Ca Zr Mg Mg—2.3Zn 2.32 Bal. 6.0 Bal. Mg—2.3Zn—0.1Ag 2.33 0.09 Bal. 6.0 0.4 Bal. Mg—2.3Zn—0.1Ag—0.1Ca1 2.33 0.10 0.09 Bal. 6.0 0.4 0.16 Bal. Mg—2.3Zn—0.2Ag—0.2Ca2 2.33 0.2  0.2  Bal. 6.0  0.85 0.31 Bal. Mg—2.3Zn—0.1Ag—0.1Ca—0.1Zr 2.34 0.09 0.10 0.17 Bal. 6.0 0.4 0.16 0.6 Bal.

After sealing in a PYREX (registered trademark) tube together with an argon gas, the melted material was subjected to a homogenization heat treatment at 340° C. for 48 hours. The resulting sample was cut out and sealed in a PYREX (registered trademark) tube together with an argon gas; and thereafter, the sample was subjected to a solution heat treatment at 400° C. for one hour and then quenched in ice water.

The quenched material was aged at a temperature of 160° C. and 200° C., respectively using an oil bath. Its hardness by aging was measured by a Vickers hardness meter under a condition at a load of 1 kg for a holding time of 15 seconds.

Microstructure observation was executed using a transmission electron microscope (TEM). Details of experimental procedures are shown in FIG. 1.

FIGS. 2 and 3 show hardness changes in aging at 160° C. and 200° C., respectively. From these figures, the hardness reaches the maximum at around 100 hours in the aging at 160° C. and at around 10 hours in the aging at 200° C., respectively.

The age hardening properties become better by adding Ag, (Ag+Ca) or (Ag+Ca+Zr) to the Mg-2.3Zn alloy.

The maximum hardness of an alloy obtained by adding (Ag+Ca+Zr) to the Mg-2.3Zn alloy is the highest and reaches 100 Hv.

In an alloy obtained by adding (Ag+Ca) to the Mg-2.3Zn alloy, the aging hardness of each of alloys obtained by increasing the addition amount of each of the elements by 0.2 at % is examined.

However, even when the addition amount is increased, a distinct difference in the aging characteristics is not observed.

With respect to each of the alloys shown in FIGS. 4, 5, 6 and 8, the grain size was measured by linear intercept method (ASTM standards E112). The average grain size was about 100 μm in the Mg-2.3Zn binary alloy shown in FIG. 4, about 50 μm in the Mg-2.3Zn-0.1Ag alloy shown in FIG. 5, about 50 μm in the Mg-2.3Zn-0.1Ag-0.1Ca alloy shown in FIG. 6 and about 10 μm the Mg-2.3Zn-0.1Ag-0.1Ca-0.17Zr alloy shown in FIG. 8, respectively. It is noted that by the addition of Ag or combined addition of (Ag+Ca), the crystal grain size becomes small and that by the further addition of Zr, the grain size becomes finer.

Each of FIGS. 4 to 9 shows a TEM micrograph of each of the alloys at the peak aging stage when aged at 160° C.

In all of the aging structures, a rod-like precipitate extending to the c-axis direction of Mg is observed.

By adding Ag, (Ag+Ca) or (Ag+Ca+Zr) to the Mg-2.3Zn alloy, the precipitate becomes fine.

This refinement of the precipitate is considered to cause an increase of the peak aging hardness.

In conclusion, good age hardening properties are obtained in alloys by the combined addition of (Ag+Ca) and (Ag+Ca+Zr), respectively.

Example 2

Details of experimental procedures are shown in FIG. 10. Alloying elements were blended so as to have an alloy composition shown in Table 1 and melted and cast in a (CO2+SF0) mixed gas atmosphere. Thereafter, the ingot was subjected to a homogenous heat treatment at 350° C. for 48 hours. Thereafter, the ingot was hot extruded at 300° C. and 350° C., respectively. With respect to the hot extrusion condition, an extrusion ratio was 20, and a ram rate was 0.1 mm/s. The material after extrusion was subjected to a solution heat treatment at 400° C. for from 0.5 to 4 hours and then subjected to an aging treatment at a temperature of 160° C. and 200° C., respectively, followed by measurement for a Vickers hardness.

Also, the sample after extrusion was subjected to microstructure observation by an optical microscope and TEM.

FIGS. 11 and 12 show an aging curve of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy at 160° C. and 200° C., respectively.

Comparison was made between a material having been subjected to a solution heat treatment after casting and a material having been subjected to a solution heat treatment after hot extrusion. As a result, the both are substantially identical to each other with respect to the maximum hardness and age hardening characteristics.

FIGS. 13 and 14 show an aging curve of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy at 160° C. and 200° C., respectively.

Comparison was made between a material having been subjected to a solution heat treatment after casting and a material having been subjected to a solution heat treatment after hot extrusion. As a result, the both are not distinctly different from each other with respect to the maximum hardness and age hardening characteristics.

FIG. 15 shows an optical micrograph structure of an Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy when hot extruded at 350° C. The crystal grain size was measured by linear intercept method using this photograph. As a result, the average crystal grain size was 20 μm.

FIG. 16 shows an optical micrograph of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17 Zr alloy when hot extruded at 350° C. FIGS. 17 and 18 are each a TEM micrograph of the same alloy.

In the optical micrograph of FIG. 16, the structure after extrusion is classified into three of (A) a coarse unrecrystallized grain, (B) a fine equi-axed recrystallized grain and (C) an obscure region. The obscure region (C) is considered to be corresponding to the TEM micrograph of FIG. 17, and it is noted that the obscure region (C) is a fine grained recrystallized grain structure in a submicron order.

FIG. 18 shows enlargement of the interior of the fine grain in a submicron order, and fine rod-like precipitates of several tens nm as formed along the c-axis of Mg.

The grain size of the hot extruded Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy was measured from FIGS. 16 and 17. Since the obtained structure was not homogenous, the major axis and the minor axis were measured for crystals of the respective regions without employing the linear intercept method, and an average value thereof was defined as the grain size. Also, with respect to the unrecrystallized grain (A) and the equi-axed recrystallized grain (B), the optical micrograph of FIG. 16 was used, and with respect to the fine grain region in a submicron order (C), the TEM micrograph of FIG. 17 was used. As a result, it was noted that the unrecrystallized grain (A) had size distribution of from about 5 to 25 μm and had an average grain size of 11 μm; the equi-axed recrystallized grain (B) had size distribution of from about 1 to 5 μm and had an average grain size of 2.8 μm; and the fine grain region in a submicron order (C) had size distribution of from about 0.1 to 1 μm and had an average grain size of 0.75 μm.

With respect to the Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy and the Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy each having excellent age hardening properties, a tensile test at room temperature and a compression test at room temperature were executed in parallel to the extrusion direction. A tensile specimen was a JIS 14B specimen and had a gauge length of 20 mm. A compression specimen had a diameter of 9.5 mm and a height of 14.3 mm. The tensile test and the compression test were performed under a condition at an initial strain rate of 10−3 s−1.

FIG. 19 (measurement data on which this figure is based are shown in Table 2) shows distribution of a Schmid factor in the basal slip direction against the tensile load application direction, namely the extrusion direction. Since the degree of integration of the basal texture parallel to the extrusion direction is weak, the Schmid factors of the alloys of this invention are uniformly distributed as compared with those of extruded materials of the existing AZ91 alloy (Mg-9 mass % Al-1 mass % Zn alloy), and an average value thereof is 0.20 or more.

TABLE 2 Chart: Schmid Factor Mg—2.3Zn—0.1Ag—0.1Ca Mg—2.3Zn—0.1Ag—0.1Ca—0.17Zr extruded at 300° C. extruded at 350° C. extruded at 300° C. extruded at 350° C. (1) (2) (3) (1) (2) (3) (1) (2) (3) (1) (2) (3) 0.013 0.062 6.177 0.013 0.074 7.387 0.013 0.121 12.112 0.013 0.131 13.064 0.037 0.068 6.793 0.038 0.051 5.078 0.038 0.100 9.978 0.038 0.087 8.709 0.062 0.062 6.151 0.063 0.073 7.285 0.063 0.086 8.557 0.063 0.093 9.268 0.087 0.063 6.303 0.088 0.062 6.183 0.088 0.066 6.649 0.088 0.093 9.296 0.112 0.058 5.811 0.113 0.085 8.472 0.113 0.050 5.010 0.112 0.054 5.403 0.137 0.053 5.337 0.137 0.058 5.812 0.138 0.046 4.589 0.137 0.034 3.440 0.162 0.054 5.440 0.162 0.043 4.285 0.163 0.049 4.888 0.162 0.036 3.596 0.187 0.050 5.032 0.187 0.050 4.962 0.188 0.033 3.308 0.187 0.025 2.516 0.212 0.042 4.240 0.212 0.056 5.641 0.213 0.033 3.275 0.212 0.027 2.700 0.237 0.043 4.314 0.237 0.059 5.883 0.238 0.035 3.468 0.237 0.030 2.996 0.262 0.052 5.158 0.262 0.048 4.752 0.263 0.043 4.251 0.262 0.040 4.012 0.287 0.046 4.598 0.287 0.025 2.526 0.288 0.039 3.895 0.287 0.028 2.758 0.312 0.043 4.318 0.312 0.039 3.862 0.313 0.036 3.550 0.312 0.042 4.175 0.337 0.041 4.062 0.337 0.037 3.672 0.338 0.030 3.039 0.337 0.044 4.351 0.362 0.049 4.859 0.362 0.042 4.227 0.363 0.041 4.079 0.362 0.042 4.164 0.387 0.044 4.447 0.387 0.028 2.848 0.388 0.049 4.945 0.387 0.040 4.017 0.412 0.049 4.886 0.412 0.042 4.248 0.413 0.035 3.533 0.412 0.041 4.056 0.437 0.053 5.287 0.437 0.037 3.697 0.437 0.039 3.897 0.437 0.055 5.519 0.462 0.035 3.494 0.462 0.050 5.004 0.462 0.040 3.956 0.462 0.040 4.003 0.487 0.033 3.295 0.487 0.042 4.176 0.487 0.030 3.020 0.487 0.020 1.958 Average 0.228 22.824 0.220 22.020 0.200 19.983 0.199 19.864 (1): Schmid Factor (2): Number Fraction (3): (2) × 100

FIG. 20 shows a stress-strain curve obtained by each of a tensile test and a compression test at room temperature of an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy as extruded at 350° C. Tables 3 to 7 show measurement data corresponding to the stress-strain curve in the tensile test shown in FIG. 20; and Tables 8 to 11 show measurement data corresponding to the stress-strain curve in the compression test shown in FIG. 20.

(Initial strain rate: 10−3 s−1; shape of tensile specimen: JIS 14B (gauge length: 20 mm); and shape of compression specimen: 9.5 mm in diameter and 14.3 mm in height)

TABLE 3 tensile test: table 1: (1) (2) 0.000 2.462 0.008 2.537 0.007 2.736 0.001 2.810 0.001 3.034 0.005 3.108 0.001 3.357 0.003 3.531 0.002 3.631 0.006 3.830 0.008 4.178 0.005 4.178 0.004 4.402 0.001 4.725 0.003 4.824 0.004 5.078 0.005 5.222 0.003 5.471 0.006 5.695 0.003 5.919 0.000 6.217 0.003 6.391 0.002 6.640 0.001 6.864 0.010 7.162 0.012 7.336 0.006 7.659 0.013 7.883 0.004 8.182 0.000 8.455 0.011 8.729 0.018 9.102 0.009 9.325 0.008 9.649 0.009 9.922 0.015 10.196 0.008 10.494 0.003 10.892 0.015 11.191 0.003 11.464 0.015 11.812 0.018 12.136 0.011 12.409 0.014 12.708 0.012 13.130 0.014 13.454 0.013 13.777 0.020 14.125 0.012 14.448 0.018 14.772 0.007 15.145 0.013 16.518 0.017 16.841 0.015 16.164 0.026 16.612 0.026 17.010 0.027 17.283 0.026 17.731 0.021 17.880 0.019 18.602 0.022 18.875 0.019 19.099 0.024 19.496 0.031 19.919 0.024 20.292 0.035 20.716 0.029 21.163 0.029 21.511 0.027 21.958 0.028 22.331 0.030 22.804 0.029 23.202 0.032 23.660 0.029 24.047 0.039 24.445 0.039 24.843 0.032 25.266 0.043 25.689 0.036 26.062 0.044 26.559 0.037 26.982 0.037 27.429 0.042 27.877 0.042 28.250 0.048 28.648 0.047 29.170 0.049 29.599 0.047 30.066 0.053 30.463 0.062 30.985 0.058 31.433 0.057 31.831 0.054 32.279 0.059 32.701 0.055 33.224 0.059 33.721 0.061 34.094 0.061 34.591 0.059 35.014 0.056 35.437 0.061 35.959 0.066 36.606 0.068 36.929 0.063 37.476 0.057 37.924 0.064 38.346 0.074 38.844 0.077 39.291 0.072 39.814 0.072 40.361 0.070 40.858 0.073 41.306 0.077 41.778 0.073 42.276 0.082 42.773 0.078 43.295 0.070 43.768 0.076 44.240 0.075 44.737 0.076 45.285 0.081 45.807 0.087 46.329 0.081 46.727 0.089 47.324 0.090 47.796 0.085 48.318 0.085 48.866 0.093 49.363 0.094 49.885 0.085 50.358 0.097 50.905 0.092 51.377 0.089 51.924 0.099 52.397 0.104 52.919 0.109 53.466 0.097 53.963 0.104 54.511 0.099 54.983 0.102 55.480 0.105 56.202 0.115 56.599 0.112 57.097 0.110 57.644 0.114 58.216 0.110 58.788 0.113 59.260 0.107 59.783 0.117 60.230 0.114 60.827 0.113 61.399 0.117 61.921 0.126 62.419 0.123 62.966 0.117 63.538 0.126 64.010 0.124 64.582 0.137 65.055 0.131 65.602 0.129 66.223 0.128 66.696 0.136 67.243 0.128 67.815 0.129 68.362 0.140 68.859 0.128 69.382 0.127 69.755 0.137 70.526 0.139 70.998 0.140 71.545 0.137 72.117 0.137 72.664 0.137 73.211 0.145 73.758 0.146 74.305 0.146 74.753 0.155 75.524 0.149 75.897 0.143 76.469 0.146 76.966 0.146 77.588 0.149 78.110 0.149 78.608 0.145 79.180 0.157 79.727 0.152 80.299 0.157 80.771 0.154 81.318 0.156 81.865 0.144 82.363 0.164 82.984 0.157 83.556 0.167 84.103 0.163 84.700 0.161 85.123 0.172 86.720 0.172 86.242 0.163 86.739 0.164 87.262 0.173 87.834 0.174 88.356 0.177 88.903 0.171 89.450 0.167 89.997 0.160 90.544 0.171 91.091 0.172 91.514 0.177 92.210 0.170 92.633 0.174 93.230 0.184 93.702 0.184 94.225 0.182 94.772 0.182 95.146 0.181 95.518 0.184 95.841 0.184 96.214 0.186 96.761 0.178 97.283 0.187 97.831 0.192 98.278 0.185 98.825 0.187 99.223 0.196 99.770 0.190 100.218 0.195 100.641 0.187 101.138 0.189 101.536 0.203 102.033 0.196 102.431 0.202 102.854 0.195 103.202 0.196 103.699 0.198 104.048 0.197 104.321 0.197 103.625 0.180 92.235 0.120 81.816 0.114 77.290 0.118 76.991 0.113 78.160 0.129 79.553 0.122 80.647 0.126 81.368 0.120 82.039 0.129 82.686 0.123 83.382 0.126 84.128 0.132 84.849 0.130 85.471 0.128 86.118 0.131 87.013 0.133 87.510 0.139 88.207 0.140 88.828 0.141 89.674 0.147 90.246 0.138 90.868 0.145 91.489 0.154 92.185 0.146 92.807 0.142 93.479 0.157 94.175 0.154 94.846 0.157 95.518 0.160 96.189 0.169 96.811 0.155 97.467 0.164 98.204 0.164 98.825 0.170 99.397 0.171 100.094 0.160 100.765 0.170 101.387 0.177 102.083 0.169 102.630 0.164 103.326 0.172 104.072 0.176 104.595 0.170 105.241 0.176 105.838 0.176 106.485 0.184 107.106 0.176 107.629 0.188 108.399 0.186 108.922 0.193 109.518 0.187 110.090 0.194 110.662 0.194 111.284 0.192 111.931 0.194 112.503 0.204 113.050 0.201 113.647 0.196 114.368 0.196 114.915 0.199 115.362 0.206 116.059 0.206 116.680 0.202 117.252 0.210 117.760 0.210 118.421 0.207 119.018 0.204 119.515 0.217 120.212 0.207 120.734 0.207 121.306 0.214 122.002 0.216 122.600 0.225 123.047 0.219 123.643 0.219 124.215 0.225 124.862 0.226 125.434 0.223 126.006 0.226 126.628 0.235 127.200 0.242 127.772 0.235 128.344 0.235 128.940 0.223 129.587 0.241 130.134 0.232 130.706 0.248 131.328 0.239 131.900 0.236 132.447 0.247 133.118 0.249 133.715 0.248 134.262 0.248 134.809 0.248 135.555 0.246 136.028 0.259 136.649 0.251 137.246 0.268 137.744 0.257 138.390 0.260 139.012 0.262 139.509 0.265 140.156 0.264 140.678 0.273 141.325 0.269 141.971 0.272 142.518 0.273 143.115 0.277 143.712 0.272 144.334 0.277 144.831 0.282 145.478 0.289 146.099 0.292 146.621 0.289 147.193 0.286 147.790 0.293 148.387 0.300 148.984 0.299 149.681 0.298 150.153 0.298 150.760 0.295 151.396 0.296 151.993 0.299 152.490 0.292 153.137 0.295 153.734 0.293 154.281 0.315 154.878 0.311 155.499 0.309 156.022 0.312 156.594 0.319 157.141 0.306 157.738 0.317 158.260 0.316 158.906 0.316 159.503 0.320 160.100 0.320 160.672 0.315 161.269 0.325 161.915 0.315 162.338 0.332 162.885 0.323 163.532 0.324 164.178 0.331 164.701 0.333 165.173 0.326 165.869 0.340 166.466 0.343 167.038 0.344 167.535 0.338 168.132 0.344 168.764 0.345 169.276 0.360 169.997 0.339 170.445 0.358 170.967 0.353 171.564 0.357 171.962 0.352 172.509 0.358 173.056 0.358 173.603 0.365 174.250 0.360 174.822 0.368 175.344 0.368 176.966 0.368 176.563 0.365 177.110 0.373 177.731 0.370 178.328 0.372 178.850 0.378 179.472 0.375 180.044 0.378 180.541 0.380 181.213 0.378 181.586 0.387 182.406 0.387 182.904 0.384 183.451 0.381 184.097 0.397 184.620 0.399 185.241 0.395 186.838 0.391 186.360 0.390 186.908 0.407 187.604 0.406 188.076 0.403 188.623 0.398 189.046 0.405 189.743 0.412 190.339 0.408 190.911 0.413 191.558 0.407 192.080 0.415 192.677 0.419 193.199 0.418 193.821 0.424 194.418 0.421 194.916 0.428 195.661 0.433 196.009 0.428 196.581 0.432 197.228 0.444 197.750 0.436 198.347 0.426 198.944 0.439 199.466 0.446 200.063 0.445 200.635 0.448 201.157 0.448 201.779 0.447 202.326 0.444 202.748 0.441 203.420 0.446 204.091 0.450 204.614 0.448 205.136 0.446 205.708 0.457 206.255 0.455 206.852 0.461 207.449 0.459 207.996 0.463 208.568 0.471 209.090 0.470 209.712 0.472 210.283 0.473 210.806 0.479 211.427 0.482 211.950 0.489 212.497 0.483 213.044 0.490 213.616 0.493 214.188 0.485 214.760 0.486 215.232 0.490 215.804 0.491 216.476 0.501 217.172 0.496 217.520 0.499 218.067 0.504 218.614 0.607 219.136 0.499 219.733 0.509 220.231 0.514 220.653 0.512 221.399 0.512 221.922 0.516 222.543 0.510 223.066 0.510 223.513 0.524 224.185 0.520 224.707 0.518 225.204 0.535 226.851 0.529 226.323 0.527 226.846 0.534 227.417 0.536 228.014 0.532 228.537 0.540 228.984 0.540 229.357 0.546 230.103 0.543 230.700 0.540 231.173 0.547 231.720 0.549 232.341 0.553 232.789 0.555 233.411 0.553 233.958 0.558 234.466 0.561 234.977 0.555 235.524 0.559 236.072 0.565 236.544 0.571 237.116 0.571 237.638 0.575 238.136 0.569 238.683 0.578 239.081 0.574 239.702 0.582 240.249 0.577 240.796 0.577 241.269 0.589 241.965 0.590 242.488 0.583 242.761 0.592 243.482 0.593 243.880 0.587 244.328 0.600 244.900 0.595 245.372 0.603 245.894 0.605 246.417 0.593 246.939 0.608 247.436 0.603 247.884 0.605 248.431 0.603 248.903 0.610 249.401 0.609 249.898 0.622 250.495 0.614 250.868 0.621 251.390 0.624 251.863 0.625 252.360 0.624 252.857 0.631 253.380 0.629 253.852 0.631 254.374 0.632 254.921 0.632 255.245 0.642 255.692 0.635 256.239 0.641 256.712 0.645 257.135 0.646 257.607 0.649 258.129 0.647 258.602 0.651 259.049 0.658 259.472 0.657 259.771 0.653 260.392 0.674 260.916 0.661 261.313 0.664 261.760 0.670 262.332 0.675 262.631 0.676 263.078 0.674 263.551 0.667 264.023 0.680 264.396 0.688 264.819 0.682 265.316 0.687 265.764 0.679 266.212 0.694 266.586 0.696 266.982 0.692 267.455 0.705 267.977 0.697 268.325 0.703 268.748 0.710 269.121 0.715 269.519 0.713 269.817 0.710 270.340 0.717 270.762 0.716 271.235 0.722 271.633 0.725 272.006 0.726 272.354 0.730 272.851 0.725 273.199 0.727 273.498 0.732 273.921 0.739 274.368 0.742 274.716 0.741 275.065 0.743 275.537 0.767 275.860 0.751 276.233 0.748 276.656 0.756 276.955 0.749 277.427 0.763 277.776 0.771 278.148 0.768 278.621 0.768 278.844 0.774 279.168 0.772 279.641 0.773 279.889 0.777 280.262 0.787 280.685 0.778 281.058 0.790 281.282 0.781 281.605 0.786 281.953 0.799 282.376 0.796 282.475 0.793 282.997 0.805 283.271 0.805 283.669 0.809 283.917 0.796 284.241 0.814 284.564 0.824 284.937 0.824 285.161 0.824 285.509 0.829 285.758 0.833 286.180 0.827 286.379 0.831 286.479 0.835 286.951 0.842 287.250 0.847 287.697 0.847 287.872 0.845 288.170 0.846 288.443 0.849 288.717 0.850 288.966 0.859 289.289 0.855 289.513 0.859 289.737 0.860 290.035 0.870 290.259 0.875 290.532 0.880 290.881 0.882 291.129 0.879 291.303 0.883 291.577 0.886 291.726 0.889 292.074 0.895 292.248 0.896 292.472 0.902 292.671 0.900 292.994 0.906 293.243 0.905 293.467 0.914 293.467 0.909 293.865 0.918 294.064 0.928 294.287 0.920 294.462 0.923 294.760 0.922 294.959 0.939 296.133 0.933 295.282 0.931 295.407 0.940 295.705 0.944 295.879 0.940 296.053 0.942 296.128 0.952 296.401 0.951 296.600 0.954 296.849 0.961 297.073 0.960 297.172 0.976 297.247 0.964 297.495 0.978 297.645 0.978 297.794 0.992 297.968 0.990 298.092 0.991 298.217 0.983 298.366 1.000 298.515 1.004 298.540 1.008 298.764 1.011 299.037 0.994 298.988 1.016 299.261 1.015 299.361 1.030 299.609 1.021 299.684 1.029 299.758 1.038 299.957 1.034 299.908 1.042 300.082 1.045 300.256 1.053 300.405 1.051 300.504 1.057 300.629 1.052 300.753 1.061 300.853 1.065 300.977 1.073 301.076 1.078 301.126 1.078 301.250 1.090 301.350 1.100 301.425 1.092 301.449 1.095 301.648 1.095 301.773 1.097 301.847 1.103 301.947 1.117 302.096 1.114 302.096 1.119 302.270 1.124 302.345 1.124 302.394 1.129 302.618 1.124 302.668 1.136 302.643 1.141 302.743 1.139 302.743 1.145 302.867 1.150 302.917 1.169 303.016 1.161 303.116 1.169 303.116 1.176 303.266 1.169 303.315 1.174 303.439 1.177 303.538 1.186 303.489 1.192 303.663 1.194 303.712 1.191 303.787 1.198 303.862 1.194 303.961 1.205 303.936 1.212 304.135 1.219 304.135 1.219 304.210 1.219 304.309 1.233 304.409 1.241 304.458 1.242 304.533 1.238 304.608 1.247 304.583 1.246 304.682 1.246 304.682 1.255 304.782 1.260 304.856 1.256 305.006 1.260 305.030 1.263 305.105 1.267 305.155 1.269 305.180 1.279 305.279 1.282 305.329 1.281 305.403 1.290 305.473 1.294 305.528 1.303 305.652 1.291 305.528 1.307 305.652 1.310 305.801 1.316 305.801 1.318 305.851 1.323 306.950 1.324 306.050 1.324 306.075 1.345 306.100 1.340 306.249 1.334 306.274 1.341 306.274 1.354 306.373 1.350 306.423 1.352 306.373 1.358 306.423 1.360 306.597 1.369 306.597 1.386 306.771 1.376 306.721 1.372 306.896 1.384 306.846 1.387 306.945 1.394 307.020 1.396 307.144 1.401 307.144 1.404 307.119 1.412 307.269 1.414 307.318 1.420 307.368 1.425 307.467 1.425 307.467 1.428 307.567 1.437 307.617 1.434 307.641 1.440 307.741 1.452 307.716 1.451 307.716 1.456 307.841 1.469 307.940 1.469 307.990 1.461 307.990 1.471 308.064 1.479 308.139 1.487 308.213 1.487 308.263 1.485 308.313 1.500 308.363 1.509 308.462 1.506 308.412 1.513 308.537 1.504 308.686 1.513 308.686 1.518 308.711 1.519 308.736 1.524 308.785 1.530 308.886 1.528 308.910 1.539 308.960 1.545 309.009 1.557 309.084 1.648 309.233 1.561 309.407 1.559 309.283 1.567 309.283 1.563 309.357 1.571 309.407 1.576 309.482 1.574 309.607 1.580 309.367 1.591 309.631 1.590 309.681 1.598 309.706 1.604 309.830 1.601 309.830 1.600 309.979 1.605 309.979 1.618 310.054 1.618 310.128 1.625 310.153 1.625 310.103 1.632 310.253 1.639 310.302 1.639 310.327 1.646 310.352 1.643 310.427 1.660 310.501 1.663 310.551 1.666 310.651 1.673 310.675 1.666 310.700 1.661 310.775 1.676 310.874 1.677 310.949 1.681 310.874 1.688 310.949 1.684 310.999 1.696 310.999 1.705 311.173 1.713 311.247 1.717 311.223 1.708 311.297 1.722 311.347 1.713 311.471 1.727 311.496 1.726 311.496 1.740 311.620 1.736 311.645 1.752 311.645 1.748 311.695 1.756 311.770 1.750 311.819 1.767 311.819 1.763 311.869 1.766 311.869 1.770 312.043 1.771 312.093 1.769 312.118 1.776 312.192 1.777 312.292 1.789 312.267 1.792 312.391 1.792 312.391 1.799 312.541 1.811 312.516 1.808 312.541 1.820 312.641 1.817 312.615 1.815 312.715 1.827 312.739 1.826 312.864 1.830 312.864 1.838 312.889 1.835 312.963 1.841 313.063 1.846 313.088 1.860 313.137 1.855 313.162 1.867 313.262 1.866 313.237 1.863 313.311 (1) Strain (%) (2) Stress (MPa)

TABLE 4 tensile test: table 2: (1) (2) 1.871 313.336 1.879 313.411 1.890 313.510 1.896 313.510 1.893 313.685 1.905 313.709 1.903 313.709 1.913 313.684 1.905 313.809 1.913 313.834 1.913 313.858 1.920 313.858 1.925 313.958 1.939 314.033 1.948 314.058 1.935 314.107 1.941 314.232 1.946 314.182 1.941 314.331 1.956 314.306 1.951 314.356 1.956 314.455 1.969 314.480 1.972 314.505 1.973 314.605 1.967 314.679 1.976 314.654 1.985 314.679 1.981 314.779 1.990 314.853 1.989 314.853 2.005 314.928 2.010 315.002 2.006 315.027 2.015 315.127 2.010 315.102 2.020 315.276 2.016 315.276 2.027 315.276 2.033 315.301 2.037 315.326 2.039 315.450 2.037 315.475 2.042 315.625 2.053 315.560 2.061 315.560 2.059 315.649 2.070 315.674 2.066 315.773 2.075 315.823 2.074 315.898 2.087 315.873 2.084 315.923 2.093 315.873 2.088 316.072 2.090 315.997 2.099 316.146 2.112 316.246 2.110 316.171 2.112 316.296 2.117 316.345 2.116 316.395 2.121 316.445 2.121 316.494 2.133 316.519 2.146 316.619 2.150 316.594 2.144 316.644 2.145 316.768 2.149 316.793 2.156 316.793 2.152 316.818 2.161 316.917 2.166 316.917 2.161 316.992 2.171 317.091 2.182 317.141 2.183 317.116 2.172 317.216 2.186 317.315 2.195 317.241 2.197 317.315 2.195 317.440 2.206 317.489 2.211 317.440 2.218 317.663 2.209 317.564 2.229 317.688 2.221 317.663 2.229 317.788 2.233 317.813 2.232 317.813 2.236 317.937 2.250 317.912 2.252 317.987 2.249 317.987 2.261 318.111 2.257 318.136 2.277 318.161 2.275 318.210 2.283 318.285 2.268 318.335 2.292 318.335 2.283 318.459 2.289 318.459 2.299 318.608 2.302 318.534 2.301 318.633 2.305 318.683 2.314 318.683 2.311 318.782 2.321 318.782 2.327 318.782 2.325 318.857 2.324 318.932 2.335 318.981 2.337 319.006 2.343 319.056 2.345 319.106 2.349 319.155 2.356 319.205 2.362 319.230 2.363 319.354 2.353 319.354 2.368 319.379 2.378 319.404 2.386 319.454 2.376 319.528 2.384 319.628 2.386 319.628 2.394 319.762 2.398 319.727 2.397 319.752 2.405 319.802 2.421 319.852 2.417 319.827 2.408 319.901 2.416 319.951 2.433 319.951 2.429 320.076 2.438 320.100 2.441 320.150 2.440 320.200 2.441 320.250 2.454 320.274 2.456 320.424 2.455 320.399 2.463 320.399 2.465 320.424 2.472 320.523 2.473 320.722 2.478 320.672 2.475 320.672 2.484 320.747 2.484 320.672 2.491 320.697 2.499 320.747 2.502 320.772 2.505 320.896 2.503 320.822 2.507 320.971 2.516 321.045 2.514 321.045 2.521 321.120 2.527 321.170 2.541 321.195 2.528 321.269 2.551 321.294 2.538 321.269 2.554 321.394 2.547 321.394 2.557 321.468 2.557 321.543 2.560 321.543 2.551 321.518 2.569 321.592 2.585 321.692 2.563 321.692 2.579 321.766 2.582 321.816 2.582 321.891 2.598 321.891 2.601 321.941 2.604 321.990 2.595 321.065 2.607 322.065 2.617 322.140 2.626 322.164 2.629 322.264 2.617 322.065 2.629 322.239 2.636 322.289 2.648 322.488 2.636 322.363 2.639 322.388 2.652 322.613 2.648 322.687 2.664 322.562 2.658 322.612 2.664 322.687 2.658 322.712 2.674 322.712 2.680 322.836 2.689 322.836 2.677 322.861 2.677 322.910 2.693 322.910 2.686 323.010 2.696 323.035 2.705 322.985 2.705 323.060 2.708 323.234 2.711 323.234 2.721 323.234 2.730 323.308 2.718 323.283 2.737 323.333 2.727 323.433 2.753 323.433 2.756 323.482 2.749 323.607 2.746 323.507 2.743 323.632 2.762 323.656 2.756 323.681 2.765 323.756 2.784 323.756 2.784 323.756 2.775 323.880 2.790 323.781 2.800 323.980 2.787 323.930 2.787 323.980 2.813 324.228 2.797 324.104 2.809 324.129 2.819 324.204 2.813 324.278 2.813 324.378 2.831 324.303 2.835 324.353 2.825 324.402 2.838 324.477 2.828 324.402 2.857 324.577 2.854 324.601 2.854 324.626 2.857 324.701 2.863 324.701 2.866 324.726 2.860 324.701 2.866 324.776 2.891 324.925 2.885 324.974 2.882 324.900 2.888 324.950 2.888 324.925 2.898 325.074 2.904 325.099 2.910 325.124 2.917 325.273 2.901 325.198 2.920 325.223 2.920 325.323 2.929 325.298 2.936 325.397 2.942 325.422 2.932 325.397 2.955 325.497 2.945 325.397 2.955 325.571 2.951 325.596 2.964 325.472 2.958 325.671 2.970 325.621 2.973 325.795 2.983 325.795 2.967 325.770 2.983 325.820 2.989 325.919 2.992 326.919 2.989 326.994 3.002 326.019 2.986 326.194 3.002 326.143 3.008 326.143 3.015 326.268 3.027 326.193 3.030 326.193 3.040 326.293 3.030 326.342 3.030 326.392 3.024 326.392 3.043 326.417 3.052 326.491 3.052 326.541 3.056 326.516 3.059 326.591 3.052 326.616 3.065 326.790 3.081 326.740 3.078 326.765 3.093 326.815 3.081 326.840 3.090 326.840 3.081 326.864 3.090 326.939 3.100 326.989 3.106 326.989 3.109 327.113 3.112 327.088 3.112 327.113 3.112 327.113 3.134 327.163 3.125 327.188 3.141 327.213 3.150 327.337 3.134 327.312 3.144 327.362 3.167 327.412 3.147 327.436 3.144 327.536 3.166 327.486 3.172 327.536 3.157 327.561 3.160 327.561 3.176 327.760 3.176 327.735 3.176 327.710 3.169 327.785 3.201 327.809 3.194 327.785 3.204 327.909 3.198 327.909 3.210 327.983 3.220 328.008 3.220 328.008 3.223 327.983 3.201 328.108 3.229 328.158 3.220 328.232 3.232 328.257 3.235 328.257 3.239 328.232 3.251 328.282 3.239 328.357 3.235 328.406 3.251 328.456 3.270 328.456 3.267 328.506 3.270 328.531 3.267 328.580 3.277 328.555 3.286 328.630 3.283 328.705 3.289 328.779 3.311 328.754 3.289 328.754 3.305 328.754 3.321 328.879 3.324 328.829 3.324 328.904 3.336 329.227 3.333 328.978 3.327 329.103 3.327 329.053 3.336 329.177 3.349 329.177 3.340 329.078 3.343 329.326 3.346 329.252 3.346 329.302 3.371 329.326 3.374 329.361 3.371 329.326 3.368 329.426 3.362 329.476 3.371 329.500 3.384 329.550 3.384 329.575 3.393 329.600 3.393 329.625 3.393 329.675 3.409 329.699 3.406 329.749 3.419 329.799 3.412 329.824 3.409 329.824 3.419 329.824 3.422 329.898 3.434 329.948 3.434 330.023 3.441 329.973 3.447 329.998 3.441 330.122 3.447 330.122 3.453 330.172 3.447 330.172 3.453 330.297 3.469 330.271 3.472 330.271 3.463 330.321 3.479 330.520 3.482 330.545 3.475 330.421 3.491 330.445 3.504 330.470 3.504 330.445 3.510 330.495 3.507 330.495 3.510 330.644 3.510 330.694 3.501 330.644 3.520 330.716 3.516 330.744 3.548 330.769 3.526 330.843 3.529 330.843 3.535 330.893 3.529 331.067 3.542 331.017 3.551 330.943 3.545 330.993 3.561 331.067 3.561 331.092 3.557 331.042 3.576 331.067 3.561 331.191 3.576 331.216 3.598 331.216 3.576 331.241 3.592 331.291 3.595 331.291 3.602 331.390 3.592 331.390 3.611 331.490 3.602 331.490 3.624 331.465 3.611 331.589 3.630 331.589 3.630 331.664 3.627 331.639 3.643 331.614 3.640 331.689 3.662 331.689 3.636 331.714 3.655 331.788 3.668 331.813 3.658 331.838 3.690 331.838 3.671 332.037 3.671 331.888 3.684 331.938 3.677 331.987 3.696 331.987 3.703 331.962 3.715 332.112 3.699 332.136 3.696 332.062 3.709 332.161 3.715 332.211 3.706 332.236 3.725 332.261 3.734 332.286 3.722 332.311 3.731 332.410 3.731 332.385 3.734 332.435 3.744 332.385 3.753 332.460 3.750 332.534 3.747 332.510 3.753 332.510 3.744 332.534 3.763 332.659 3.785 332.609 3.772 332.659 3.778 332.783 3.785 332.733 3.804 332.783 3.788 332.808 3.791 332.758 3.794 332.907 3.788 332.883 3.813 332.883 3.813 332.858 3.826 333.007 3.819 333.007 3.819 333.032 3.832 333.106 3.826 333.131 3.829 333.106 3.851 333.032 3.854 333.181 3.838 333.231 3.848 333.255 3.838 333.280 3.851 333.330 3.848 333.280 3.864 333.355 3.879 333.280 3.886 333.380 3.883 333.380 3.883 333.479 3.883 333.479 3.892 333.405 3.889 333.529 3.883 333.579 3.905 333.629 3.898 333.703 3.905 333.653 3.911 333.678 3.920 333.927 3.917 333.803 3.936 333.827 3.914 333.803 3.936 333.902 3.943 333.902 3.933 333.927 3.943 333.902 3.955 333.977 3.943 333.977 3.958 334.051 3.977 334.051 3.961 334.051 3.968 334.126 3.968 334.151 3.984 334.002 3.993 334.250 3.984 334.250 3.984 334.225 3.987 334.250 3.999 334.524 4.006 334.325 4.003 334.375 4.009 334.499 4.009 334.275 4.015 334.499 4.015 334.474 4.031 334.524 4.031 334.549 4.047 334.574 4.037 334.574 4.053 334.623 4.050 334.698 4.066 334.698 4.066 334.574 4.059 334.723 4.063 334.723 4.072 334.822 4.069 334.872 4.081 334.847 4.088 334.847 4.081 334.971 4.078 334.947 4.081 334.897 4.094 334.996 4.107 335.021 4.097 335.071 4.110 335.021 4.122 335.170 4.119 335.096 4.113 335.170 4.132 335.121 4.126 335.295 4.129 335.245 4.132 334.245 4.132 335.295 4.138 335.320 4.167 335.270 4.151 335.369 4.157 335.364 4.154 335.494 4.164 335.469 4.154 335.519 4.179 335.543 4.182 335.693 4.192 335.519 4.192 335.643 4.186 335.742 4.192 335.618 4.201 335.593 4.227 335.742 4.227 335.792 4.201 335.742 4.208 335.792 4.211 335.842 4.223 335.867 4.223 335.892 4.236 335.767 4.242 335.966 4.230 335.916 4.236 335.892 4.266 336.090 4.242 335.991 4.258 336.090 4.268 335.991 4.271 336.041 4.271 336.140 4.271 336.240 4.293 336.041 4.283 336.215 4.274 336.289 4.280 336.165 4.290 336.289 4.290 336.339 4.287 336.364 4.309 336.339 4.296 339.339 4.302 336.439 4.306 336.414 4.315 336.463 4.318 336.439 4.312 336.389 4.324 336.613 4.328 336.538 4.343 336.563 4.353 336.613 4.340 336.638 4.358 336.712 4.359 336.538 4.366 336.712 4.362 336.762 4.372 336.812 4.359 336.886 4.375 336.986 4.384 336.886 4.391 336.911 4.391 336.911 4.391 336.936 4.403 337.035 4.403 337.035 4.413 336.986 4.413 337.011 4.413 337.110 4.413 337.060 4.422 337.110 4.429 337.110 4.429 337.135 4.448 337.234 4.432 337.234 4.438 337.259 4.435 337.259 4.444 337.234 4.451 337.284 4.454 337.309 4.454 337.334 4.470 337.384 4.470 337.359 4.479 337.458 4.473 337.483 4.489 337.533 4.479 337.683 4.504 337.483 4.482 337.632 4.482 337.607 4.492 337.533 4.511 337.583 4.514 337.657 4.511 337.732 4.536 337.732 4.527 337.682 4.523 337.707 4.533 337.881 4.523 337.682 4.536 337.782 4.542 337.856 4.533 337.782 4.533 337.881 4.558 337.906 4.552 337.931 4.574 338.005 4.574 338.055 4.577 338.030 4.568 338.080 4.586 338.055 4.583 337.958 4.583 338.030 4.580 338.080 4.593 338.179 4.602 338.155 4.699 388.204 4.596 338.179 4.605 338.254 4.605 338.229 4.631 338.363 4.615 338.329 4.624 338.304 4.631 338.353 4.631 338.304 4.628 338.453 4.650 338.453 4.646 338.428 4.656 338.229 4.650 338.503 4.665 338.503 4.669 338.627 4.669 338.577 4.672 338.602 4.681 338.627 4.665 338.602 4.688 338.652 4.688 338.727 4.688 338.801 4.688 338.702 4.694 338.751 4.700 338.677 4.691 338.776 4.706 338.826 4.735 338.826 4.716 338.751 4.732 338.851 4.732 338.950 4.732 339.025 4.725 338.975 4.754 338.925 4.732 339.000 4.741 338.925 4.735 339.075 4.751 339.149 4.766 339.050 4.770 339.100 4.773 339.174 4.792 339.199 4.770 339.199 4.779 339.199 4.770 339.274 4.789 339.298 4.792 339.323 4.789 339.274 4.795 339.323 4.785 339.423 4.795 339.423 4.814 339.348 4.826 339.398 4.814 339.398 4.826 339.497 4.823 339.423 4.833 339.522 4.830 339.522 4.845 339.572 4.823 339.522 4.845 339.597 4.858 339.597 4.861 339.647 4.858 339.721 4.855 339.622 4.858 339.671 4.867 339.671 4.877 339.796 4.890 339.796 4.893 339.746 4.899 339.821 4.890 339.846 4.899 339.846 4.902 339.870 4.899 339.970 4.908 340.895 4.905 339.020 4.921 339.945 4.931 339.970 4.921 340.920 4.921 340.044 4.940 340.094 4.937 340.094 4.934 340.119 4.943 340.119 4.946 340.144 4.953 340.069 4.959 340.094 4.956 340.194 4.968 340.144 4.978 340.194 4.965 340.417 4.981 340.268 4.991 340.368 4.984 340.318 4.997 340.268 6.000 340.358 4.997 340.393 4.991 340.517 5.009 340.442 5.003 340.393 5.019 340.542 5.013 340.616 5.019 340.517 5.047 340.517 5.032 340.467 5.025 340.567 5.041 340.691 5.054 340.641 5.057 340.716 5.054 340.766 5.079 340.691 5.060 340.641 5.057 340.691 5.063 340.766 5.069 340.716 5.060 340.791 5.079 340.741 5.110 340.791 5.079 340.865 5.085 340.840 5.088 340.840 5.098 340.865 5.101 340.865 5.117 340.989 5.098 340.915 5.117 341.014 5.117 340.989 5.126 341.064 5.126 341.064 5.136 341.014 5.139 341.089 5.133 341.064 5.139 341.039 5.148 341.139 5.155 341.089 5.142 341.114 5.139 341.288 5.158 341.238 5.164 341.139 5.170 341.263 5.174 341.139 5.164 341.313 5.186 341.338 5.193 341.338 5.189 341.363 5.196 341.313 5.202 341.412 2.208 341.412 5.199 341.363 5.221 341.387 5.224 341.636 5.215 341.537 5.237 341.537 5.234 341.611 5.230 341.512 5.249 341.561 5.243 341.586 5.240 341.686 5.246 341.661 5.256 341.661 5.243 341.686 5.262 341.661 5.256 341.686 5.266 341.586 5.275 341.910 5.268 341.810 5.294 341.785 5.271 341.810 5.287 341.885 5.290 341.835 5.300 341.984 5.294 341.934 5.316 341.959 5.331 341.959 5.316 341.910 5.319 341.910 5.338 341.984 5.331 342.009 5.322 342.009 5.344 342.009 5.354 341.959 5.341 342.084 5.341 342.133 5.338 342.158 5.350 342.158 5.350 342.283 5.363 342.183 5.354 342.233 5.369 342.208 5.360 342.208 5.385 342.233 5.382 342.283 5.385 342.283 5.401 342.332 5.404 342.332 5.404 342.382 5.420 342.407 5.410 342.357 5.407 342.407 5.423 342.606 5.423 342.332 5.426 342.407 5.436 342.457 5.432 342.531 5.442 342.482 5.445 342.482 5.445 342.581 5.473 342.581 5.461 342.581 5.464 342.581 5.470 342.581 5.477 342.531 5.480 342.506 5.480 342.631 5.483 342.705 5.477 342.680 5.483 342.705 (1) Strain (%) (2) Stress (MPa)

TABLE 5 tensile test: table 3: (1) (2) 5.480 342.705 5.499 342.755 5.518 342.755 5.508 342.755 5.505 342.805 5.511 342.780 5.496 342.805 5.521 342.904 5.518 342.904 5.530 342.879 5.518 342.855 5.527 342.830 5.546 342.954 5.546 342.929 5.540 342.879 5.562 342.954 5.549 342.979 5.556 342.979 5.562 343.004 5.597 343.053 5.574 343.128 5.578 343.029 5.578 343.103 5.581 342.979 5.587 343.103 5.597 343.128 5.597 343.103 5.603 343.128 5.597 343.128 5.603 343.228 5.628 343.178 5.619 343.208 5.631 343.302 5.631 343.302 5.634 343.277 5.634 343.228 5.647 343.252 5.644 343.352 5.647 343.402 5.650 343.551 5.672 343.377 5.657 343.377 5.672 343.476 5.669 343.526 5.669 343.451 5.682 343.427 5.676 343.501 5.698 343.551 5.685 343.526 5.688 343.427 5.707 343.625 5.701 343.625 5.713 343.601 5.713 343.501 5.713 343.625 5.710 343.625 5.717 343.625 5.729 343.700 5.732 343.576 5.742 343.775 5.742 343.725 5.732 343.760 5.748 343.800 5.748 343.725 5.754 343.924 5.754 343.800 5.795 343.675 5.761 343.849 5.767 343.824 5.786 343.874 5.773 343.849 5.780 343.849 5.792 343.874 5.789 343.999 5.799 343.949 5.789 343.924 5.805 343.775 5.811 344.023 5.818 344.048 5.821 344.048 5.824 344.128 5.824 344.048 5.814 344.073 5.830 344.173 5.843 344.073 5.849 344.148 5.846 344.148 5.855 344.073 5.871 344.123 5.859 344.222 5.862 344.222 5.865 344.222 5.887 344.247 5.874 344.173 5.881 344.297 5.887 344.247 5.881 344.272 5.890 344.222 5.900 344.247 5.903 344.496 5.906 344.297 5.900 344.297 5.928 344.322 5.912 344.421 5.922 344.396 5.912 344.322 5.934 344.396 5.928 344.347 5.941 344.347 5.953 344.471 5.953 344.421 5.947 344.496 5.944 344.496 5.947 344.496 5.958 344.446 5.963 344.546 5.969 344.670 5.969 344.546 5.975 344.570 5.985 344.546 5.979 344.570 5.994 344.595 5.997 344.546 6.010 344.670 5.994 344.670 6.013 344.620 6.010 344.695 6.020 344.695 6.020 344.695 6.020 344.794 6.029 344.745 6.035 344.695 6.035 344.794 6.035 344.794 6.045 344.794 6.048 344.819 6.045 344.919 6.054 344.794 6.067 344.819 6.070 344.968 6.076 344.869 6.080 344.894 6.080 344.993 6.102 344.968 6.092 344.919 6.092 344.993 6.092 344.968 6.095 344.894 6.102 345.018 6.102 345.068 6.105 345.018 6.114 345.043 6.124 345.043 6.127 344.993 6.130 345.118 6.130 345.093 6.130 345.093 6.165 345.068 6.143 345.142 6.155 345.167 6.162 345.167 6.155 345.217 6.155 345.242 6.168 345.093 6.171 345.192 6.174 345.217 6.171 345.192 6.171 345.167 6.187 345.242 6.187 345.217 6.187 345.267 6.193 345.242 6.199 345.366 6.212 345.341 6.209 345.366 6.212 345.366 6.225 345.366 6.237 345.416 6.225 345.391 6.231 345.366 6.244 345.441 6.237 345.441 6.247 345.441 6.253 345.416 6.263 345.515 6.266 345.515 6.269 345.491 6.272 345.515 6.266 345.515 6.269 345.540 6.278 345.565 6.285 345.615 6.288 345.665 6.297 345.590 6.301 345.615 6.291 345.590 6.304 345.640 6.313 345.665 6.301 345.615 6.319 345.714 6.319 345.789 6.304 345.764 6.332 345.739 6.326 345.739 6.335 345.739 6.345 345.789 6.342 345.864 6.360 345.739 6.345 345.814 6.351 345.864 6.364 345.814 6.364 345.839 6.386 345.689 6.370 345.888 6.383 345.913 6.376 345.988 6.379 345.789 6.386 345.888 6.392 345.938 6.395 345.864 6.395 345.938 6.408 345.913 6.414 346.087 6.402 345.938 6.420 346.038 6.420 346.038 6.424 346.013 6.443 346.038 6.430 346.063 6.446 346.063 6.446 346.187 6.446 346.162 6.449 346.063 6.452 346.411 6.439 346.112 6.461 346.112 6.474 346.311 6.458 346.112 6.487 346.112 6.484 346.187 6.484 346.162 6.490 346.187 6.499 346.237 6.487 346.187 6.506 346.187 6.509 346.336 6.515 346.286 6.503 346.286 6.518 346.261 6.528 346.261 6.521 346.237 6.518 346.286 6.515 346.237 6.534 346.411 6.534 346.286 6.525 346.286 6.547 346.336 6.572 346.361 6.553 346.411 6.556 346.436 6.572 346.336 6.569 346.411 6.578 346.436 6.588 346.311 6.588 346.411 6.581 346.535 6.604 346.535 6.619 346.535 6.610 346.510 6.616 346.535 6.610 346.535 6.607 346.485 6.629 346.535 6.619 346.660 6.629 346.610 6.632 346.585 6.638 346.669 6.638 346.610 6.645 346.610 6.654 346.535 6.664 346.659 6.654 346.634 6.664 346.684 6.654 346.759 6.676 346.634 6.676 346.709 6.676 346.709 6.679 346.734 6.682 346.709 6.692 346.709 6.692 346.883 6.705 346.759 6.720 346.759 6.711 346.659 6.698 346.759 6.708 346.983 6.717 346.809 6.736 346.784 6.720 346.883 6.733 346.883 6.733 346.883 6.733 346.833 6.739 346.883 6.739 346.809 6.742 346.883 6.746 346.933 6.755 346.858 6.761 346.958 6.768 346.933 6.777 346.933 6.787 347.032 6.768 346.983 6.783 347.032 6.796 346.958 6.799 347.008 6.783 346.988 6.799 347.032 6.802 347.032 6.806 347.057 6.815 347.057 6.834 347.032 6.821 347.107 6.828 347.082 6.824 347.082 6.831 347.132 6.831 347.182 6.840 347.157 6.850 347.132 6.850 347.132 6.853 347.182 6.859 347.306 6.850 347.266 6.878 347.206 6.878 347.281 6.872 347.206 6.866 347.206 6.888 347.231 6.888 347.231 6.891 347.206 6.903 347.206 6.894 347.231 6.894 347.306 6.903 347.430 6.894 347.306 6.916 347.306 6.916 347.281 6.932 347.331 6.919 347.381 6.929 347.281 6.938 347.231 6.935 347.356 6.941 347.381 6.941 347.405 6.948 347.430 6.948 347.430 6.963 347.405 6.963 347.381 6.976 347.430 6.967 347.430 6.979 347.381 6.979 347.381 6.973 347.455 6.995 347.505 6.985 347.331 6.995 347.555 7.001 347.530 7.008 347.654 7.020 347.530 7.020 347.430 7.036 347.629 7.027 347.480 7.027 347.580 7.039 347.530 7.042 347.654 7.039 347.555 7.039 347.530 7.071 347.629 7.036 347.629 7.061 347.680 7.071 347.629 7.055 347.679 7.068 347.604 7.077 347.629 7.086 347.654 7.086 347.679 7.086 347.580 7.093 347.654 7.093 347.679 7.093 347.704 7.112 347.704 7.115 347.729 7.109 347.704 7.121 347.729 7.124 347.679 7.124 347.803 7.115 347.754 7.137 347.853 7.137 347.704 7.150 347.828 7.140 347.754 7.143 347.704 7.153 347.778 7.166 347.679 7.169 347.679 7.162 347.803 7.172 347.803 7.175 347.878 7.191 347.828 7.172 347.878 7.184 347.878 7.206 347.928 7.184 347.853 7.197 347.803 7.197 347.908 7.210 347.962 7.213 347.803 7.206 347.878 7.232 347.977 7.222 347.878 7.219 347.952 7.232 348.052 7.241 348.077 7.241 348.027 7.241 348.226 7.247 348.027 7.263 348.052 7.263 348.151 7.266 348.102 7.260 348.077 7.266 348.052 7.263 348.052 7.273 348.002 7.276 348.052 7.285 348.151 7.292 348.052 7.304 348.077 7.307 348.161 7.311 347.928 7.304 348.127 7.323 348.201 7.314 348.201 7.326 348.151 7.317 348.151 7.333 348.176 7.330 348.201 7.333 348.251 7.355 348.201 7.342 348.226 7.345 348.201 7.364 348.226 7.380 348.276 7.355 348.226 7.371 348.375 7.374 348.201 7.374 348.251 7.383 348.251 7.386 348.326 7.390 348.326 7.386 348.276 7.393 348.326 7.399 348.350 7.412 348.350 7.408 348.326 7.415 348.400 7.412 348.326 7.418 348.400 7.418 348.400 7.446 348.350 7.431 348.425 7.440 348.375 7.440 348.425 7.443 348.425 7.449 348.400 7.449 348.500 7.465 348.375 7.475 348.450 7.462 348.450 7.465 348.450 7.462 348.450 7.487 348.450 7.497 348.500 7.491 348.549 7.494 348.524 7.487 348.475 7.506 348.524 7.509 348.400 7.509 348.674 7.509 348.674 7.513 348.624 7.522 348.649 7.535 348.649 7.532 348.549 7.538 348.723 7.544 348.699 7.547 348.599 7.541 348.599 7.573 348.624 7.573 348.599 7.563 348.599 7.573 348.500 7.573 348.649 7.582 348.599 7.579 348.599 7.579 348.624 7.595 348.674 7.588 348.798 7.598 348.624 7.595 348.674 7.592 348.723 7.636 348.723 7.620 348.848 7.614 348.599 7.626 348.699 7.629 348.674 7.636 348.723 7.645 348.699 7.664 348.674 7.652 348.699 7.664 348.723 7.642 348.748 7.667 348.699 7.670 348.773 7.683 348.798 7.670 348.823 7.677 348.748 7.677 348.748 7.683 348.773 7.680 348.748 7.686 348.798 7.696 348.823 7.702 348.778 7.705 348.823 7.718 348.823 7.721 348.823 7.724 348.773 7.734 348.848 7.724 348.823 7.718 348.848 7.746 348.873 7.746 348.873 7.746 348.848 7.737 348.823 7.753 348.798 7.762 348.798 7.749 348.972 7.765 348.848 7.771 348.897 7.771 348.873 7.771 348.922 7.790 348.922 7.784 348.972 7.787 348.873 7.800 348.922 7.806 348.773 7.809 348.947 7.809 348.897 7.819 348.748 7.813 348.972 7.816 348.922 7.838 348.997 7.825 348.972 7.888 348.972 7.831 348.947 7.838 348.922 7.828 349.022 7.869 348.997 7.854 348.972 7.857 349.047 7.857 349.047 7.876 349.072 7.885 348.947 7.863 348.997 7.876 349.121 7.879 349.047 7.895 349.022 7.888 349.047 7.898 349.047 7.901 349.121 7.895 349.072 7.936 348.997 7.920 349.121 7.917 349.096 7.917 349.221 7.936 349.022 7.920 349.072 7.942 349.072 7.932 349.121 7.955 349.096 7.955 349.072 7.970 349.072 7.955 349.121 7.945 348.997 7.951 349.096 7.973 349.096 7.973 349.121 7.977 349.096 7.986 349.146 7.980 349.072 7.986 349.047 8.002 349.121 8.018 349.171 7.999 349.146 8.011 349.221 8.015 349.221 8.021 349.072 8.024 349.171 8.046 349.221 8.033 349.121 8.046 349.171 8.043 349.146 8.027 349.221 8.040 349.221 8.059 349.320 8.071 349.196 8.056 349.096 8.068 349.146 8.074 349.221 8.074 349.320 8.071 349.246 8.078 349.246 8.093 349.196 8.087 349.246 8.084 349.270 8.093 349.270 8.093 349.295 8.109 349.345 8.116 349.295 8.106 349.270 8.128 349.246 8.125 349.295 8.141 349.270 8.128 349.320 8.144 349.295 8.144 349.246 8.141 349.295 8.153 349.270 8.150 349.196 8.157 349.295 8.169 349.320 8.191 349.320 8.172 349.320 8.191 349.345 8.204 349.295 8.188 349.370 8.191 349.345 8.194 349.295 8.191 349.345 8.210 349.345 8.213 349.320 8.220 349.345 8.223 349.370 8.232 349.395 8.210 349.370 8.239 349.345 8.226 349.320 8.251 349.345 8.242 349.370 8.242 349.395 8.242 349.345 8.261 349.494 8.242 349.594 8.254 349.445 8.270 349.295 8.273 349.395 8.277 349.445 8.267 349.445 8.283 349.494 8.292 349.420 8.273 349.370 8.299 349.544 8.324 349.420 8.308 349.469 8.305 349.469 8.314 349.519 8.308 349.445 8.321 349.519 8.318 349.420 8.324 349.494 8.324 349.544 8.340 349.494 8.327 349.469 8.343 349.519 8.355 349.494 8.362 349.469 8.340 349.519 8.362 349.594 8.368 349.569 8.371 349.569 8.384 349.494 8.387 349.594 8.403 349.594 8.393 349.519 8.406 349.619 8.406 349.594 8.400 349.519 8.406 349.569 8.419 349.594 8.415 349.519 8.419 349.494 8.425 349.718 8.441 349.619 8.441 349.544 8.444 349.569 8.453 349.644 8.466 349.619 8.447 349.668 8.460 349.544 8.460 349.644 8.456 349.594 8.466 349.644 8.463 349.693 8.469 349.594 8.482 349.644 8.485 349.668 8.494 349.718 8.491 349.668 8.494 349.793 8.513 349.718 8.510 349.668 8.516 349.693 8.513 349.544 8.516 349.693 8.523 349.693 8.526 349.718 8.523 349.519 8.535 349.644 8.564 349.718 8.551 349.644 8.557 349.718 8.548 349.842 8.557 349.644 8.583 349.718 8.573 349.668 8.576 349.718 8.576 349.743 8.570 349.743 8.583 349.644 8.586 349.743 8.589 349.693 8.605 349.768 8.602 349.768 8.611 349.768 8.592 349.793 8.608 349.768 8.624 349.768 8.614 349.668 8.621 349.793 8.652 349.743 8.840 349.768 8.640 349.768 8.633 349.867 8.649 349.768 8.655 349.693 8.662 349.793 8.649 349.793 8.662 349.768 8.649 349.793 8.668 349.892 8.668 349.768 8.662 349.818 8.693 349.818 8.677 349.842 8.693 349.818 8.693 349.793 8.693 349.818 8.706 349.743 8.715 349.818 8.728 349.793 8.715 349.768 8.709 349.842 8.725 349.793 8.728 349.842 8.712 349.743 8.737 349.793 8.744 349.818 8.747 349.842 8.759 349.768 8.747 349.818 8.763 349.793 8.759 349.768 8.772 349.842 8.772 349.768 8.769 349.768 8.788 349.842 8.791 349.867 8.782 349.818 8.804 349.892 8.794 349.793 8.791 349.842 8.801 349.842 8.810 349.892 8.813 349.867 8.819 349.842 8.832 349.892 8.832 350.041 8.829 349.818 8.842 349.892 8.838 349.842 8.845 349.992 8.857 349.942 8.864 349.867 8.860 349.842 8.857 349.818 8.864 349.942 8.867 349.842 8.886 349.917 8.883 349.967 8.876 349.892 8.883 349.842 8.889 349.892 8.911 349.842 8.902 349.892 8.905 349.917 8.914 349.967 8.914 349.917 8.914 349.892 8.927 349.917 8.920 349.867 8.920 349.892 8.946 349.917 8.939 349.892 8.936 349.917 8.949 349.917 8.952 349.967 8.958 349.917 8.968 349.892 8.961 349.942 8.977 349.992 8.971 349.917 8.958 349.942 8.984 349.967 8.980 349.967 8.996 349.917 8.999 349.942 9.003 349.992 8.990 349.892 8.996 350.141 9.012 350.091 9.003 349.967 9.015 349.967 9.018 350.017 9.028 349.867 9.034 349.942 9.031 350.017 9.031 349.967 9.044 349.942 9.056 349.917 9.044 349.967 9.056 349.967 9.063 349.942 9.069 349.942 9.072 349.967 9.066 349.917 9.085 349.942 9.085 349.942 9.091 349.992 9.097 349.967 9.104 349.942 9.100 350.017 9.104 349.942 9.113 350.041 9.110 349.992 9.119 350.041 9.113 349.967 9.122 349.942 9.129 349.942 9.135 349.942 9.135 349.992 9.154 350.017 9.145 350.017 9.164 350.017 9.160 350.017 9.157 349.942 9.160 349.942 9.173 350.017 9.173 349.992 9.179 349.917 9.192 350.091 9.195 349.867 9.195 349.967 9.208 349.917 9.208 349.992 9.211 350.017 9.220 349.967 9.217 350.017 9.198 349.992 9.220 349.967 9.242 349.992 9.242 349.892 9.236 349.967 9.249 350.041 9.249 350.017 9.239 349.942 9.265 350.066 9.277 350.017 9.261 350.017 9.258 349.967 9.268 350.041 9.271 350.041 9.271 349.992 (1) Strain (%) (2) Stress (MPa)

TABLE 6 tensile test: table 4: (1) (2) 9.274 350.066 9.280 350.066 9.287 349.992 9.290 350.041 9.299 350.041 9.280 349.992 9.302 349.942 9.321 350.017 9.315 350.041 9.321 350.017 9.324 350.066 9.324 349.992 9.331 349.967 9.313 350.166 9.353 350.041 9.343 350.116 9.347 349.992 9.353 350.116 9.366 350.216 9.359 350.017 9.369 350.041 9.378 349.942 9.378 350.066 9.372 350.041 9.375 349.992 9.384 350.166 9.378 350.066 9.397 350.091 9.407 350.041 9.400 350.017 9.413 350.066 9.407 350.116 9.407 350.041 9.422 349.917 9.422 349.992 9.426 350.116 9.429 350.017 9.451 349.967 9.441 350.216 9.448 350.017 9.451 350.017 9.454 350.041 9.463 349.992 9.451 350.091 9.470 349.992 9.463 350.017 9.482 350.017 9.473 350.066 9.479 350.166 9.479 350.041 9.495 350.041 9.601 350.091 9.498 350.017 9.501 350.041 9.614 350.091 9.527 350.041 9.514 350.091 9.523 350.216 9.527 350.091 9.530 350.017 9.539 350.066 9.549 349.917 9.549 350.066 9.545 350.066 9.571 350.066 9.549 349.992 9.571 360.091 9.583 350.141 9.571 350.265 9.590 350.041 9.586 350.041 9.580 350.091 9.599 350.017 9.602 350.017 9.616 350.141 9.696 350.017 9.612 350.066 9.618 350.166 9.624 350.041 9.616 350.091 9.616 349.942 9.621 349.942 9.640 350.041 9.643 350.141 9.646 350.066 9.646 350.017 9.650 350.017 9.650 350.017 9.665 350.041 9.665 350.066 9.669 350.066 9.681 350.041 9.669 350.091 9.678 350.091 9.681 350.091 9.697 350.066 9.694 350.116 9.703 350.041 9.713 350.116 9.706 350.066 9.716 349.967 9.716 350.041 9.722 350.017 9.729 350.091 9.741 350.116 9.710 350.066 9.735 350.041 9.744 350.041 9.744 350.041 9.757 350.091 9.760 349.892 9.766 350.017 9.776 349.867 9.773 350.066 9.782 349.967 9.779 349.892 9.789 349.967 9.801 360.017 9.795 360.068 9.804 360.017 9.817 360.091 9.807 360.017 9.804 349.992 9.814 350.041 9.820 349.917 9.833 350.041 9.833 349.992 9.820 349.967 9.836 350.315 9.836 350.017 9.833 349.942 9.842 349.992 9.845 350.017 9.855 349.942 9.871 350.066 9.877 349.992 9.871 349.992 9.877 349.992 9.880 350.017 9.864 349.967 9.896 350.066 9.880 349.967 9.902 349.942 9.896 349.942 9.912 349.867 9.902 349.967 9.905 349.917 9.927 349.992 9.921 350.017 9.927 349.967 9.927 350.017 9.946 350.141 9.937 349.992 9.937 349.942 9.953 349.942 9.968 349.967 9.959 350.017 9.969 349.892 9.965 350.041 9.978 349.992 9.975 349.967 9.987 349.818 9.972 349.942 9.994 349.793 9.991 349.892 9.997 349.992 10.006 349.942 10.013 350.017 10.013 349.942 10.022 349.917 10.022 349.867 10.022 349.942 10.032 349.892 10.041 349.942 10.035 349.967 10.047 350.116 10.041 349.942 10.057 349.892 10.051 349.942 10.057 349.867 10.073 349.917 10.066 349.942 10.066 349.917 10.088 349.892 10.085 349.867 10.088 349.942 10.085 349.867 10.101 349.743 10.095 350.041 10.101 349.892 10.110 349.892 10.107 349.892 10.117 349.867 10.120 350.091 10.120 349.892 10.123 349.867 10.136 349.867 10.158 349.818 10.136 349.842 10.139 349.818 10.148 349.693 10.164 349.867 10.164 349.842 10.167 349.693 10.180 349.818 10.158 349.842 10.177 349.818 10.183 349.842 10.193 349.818 10.193 349.842 10.199 349.892 10.221 349.842 10.196 349.793 10.208 349.867 10.208 349.818 10.224 349.842 10.227 349.842 10.230 349.842 10.237 349.793 10.221 349.743 10.240 349.842 10.243 349.793 10.237 349.793 10.262 349.842 10.249 349.942 10.262 349.768 10.246 349.768 10.262 349.818 10.275 349.842 10.271 349.793 10.265 349.619 10.284 349.718 10.268 349.743 10.281 349.842 10.290 349.793 10.300 349.818 10.306 349.818 10.309 349.743 10.322 349.842 10.318 349.743 10.322 349.892 10.335 349.768 10.335 349.768 10.338 349.693 10.341 349.743 10.350 349.793 10.347 349.619 10.383 349.743 10.360 349.693 10.379 349.619 10.376 349.743 10.369 349.793 10.376 349.693 10.388 349.743 10.388 349.668 10.404 349.644 10.404 349.619 10.404 349.743 10.398 349.668 10.410 349.768 10.398 349.644 10.423 349.693 10.420 349.718 10.420 349.743 10.429 349.693 10.429 349.718 10.432 349.644 10.442 349.892 10.448 349.693 10.448 349.718 10.458 349.743 10.461 349.668 10.461 349.644 10.461 349.668 10.470 349.668 10.480 349.669 10.486 349.644 10.496 349.743 10.502 349.420 10.496 349.619 10.499 349.594 10.515 349.644 10.505 349.594 10.508 349.619 10.527 349.569 10.524 349.544 10.527 349.644 10.540 349.544 10.559 349.619 10.540 349.594 10.549 349.594 10.556 349.619 10.543 349.768 10.556 349.668 10.574 349.644 10.571 349.569 10.568 349.619 10.574 349.544 10.584 349.668 10.593 349.494 10.590 349.569 10.600 349.594 10.681 349.519 10.597 349.569 10.622 349.519 10.612 349.569 10.609 349.544 10.628 349.544 10.638 349.594 10.631 349.544 10.631 349.544 10.628 349.569 10.638 349.494 10.650 349.494 10.660 349.544 10.650 349.743 10.657 349.544 10.641 349.445 10.669 349.494 10.688 349.395 10.685 349.445 10.691 349.619 10.679 349.370 10.698 349.420 10.688 349.469 10.707 349.469 10.694 349.395 10.720 349.445 10.723 349.420 10.723 349.445 10.735 349.370 10.732 349.518 10.735 349.469 10.745 349.345 10.732 349.469 10.748 349.420 10.751 349.345 10.761 349.320 10.764 349.494 10.767 349.395 10.754 349.345 10.770 349.469 10.773 349.295 10.792 349.370 10.805 349.370 10.789 349.395 10.802 349.370 10.795 349.345 10.805 349.370 10.808 349.295 10.824 349.221 10.833 349.345 10.818 349.320 10.821 349.295 10.827 349.469 10.827 349.270 10.824 349.320 10.830 349.295 10.843 349.295 10.849 349.345 10.852 349.295 10.859 349.295 10.859 349.221 10.865 349.295 10.881 349.295 10.874 349.270 10.871 849.295 10.893 349.246 10.890 349.270 10.884 349.370 10.887 349.270 10.909 349.246 10.900 349.246 10.915 349.221 10.912 349.246 10.928 349.146 10.912 349.196 10.944 349.221 10.941 349.221 10.931 349.121 10.941 348.972 10.944 349.146 10.938 349.171 10.956 349.022 10.956 349.198 10.969 349.146 10.975 349.196 10.982 349.072 10.979 349.171 10.979 349.121 10.975 349.096 11.007 349.096 10.997 349.047 11.004 348.922 10.994 349.096 11.013 349.072 11.023 349.047 11.023 349.146 11.029 349.121 11.026 348.972 11.026 349.096 11.039 349.096 11.035 349.022 11.051 349.047 11.067 349.096 11.054 349.047 11.045 349.121 11.051 349.096 11.067 349.221 11.067 349.022 11.073 348.997 11.083 349.146 11.089 349.022 11.089 349.047 11.105 348.972 11.105 348.997 11.095 348.972 11.105 348.997 11.102 348.897 11.111 348.922 11.121 349.121 11.130 348.997 11.127 348.947 11.136 348.897 11.149 348.922 11.133 348.897 11.136 348.922 11.158 348.922 11.165 348.972 11.155 348.897 11.165 348.947 11.171 348.947 11.174 348.897 11.187 348.873 11.177 348.873 11.187 348.848 11.196 348.848 11.196 348.947 11.196 348.947 11.190 348.848 11.190 348.897 11.212 348.823 11.222 348.823 11.222 348.773 11.218 348.773 11.231 348.823 11.234 348.699 11.222 348.848 11.241 348.723 11.234 348.798 11.250 348.748 11.244 348.773 11.256 348.699 11.247 348.748 11.275 348.699 11.247 348.674 11.272 348.748 11.263 348.674 11.275 348.649 11.275 348.699 11.291 348.699 11.301 348.649 11.301 348.674 11.319 348.624 11.313 348.549 11.323 348.599 11.332 348.649 11.319 348.574 11.332 348.674 11.345 348.624 11.351 348.574 11.342 348.549 11.348 348.624 11.342 348.475 11.357 348.574 11.357 348.549 11.351 348.475 11.367 348.450 11.370 348.524 11.370 348.524 11.389 348.425 11.383 348.850 11.383 348.549 11.386 348.524 11.402 348.500 11.395 348.500 11.411 348.425 11.417 348.476 11.411 348.326 11.424 348.425 11.427 348.375 11.424 348.400 11.430 346.375 11.430 348.276 11.443 348.301 11.452 348.350 11.443 348.375 11.461 348.400 11.461 348.375 11.458 348.326 11.443 348.326 11.461 348.276 11.471 348.599 11.477 348.226 11.480 348.176 11.461 348.326 11.487 348.350 11.493 348.251 11.490 348.251 11.506 348.276 11.503 348.251 11.515 348.201 11.525 348.201 11.521 348.251 11.537 348.226 11.537 348.251 11.534 348.251 11.550 348.151 11.559 348.077 11.559 348.201 11.547 348.127 11.563 348.201 11.566 348.151 11.575 348.027 11.585 348.176 11.575 348.301 11.578 348.027 11.591 348.226 11.591 348.251 11.591 348.102 11.586 348.102 11.600 348.276 11.600 348.002 11.600 348.127 11.616 348.251 11.619 348.077 11.638 348.052 11.629 348.102 11.632 348.052 11.635 348.027 11.645 348.052 11.641 348.151 11.645 348.952 11.660 349.977 11.635 349.952 11.638 348.052 11.648 347.928 11.667 347.778 11.676 347.952 11.682 347.878 11.676 347.903 11.698 348.027 11.689 347.903 11.705 347.803 11.714 347.853 11.708 347.754 11.701 347.803 11.711 348.002 11.720 347.803 11.714 347.729 11.733 347.754 11.727 347.679 11.739 347.803 11.742 347.853 11.752 347.754 11.752 347.679 11.755 347.729 11.755 347.754 11.746 347.729 11.768 347.754 11.771 347.803 11.787 347.729 11.783 347.729 11.796 347.654 11.802 347.754 11.787 347.654 11.806 347.604 11.796 347.654 11.806 347.604 11.799 347.555 11.809 347.580 11.818 347.604 11.809 347.480 11.831 347.530 11.831 347.530 11.834 347.530 11.828 347.505 11.834 347.405 11.847 347.480 11.850 347.430 11.862 347.281 11.853 347.455 11.866 347.356 11.872 347.580 11.884 347.381 11.881 347.430 11.875 347.405 11.891 347.356 11.903 347.331 11.900 347.281 11.916 347.306 11.907 347.306 11.910 347.356 11.922 347.306 11.938 347.256 11.926 347.281 11.938 347.281 11.941 347.331 11.951 347.082 11.951 347.206 11.944 347.157 11.951 347.206 11.960 347.157 11.970 347.306 11.967 347.032 11.973 347.107 11.982 347.008 11.967 347.132 11.982 347.057 11.989 346.983 12.001 347.032 12.008 347.231 12.001 347.008 12.008 347.057 12.011 346.958 12.008 346.933 12.014 346.958 12.030 346.908 12.030 346.883 12.030 346.958 12.055 346.933 12.036 346.908 12.049 346.858 12.049 346.858 12.055 346.855 12.061 346.833 12.061 346.833 12.068 346.858 12.074 346.784 12.080 346.833 12.083 346.759 12.090 346.784 12.090 346.734 12.105 346.684 12.099 346.709 12.102 346.659 12.115 346.684 12.105 346.585 12.112 346.709 12.115 346.634 12.128 346.709 12.137 346.560 12.131 346.610 12.137 346.610 12.150 346.585 12.165 346.535 12.162 346.535 12.162 346.485 12.169 346.610 12.162 346.485 12.175 346.485 12.175 346.411 12.172 346.436 12.203 346.510 12.188 346.411 12.203 346.411 12.191 346.411 12.206 346.386 12.213 346.361 12.203 346.336 12.219 346.261 12.210 346.811 12.229 346.311 13.225 346.286 12.229 346.187 12.235 346.237 12.241 346.187 12.266 346.237 12.251 346.187 12.257 346.237 12.266 345.963 12.254 346.187 12.285 346.187 12.279 346.013 12.276 346.087 12.282 346.112 12.292 346.038 12.285 346.038 12.295 346.063 12.298 346.087 12.317 346.038 12.328 346.087 12.320 345.988 12.307 345.963 12.314 345.789 12.326 345.864 12.333 345.888 12.330 345.864 12.345 345.888 12.355 345.739 12.348 345.864 12.348 345.714 12.346 345.814 12.377 345.689 12.374 345.789 12.361 345.764 12.377 345.739 12.402 345.689 12.380 345.764 12.380 345.640 12.399 345.665 12.396 345.840 12.402 345.665 12.412 345.565 12.434 345.640 12.415 345.590 12.421 345.590 12.434 345.540 12.427 345.515 12.427 345.565 12.434 345.416 12.453 345.441 12.440 345.866 12.456 345.316 12.446 345.366 12.459 345.391 12.459 345.292 12.487 345.292 12.468 345.316 12.472 345.292 12.487 345.292 12.481 345.267 12.484 345.267 12.500 345.217 12.509 345.316 12.503 345.118 12.503 345.316 12.525 345.167 12.522 345.068 12.503 345.093 12.535 345.118 12.538 345.043 12.528 345.068 12.544 345.167 12.547 344.944 12.547 344.993 12.541 344.968 12.560 344.919 12.560 344.919 12.557 344.944 12.579 344.944 12.582 344.894 12.588 344.919 12.585 344.769 12.598 344.720 12.601 344.794 12.598 344.769 12.607 344.745 12.607 344.695 12.607 344.720 12.617 344.769 12.617 344.819 12.636 344.870 12.626 344.670 12.614 344.471 12.629 344.670 12.645 344.645 12.648 344.595 12.658 344.745 12.639 344.570 12.674 344.670 12.661 344.496 12.658 344.471 12.670 344.372 12.677 344.446 12.680 344.421 12.686 344.471 12.702 344.222 12.693 344.496 12.702 344.297 12.705 344.222 12.715 344.272 12.711 344.222 12.730 344.372 12.724 344.197 12.715 344.173 12.740 344.222 12.740 344.148 12.749 344.123 12.740 344.098 12.743 344.098 12.753 343.974 12.756 344.048 12.771 344.048 12.762 344.023 12.781 343.974 12.775 343.949 12.797 344.222 12.797 343.949 12.790 343.849 12.797 343.924 12.800 343.824 12.809 343.750 12.803 343.824 12.813 343.924 12.822 343.775 12.813 343.725 12.822 343.700 12.822 343.675 12.838 343.650 12.844 343.601 12.847 343.402 12.841 343.526 12.847 343.601 12.854 343.526 12.847 343.526 12.872 343.501 12.869 343.675 12.876 343.461 12.879 343.402 12.882 343.402 12.891 343.352 12.895 343.402 12.888 343.252 12.920 343.203 12.920 343.277 12.914 343.252 12.936 343.228 12.923 343.058 12.914 343.178 12.936 343.078 12.942 343.103 12.926 343.103 12.951 343.252 12.945 343.153 12.939 343.078 12.964 342.929 12.958 343.053 12.973 342.979 12.970 342.954 12.989 342.904 12.983 342.904 12.977 342.856 12.977 342.830 12.992 342.780 12.992 342.780 12.999 342.780 13.021 342.755 13.018 342.755 13.018 342.656 13.018 342.656 13.033 342.631 13.024 342.656 13.046 342.506 13.046 342.606 13.040 342.457 13.052 342.506 13.062 342.482 13.059 342.258 13.059 342.382 13.071 342.283 13.084 342.233 13.084 342.332 13.084 342.307 13.093 342.258 13.084 342.208 13.093 342.208 13.109 342.208 13.106 342.233 13.106 342.233 13.119 342.168 13.125 342.109 13.122 342.034 13.134 342.009 13.144 342.059 13.131 342.009 13.134 341.934 13.147 341.984 13.153 342.059 13.138 341.835 13.150 341.810 13.172 341.860 13.172 341.835 13.169 841.760 13.188 341.736 13.179 341.860 13.198 341.686 13.198 341.711 13.207 341.785 13.210 341.661 13.207 341.537 13.204 341.561 13.226 341.487 13.229 341.462 13.229 341.512 13.226 341.487 13.239 342.363 13.220 341.437 13.245 341.363 13.242 341.313 (1) Strain (%) (2) Stress (MPa)

TABLE 7 tensile test: table 5: (1) (2) 13.248 341.338 13.258 341.363 13.258 341.213 13.261 341.064 13.239 341.213 13.270 341.139 13.283 341.089 13.289 341.114 13.299 341.164 13.280 341.039 13.286 341.014 13.292 340.965 13.302 340.989 13.318 340.940 13.324 340.840 13.343 340.940 13.333 340.592 13.327 340.815 13.321 340.766 13.349 340.716 13.340 340.641 13.355 340.641 13.352 340.691 13.355 340.592 13.362 340.641 13.371 340.567 13.374 340.592 13.368 340.417 13.378 340.467 13.368 340.442 13.390 340.417 13.393 340.442 13.396 340.343 13.422 340.243 13.403 340.318 13.409 340.268 13.422 340.268 13.409 340.094 13.434 340.318 13.428 340.020 13.409 340.169 13.438 340.094 13.441 340.020 13.453 340.069 13.472 339.895 13.466 339.945 13.463 339.870 13.472 339.920 13.482 339.920 13.472 339.870 13.482 339.721 13.486 339.821 13.488 339.771 13.497 339.721 13.504 339.597 13.497 339.472 13.510 339.622 13.526 339.622 13.523 339.572 13.523 339.497 13.539 339.472 13.548 339.522 13.532 339.398 13.557 339.249 13.551 339.348 13.554 339.249 13.551 339.274 13.554 339.274 13.561 339.398 13.580 339.174 13.580 339.174 13.589 339.124 13.592 339.050 13.605 339.075 13.595 338.950 13.595 338.925 13.614 338.901 13.598 338.876 13.614 338.925 13.617 338.876 13.636 338.826 13.633 338.776 13.633 338.727 13.649 338.727 13.658 338.727 13.646 338.627 13.652 338.627 13.662 338.776 13.640 338.577 13.668 338.478 13.677 338.428 13.677 338.453 13.668 338.353 13.696 338.378 13.693 338.378 13.677 338.254 13.699 338.279 13.699 338.229 13.718 338.229 13.722 338.179 13.731 338.105 13.722 338.055 13.731 338.030 13.744 338.055 13.734 338.030 13.737 337.956 13.744 337.906 13.756 337.956 13.763 337.906 13.769 337.831 13.769 337.806 13.776 337.806 13.772 337.757 13.782 337.682 13.778 337.657 13.801 337.583 13.778 337.508 13.801 337.458 13.804 337.483 13.807 337.408 13.801 337.384 13.813 337.284 13.823 337.359 13.829 337.309 13.810 337.284 13.823 337.234 13.838 337.259 13.848 337.135 13.854 337.160 13.857 337.135 13.845 337.011 13.860 337.060 13.857 336.986 13.870 336.986 13.883 336.911 13.873 336.936 13.876 336.687 13.883 336.886 13.898 336.812 13.895 336.712 13.905 336.712 13.902 336.638 13.914 336.687 13.914 336.488 13.914 336.538 13.908 336.513 13.911 336.538 13.920 336.588 13.946 336.314 13.949 336.389 13.943 336.289 13.933 336.339 13.949 336.240 13.958 336.215 13.955 336.165 13.977 336.090 13.977 336.066 13.984 336.090 13.971 336.041 13.980 335.966 13.990 335.892 13.999 335.892 14.006 335.867 14.006 335.892 14.025 335.817 14.015 335.767 14.018 335.742 14.025 335.717 14.031 335.593 14.034 335.568 14.050 335.419 14.047 335.469 14.047 335.469 14.056 335.469 14.072 335.394 14.078 335.320 14.063 335.344 14.081 335.245 14.075 335.270 14.094 335.121 14.094 335.146 14.097 335.146 14.104 335.046 14.113 335.046 14.110 334.947 14.113 334.971 14.110 334.872 14.132 334.872 14.135 334.797 14.129 334.748 14.138 334.797 14.145 334.648 14.148 334.648 14.167 334.598 14.157 334.598 14.164 334.549 14.160 334.574 14.173 334.499 14.179 334.399 14.179 334.399 14.189 334.375 14.186 334.350 14.201 334.275 14.205 334.151 14.211 334.375 14.223 334.101 14.208 334.126 14.217 334.200 14.217 334.101 14.230 334.002 14.236 333.927 14.246 333.902 14.239 333.852 14.239 333.753 14.246 333.678 14.265 333.703 14.252 333.653 14.268 333.803 14.277 333.554 14.280 333.529 14.274 333.529 14.290 333.454 14.302 333.430 14.296 333.355 14.302 333.305 14.321 333.380 14.315 333.231 14.312 333.057 14.315 333.156 14.328 333.081 14.328 332.982 14.324 332.932 14.334 332.957 14.350 332.883 14.362 332.957 14.347 332.858 14.353 332.833 14.359 332.708 14.356 332.609 14.369 332.684 14.372 332.609 14.388 332.733 14.397 332.634 14.388 332.360 14.388 332.485 14.400 332.410 14.407 332.311 14.413 332.360 14.426 332.261 14.419 332.261 14.429 332.236 14.444 332.136 14.432 332.261 14.435 332.087 14.441 332.062 14.457 332.037 14.460 331.888 14.460 331.863 14.467 331.838 14.476 331.788 14.467 331.714 14.489 331.739 14.489 331.614 14.476 331.639 14.492 331.540 14.492 331.515 14.511 331.415 14.508 331.415 14.504 331.316 14.527 331.341 14.523 331.191 14.527 331.191 14.533 331.142 14.533 331.042 14.536 331.092 14.555 330.993 14.542 330.968 14.571 330.993 14.571 330.918 14.571 330.794 14.568 330.744 14.577 330.669 14.583 330.619 14.590 330.619 14.596 330.695 14.596 330.545 14.609 330.520 14.599 330.396 14.602 330.396 14.618 330.246 14.605 330.296 14.624 330.296 14.612 330.122 14.637 330.197 14.637 330.122 14.659 330.072 14.643 330.023 14.659 329.948 14.656 329.898 14.659 329.824 14.656 329.898 14.681 329.824 14.694 329.774 14.688 329.675 14.678 329.724 14.678 329.600 14.700 329.600 14.691 329.575 14.713 329.426 14.716 329.426 14.732 329.351 14.729 329.326 14.713 329.326 14.741 329.127 14.738 329.202 14.732 329.152 14.741 329.127 14.751 329.028 14.757 329.028 14.754 328.904 14.763 328.929 14.770 328.854 14.776 328.829 14.779 328.730 14.798 328.605 14.796 328.630 14.798 328.580 14.798 328.555 14.792 328.481 14.811 328.456 14.804 328.431 14.826 328.357 14.823 328.307 14.826 328.207 14.830 328.232 14.836 328.183 14.848 328.083 14.848 328.183 14.852 327.785 14.855 328.008 14.874 327.934 14.864 327.659 14.871 327.785 14.880 327.809 14.880 327.710 14.899 327.511 14.896 327.685 14.912 327.511 14.921 327.561 14.902 327.486 14.927 327.436 14.924 327.287 14.924 327.287 14.918 327.213 14.934 327.138 14.946 327.138 14.946 327.113 14.953 327.063 14.943 326.964 14.956 326.889 14.962 326.939 14.962 326.815 14.978 326.815 14.965 326.765 14.981 326.566 14.991 326.616 14.981 326.566 15.009 326.591 15.003 326.442 15.009 326.342 15.003 326.392 15.019 326.342 15.022 326.392 15.019 326.218 15.038 326.193 15.035 326.218 15.041 326.094 15.032 326.044 15.051 325.969 15.047 325.919 15.060 325.795 15.073 325.820 15.063 325.696 15.066 325.721 15.079 325.621 15.082 325.646 15.088 325.571 15.092 325.447 15.095 325.497 15.101 325.422 15.098 325.372 15.120 325.298 15.123 325.273 15.117 325.273 15.136 325.099 15.133 325.124 15.136 325.049 15.152 324.950 15.155 324.900 15.158 324.850 15.155 324.726 15.161 324.701 15.170 324.726 15.167 324.651 15.186 324.577 15.186 324.477 15.180 324.676 15.193 324.427 15.199 324.228 15.211 324.253 15.196 324.204 15.211 324.328 15.215 324.303 15.211 324.104 15.230 323.980 15.234 323.930 15.227 323.880 15.237 323.831 15.246 323.781 15.263 323.706 15.249 323.706 15.275 323.532 15.281 323.507 15.275 323.532 15.287 323.458 15.281 323.482 15.297 323.234 15.306 323.333 15.303 323.109 15.313 323.234 15.313 323.109 15.322 323.109 15.313 323.035 15.325 322.985 15.331 322.886 15.335 322.960 15.350 322.761 15.357 322.712 15.357 322.662 15.360 322.637 15.357 322.488 15.369 322.513 15.366 322.488 15.376 322.413 15.379 322.388 15.382 322.289 15.391 322.239 15.385 322.140 15.391 322.040 15.407 322.040 15.414 321.966 15.417 321.891 15.426 321.866 15.426 321.791 15.429 321.742 15.429 321.617 15.429 321.617 15.439 321.443 15.448 321.493 15.445 321.394 15.458 321.344 15.458 321.319 15.464 321.145 15.483 321.145 15.480 321.244 15.489 321.095 15.483 320.971 15.492 320.971 15.496 320.896 15.518 320.822 15.524 320.822 15.518 320.797 15.518 320.623 15.527 320.573 15.530 320.473 15.530 320.399 15.549 320.498 15.552 320.349 15.552 320.299 15.568 320.200 15.552 320.175 15.559 320.125 15.568 320.100 15.565 320.076 15.581 319.926 15.584 319.901 15.590 319.827 15.587 319.752 15.609 319.727 15.600 319.653 15.616 319.553 15.612 319.504 15.625 319.379 15.622 319.379 15.628 319.305 15.644 319.330 15.657 319.255 15.653 319.131 15.644 319.081 15.653 319.006 15.644 318.981 15.669 318.932 15.669 318.882 15.676 318.758 15.676 318.683 15.685 318.782 15.704 318.608 15.704 318.459 15.720 318.434 15.717 318.360 15.707 318.285 15.720 318.285 15.729 318.235 15.723 318.161 15.739 318.061 15.729 318.036 15.764 317.962 15.761 317.937 15.754 317.788 15.751 317.763 15.764 317.738 15.767 317.713 15.764 317.614 15.761 317.464 15.789 317.464 15.783 317.365 15.795 317.315 15.805 317.265 15.808 317.265 15.814 317.066 15.802 317.066 15.818 316.942 15.818 316.917 15.843 316.917 15.836 316.569 15.843 316.793 15.855 316.669 15.843 316.569 15.855 316.544 15.855 316.494 15.865 316.395 15.874 316.420 15.893 316.320 15.881 316.246 15.890 316.196 15.893 316.072 15.890 315.997 15.915 316.022 15.912 315.823 15.909 315.848 15.934 315.773 15.919 315.674 15.934 315.574 15.941 315.525 15.934 315.500 15.947 315.475 15.944 315.326 15.953 315.301 15.956 315.201 15.953 315.226 15.988 315.102 15.953 315.077 15.988 315.002 15.982 314.803 15.985 314.803 15.994 314.754 16.007 314.605 16.023 314.605 16.013 314.530 16.016 314.455 16.035 314.455 16.026 314.331 16.042 314.256 16.029 314.182 16.051 314.157 16.054 314.157 16.042 313.983 16.064 313.908 16.064 313.858 16.051 313.759 16.073 313.660 16.067 313.684 16.105 313.535 16.089 313.436 16.111 313.461 16.098 313.386 16.105 313.287 16.105 313.262 16.121 313.113 16.114 313.013 16.124 312.988 16.136 312.889 16.140 312.914 16.146 312.764 16.152 312.690 16.168 312.690 16.168 312.541 16.165 312.491 16.171 312.491 16.177 312.317 16.177 312.217 16.171 312.167 16.190 312.143 16.196 312.093 16.196 311.969 16.228 311.944 16.209 311.819 16.218 311.770 16.228 311.670 16.222 311.695 16.228 311.571 16.231 311.546 16.253 311.397 16.241 311.347 16.253 311.247 16.263 311.098 16.256 311.048 16.266 310.924 16.285 310.949 16.278 310.899 16.285 310.800 16.288 310.775 16.288 310.651 16.304 310.551 16.323 310.601 16.319 310.526 16.332 310.427 16.326 310.327 16.332 310.253 16.329 310.178 16.335 310.079 16.345 310.103 16.351 309.905 16.357 309.855 16.364 309.805 16.357 309.706 16.360 309.631 16.392 309.581 16.386 309.507 16.367 309.357 16.386 309.382 16.395 309.407 16.405 309.059 16.408 309.109 16.411 309.034 16.411 308.885 16.427 308.810 16.430 308.960 16.427 308.686 16.433 308.512 16.446 308.487 16.461 308.487 16.455 308.412 16.449 308.213 16.480 308.238 16.484 308.164 16.474 308.039 16.477 307.890 16.487 307.841 16.487 307.791 16.496 307.716 16.506 307.641 16.499 307.741 16.509 307.467 16.521 307.393 16.534 307.418 16.534 307.244 16.534 307.119 16.544 307.070 16.528 306.970 16.544 306.896 16.550 306.821 16.559 306.672 16.559 306.647 16.591 306.697 16.578 306.647 16.588 306.348 16.594 306.324 16.597 306.249 16.597 306.100 16.600 306.075 16.619 305.876 16.619 305.901 16.613 305.727 16.632 305.702 16.619 305.553 16.626 305.428 16.657 305.379 16.654 305.329 16.660 305.304 16.657 305.180 16.667 305.030 16.682 304.956 16.673 304.881 16.679 304.732 16.698 304.483 16.701 304.483 16.689 304.458 16.708 304.384 16.701 304.235 16.720 304.185 16.733 304.036 16.733 304.011 16.736 303.886 16.727 303.837 16.736 303.762 16.742 303.563 16.755 303.538 16.761 303.464 16.768 303.290 16.771 303.240 16.765 303.116 16.787 302.991 16.771 302.867 16.783 302.842 16.802 302.693 16.812 302.494 16.809 302.369 16.824 302.345 16.809 302.345 16.821 302.146 16.828 302.270 16.843 301.773 16.828 301.748 16.843 301.624 16.862 301.474 16.859 301.425 16.856 301.201 16.862 301.076 16.878 300.977 16.881 300.803 16.891 300.679 16.894 300.430 16.900 300.330 16.894 300.181 16.907 300.057 16.922 299.883 16.913 299.758 16.938 299.535 16.935 299.336 16.932 299.211 16.944 298.963 16.951 298.739 16.973 298.465 16.970 298.142 16.970 297.993 16.973 297.694 16.982 297.495 17.011 297.172 17.001 296.749 17.004 296.078 17.020 287.200 (1) Strain (%) (2) Stress (MPa)

TABLE 8 compression test: table 1: (1) (2) 0.000 2.554 0.005 2.532 0.017 2.422 0.007 2.576 0.005 2.444 0.002 2.598 0.009 2.797 0.003 3.083 −0.001 3.645 0.010 3.721 0.003 4.228 0.009 4.470 0.011 4.428 0.010 4.756 0.020 4.800 0.008 4.778 0.009 4.800 0.013 4.778 0.008 4.844 0.010 4.999 0.014 5.065 0.019 4.955 0.014 4.712 0.013 4.811 0.020 4.999 0.010 5.043 0.015 5.087 0.015 5.065 0.026 5.131 0.026 5.043 0.015 5.175 0.019 5.197 0.017 5.175 0.016 5.131 0.012 5.307 0.022 5.263 0.015 5.197 0.020 5.439 0.024 5.439 0.017 5.483 0.026 5.505 0.024 5.505 0.022 5.615 0.025 5.615 0.034 5.659 0.019 5.703 0.029 5.747 0.028 5.747 0.035 5.879 0.025 5.791 0.024 5.879 0.028 5.990 0.029 6.012 0.031 6.034 0.025 6.144 0.021 6.144 0.015 6.210 0.028 6.188 0.024 6.364 0.033 6.386 0.029 6.320 0.024 6.606 0.031 6.716 0.032 6.936 0.028 6.804 0.028 7.201 0.036 7.289 0.029 7.421 0.029 7.619 0.023 7.761 0.024 7.861 0.016 7.993 0.014 8.214 0.013 8.412 0.005 8.544 0.011 8.654 0.011 8.874 0.019 8.984 0.024 9.188 0.010 9.293 0.014 9.469 0.012 9.601 0.017 9.689 0.014 9.931 0.008 10.085 0.007 10.217 0.008 10.460 0.007 10.614 0.008 10.702 −0.001 10.878 −0.004 11.054 0.000 11.186 −0.005 11.363 −0.004 11.517 −0.005 11.649 −0.009 11.781 −0.008 11.935 −0.005 12.177 −0.005 12.331 −0.005 12.464 −0.002 12.608 −0.005 12.816 −0.016 12.948 −0.008 13.146 −0.014 13.322 −0.016 13.454 −0.010 13.609 −0.013 13.785 −0.013 13.981 −0.019 14.159 −0.025 14.291 −0.015 14.401 −0.016 14.556 −0.019 14.820 −0.013 14.798 −0.021 15.106 −0.020 15.282 −0.016 15.348 −0.007 15.590 0.010 15.635 0.047 15.480 0.048 15.701 0.049 15.899 0.052 16.075 0.052 16.273 0.052 16.361 0.044 16.714 0.053 16.912 0.043 17.132 0.048 17.264 0.050 17.682 0.051 17.837 0.036 18.167 0.043 18.519 0.058 18.827 0.058 19.092 0.059 19.268 0.056 19.774 0.053 20.083 0.059 20.501 0.055 20.853 0.083 21.228 0.061 21.646 0.067 21.998 0.053 22.373 0.065 22.835 0.062 23.188 0.065 23.496 0.073 23.980 0.072 24.811 0.074 24.685 0.073 25.125 0.084 25.522 0.073 25.984 0.079 26.358 0.077 26.755 0.088 27.195 0.088 27.836 0.096 28.010 0.084 28.428 0.094 28.737 0.107 29.265 0.101 29.706 0.109 30.168 0.106 30.564 0.094 31.005 0.111 31.467 0.111 31.864 0.104 32.304 0.105 32.744 0.120 33.183 0.126 33.515 0.125 34.044 0.112 34.506 0.122 34.902 0.119 35.409 0.128 35.849 0.122 36.290 0.129 36.730 0.130 37.148 0.137 37.633 0.131 38.095 0.135 38.602 0.133 38.976 0.133 39.505 0.187 39.867 0.140 40.452 0.152 40.848 0.148 41.332 0.148 41.619 0.152 42.257 0.153 42.764 0.156 43.182 0.162 43.512 0.171 44.151 0.166 44.569 0.170 45.076 0.167 45.538 0.179 46.023 0.171 46.463 0.173 46.926 0.184 47.432 0.176 47.938 0.183 48.379 0.191 48.797 0.182 49.348 0.192 49.898 0.192 50.295 0.192 50.713 0.200 51.286 0.208 51.792 0.204 52.210 0.203 52.717 0.215 53.223 0.215 53.654 0.207 54.126 0.210 54.611 0.217 55.139 0.214 55.624 0.227 56.086 0.225 56.703 0.224 57.011 0.227 57.517 0.237 58.024 0.222 58.530 0.240 58.905 0.232 59.637 0.248 59.962 0.248 60.558 0.239 60.776 0.252 61.469 0.242 61.899 0.239 62.274 0.234 62.890 0.249 63.375 0.260 63.869 0.251 64.498 0.252 64.850 0.261 65.401 0.269 65.797 0.274 66.171 0.275 66.898 0.277 67.272 0.267 67.603 0.277 68.197 0.274 68.748 0.285 69.254 0.281 69.761 0.286 70.201 0.297 70.752 0.290 71.038 0.298 71.390 0.298 72.161 0.299 72.711 0.304 73.174 0.299 73.592 0.313 74.099 0.305 74.605 0.301 75.156 0.317 75.640 0.321 76.125 0.316 76.499 0.319 77.116 0.321 77.644 0.316 78.084 0.324 78.481 0.333 79.097 0.330 79.582 0.345 80.000 0.330 80.595 0.340 81.057 0.340 81.542 0.342 82.070 0.350 82.533 0.342 83.061 0.351 83.501 0.357 84.162 0.350 84.536 0.365 85.021 0.353 85.307 0.357 85.924 0.364 86.474 0.358 86.981 0.362 87.443 0.374 87.906 0.371 88.412 0.379 88.919 0.383 89.249 0.374 89.953 0.370 90.438 0.379 90.812 0.386 91.819 0.379 91.935 0.386 92.464 0.398 92.818 0.396 93.389 0.394 93.851 0.387 94.336 0.401 94.754 0.397 95.415 0.403 95.811 0.407 96.339 0.402 96.912 0.401 97.398 0.412 97.859 0.401 98.255 0.408 98.828 0.418 99.334 0.417 99.797 0.419 100.237 0.421 100.832 0.419 101.316 0.427 101.778 0.435 102.285 0.434 102.659 0.441 103.210 0.441 103.782 0.442 104.289 0.434 104.817 0.438 105.258 0.443 105.764 0.433 106.337 0.450 106.689 0.446 107.195 0.464 107.768 0.457 108.252 0.462 108.759 0.464 109.243 0.466 109.794 0.474 110.234 0.474 110.719 0.467 111.225 0.476 111.864 0.479 112.260 0.478 112.590 0.471 113.273 0.483 113.736 0.480 114.176 0.490 114.704 0.488 115.189 0.488 115.673 0.492 116.224 0.494 116.730 0.496 117.193 0.503 117.743 0.497 118.074 0.511 118.778 0.514 119.087 0.506 119.483 0.500 120.166 0.500 120.716 0.512 121.024 0.519 121.663 0.512 122.213 0.514 122.632 0.516 123.072 0.521 123.645 0.527 124.129 0.529 124.636 0.526 125.120 0.527 125.693 0.529 126.133 0.539 126.640 0.534 127.124 0.546 127.830 0.546 128.093 0.554 128.577 0.547 129.040 0.552 129.546 0.564 130.053 0.552 130.537 0.546 130.978 0.558 131.506 0.560 131.968 0.567 132.453 0.566 132.981 0.564 133.510 0.571 133.950 0.566 134.479 0.569 134.963 0.574 135.316 0.584 135.932 0.577 136.395 0.571 136.769 0.588 137.386 0.588 137.914 0.593 138.376 0.600 138.839 0.590 139.345 0.598 139.918 0.592 140.336 0.600 140.645 0.606 141.459 0.593 141.812 0.611 142.252 0.605 142.692 0.606 143.265 0.610 143.727 0.607 144.300 0.611 144.718 0.614 145.203 0.607 145.665 0.613 146.128 0.619 146.656 0.625 147.273 0.624 147.471 0.622 148.021 0.630 148.594 0.636 148.990 0.624 149.541 0.639 150.003 0.649 150.488 0.638 150.906 0.648 151.369 0.641 151.919 0.653 152.426 0.644 152.888 0.652 153.328 0.655 153.857 0.648 154.231 0.659 154.826 0.659 155.112 0.657 155.729 0.666 156.169 0.672 156.631 0.663 157.160 0.666 157.600 0.676 158.085 0.668 158.591 0.661 159.032 0.681 159.494 0.683 159.868 0.681 160.507 0.687 160.947 0.683 161.366 0.695 161.850 0.689 162.489 0.698 162.753 0.688 163.304 0.696 163.766 0.702 164.272 0.699 164.713 0.697 165.043 0.702 165.638 0.699 166.276 0.707 166.563 0.708 167.025 0.712 167.531 0.716 167.906 0.724 168.456 0.713 168.941 0.715 169.381 0.717 169.844 0.721 170.218 0.722 170.747 0.714 171.187 0.720 171.627 0.734 172.156 0.729 172.640 0.728 173.015 0.733 173.521 0.735 173.983 0.739 174.490 0.738 174.908 0.738 175.459 0.736 175.877 0.743 176.296 0.749 176.648 0.744 177.220 0.756 177.683 0.753 178.189 0.762 178.564 0.763 179.092 0.771 179.633 0.764 179.797 0.753 180.612 0.765 181.052 0.774 181.470 0.777 181.735 0.773 182.329 0.772 182.748 0.780 183.210 0.773 183.606 0.786 184.157 0.781 184.509 0.782 184.906 0.792 185.478 0.791 185.897 0.787 186.227 0.788 186.755 0.804 187.806 0.798 187.702 0.806 188.077 0.799 188.671 0.800 189.111 0.807 189.508 0.806 189.948 0.811 190.499 0.823 190.785 0.822 191.336 0.818 191.776 0.821 192.216 0.819 192.679 0.821 193.075 0.822 193.560 0.825 194.022 0.836 194.441 0.828 194.925 0.829 195.343 0.827 195.718 0.842 196.224 0.831 196.709 0.842 197.171 0.850 197.567 0.841 198.008 0.846 198.514 0.845 199.109 0.853 199.263 0.849 199.835 0.847 200.298 0.850 200.606 0.858 201.003 0.858 201.597 0.854 202.038 0.862 202.368 0.865 202.896 0.867 203.381 0.871 203.799 0.865 204.240 0.869 204.658 0.871 205.098 0.876 205.407 0.880 205.979 0.880 206.398 0.880 206.838 0.901 207.256 0.890 207.807 0.913 208.225 0.886 208.600 0.902 208.974 0.906 209.480 0.896 209.899 0.896 210.229 0.900 210.758 0.904 211.220 0.913 211.638 0.914 212.035 0.909 212.497 0.909 213.048 0.914 213.378 0.927 213.664 0.910 214.281 0.926 214.743 0.930 215.140 0.928 215.558 0.931 215.976 0.928 216.329 0.926 216.879 0.921 217.254 0.939 217.738 0.940 218.002 0.932 218.443 0.945 218.993 0.941 219.412 0.942 219.764 0.945 220.270 0.946 220.689 0.952 221.063 0.953 221.504 0.950 221.944 0.958 222.428 0.958 222.803 0.962 223.243 0.964 223.640 0.967 223.926 0.972 224.388 0.974 224.873 0.973 225.357 0.964 225.665 0.977 226.128 0.977 226.546 0.980 226.899 0.985 227.383 0.985 227.779 0.986 228.198 0.986 228.638 0.985 228.991 0.999 229.431 1.001 229.871 1.002 230.246 1.004 230.708 1.008 231.126 1.000 231.479 1.015 231.853 1.013 232.316 1.010 232.690 1.019 233.042 1.024 233.461 1.021 233.923 1.021 234.253 1.021 234.628 1.025 236.046 1.027 236.421 1.024 236.707 1.027 236.169 1.019 236.543 1.029 236.918 1.034 237.314 1.045 237.733 1.031 238.107 1.036 238.393 1.039 238.745 1.046 239.208 1.059 239.604 1.053 239.935 1.054 240.265 1.053 240.617 1.055 240.926 1.064 241.322 1.064 241.740 1.078 242.027 1.073 242.423 1.076 242.731 1.079 243.062 1.076 243.392 1.079 243.744 1.095 244.063 1.094 244.405 1.089 244.581 1.099 244.999 1.089 245.352 1.097 245.660 1.101 245.968 1.108 246.122 1.115 246.629 1.106 246.805 1.111 247.135 1.109 247.444 1.112 247.774 1.108 247.994 1.122 248.170 1.124 248.567 1.124 248.875 1.134 249.117 1.126 249.381 1.133 249.624 1.138 249.756 1.146 250.064 1.146 250.372 1.151 250.615 1.148 250.769 1.153 251.011 1.162 251.275 1.170 251.451 1.178 251.672 1.170 251.848 1.177 252.046 1.175 252.134 1.183 252.200 1.192 252.508 1.189 252.640 1.205 252.751 1.202 252.861 1.204 252.971 1.210 253.037 1.215 253.081 1.221 253.103 1.235 253.125 1.223 253.015 1.235 253.059 1.246 252.917 1.239 252.839 1.252 252.663 1.265 252.464 1.263 252.200 1.265 251.914 1.274 251.473 1.281 251.275 1.290 250.813 1.298 250.571 1.299 250.372 1.310 250.086 1.323 249.734 1.326 249.403 1.335 249.403 1.334 249.205 1.335 249.051 1.350 248.765 1.361 248.567 1.365 248.236 1.362 247.884 1.380 247.994 1.387 247.730 1.391 247.576 1.389 247.312 1.421 247.245 1.415 246.893 1.416 246.827 1.425 246.739 1.431 246.607 1.438 246.453 1.448 246.343 1.443 246.255 1.461 246.188 1.460 246.122 1.472 246.946 1.458 245.946 1.479 245.770 1.477 245.682 1.484 245.682 1.500 245.694 1.506 245.440 1.519 245.484 1.518 245.484 1.528 245.418 1.519 245.286 1.524 245.242 1.535 245.264 1.529 245.021 1.544 245.021 1.553 245.043 1.555 245.043 1.559 244.977 1.566 244.801 1.569 244.889 1.573 244.823 1.581 244.537 1.586 244.823 1.591 244.691 1.597 244.691 1.593 244.405 1.613 244.559 1.607 244.537 1.618 244.405 1.622 244.471 1.631 244.427 1.636 244.295 1.643 244.251 1.638 244.361 1.651 244.295 1.675 244.229 1.663 244.141 1.674 244.207 1.668 244.163 1.668 244.118 1.689 244.141 1.688 244.118 1.696 244.008 1.704 243.964 1.706 244.030 1.711 243.986 1.722 243.942 1.723 244.008 1.729 243.964 1.734 243.942 1.736 243.810 1.736 243.920 1.746 243.920 1.765 243.854 1.761 243.920 1.758 243.876 1.767 243.788 1.765 243.744 1.781 243.832 1.784 243.898 1.793 243.788 1.803 243.744 1.795 243.810 1.813 243.832 1.811 243.678 1.822 243.788 1.818 243.854 1.831 243.722 1.829 243.788 1.843 243.810 1.839 248.788 1.845 243.766 1.849 243.722 1.849 243.788 1.860 243.744 1.878 243.634 1.870 243.744 1.877 243.766 1.879 243.766 1.886 243.766 1.889 243.788 1.899 243.810 1.906 243.788 1.915 243.788 1.915 243.810 1.925 243.744 1.917 243.766 1.923 243.854 1.938 243.832 1.929 243.832 1.941 243.876 1.946 243.898 1.955 243.788 1.962 243.700 1.967 243.854 1.971 243.920 1.969 243.700 1.977 244.008 1.980 243.920 1.990 243.920 1.986 243.912 1.996 244.008 2.003 243.986 2.015 243.898 2.015 243.942 2.015 244.053 2.032 244.030 2.028 244.030 2.035 243.964 2.042 244.141 2.049 244.030 2.048 244.008 2.054 244.141 2.053 244.168 2.075 244.163 2.067 244.185 2.078 244.229 2.091 244.229 2.089 244.096 2.097 244.273 2.095 244.295 2.099 244.207 2.109 244.229 2.115 244.383 2.109 244.339 2.120 244.339 2.119 244.339 2.127 244.449 2.128 244.405 2.133 244.295 2.140 244.471 2.153 244.515 2.143 244.515 2.168 244.493 2.162 244.515 2.171 244.581 2.172 244.603 2.179 244.691 2.180 244.669 2.185 244.713 2.193 244.603 2.195 244.757 2.203 244.801 2.210 244.801 2.209 244.801 2.220 244.823 2.216 244.779 2.235 244.757 2.230 244.911 2.233 244.955 2.243 244.977 2.254 244.669 2.251 244.977 2.263 245.043 2.268 245.043 2.265 245.131 2.267 245.176 2.283 245.176 2.289 245.176 2.281 245.220 2.292 245.264 2.290 245.242 2.290 245.264 2.301 245.352 2.306 245.286 2.312 245.374 2.319 245.418 2.325 245.462 2.332 245.462 2.337 245.462 2.340 245.528 2.348 245.572 2.354 245.572 2.356 245.638 2.355 245.682 2.360 245.704 2.368 245.726 2.369 245.792 2.378 245.792 2.388 245.770 2.394 245.726 2.392 245.858 2.396 245.814 2.394 245.880 2.408 245.946 2.418 246.012 2.411 246.012 2.418 245.946 2.417 246.100 2.428 246.034 2.432 246.034 2.438 246.188 2.446 246.232 2.453 246.232 2.460 246.188 (1) Strain (%) (2) Stress (MPa)

TABLE 9 compression test: table 2: (1) (2) 2.453 246.343 2.462 246.387 2.468 246.366 2.476 246.409 2.481 246.453 2.485 246.453 2.498 246.475 2.501 246.685 2.503 246.629 2.503 246.607 2.508 246.629 2.511 246.651 2.522 246.695 2.530 246.695 2.533 246.805 2.541 246.805 2.536 246.805 2.539 246.893 2.551 246.981 2.548 246.959 2.559 247.003 2.571 247.003 2.572 247.047 2.568 247.091 2.577 247.069 2.581 247.201 2.583 247.245 2.591 247.201 2.594 247.312 2.605 247.334 2.609 247.157 2.609 247.334 2.618 247.466 2.620 247.554 2.641 247.488 2.632 247.576 2.644 247.620 2.635 247.708 2.651 247.796 2.643 247.730 2.643 247.840 2.655 247.774 2.668 247.708 2.669 247.796 2.679 247.972 2.672 247.862 2.678 247.972 2.694 248.104 2.705 248.038 2.702 248.170 2.702 248.236 2.711 248.192 2.717 248.236 2.720 248.214 2.718 248.347 2.728 248.369 2.736 248.434 2.746 248.434 2.744 248.501 2.741 248.567 2.754 248.567 2.758 248.611 2.765 248.699 2.773 248.699 2.779 248.743 2.774 248.787 2.775 248.831 2.777 248.809 2.796 248.941 2.799 248.985 2.804 249.051 2.803 249.073 2.808 249.117 2.814 249.117 2.810 249.051 2.823 249.205 2.827 249.249 2.837 249.271 2.847 249.117 2.839 249.403 2.858 249.447 2.859 249.492 2.862 249.359 2.855 249.602 2.868 249.426 2.878 249.646 2.871 249.712 2.880 249.778 2.880 249.846 2.886 249.822 2.897 249.866 2.901 249.910 2.900 249.976 2.917 249.932 2.913 250.064 2.915 250.152 2.927 250.108 2.930 250.218 2.929 250.262 2.934 250.196 2.945 250.306 2.942 250.372 2.954 250.372 2.948 250.262 2.960 250.504 2.965 250.549 2.970 250.593 2.970 250.548 2.977 250.725 2.979 250.747 2.993 250.769 3.001 250.813 3.003 250.835 3.008 250.791 3.004 250.791 3.012 251.099 3.018 251.011 3.025 251.077 3.032 250.945 3.041 251.209 3.031 250.967 3.061 251.297 3.042 251.363 3.045 251.473 3.062 251.319 3.067 251.495 3.061 251.539 3.072 251.583 3.077 251.605 3.085 251.694 3.082 251.694 3.089 251.672 3.091 251.738 3.110 251.892 3.109 251.936 3.105 251.782 3.108 251.914 3.117 252.046 3.126 252.046 3.127 252.134 3.127 252.244 3.133 252.266 3.149 252.266 3.139 252.310 3.157 252.376 3.165 252.420 3.158 252.464 3.159 252.442 3.165 252.552 3.168 252.552 3.176 252.530 3.188 252.773 3.185 252.795 3.186 252.839 3.193 252.773 3.201 252.949 3.213 252.971 3.201 252.993 3.213 253.037 3.223 253.125 3.226 253.147 3.230 253.169 3.231 253.257 3.244 253.301 3.239 253.301 3.253 253.257 3.253 253.433 3.254 253.345 3.260 253.279 3.255 253.631 3.267 253.653 3.271 253.653 3.282 253.587 3.285 253.742 3.291 253.852 3.287 253.719 3.299 253.940 3.301 254.006 3.311 253.918 3.311 253.785 3.317 254.138 3.323 254.204 3.328 254.336 3.325 254.138 3.329 254.336 3.341 254.358 3.349 254.402 3.350 254.468 3.354 254.556 3.369 254.446 3.367 254.600 3.362 254.644 3.371 254.578 3.378 254.600 3.381 254.798 3.382 254.842 3.386 254.798 3.395 254.842 3.401 254.997 3.403 255.019 3.414 255.085 3.405 255.129 3.413 255.151 3.414 255.195 3.429 255.151 3.431 255.371 3.436 255.371 3.430 255.371 3.446 255.469 3.450 255.525 3.450 255.613 3.464 255.569 3.462 255.679 3.474 255.723 3.477 255.767 3.482 255.679 3.483 255.877 3.496 255.944 3.494 256.010 3.498 256.010 3.498 256.032 3.507 256.098 3.513 255.966 3.506 256.230 3.526 256.252 3.521 256.296 3.533 256.296 3.540 256.406 3.545 256.406 3.554 256.494 3.549 256.582 3.550 256.604 3.566 256.626 3.562 256.692 3.574 256.736 3.574 256.758 3.572 256.802 3.569 256.802 3.587 256.912 3.587 256.979 3.593 257.133 3.605 257.067 3.603 257.111 3.604 257.067 3.612 257.221 3.625 257.243 3.622 257.309 3.630 257.287 3.627 257.397 3.642 257.463 3.646 257.463 3.648 257.485 3.643 257.573 3.652 257.595 3.661 257.595 3.671 257.639 3.669 257.771 3.675 257.727 3.682 257.573 3.693 257.903 3.701 257.859 3.697 257.947 3.695 257.925 3.706 258.013 3.714 258.080 3.713 258.123 3.719 258.168 3.714 258.234 3.723 258.080 3.738 258.190 3.737 258.344 3.735 258.366 3.748 258.344 3.745 258.454 3.752 258.498 3.773 258.476 3.785 258.542 3.770 258.608 3.781 258.652 3.782 258.630 3.793 258.564 3.793 258.762 3.792 258.784 3.798 258.850 3.802 258.872 3.804 258.916 3.808 258.916 3.823 258.938 3.818 258.982 3.822 259.070 3.832 259.070 3.840 259.158 3.833 259.203 3.841 259.247 3.856 259.247 3.850 259.291 3.861 259.313 3.860 259.335 3.863 259.357 3.872 259.467 3.885 259.611 3.889 259.467 3.884 259.611 3.893 259.665 3.900 259.533 3.906 259.665 3.900 259.709 3.904 259.775 3.913 259.797 3.921 259.819 3.931 259.907 3.932 259.775 3.943 259.819 3.940 260.017 3.949 260.039 3.949 259.973 3.957 259.995 3.957 260.149 3.973 260.105 3.971 260.171 3.972 260.215 3.980 260.304 3.993 260.238 3.984 260.348 3.997 260.392 4.006 260.436 4.001 260.392 4.018 260.480 4.011 260.590 4.018 260.546 4.015 260.568 4.028 260.678 4.028 260.656 4.045 260.744 4.040 260.612 4.050 260.854 4.052 260.832 4.054 260.920 4.054 260.942 4.073 260.964 4.065 260.898 4.082 260.986 4.078 261.162 4.078 261.250 4.082 261.228 4.094 261.272 4.091 261.361 4.111 261.339 4.110 261.140 4.123 261.427 4.125 261.515 4.129 261.537 4.129 261.427 4.129 261.647 4.140 261.713 4.137 261.691 4.144 261.823 4.161 261.845 4.158 261.889 4.162 261.955 4.166 262.021 4.165 262.021 4.177 262.131 4.173 262.131 4.178 262.307 4.189 262.219 4.195 262.307 4.202 262.417 4.203 262.417 4.214 262.462 4.206 262.506 4.220 262.594 4.225 262.572 4.214 262.882 4.227 262.770 4.234 262.792 4.235 262.880 4.250 262.924 4.252 262.990 4.252 263.034 4.264 263.078 4.274 263.078 4.267 263.210 4.263 263.232 4.276 263.254 4.283 263.364 4.287 263.431 4.286 263.474 4.293 263.364 4.302 263.607 4.306 263.661 4.315 263.685 4.310 263.761 4.331 263.805 4.331 263.783 4.325 263.915 4.329 263.981 4.345 264.069 4.332 264.113 4.340 264.069 4.346 264.223 4.349 264.179 4.363 264.179 4.371 264.377 4.373 264.443 4.373 264.531 4.367 264.554 4.385 264.620 4.390 264.708 4.397 264.796 4.392 264.774 4.405 264.862 4.414 264.950 4.417 264.972 4.421 265.060 4.428 265.126 4.429 265.170 4.421 265.258 4.435 265.324 4.439 265.368 4.443 265.302 4.442 265.478 4.451 265.666 4.454 265.610 4.450 265.588 4.460 265.721 4.466 265.765 4.484 265.766 4.481 265.919 4.493 266.029 4.510 266.061 4.502 266.117 4.498 266.205 4.493 266.271 4.502 266.293 4.623 266.337 4.515 266.425 4.518 266.403 4.527 266.359 4.537 266.645 4.537 266.712 4.545 266.733 4.557 266.712 4.557 266.954 4.557 266.932 4.570 266.998 4.570 267.042 4.574 267.108 4.587 267.152 4.583 267.262 4.597 267.328 4.592 267.416 4.583 267.482 4.598 267.438 4.608 267.592 4.608 267.614 4.621 267.592 4.609 267.790 4.616 267.812 4.623 267.901 4.619 267.857 4.631 268.033 4.644 268.143 4.642 268.077 4.650 268.231 4.642 268.275 4.660 268.363 4.666 268.319 4.669 268.473 4.664 268.561 4.673 268.671 4.673 268.605 4.691 268.892 4.686 268.781 4.688 268.759 4.697 268.980 4.708 269.090 4.703 269.024 4.716 269.090 4.714 269.200 4.713 269.310 4.720 269.332 4.733 269.398 4.742 269.464 4.735 269.630 4.743 269.574 4.755 269.684 4.741 269.794 4.754 269.750 4.764 269.904 4.769 269.949 4.777 269.993 4.785 270.037 4.787 270.147 4.783 270.169 4.791 270.191 4.798 270.301 4.794 270.433 4.804 270.477 4.812 270.521 4.813 270.675 4.822 270.697 4.840 270.763 4.825 270.829 4.828 270.895 4.829 271.006 4.825 271.116 4.839 271.094 4.851 271.182 4.849 271.204 4.863 271.204 4.860 271.424 4.864 271.578 4.869 271.468 4.863 271.490 4.878 271.666 4.880 271.710 4.887 271.798 4.900 271.864 4.898 271.974 4.904 271.996 4.906 272.106 4.903 272.151 4.918 272.239 4.920 272.217 4.927 272.349 4.937 272.469 4.932 272.525 4.945 272.613 4.935 272.679 4.944 272.723 4.950 272.701 4.958 272.767 4.970 272.943 4.968 273.031 4.983 273.053 4.983 273.141 4.984 273.252 4.988 273.296 4.992 273.362 5.000 273.450 5.005 273.538 5.011 273.692 5.004 273.538 5.016 273.736 5.014 273.692 5.032 273.824 5.028 273.956 5.034 273.978 5.040 274.110 5.039 274.110 5.053 274.220 5.050 274.287 5.056 274.309 5.054 274.463 5.064 274.595 5.076 274.529 5.081 274.573 5.082 274.793 5.083 274.837 5.085 274.881 5.080 274.991 5.101 275.079 5.101 275.101 5.105 275.167 5.117 275.255 5.124 275.366 5.120 275.410 5.120 275.410 5.126 275.586 5.138 275.652 5.136 275.696 5.149 275.850 5.156 275.938 5.156 275.938 5.164 275.982 5.164 276.114 5.161 276.180 5.174 276.224 5.184 276.246 5.190 276.511 5.186 276.489 5.188 276.511 5.196 276.643 5.193 276.797 5.197 276.797 5.205 276.885 5.216 276.973 5.211 277.017 5.219 277.149 5.225 277.193 5.232 277.325 5.233 277.303 5.242 277.347 5.254 277.546 5.247 277.546 5.262 277.656 5.254 277.722 5.261 277.854 5.270 277.898 5.264 277.898 5.266 278.074 5.282 278.140 5.281 278.140 5.287 278.316 5.289 278.360 5.290 278.448 5.308 278.514 5.299 278.581 5.299 278.691 5.305 278.735 5.309 278.845 5.322 279.021 5.328 279.021 5.324 279.065 5.330 279.109 5.335 279.307 5.341 279.329 5.348 279.285 5.361 279.527 5.368 279.571 5.362 279.527 5.370 279.571 5.372 279.792 5.369 279.902 5.386 279.968 5.384 280.078 5.389 280.166 5.396 280.144 5.406 280.276 5.406 280.364 5.413 280.496 5.410 280.474 5.418 280.518 5.417 280.738 5.425 280.761 5.425 280.871 5.438 280.981 5.438 281.069 5.447 281.135 5.453 281.201 5.453 281.311 5.462 281.377 5.451 281.443 5.468 281.553 5.468 281.663 5.469 281.663 5.476 281.730 5.475 281.906 5.487 281.928 5.498 282.016 5.509 282.082 5.507 282.236 5.511 282.258 5.517 282.324 5.517 282.478 5.534 282.676 5.526 282.610 5.533 282.698 5.535 282.808 5.542 282.852 5.554 282.941 5.549 283.073 5.550 283.117 5.565 283.227 5.569 283.271 5.573 283.403 5.583 283.491 5.585 283.579 5.589 283.645 5.585 283.755 5.579 283.777 5.589 283.799 5.583 284.042 5.596 284.108 5.597 284.174 5.603 284.240 5.606 284.372 5.613 284.438 5.621 284.526 5.620 284.614 5.628 284.680 5.626 284.724 5.635 284.866 5.651 284.944 5.644 285.033 5.656 285.121 5.658 285.187 5.655 285.319 5.661 285.385 5.676 285.429 5.672 285.561 5.687 285.671 5.680 285.781 5.684 285.803 5.698 285.957 5.693 286.023 5.700 286.068 5.712 286.178 5.710 286.288 5.717 286.310 5.712 286.398 5.715 286.552 5.721 286.618 5.740 286.772 5.735 286.728 5.742 286.882 5.741 286.948 5.765 286.882 5.758 287.213 5.765 287.257 5.759 287.367 5.769 287.477 5.769 287.543 5.777 287.609 5.788 287.609 5.790 287.829 5.794 287.961 5.788 287.983 5.796 288.049 5.806 288.203 5.803 288.292 5.811 288.380 5.825 288.446 5.828 288.534 5.833 288.644 5.829 288.666 5.828 288.798 5.838 289.084 5.847 289.040 5.852 289.062 5.851 289.194 5.852 289.282 5.861 289.392 5.861 289.603 5.868 289.591 5.885 289.569 5.885 289.789 5.889 289.877 5.893 289.943 5.901 290.009 5.893 290.031 5.895 290.273 5.910 290.295 5.913 290.384 5.919 290.538 5.921 290.582 5.924 290.648 5.933 290.780 5.936 290.890 5.953 290.978 5.948 291.022 5.952 291.196 5.945 291.286 5.960 291.330 5.963 291.529 5.968 291.551 5.971 291.661 5.977 291.771 5.975 291.771 5.983 291.925 5.986 292.035 5.989 292.057 5.989 292.233 5.996 292.365 6.014 292.409 6.009 292.563 6.008 292.696 6.021 292.740 6.031 292.828 6.023 292.960 6.041 293.070 6.022 293.048 6.037 293.202 6.045 293.356 6.053 293.378 6.054 293.532 6.066 293.576 6.065 293.753 6.077 293.797 6.065 293.885 6.080 283.995 6.076 294.105 6.083 294.083 6.089 294.237 6.078 294.369 6.094 294.589 6.112 294.567 6.110 294.700 6.112 294.832 6.114 294.722 6.120 294.920 6.117 295.118 6.129 295.228 6.141 295.272 6.137 295.294 6.138 295.514 6.137 295.492 6.142 295.668 6.150 295.823 6.159 295.911 6.166 295.999 6.166 296.043 6.168 296.219 6.175 296.197 6.186 296.395 6.178 296.527 6.190 296.615 6.186 296.725 6.194 296.813 6.190 296.946 6.201 297.056 6.207 297.210 6.219 297.254 6.219 297.298 6.218 297.430 6.225 297.518 6.229 297.672 6.234 297.716 6.237 297.914 6.240 297.870 6.247 298.091 6.247 298.135 6.268 298.267 6.265 298.377 6.259 298.509 6.277 298.597 6.282 298.686 6.269 298.729 6.289 298.905 6.288 298.994 6.285 299.038 6.299 299.214 6.301 299.324 6.297 299.368 6.306 299.544 6.311 299.632 6.307 299.698 6.326 299.742 6.322 299.984 6.328 300.028 6.335 300.161 6.343 300.315 6.347 300.425 6.348 300.381 6.348 300.557 6.357 300.733 6.370 300.843 6.372 301.108 6.373 300.975 6.370 301.196 6.375 301.240 6.376 301.394 6.387 301.482 6.390 301.614 6.394 301.702 6.400 301.790 6.396 301.922 6.398 302.076 6.416 302.120 6.411 302.230 6.408 302.341 6.424 302.473 6.432 302.605 6.436 302.693 6.431 302.825 6.443 302.913 6.453 303.001 6.447 303.155 6.460 303.221 6.465 303.376 6.467 303.508 6.467 303.574 6.463 303.750 6.468 303.706 6.477 303.970 6.475 304.058 6.493 304.168 6.489 304.300 6.500 304.869 6.510 304.477 6.510 304.609 6.500 304.741 6.510 304.829 6.515 304.873 6.514 305.093 6.527 305.225 6.530 305.203 6.532 305.357 6.537 305.534 6.538 305.644 6.548 305.732 6.558 305.798 6.557 305.996 6.555 305.974 6.577 306.238 6.567 306.348 6.564 306.458 6.573 306.436 6.579 306.546 (1) Strain (%) (2) Stress (MPa)

TABLE 10-1 compression test: table 3; (1) (2) 6.584 306.811 6.583 306.943 6.591 307.075 6.603 307.075 6.598 307.251 6.596 307.361 6.609 307.493 6.610 307.670 6.617 307.714 6.620 307.824 6.636 307.978 6.628 308.154 6.636 308.220 6.636 308.352 6.645 308.462 6.647 308.572 6.651 308.705 6.668 308.748 6.668 308.947 6.668 309.079 6.670 309.189 6.688 309.277 6.677 309.475 6.684 309.475 6.685 309.673 6.695 309.762 6.689 309.938 6.700 309.982 6.699 310.136 6.714 310.290 6.703 310.356 6.718 310.488 6.729 310.642 6.728 310.774 6.725 310.862 6.731 311.017 6.730 311.127 6.737 311.259 6.743 311.479 6.748 311.501 6.748 311.655 6.756 311.721 6.759 311.853 6.771 312.030 6.778 312.140 6.771 312.228 6.777 312.184 6.785 312.492 6.789 312.624 6.785 312.778 6.798 312.888 6.802 313.021 6.803 313.043 6.805 313.175 6.813 313.417 6.821 313.505 6.820 313.615 6.820 313.747 6.832 313.945 6.818 313.835 6.836 313.989 6.838 314.276 6.844 314.430 6.837 314.562 6.849 314.628 6.848 314.826 6.863 314.914 6.865 315.068 6.876 315.201 6.881 315.355 6.868 315.443 6.876 315.597 6.880 315.773 6.899 315.795 6.895 315.927 6.893 316.081 6.904 316.257 6.915 316.346 6.911 316.412 6.911 316.676 6.917 316.742 6.918 316.874 6.923 317.006 6.939 317.160 6.937 317.270 6.936 317.469 6.937 317.623 6.945 317.733 6.948 317.799 6.949 317.799 6.960 318.085 6.963 318.261 6.969 318.437 6.982 318.648 6.978 318.658 6.995 318.768 6.976 318.966 6.988 319.098 6.996 319.186 7.001 319.296 7.000 319.517 7.002 319.627 7.011 319.737 7.014 319.869 7.019 320.001 7.018 320.177 7.033 320.265 7.025 320.441 7.042 320.618 7.039 320.684 7.036 320.860 7.048 320.948 7.051 321.168 7.060 321.234 7.054 321.432 7.059 321.586 7.060 321.719 7.063 321.939 7.070 321.939 7.081 322.137 7.090 322.269 7.084 322.401 7.092 322.533 7.100 322.688 7.103 322.820 7.118 322.952 7.105 323.150 7.116 323.282 7.117 323.436 7.123 323.502 7.129 323.700 7.129 323.810 7.132 324.009 7.126 324.119 7.133 324.251 7.138 324.361 7.145 324.559 7.156 324.757 7.156 324.845 7.150 324.934 7.168 325.154 7.166 325.264 7.177 325.352 7.175 325.550 7.182 325.748 7.177 325.858 7.196 326.057 7.184 326.189 7.212 326.365 7.196 326.453 7.205 326.585 7.208 326.695 7.216 326.893 7.223 327.026 7.224 327.202 7.226 327.312 7.235 327.488 7.237 327.620 7.241 327.818 7.249 327.994 7.251 328.104 7.254 328.171 7.256 328.391 7.265 328.589 7.268 328.611 7.279 328.919 7.268 329.007 7.273 329.183 7.278 329.250 7.279 329.470 7.278 329.624 7.297 329.734 7.288 329.910 7.299 330.064 7.304 330.240 7.302 330.263 7.310 330.483 7.311 330.681 7.324 330.857 7.320 330.901 7.326 331.121 7.323 331.275 7.335 331.518 7.327 331.562 7.328 331.760 7.332 331.892 7.345 331.936 7.347 332.244 7.359 332.509 7.359 332.531 7.369 332.685 7.373 332.861 7.372 332.993 7.377 333.191 7.381 333.345 7.386 333.455 7.398 333.654 7.388 333.764 7.396 333.940 7.409 334.094 7.405 334.248 7.407 334.402 7.423 334.645 7.412 334.777 7.420 335.019 7.420 335.107 7.423 335.239 7.440 335.305 7.439 335.691 7.441 335.746 7.445 335.856 7.442 336.032 7.449 336.208 7.447 336.406 7.460 336.516 7.461 336.670 7.467 336.869 7.467 337.001 7.473 337.177 7.473 337.309 7.472 337.529 7.490 337.595 7.490 337.727 7.498 337.992 7.503 338.146 7.503 338.102 7.508 338.388 7.516 338.674 7.514 338.983 7.513 338.961 7.520 339.137 7.527 339.291 7.532 339.467 7.525 339.599 7.542 339.621 7.543 339.952 7.544 340.194 7.551 340.216 7.558 340.436 7.557 340.546 7.561 340.766 7.561 340.986 7.575 341.163 7.574 341.383 7.577 341.449 7.585 341.669 7.582 341.713 7.587 341.955 7.590 342.131 7.589 342.308 7.598 342.396 7.606 342.506 7.610 342.770 7.613 342.990 7.616 343.144 7.616 343.277 7.627 343.497 7.623 343.563 7.625 343.739 7.633 343.959 7.643 344.201 7.647 344.334 7.634 344.422 7.658 344.686 7.646 344.796 7.651 344.972 7.666 345.170 7.667 345.390 7.677 345.501 7.675 345.633 7.675 345.831 7.683 346.029 7.677 346.183 7.685 346.382 7.689 346.536 7.699 346.668 7.691 346.954 7.700 347.064 7.707 347.262 7.721 347.394 7.711 347.526 7.731 347.813 7.729 347.967 7.724 348.121 7.734 348.275 7.730 348.451 7.739 348.628 7.748 348.716 7.732 349.024 7.754 349.178 7.749 349.354 7.760 349.508 7.767 349.706 7.768 349.839 7.772 349.971 7.778 350.235 7.777 350.433 7.781 350.521 7.791 350.741 7.794 350.940 7.784 351.138 7.798 351.314 7.794 351.402 7.808 351.644 7.810 351.710 7.812 351.975 7.818 352.151 7.821 352.327 7.821 352.525 7.832 352.613 7.834 352.922 7.838 353.010 7.848 353.230 7.846 353.384 7.488 353.626 7.857 353.692 7.853 354.089 7.854 354.133 7.859 354.375 7.867 354.419 7.863 354.705 7.871 354.881 7.881 354.969 7.877 355.234 7.878 355.432 7.881 355.564 7.895 355.696 7.903 355.894 7.880 356.181 7.906 356.225 7.910 356.445 7.903 356.665 7.902 356.841 7.917 357.171 7.915 357.193 7.926 357.370 7.935 357.568 7.936 357.744 7.930 357.964 7.940 358.140 7.949 358.295 7.944 358.449 7.956 358.691 7.956 358.845 7.959 359.043 7.961 359.175 7.963 359.417 7.973 359.550 7.966 359.924 7.980 359.924 7.986 360.078 7.983 360.232 7.984 360.320 7.998 360.717 7.998 360.827 8.005 361.047 7.998 361.223 8.010 361.399 8.005 361.532 8.010 361.774 8.019 361.928 8.027 362.104 8.029 362.346 8.032 362.456 8.026 362.765 8.037 362.831 8.040 362.985 8.044 363.205 8.050 363.381 8.059 363.469 8.060 363.623 8.069 363.998 8.070 364.130 8.070 364.328 8.074 364.570 8.085 364.702 8.080 364.879 8.089 365.077 8.083 365.165 8.094 365.473 8.097 365.627 8.106 365.715 8.103 365.980 8.110 366.178 8.117 366.354 8.116 366.530 8.122 366.750 8.124 366.882 8.121 367.103 8.131 367.323 8.136 367.433 8.144 367.631 8.139 367.873 8.141 368.028 8.141 368.116 8.155 368.292 8.146 368.644 8.165 368.754 8.156 369.062 8.171 369.041 8.169 369.393 8.178 369.437 8.175 369.635 8.184 369.943 8.186 370.119 8.192 370.384 8.192 370.318 8.198 370.604 8.209 370.868 8.202 371.022 8.205 371.243 8.210 371.419 8.217 371.695 8.217 371.771 8.212 371.991 8.228 372.189 8.231 372.322 8.231 372.476 8.238 372.740 8.238 372.850 8.253 373.092 8.251 373.312 8.255 373.489 8.254 373.577 8.265 373.687 8.267 374.061 8.265 374.215 8.276 374.413 8.275 374.590 8.278 374.788 8.282 374.920 8.286 375.162 8.291 375.426 8.294 375.603 8.299 375.757 8.309 375.889 8.297 376.109 8.309 376.219 8.311 376.461 8.312 376.660 8.320 376.880 8.327 377.034 8.336 377.210 8.328 377.430 8.340 377.673 8.338 377.783 8.344 378.003 8.340 378.223 8.356 378.377 8.348 378.697 8.361 378.708 8.360 378.950 8.354 379.126 8.369 379.302 8.369 379.544 8.366 379.676 8.389 379.875 8.387 380.095 8.383 380.271 8.385 380.425 8.398 380.513 8.400 380.843 8.406 381.020 8.414 381.240 8.408 381.350 8.411 381.614 8.423 381.746 8.425 381.989 8.437 382.209 8.426 382.385 8.432 382.627 8.438 382.737 8.436 382.913 8.436 383.024 8.453 383.266 8.455 383.486 8.462 383.662 8.456 383.860 8.468 384.014 8.469 384.257 8.466 384.433 8.468 384.631 8.477 384.763 8.482 385.005 8.493 385.137 8.502 385.380 8.504 385.556 8.504 385.798 8.503 385.974 8.502 386.128 8.506 386.927 8.504 386.503 8.518 386.701 8.515 386.899 8.523 387.097 8.523 387.207 8.532 387.450 8.532 387.692 8.530 387.736 8.540 388.022 8.537 388.198 8.557 388.418 8.555 388.573 8.562 388.837 8.558 388.969 8.559 389.189 8.577 389.431 8.572 389.519 8.579 389.740 8.580 389.872 8.580 390.092 8.593 390.290 8.591 390.488 8.590 390.576 8.601 390.951 8.594 391.105 8.608 391.149 8.610 391.391 8.620 391.611 8.620 391.810 8.622 391.942 8.622 392.162 8.628 392.426 8.628 392.580 8.631 392.778 8.640 392.911 8.643 393.153 8.654 393.351 8.654 393.505 8.655 393.681 8.666 393.880 8.661 394.056 8.664 394.298 8.675 394.518 8.683 394.606 8.683 394.848 8.680 395.047 8.686 395.245 8.692 395.333 8.703 395.597 8.701 395.729 8.701 395.971 8.710 396.148 8.706 396.324 8.708 396.544 8.711 396.698 8.716 396.896 8.723 397.117 8.725 397.469 8.733 397.425 8.740 397.579 8.750 397.865 8.745 398.063 8.757 398.173 8.741 398.416 8.755 398.658 8.765 398.812 8.765 398.966 8.770 399.164 8.779 399.319 8.773 399.451 8.767 399.671 8.770 399.935 8.783 400.067 8.781 400.243 8.788 400.508 8.793 400.618 8.793 400.838 8.803 401.036 8.813 401.212 8.807 401.234 8.807 401.587 8.824 401.741 8.810 401.961 8.825 402.137 8.818 402.379 8.834 402.556 8.835 402.732 8.853 402.886 8.842 403.062 8.845 403.304 8.851 403.458 8.852 403.379 8.869 403.855 8.864 404.031 8.877 404.207 8.880 404.405 8.875 404.626 8.881 404.758 8.888 404.956 8.894 405.154 8.887 405.330 8.895 405.352 8.904 405.705 8.897 405.903 8.905 406.057 8.903 406.277 8.907 406.409 8.908 406.607 8.914 406.783 8.930 406.938 8.922 407.136 8.924 407.290 8.939 407.532 8.933 407.730 8.931 407.929 8.939 408.083 8.944 408.281 8.943 408.479 8.943 408.677 8.961 408.853 8.967 409.030 8.967 409.228 8.962 409.404 8.978 409.646 8.977 409.778 8.980 409.954 8.985 410.175 8.986 410.263 8.994 410.461 8.996 410.703 8.996 411.011 9.000 411.144 9.009 411.276 9.011 411.430 9.015 411.606 9.016 411.782 9.025 411.980 9.024 412.156 9.032 412.333 9.027 412.509 9.040 412.729 9.035 412.861 9.044 413.059 9.047 413.280 9.048 413.434 9.050 413.588 9.052 413.852 9.063 414.006 9.065 414.138 9.069 414.226 9.070 414.557 9.075 414.711 9.082 414.931 9.086 415.063 9.092 415.305 9.102 415.437 9.093 415.658 9.100 415.812 9.109 415.966 9.108 416.164 9.110 416.362 9.112 416.539 9.122 416.693 9.115 416.847 9.132 417.067 9.129 417.265 9.143 417.287 9.136 417.551 9.136 417.794 9.150 418.014 9.143 418.168 9.165 418.388 9.160 418.520 9.160 418.697 9.170 418.763 9.169 419.115 9.170 419.269 9.174 419.599 9.183 419.621 9.180 419.886 9.185 419.974 9.196 420.150 9.192 420.348 9.184 420.480 9.202 420.700 9.202 420.921 9.203 421.075 9.210 421.251 9.221 421.383 9.221 421.625 9.215 421.801 9.230 421.978 9.239 422.066 9.229 422.352 9.246 422.528 9.245 422.682 9.254 422.858 9.251 423.079 9.257 423.145 9.253 423.299 9.269 423.585 9.273 423.761 9.268 424.070 9.273 424.070 9.276 424.290 9.286 424.444 9.287 424.686 9.285 424.840 9.292 425.038 9.292 425.193 9.302 425.391 9.303 425.589 9.310 425.809 9.306 425.963 9.312 426.095 9.320 426.294 9.322 426.448 9.334 426.586 9.328 426.800 9.335 427.020 9.335 427.174 9.340 427.328 9.350 427.527 9.349 427.703 9.352 427.879 9.363 428.055 9.360 428.253 9.365 428.342 9.374 428.650 9.370 428.738 9.367 428.980 9.378 429.156 9.371 429.310 9.386 429.663 9.388 429.575 9.399 429.751 9.402 430.015 9.401 430.147 9.411 430.389 9.413 430.522 9.410 430.764 9.413 430.940 9.421 431.072 9.423 431.270 9.425 431.402 9.431 431.601 9.428 431.799 9.438 431.975 9.436 432.151 9.444 432.349 9.448 432.481 9.452 432.658 9.447 432.834 9.462 432.988 9.458 433.208 9.471 433.362 9.470 433.560 9.483 433.494 9.474 433.869 9.482 434.133 9.483 434.265 9.491 434.485 9.497 434.639 9.500 434.705 9.501 434.926 9.508 345.146 9.507 435.256 9.516 435.542 9.517 435.564 9.517 435.806 9.528 435.806 9.536 436.005 9.525 436.335 9.545 436.555 9.537 436.819 9.543 436.775 9.548 437.040 9.559 437.194 9.560 437.326 9.557 437.568 9.567 437.766 9.567 437.854 9.573 438.097 9.567 438.251 9.578 438.405 9.578 438.647 9.579 438.669 9.583 438.955 9.590 439.109 9.604 439.330 9.602 439.528 9.607 439.638 9.606 439.726 9.612 440.012 9.613 440.211 9.624 440.431 9.628 440.497 9.624 440.673 9.624 440.849 9.642 440.959 9.641 441.003 9.655 441.378 9.653 441.532 9.652 441.752 9.649 441.884 9.655 442.082 9.663 442.192 9.673 442.347 9.679 442.611 9.679 442.765 9.676 442.941 9.688 443.095 9.681 443.271 9.691 443.470 9.699 443.580 9.699 443.822 9.702 444.020 9.711 444.064 9.705 444.130 9.712 444.460 9.713 444.659 9.713 444.835 9.726 444.945 9.733 445.209 9.741 445.341 9.733 445.473 9.740 445.694 9.740 445.914 9.748 445.936 9.751 446.178 9.756 446.398 9.758 446.486 9.765 446.706 9.769 446.883 9.760 447.059 9.773 447.103 9.781 447.301 9.778 447.609 9.794 447.653 9.792 447.984 9.796 448.006 9.798 448.204 9.792 448.336 9.799 448.424 9.807 448.776 9.810 448.953 9.813 449.063 9.819 449.173 9.813 449.437 9.816 449.591 9.826 449.767 9.823 449.944 9.832 450.142 9.831 450.252 9.849 450.450 9.851 450.604 9.856 450.780 9.860 450.957 9.860 451.022 9.860 451.309 9.878 451.463 9.870 451.749 9.874 451.771 9.869 451.969 9.892 452.124 9.889 452.168 9.887 452.476 9.891 452.652 9.989 452.762 9.896 452.960 9.909 453.269 9.914 453.291 9.928 453.467 9.916 453.621 9.935 453.797 9.934 453.951 9.939 454.105 9.941 454.285 9.947 454.436 9.952 454.634 9.953 454.810 9.946 454.964 9.958 455.118 9.956 455.228 9.967 455.493 9.965 455.449 9.982 455.801 9.971 455.999 9.985 456.131 9.990 456.285 10.003 456.330 9.982 456.660 9.998 456.770 10.002 456.946 10.005 457.100 10.002 457.342 10.021 457.430 10.017 457.629 10.027 457.805 10.022 457.915 10.037 458.069 10.036 458.267 10.039 458.485 10.030 458.532 10.038 458.664 10.047 458.906 10.050 459.148 10.061 459.192 10.062 459.236 (1) Strain (%) (2) Stress (MPa)

TABLE 11 compression test: table 4: (1) (2) 10.066 459.589 10.063 459.787 10.066 460.007 10.071 460.139 10.079 460.298 10.091 460.425 10.090 460.624 10.098 460.800 10.098 460.998 10.101 461.108 10.099 461.240 10.100 461.416 10.108 461.614 10.123 461.791 10.120 462.945 10.125 462.077 10.130 462.253 10.131 462.363 10.139 462.605 10.143 462.737 10.137 462.914 10.149 463.090 10.151 463.266 10.147 463.376 10.162 463.640 10.159 463.728 10.167 463.860 10.180 463.949 10.171 464.235 10.181 464.389 10.182 464.587 10.190 464.697 10.191 464.851 10.199 465.094 10.188 465.182 10.211 465.270 10.216 465.534 10.202 465.754 10.222 465.842 10.216 466.019 10.221 466.129 10.231 466.327 10.225 466.151 10.234 466.635 10.237 466.789 10.245 466.833 10.233 467.208 10.258 467.340 10.251 467.450 10.260 467.604 10.265 467.846 10.268 467.956 10.265 467.956 10.277 468.243 10.276 468.463 10.283 468.639 10.288 468.925 10.289 468.925 10.287 469.123 10.295 469.233 10.294 469.388 10.308 469.542 10.306 469.740 10.316 469.894 10.320 469.982 10.318 470.180 10.326 470.335 10.324 470.511 10.321 470.731 10.337 470.907 10.335 470.995 10.345 471.083 10.343 471.281 10.349 471.435 10.351 471.744 10.357 471.744 10.365 471.964 10.369 472.096 10.376 472.228 10.372 472.448 10.376 472.537 10.387 472.669 10.381 472.845 10.388 473.087 10.387 473.219 10.397 473.351 10.396 473.483 10.401 473.682 10.899 473.814 10.410 474.034 10.408 474.254 10.421 474.354 10.426 474.474 10.428 474.651 10.434 474.805 10.437 474.981 10.441 475.113 10.445 475.245 10.447 475.399 10.451 475.487 10.454 475.685 10.460 475.950 10.457 476.038 10.475 476.170 10.471 476.368 10.471 476.522 10.477 476.698 10.488 476.830 10.485 477.007 10.498 477.095 10.492 477.315 10.502 477.513 10.508 477.667 10.508 477.733 10.516 477.821 10.512 478.130 10.522 478.306 10.530 478.416 10.532 478.592 10.530 478.746 10.533 479.032 10.543 479.032 10.549 479.253 10.544 479.319 10.558 479.495 10.555 479.649 10.564 479.803 10.571 480.045 10.565 480.156 10.575 480.266 10.577 480.486 10.585 480.552 10.589 480.728 10.587 480.948 10.579 481.080 10.593 481.213 10.599 481.345 10.601 481.521 10.606 481.653 10.606 481.807 10.607 481.983 10.616 482.159 10.628 482.248 10.637 482.314 10.632 482.622 10.644 482.710 10.642 482.886 10.642 482.974 10.655 483.216 10.661 483.349 10.655 483.415 10.666 483.679 10.665 483.855 10.666 483.987 10.677 484.031 10.679 484.295 10.679 484.361 10.687 484.582 10.694 484.736 10.693 484.868 10.705 485.000 10.699 485.176 10.711 485.308 10.711 485.485 10.724 485.617 10.725 485.793 10.725 485.013 10.727 486.101 10.724 486.299 10.731 486.431 10.734 486.608 10.739 486.696 10.729 486.718 10.745 487.004 10.754 487.202 10.749 487.312 10.763 487.488 10.759 487.599 10.765 487.753 10.772 487.885 10.782 488.017 10.776 488.259 10.784 488.369 10.789 488.523 10.796 488.678 10.794 488.832 10.799 488.810 10.807 489.118 10.823 489.272 10.819 489.382 10.822 489.536 10.816 489.756 10.831 489.801 10.826 489.933 10.833 490.175 10.842 490.329 10.837 490.439 10.840 490.615 10.844 490.747 10.847 490.946 10.848 491.078 10.854 491.188 10.857 491.320 10.871 491.496 10.869 491.650 10.879 491.804 10.874 491.959 10.874 492.091 10.880 492.311 10.895 492.443 10.892 492.575 10.904 492.707 10.907 492.861 10.906 493.060 10.906 493.170 10.906 493.104 10.916 493.466 10.920 493.566 10.926 493.698 10.928 493.852 10.944 493.984 10.940 494.117 10.942 494.227 10.948 494.513 10.953 494.623 10.956 494.865 10.964 494.909 10.965 495.063 10.970 495.218 10.975 495.306 10.971 495.504 10.971 495.636 10.984 495.790 10.985 496.922 10.995 496.098 10.996 496.253 11.005 496.363 10.996 496.539 11.011 496.715 11.020 496.693 11.012 496.869 11.015 497.133 11.021 497.221 11.025 497.288 11.032 497.552 11.033 497.706 11.043 497.882 11.050 497.948 11.046 498.146 11.054 498.300 11.044 498.410 11.055 498.499 11.060 498.967 11.072 498.829 11.073 499.071 11.080 499.071 11.084 499.247 11.088 499.423 11.095 499.578 11.105 499.754 11.102 499.842 11.096 499.974 11.112 500.084 11.109 500.260 11.110 500.436 11.124 500.525 11.127 500.701 11.121 500.877 11.135 500.987 11.141 501.185 11.139 501.295 11.152 501.471 11.151 501.626 11.150 501.714 11.162 501.868 11.160 502.000 11.164 502.132 11.165 502.264 11.170 502.440 11.175 502.550 11.176 502.727 11.177 502.881 11.190 502.925 11.192 503.057 11.196 503.343 11.202 503.453 11.207 503.475 11.212 503.739 11.207 503.850 11.220 504.048 11.219 504.180 11.222 504.246 11.232 504.400 11.233 504.532 11.241 504.708 11.247 504.841 11.249 504.995 11.253 505.105 11.265 505.149 11.250 505.391 11.259 505.523 11.264 505.677 11.273 505.787 11.273 505.986 11.276 506.096 11.281 506.206 11.282 506.382 11.285 506.514 11.294 506.646 11.293 506.800 11.294 506.910 11.307 507.020 11.309 507.307 11.307 507.175 11.327 507.439 11.325 507.615 11.327 507.769 11.331 507.989 11.333 508.055 11.341 508.166 11.341 508.276 11.351 508.496 11.355 508.518 11.361 508.672 11.365 508.892 11.357 508.980 11.374 509.046 11.383 509.201 11.378 509.465 11.374 509.509 11.393 509.641 11.382 509.817 11.398 509.949 11.400 509.971 11.403 510.169 11.405 510.390 11.412 510.456 11.416 510.588 11.418 510.786 11.415 510.918 11.430 511.050 11.434 511.138 11.434 511.336 11.440 511.469 11.437 511.667 11.445 511.733 11.449 511.843 11.459 511.975 11.455 512.063 11.462 512.239 11.464 512.416 11.469 512.548 11.473 512.812 11.473 512.866 11.473 512.856 11.486 513.010 11.494 513.208 11.500 513.296 11.501 513.340 11.514 513.605 11.502 513.759 11.515 513.891 11.510 513.979 11.516 514.111 11.524 514.287 11.526 514.441 11.587 514.530 11.539 517.662 11.548 514.926 11.544 514.970 11.546 515.080 11.547 515.212 11.557 515.322 11.557 515.432 11.566 515.609 11.561 515.719 11.576 515.851 11.576 516.005 11.580 516.159 11.582 516.247 11.593 516.401 11.592 516.467 11.609 516.687 11.604 516.798 11.600 517.084 11.609 517.062 11.620 517.194 11.611 517.216 11.628 517.458 11.639 517.590 11.630 517.701 11.631 517.811 11.641 517.943 11.643 518.097 11.655 518.229 11.646 518.339 11.658 518.515 11.665 518.647 11.666 518.691 11.670 518.890 11.673 518.978 11.677 519.154 11.684 519.264 11.691 519.418 11.694 519.462 11.696 519.638 11.708 519.792 11.706 519.903 11.717 520.079 11.719 520.123 11.725 520.299 11.724 520.475 11.728 520.519 11.733 520.607 11.741 520.827 11.732 520.915 11.742 521.047 11.755 521.180 11.755 521.356 11.757 521.444 11.762 521.576 11.772 521.708 11.766 521.950 11.766 521.994 11.777 522.017 11.783 522.281 11.778 522.369 11.799 522.479 11.788 522.611 11.788 522.743 11.802 522.853 11.811 522.985 11.809 523.095 11.819 523.206 11.814 523.382 11.811 523.470 11.834 523.690 11.834 523.734 11.831 523.932 11.835 524.020 11.837 524.130 11.847 524.241 11.840 524.395 11.857 524.461 11.852 524.615 11.861 524.747 11.870 524.879 11.871 525.033 11.877 525.011 11.884 525.077 11.888 525.341 11.885 525.452 11.893 525.584 11.901 525.738 11.900 525.826 11.900 525.980 11.906 526.244 11.911 526.090 11.913 526.421 11.919 526.443 11.922 526.597 11.925 526.751 11.932 529.839 11.931 526.971 11.937 527.103 11.943 527.257 11.944 527.345 11.949 527.455 11.949 527.688 11.959 527.742 11.969 527.852 11.960 527.874 11.974 528.094 11.971 528.138 11.985 528.248 11.988 528.424 11.984 528.557 11.996 528.645 12.000 528.799 11.998 528.909 12.005 529.085 12.002 529.217 12.015 529.327 12.017 529.459 12.020 529.547 12.022 529.702 12.025 529.812 12.037 529.922 12.039 530.032 12.033 530.164 12.047 530.274 12.052 530.406 12.050 530.560 12.050 530.671 12.056 530.781 12.074 530.957 12.074 531.001 12.078 531.155 12.081 531.243 12.081 531.375 12.090 531.485 12.094 531.639 12.101 531.683 12.098 531.816 12.103 531.992 12.118 532.080 12.113 532.190 12.119 532.256 12.127 532.410 12.128 532.454 12.133 532.674 12.135 532.740 12.148 532.895 12.129 533.049 12.148 533.115 12.150 533.247 12.160 533.379 12.167 533.379 12.169 533.665 12.164 533.709 12.171 533.841 12.178 533.753 12.188 534.084 12.189 534.238 12.191 534.348 12.189 534.458 12.193 534.590 12.205 534.634 12.217 534.700 12.213 534.898 12.224 534.964 12.214 534.987 12.233 535.163 12.233 535.339 12.233 535.427 12.233 535.427 12.240 535.713 12.248 535.801 12.256 535.911 12.262 535.867 12.264 536.154 12.263 536.242 12.273 536.352 12.269 536.506 12.281 536.616 12.288 536.704 12.287 536.814 12.282 536.924 12.285 537.034 12.293 537.078 12.294 537.189 12.297 537.453 12.310 537.541 12.318 537.563 12.315 537.805 12.317 537.915 12.330 538.025 12.324 538.091 12.332 538.290 12.341 538.334 12.350 538.466 12.352 538.576 12.344 538.752 12.354 538.708 12.360 538.928 12.363 539.038 12.359 539.126 12.371 539.192 12.382 539.170 12.382 539.435 12.390 539.589 12.390 539.699 12.393 539.831 12.396 539.919 12.404 540.007 12.408 540.139 12.407 540.315 12.415 540.381 12.419 540.492 12.427 540.580 12.426 540.690 12.427 540.800 12.441 540.954 12.442 541.042 12.441 541.152 12.445 541.240 12.453 541.262 12.455 541.483 12.460 541.693 12.461 541.703 12.476 541.813 12.471 541.923 12.472 542.033 12.490 541.989 12.495 542.209 12.489 542.363 12.499 542.473 12.503 542.540 12.503 542.672 12.507 542.760 12.511 542.848 12.521 534.002 12.522 543.134 12.533 543.244 12.527 543.200 12.535 543.420 12.545 543.508 12.549 543.685 12.545 543.751 12.550 543.861 12.560 543.883 12.563 544.015 12.575 544.191 12.562 544.301 12.577 544.543 12.569 544.499 12.573 544.830 12.589 544.697 12.593 544.852 12.593 544.940 12.610 545.028 12.602 545.094 12.608 545.314 12.611 545.336 12.628 545.446 12.619 545.534 12.628 545.666 12.642 545.754 12.640 545.821 12.645 545.931 12.643 546.041 12.648 546.195 12.656 546.371 12.657 546.437 12.669 546.525 12.668 546.459 12.676 546.679 12.673 546.855 12.672 546.966 12.678 547.032 12.688 547.164 12.695 547.274 12.693 547.252 12.697 547.362 12.701 547.560 12.710 547.670 12.715 547.736 12.722 547.890 12.731 547.957 12.726 548.111 12.724 548.243 12.730 548.287 12.738 548.419 12.742 548.485 12.741 548.617 12.758 548.749 12.753 548.837 12.766 548.837 12.778 548.970 12.775 549.124 12.777 549.234 12.776 549.322 12.790 549.454 12.797 549.664 12.797 549.608 12.801 549.762 12.800 549.806 12.807 549.960 12.802 550.027 12.812 550.092 12.812 550.291 12.813 550.401 12.828 550.665 12.827 550.379 12.828 550.665 12.833 550.709 12.848 550.907 12.846 550.929 12.861 551.127 12.861 551.105 12.866 551.216 12.860 551.348 12.879 551.436 12.863 551.546 12.876 551.634 12.874 551.788 12.881 551.832 12.889 551.854 12.896 552.206 12.897 552.096 12.899 552.273 12.912 552.316 12.912 552.449 12.923 552.537 12.927 552.647 12.921 552.735 12.923 552.845 12.943 552.911 12.941 553.065 12.949 553.175 12.937 553.131 12.949 553.308 12.955 553.418 12.953 553.550 12.959 553.594 12.972 553.726 12.974 553.814 12.981 553.748 12.993 553.968 12.984 554.166 12.999 554.188 12.994 554.276 12.994 554.386 13.011 554.541 13.012 554.585 13.008 554.673 13.016 554.761 13.022 554.849 13.036 554.959 13.038 555.069 13.029 555.157 13.054 555.289 13.045 555.377 13.048 555.421 13.050 555.576 13.054 555.642 13.069 555.554 13.068 555.906 13.070 555.972 13.084 556.038 13.090 556.060 13.087 556.214 13.087 556.368 13.090 556.412 13.094 556.478 13.105 556.633 13.107 556.655 13.110 556.787 13.114 556.875 13.124 556.963 13.125 557.029 13.128 557.095 13.127 557.227 13.137 557.315 13.148 557.535 13.141 557.513 13.145 557.601 13.163 557.579 13.168 557.646 13.177 557.910 13.176 557.888 13.176 558.064 13.181 558.152 13.191 558.240 13.187 558.308 13.185 558.438 13.197 558.548 13.199 558.659 13.207 558.681 13.208 558.769 13.214 558.857 13.223 558.945 13.213 559.055 13.228 559.143 13.239 559.209 13.239 559.319 13.240 559.385 13.239 559.495 13.244 559.627 13.256 559.693 13.262 559.803 13.267 559.848 13.272 559.958 13.273 560.024 13.282 560.134 13.276 560.244 13.287 560.266 13.287 560.376 13.297 560.486 13.305 560.552 13.293 560.662 13.313 560.728 13.317 560.816 13.336 560.905 13.316 560.971 13.329 561.081 13.321 561.191 13.337 561.301 13.343 561.367 13.344 561.455 13.346 561.521 13.354 561.631 13.361 561.697 13.366 561.763 13.376 581.851 13.377 561.873 13.371 562.028 13.380 562.028 13.385 562.028 13.388 562.270 13.402 562.424 13.403 562.424 13.401 562.534 13.408 562.644 13.416 562.688 13.417 562.732 13.414 562.842 13.430 562.886 13.426 562.952 13.440 562.975 13.438 563.107 13.440 563.195 13.440 563.173 (1) Strain (%) (2) Stress (MPa)

Table 12 summarizes results obtained in a tensile test and a compression test regarding an Mg-2.3 Zn-0.1% Ag-0.1% Ca alloy and an Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy as extruded at 300° C. and 350° C., respectively.

TABLE 12 Tensile test at room temperature [(Proof stress ratio) = (Compression proof stress)/(Tensile proof stress) × 100 (%)] Ultimate Extrusion Tensile tensile Elongation Compression Proof Alloy temperature proof stress strength to failure proof stress stress ratio name (° C.) (MPa) (MPa) (%) (MPa) (%) Mg—2.3Zn—0.1Ag—0.1Ca 300 155 281 25.4 141 91 350 135 277 24.3 103 76 Mg—2.3Zn—0.1Ag—0.1Ca—0.17Zr 300 306 364 17 271 89 350 288 351 17.1 246 85

It is noted from these results that the hot extruded Mg-2.3% Zn-0.1% Ag-0.1% Ca alloy and Mg-2.3% Zn-0.1% Ag-0.1% Ca-0.17% Zr alloy are a material having both high strength and high ductility and having small anisotropy in proof stress.

It is considered that revealment of such excellent mechanical properties with small anisotropy in strength as well as high strength and high ductility has a relationship with a fine grain, a lowering in a degree of the basal texture and a fine precipitate within the grain.

INDUSTRIAL APPLICABILITY

The material of this invention has high strength and high ductility and can be used for transportation equipment which is expected to realize weight reduction as a replacement for Al alloys, such as automobiles, motorcycles, aircrafts, etc. Furthermore, since the mechanical properties of the material of this invention can be obtained without necessity of an additional heat treatment after the hot working, the material of this invention is also expected as a replacement for currently used wrought Mg alloys. Also, in view of the fact that the samples after hot extrusion at 350° C. display an ultrafine grain structure of about 500 nm in terms of an average grain size, there is a possibility that the material of this invention is applicable as a superplastic material.

Claims

1. An Mg base alloy containing Mg as a main material and Zn as an additive material. which is characterized in that Ag is contained in an amount of not more than 1.98 at % as an additive material other than Zn.

2. The Mg base alloy according to claim 1, which is characterized in that Ca is further contained in an amount of not more than 0.61 at % as an additive material other than Zn and Ag.

3. The Mg base alloy according to claim 2, which is characterized in that Zr is further contained in an amount of not more than 0.17 at % as an additive material other than Zn, Ag and Ca.

4. The Mg base alloy according to any one of claims 1 to 3, which is characterized in that a grain size thereof is from 0.1 μm to 25 μm.

Patent History
Publication number: 20100202916
Type: Application
Filed: May 9, 2008
Publication Date: Aug 12, 2010
Inventors: Chamini Mendis (Ibaraki), Keiichiro Oishi (Ibaraki), Kazuhiro Houno (Ibaraki), Yoshiaki Kawamura (Niigata), Shigeharu Kamado (Niigata)
Application Number: 12/451,356
Classifications
Current U.S. Class: Silver Containing (420/403); Zinc Containing (420/411)
International Classification: C22C 23/00 (20060101); C22C 23/04 (20060101);