Specified Orientation, Shape, Crystallography, Or Size Of Seed Or Substrate Patents (Class 117/902)
  • Patent number: 6800135
    Abstract: A ZnO/sapphire substrate includes an R-plane sapphire substrate whose (0 1-1 2) planes are parallel to the surface thereof and a ZnO epitaxial film formed on the R-plane sapphire substrate. The (1 1-2 0) planes of the ZnO epitaxial film are disposed with an interplanar spacing in the range of about 1.623 to 1.627 Å parallel to the (0 1-1 2) planes of the R-plane sapphire substrate.
    Type: Grant
    Filed: June 17, 2002
    Date of Patent: October 5, 2004
    Assignee: Murata Manufacturing Co., Ltd.
    Inventors: Jun Koike, Hideharu Ieki
  • Patent number: 6752868
    Abstract: A three dimensional photonic crystal and layer-by-layer processes of fabricating the photonic crystal. A templated substrate is exposed to a plurality of first microspheres made of a first material, the first material being of a type that will bond to the templated substrate and form a self-passivated layer of first microspheres to produce a first layer. The first layer is exposed to a plurality of second microspheres made of a second material, the second material being of a type that will bond to the first layer and form a self-passivated layer of second microspheres. This layering of alternating first and second microspheres can be repeated as desired to build a three dimensional photonic crystal of desired geometry.
    Type: Grant
    Filed: July 31, 2002
    Date of Patent: June 22, 2004
    Assignee: MCNC Research & Development Institute
    Inventors: John South Lewis, III, Scott Halden Goodwin-Johansson, Brian Rhys Stoner, Sonia Grego, David Edward Dausch
  • Patent number: 6743292
    Abstract: A thin film structure is provided including a silicon substrate with a layer of silicon dioxide on a surface thereof, and a layer of cubic oxide material deposited upon the layer of silicon dioxide by ion-beam-assisted-deposition, said layer of cubic oxide material characterized as biaxially oriented. Preferably, the cubic oxide material is yttria-stabilized zirconia. Additional thin layers of biaxially oriented ruthenium oxide or lanthanum strontium cobalt oxide are deposited upon the layer of yttria-stabilized zirconia. An intermediate layer of cerium oxide is employed between the yttria-stabilized zirconia layer and the lanthanum strontium cobalt oxide layer. Also, a layer of barium strontium titanium oxide can be upon the layer of biaxially oriented ruthenium oxide or lanthanum strontium cobalt oxide.
    Type: Grant
    Filed: September 18, 2001
    Date of Patent: June 1, 2004
    Assignee: The Regents of the University of California
    Inventors: Quanxi Jia, Paul N. Arendt
  • Patent number: 6685773
    Abstract: A crystal growth method for growing a nitride semiconductor crystal on a sapphire substrate in a vapor phase, includes the steps of: providing a sapphire substrate having a substrate orientation inclined by about 0.05° to about 0.2° from a <0001>orientation; and allowing a nitride semiconductor crystal to grow on the surface of the sapphire substrate.
    Type: Grant
    Filed: May 3, 2001
    Date of Patent: February 3, 2004
    Assignee: Sharp Kabushiki Kaisha
    Inventors: Yoshihiro Ueta, Takayuki Yuasa
  • Publication number: 20040003768
    Abstract: A method for forming a sharply biaxially textured substrate, such as a single crystal substrate, includes the steps of providing a deformed metal substrate, followed by heating above the secondary recrystallization temperature of the deformed substrate, and controlling the secondary recrystallization texture by either using thermal gradients and/or seeding. The seed is selected to shave a stable texture below a predetermined temperature. The sharply biaxially textured substrate can be formed as a tape having a length of 1 km, or more. Epitaxial articles can be formed from the tapes to include an epitaxial electromagnetically active layer. The electromagnetically active layer can be a superconducting layer.
    Type: Application
    Filed: July 3, 2002
    Publication date: January 8, 2004
    Inventor: Amit Goyal
  • Patent number: 6670036
    Abstract: There are disclosed a silicon seed crystal which is composed of silicon single crystal and used for the Czochralski method, wherein oxygen concentration in the seed crystal is 15 ppma (JEIDA) or less, a silicon seed crystal which is used for the Czochralski method, wherein the silicon seed crystal does not have a straight body, and a method for producing a silicon single crystal by the Czochralski method comprising using said seed crystal, bringing a tip end of the seed crystal into contact with a silicon melt to melt the tip end of the seed crystal, with or without performing necking operation, and growing a silicon single crystal. The method is capable of improving the rate of success in making crystals dislocation-free and the productivity of single crystal rods regardless of the use of necking operation.
    Type: Grant
    Filed: April 6, 1999
    Date of Patent: December 30, 2003
    Assignee: Shin-Etsu Handotai Co., Ltd.
    Inventors: Eiichi Iino, Masanori Kimura
  • Patent number: 6617668
    Abstract: A layer comprising silicon oxide (SiO2) is formed on (111) plane of a silicon (Si) substrate in a striped pattern which is longer in the [1-10] axis direction perpendicular to the [110] axis direction. Then a group III nitride compound semiconductor represented by a general formula AlxGayIn1-x-yN (0≦x≦1, 0≦y≦1, 0≦x+y≦1) is laminated thereon. The group III nitride compound semiconductor represented by a general formula AlxGayIn1-x-yN (0≦x≦1, 0≦y≦1, 0≦x+y≦1) grows epitaxially on the substrate-exposed regions B which are not covered by the SiO2 layer, and grows epitaxially on the SiO2 layer in lateral direction from the regions B. Consequently, a group III nitride compound semiconductor having no dislocations can be obtained.
    Type: Grant
    Filed: May 19, 2000
    Date of Patent: September 9, 2003
    Assignee: Toyoda Gosei Co., Ltd.
    Inventors: Norikatsu Koide, Hisaki Kato
  • Patent number: 6607593
    Abstract: When a crystalline nucleus generated from an under-cooled silicon droplet is grown up to a mono-crystalline silicon ball, a critical under-cooling &Dgr;Tcr is determined in response to a diameter d of the silicon droplet so as to satisfy the relationships of (d=5 mm, &Dgr;Tcr=100K), (d=3 mm, &Dgr;Tcr=120K) and (d=1 mm, &Dgr;Tcr=150K). A crystal grown up from the crystalline nucleus at an under-cooling &Dgr;T less than the critical under-cooling &Dgr;Tcr is a mono-crystalline silicon ball with high quality free from cracks or twins.
    Type: Grant
    Filed: July 27, 2001
    Date of Patent: August 19, 2003
    Assignee: Agency of Industrial Science and Technology
    Inventors: Kazuhiko Kuribayashi, Tomotsugu Aoyama
  • Patent number: 6558465
    Abstract: In an optical element which includes a single crystal having at least one flat light-transmitting end surface, the at least one light-transmitting end surface is inclined at at least 0.5 degrees relative to a plane perpendicular to one of an a-axis and a c-axis of the single crystal. In a process of producing such an optical element, a single crystal is cut out so that the single crystal has at least one surface which is inclined at at least 0.5 degrees relative to a plane perpendicular to one of an a-axis and a c-axis of the single crystal, and then the at least one surface is polished into at least one light-transmitting end surface.
    Type: Grant
    Filed: March 31, 2000
    Date of Patent: May 6, 2003
    Assignee: Fuji Photo Film Co., Ltd.
    Inventor: Takayuki Katoh
  • Patent number: 6508880
    Abstract: A low defect (e.g., dislocation and micropipe) density silicon carbide (SiC) is provided as well as an apparatus and method for growing the same. The SiC crystal, grown using sublimation techniques, is preferably divided into two stages of growth. During the first stage of growth, the crystal grows in a normal direction while simultaneously expanding laterally. Although dislocations and other material defects may propagate within the axially grown material, defect propagation and generation in the laterally grown material are substantially reduced, if not altogether eliminated. After the crystal has expanded to the desired diameter, the second stage of growth begins in which lateral growth is suppressed and normal growth is enhanced. A substantially reduced defect density is maintained within the axially grown material that is based on the laterally grown first stage material.
    Type: Grant
    Filed: February 14, 2001
    Date of Patent: January 21, 2003
    Assignee: The Fox Group, Inc.
    Inventors: Yury Alexandrovich Vodakov, Mark Grigorievich Ramm, Evgeny Nikolaevich Mokhov, Alexandr Dmitrievich Roenkov, Yury Nikolaevich Makarov, Sergei Yurievich Karpov, Mark Spiridonovich Ramm, Heikki I. Helava
  • Patent number: 6461003
    Abstract: A corner cube array device (20) is disclosed having a silicon substrate (30) with a generally cubic crystal lattice. A number of silicon crystal projections (62a, 62b, 62c, 62d, 62e, 62f, 62g) extend from the substrate (30). The projections (62a, 62b, 62c, 62d, 62e, 62f, 62g) each have three generally planar surfaces, as exemplified by surfaces (70, 72, 74) of projection (62a), to provide a cube corner shape. Projections (62a, 62b, 62c, 62d, 62e, 62f, 62g) are spaced apart from each other in accordance with a predetermined spatial pattern to define a cube corner array (60) suitable for optical device applications and the mass production of articles having a substantially similar corner cube array shape.
    Type: Grant
    Filed: November 30, 1999
    Date of Patent: October 8, 2002
    Assignee: Purdue Research Foundation
    Inventor: Gerold W. Neudeck
  • Patent number: 6458206
    Abstract: AFM/STM probes are based on whiskers grown by the vapor-liquid-solid (VLS) mechanism. Silicon cantilevers oriented along the crystallographic plane (111) are prepared from silicon-on-insulator structures that contain a thin layer (111) on a (100) substrate with SiO2 interposed layer. At removal of solidified alloy globules inherent in the growth mechanism sharpening of the whiskers takes place and, in such a way, the probes are formed. Cross-sections of the wiskers grown by the mechanism on the cantilevers can be controllably changed during the growth process so that step-shaped whiskers optimal for fabrication of the probes can be prepared. Also, whiskers with expansions/contractions can be formed that are important for fabrication of probes suitable for investigations in coarse surfaces, complicated cavitites, grooves typical for semiconductor microelectronics, etc.
    Type: Grant
    Filed: March 9, 2001
    Date of Patent: October 1, 2002
    Assignee: Crystals and Technologies, Ltd.
    Inventors: Evgeny Invievich Givargizov, Lidiya Nikolaevna Obolenskaya, Ala Nikolaevna Stepanova, Evgeniya Sergeevna Mashkova, Michail Evgenievich Givargizov
  • Patent number: 6428621
    Abstract: A low defect (e.g., dislocation and micropipe) density silicon carbide (SiC) is provided as well as an apparatus and method for growing the same. The SiC crystal, growing using sublimation techniques, is preferably divided into two stages of growth. During the first stage of growth, the crystal grows in a normal direction while simultaneously expanding laterally. Although dislocation and other material defects may propagate within the axially grown material, defect propagation and generation in the laterally grown material are substantially reduced, if not altogether eliminated. After the crystal has expanded to the desired diameter, the second stage of growth begins in which lateral growth is suppressed and normal growth is enhanced. A substantially reduced defect density is maintained within the axially grown material that is based on the laterally grown first stage material.
    Type: Grant
    Filed: February 14, 2001
    Date of Patent: August 6, 2002
    Assignee: The Fox Group, Inc.
    Inventors: Yury Alexandrovich Vodakov, Mark Grigorievich Ramm, Evgeny Nikolaevich Mokhov, Alexandr Dmitrievich Roenkov, Yury Nikolaevich Makarov, Sergei Yurievich Karpov, Mark Spiridonovich Ramm, Heikki I. Helava
  • Patent number: 6372981
    Abstract: A group-IV semiconductor substrate has an inclined front surface, the inclination being toward a direction differing from the <010>crystal lattice direction. The substrate is cleansed by heating in the presence of a gas including a compound of the group-IV substrate element. A source gas of a group-III element is then supplied, forming an atomic film of the group-III element on the substrate surface. Starting at the same time, or shortly afterward, a source gas of a group-V element is supplied, and a III-V compound semiconductor hetero-epitaxial layer is grown. Chemical bonding of the group-III element to the group-IV substrate surface produces a crystal alignment of the hetero-epitaxial layer that leads to improved conversion efficiency when the semiconductor substrate is used in the fabrication of solar cells with compound semiconductor base and emitter layers.
    Type: Grant
    Filed: August 8, 2000
    Date of Patent: April 16, 2002
    Assignee: Oki Electric Industry Co., Ltd.
    Inventors: Takashi Ueda, Chouho Yamagishi, Osamu Goto
  • Patent number: 6329070
    Abstract: The periodic stress and strain fields produced by a pure twist grain boundary between two single crystals bonded together in the form of a bicrystal are used to fabricate a two-dimensional surface topography with controllable, nanometer-scale feature spacings (e.g., from 50 nanometers down to 1.5 nanometers). The spacing of the features is controlled by the misorientation angle used during crystal bonding. One of the crystals is selected to be thin, on the order of 5-100 nanometers. A buried periodic array of screw dislocations is formed at the twist grain boundary. To bring the buried periodicity to the surface, the thin single crystal is etched to reveal an array of raised elements, such as pyramids, that have nanometer-scale dimensions. The process can be employed with numerous materials, such as gold, silicon and sapphire. In addition, the process can be used with different materials for each crystal such that a periodic array of misfit dislocations is formed at the interface between the two crystals.
    Type: Grant
    Filed: December 7, 2000
    Date of Patent: December 11, 2001
    Assignee: Cornell Research Foundation, Inc.
    Inventors: Stephen L. Sass, Christopher K. Ober, Yuri Suzuki
  • Patent number: 6312819
    Abstract: A thin film structure is provided including a silicon substrate with a layer of silicon dioxide on a surface thereof, and a layer of cubic oxide material deposited upon the layer of silicon dioxide by ion-beam-assisted-deposition, said layer of cubic oxide material characterized as biaxially oriented. Preferably, the cubic oxide material is yttria-stabilized zirconia. Additional thin layers of biaxially oriented ruthenium oxide or lanthanum strontium cobalt oxide are deposited upon the layer of yttria-stabilized zirconia. An intermediate layer of cerium oxide is employed between the yttria-stabilized zirconia layer and the lanthanum strontium cobalt oxide layer. Also, a layer of barium strontium titanium oxide can be upon the layer of biaxially oriented ruthenium oxide or lanthanum strontium cobalt oxide.
    Type: Grant
    Filed: May 26, 1999
    Date of Patent: November 6, 2001
    Assignee: The Regents of the University of California
    Inventors: Quanxi Jia, Paul N. Arendt
  • Patent number: 6224666
    Abstract: A cylindrical alkali halide melt-grown single-crystal-type ingot is axially compressed in a heated dual-platen press while in a plastic state. The ingot is located mid-way between two parallel, planar, vertically extending barriers. By properly orienting the platens and the barriers with respect to the crystal lattice structure of the ingot, the ingot can be forged into a rectangular block that is not only devoid of peripheral cracks and fissures but that also has more uniform properties even when impurities and activator (Tl, in the case of NaI(Tl)) are not uniformly distributed within the initial single-crystal ingot.
    Type: Grant
    Filed: June 15, 1999
    Date of Patent: May 1, 2001
    Assignee: Siemens Medical Systems, Inc.
    Inventors: Robert S. Zwolinski, Lev G. Eidelman
  • Patent number: 6217650
    Abstract: In an epitaxial-wafer fabricating process for epitaxially growing a silicon layer on the surface of a silicon wafer having the crystal orientation <100> or <111> and an inclination angle of 0°±1° in a reactive gas at a atmosphereicpressure, a growth temperature T is lower than a normal growth temperature by 50° C. to 100° C. during the process of epitaxial growth.
    Type: Grant
    Filed: June 15, 1999
    Date of Patent: April 17, 2001
    Assignee: Komatsu Electronic Metals Co., Ltd.
    Inventors: Takeshi Hirose, Hiroyuki Kawahara, Takeo Tamura, Masayoshi Danbata
  • Patent number: 6210477
    Abstract: The present invention relates to methods for pulling a single crystal wherein the induction of dislocation can be inhibited and a single crystal can be held safely. An apparatus for pulling a single crystal having a straightening vane in the shape of an inverted truncated cone whose upper and lower planes are removed, which is located between a crucible and a single crystal, is used. The gap between the lower end portion of the straightening vane and the surface of a melt filled into the crucible can be selected in the range of 30-200 mm. Where the gap is set large in the range of 30-200 mm, the temperature of the front portion of a seed crystal is raised till the difference in temperature between the front portion thereof and the melt (the range of 1380-1480° C.) becomes almost zero. The seed crystal is brought into contact with the melt, a neck is formed with being heated, and a main body is pulled from the melt.
    Type: Grant
    Filed: December 22, 1998
    Date of Patent: April 3, 2001
    Assignee: Sumitomo Metal Industries, Ltd.
    Inventors: Teruo Izumi, Hideki Watanabe
  • Patent number: 6171393
    Abstract: A seed crystal 1 for manufacturing a single crystal incorporating an unconformity portion B formed at a predetermined position apart from a leading end thereof and structured to conduct the heat of melt and interrupt propagation of dislocation caused from thermal stress produced when dipping in the melt has been performed.
    Type: Grant
    Filed: February 17, 1999
    Date of Patent: January 9, 2001
    Assignee: Komatsu Electronic Metals Co., Ltd.
    Inventors: Shoei Kurosaka, Junsuke Tomioka, Masakazu Kobayashi, Shuji Onoue, Tsuyoshi Sadamatsu
  • Patent number: 6159284
    Abstract: A process and a device will produce a cylindrical single crystal of semicuctor material with the smallest possible alignment error of the crystal lattice. A process for cutting semiconductor wafers from two or more such single crystals is by means of wire sawing. The process for producing the single crystal is as follows: (a) a single crystal with an alignment error of the crystal lattice equal to at most 1.5.degree.
    Type: Grant
    Filed: May 25, 1999
    Date of Patent: December 12, 2000
    Assignee: Wacker Siltronic Gesellschaft fur Halbleitermaterialien AG
    Inventors: Hans Olkrug, Holger Lundt, Christian Andrae, Josef Frumm
  • Patent number: 6159285
    Abstract: A new ingot of a desired orientation formed from an original ingot of a different orientation by cutting the new ingot from within the original ingot. In one aspect, to form a <110> ingot from a <100> ingot, a {110} flat is formed on the <100> ingot. The flat is used as a reference for cutting the <100> ingot. The <100> ingot is cut into sections by cutting in a plane perpendicular to the <100> ingot's longitudinal axis and to the flat. A <110> ingot can be formed by grinding a section of the <100> ingot to form a new cylinder. The new cylinder has a longitudinal axis which is perpendicular to the <100> ingot's longitudinal axis and to the flat. The resulting cylinder is a <110> ingot.
    Type: Grant
    Filed: May 6, 1999
    Date of Patent: December 12, 2000
    Assignee: Virginia Semiconductor, Inc.
    Inventors: Marshall P. Toombs, Thomas G. Digges, Jr.
  • Patent number: 6120602
    Abstract: An apparatus and a method for producing single crystal semiconductor particulate in near spherical shape and the particulate product so formed is accomplished by producing uniform, monosized, near spherical droplets; identifying the position of an undercooled droplet in a nucleation zone; and seeding the identified droplet in the nucleation zone to initiate single crystal growth in the droplet.
    Type: Grant
    Filed: December 28, 1999
    Date of Patent: September 19, 2000
    Assignee: Starmet Corporation
    Inventors: Matthew D. Stephens, Steven A. Miller, Jessica Belcher
  • Patent number: 6096129
    Abstract: An initial single-crystalline diamond base material is prepared from a flat plate having a major surface and side surfaces consisting of low-index planes. Then, single crystalline diamond is homoepitaxially vapor-deposited on the single-crystalline diamond base material, and a resulting diamond material is cut and polished in a particular manner to provide a successive base material on which single-crystalline diamond is again grown, thereby forming a single-crystalline diamond having a large area. A holder for the single-crystalline diamond base material consists of or is coated with a material hardly forming a compound with carbon. Single crystalline diamond can be stably formed on the surfaces of the base material. Consequently, single-crystalline diamond of high quality having a large area can be stably produced in a shorter time using either plasma CVD or a thermal filament method.
    Type: Grant
    Filed: April 15, 1998
    Date of Patent: August 1, 2000
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Hirohisa Saito, Takashi Tsuno, Takahiro Imai, Yoshiaki Kumazawa
  • Patent number: 6090202
    Abstract: A method and apparatus for hydrothermally growing crystals in a pressure vessel containing feed crystals immersed in a mineralizing solution. The apparatus is disposed in the pressure vessel, above the mineralizing solution. The apparatus includes an enclosure having opposing major walls with passages extending therethrough. The enclosure completely surrounds a seed plate having opposing major faces. A restraining structure holds the seed plate within the enclosure such that the major faces of the seed plate are spaced inwardly from the major walls.
    Type: Grant
    Filed: April 29, 1998
    Date of Patent: July 18, 2000
    Assignee: Sawyer Research Products, Inc.
    Inventor: Vladimir A. Klipov
  • Patent number: 6086670
    Abstract: An n-type wafer is provided having a <111> crystal axis in which the resistivity distribution in the surface of the wafer is uniform. The wafer is suitable for use in, e.g., a zener diode. A method is provided for growing a single crystal of n-type silicon doped with a group V element such as phosphorus using the Czochralski method or the floating zone melting (FZ) method wherein the center axis of the silicon single crystal is tilted by a tilt angle of 1-6 degrees from the <111> crystal axis. The silicon single crystal is sliced obliquely at the angle corresponding to the tilt angle to yield an n-type wafer having a <111> crystal axis.
    Type: Grant
    Filed: December 21, 1998
    Date of Patent: July 11, 2000
    Assignee: Sumitomo Sitix Corporation
    Inventor: Makoto Ito
  • Patent number: 6074476
    Abstract: A system and method for forming spherical semiconductor crystals is disclosed. The system includes a receiver tube 18 for receiving semiconductor granules 104. The granules are then directed to a chamber 14 defined within an enclosure 20. The chamber maintains a heated, inert atmosphere with which to melt the semiconductor granules into a molten mass. A nozzle, 40, creates droplets from the molten mass, which then drop through a long drop tube 16. As the droplets move through the drop tube, they form spherical shaped semiconductor crystals 112. The drop tube is heated and the spherical shaped semiconductor crystals may be single crystals. An inductively coupled plasma torch positioned between the nozzle and the drop tube melts the droplets, but leaving a seed in-situ. The seed can thereby facilitate crystallization.
    Type: Grant
    Filed: December 10, 1998
    Date of Patent: June 13, 2000
    Assignee: Ball Semiconductor, Inc.
    Inventors: Murali Hanabe, Nainesh J. Patel, Evangellos Vekris
  • Patent number: 6045611
    Abstract: An LiGaO.sub.2 single crystal manufactured by the Czochralski method has a crystallographic axis as a pulling direction set within an angle range of 30.degree. from a b- or a-axis direction. An LiGaO.sub.2 single-crystal substrate and a method of manufacturing the single crystal and the substrate are also disclosed.
    Type: Grant
    Filed: January 27, 1998
    Date of Patent: April 4, 2000
    Assignee: Nippon Telegraph and Telephone Corporation
    Inventors: Takao Ishii, Shintaro Miyazawa, Yasuo Tazou
  • Patent number: 6039803
    Abstract: A method of processing semiconductor materials, including providing a monocrystalline silicon substrate having a (001) crystallographic surface orientation; off-cutting the substrate to an orientation from about 2.degree. to about 6.degree. offset towards the [110] direction; and epitaxially growing a relaxed graded layer of a crystalline GeSi on the substrate. A semiconductor structure including a monocrystalline silicon substrate having a (001) crystallographic surface orientation, the substrate being off-cut to an orientation from about 2.degree. to about 6.degree. offset towards the [110] direction; and a relaxed graded layer of a crystalline GeSi which is epitaxially grown on the substrate.
    Type: Grant
    Filed: February 27, 1997
    Date of Patent: March 21, 2000
    Assignee: Massachusetts Institute of Technology
    Inventors: Eugene A. Fitzgerald, Srikanth B. Samavedam
  • Patent number: 6001171
    Abstract: ST-cut and AT-cut quartz seed bodies (18,40) for quartz crystal synthesis and method (100) for making the same are disclosed. An extended quartz seed body (18) having an angle of about 42.75.degree. rotated about a X axis (20) from a +Z axis (22) to a -Y axis (24) and defining a ST-cut is provided and a quartz crystal bar (32) is grown thereupon. Analogously, an extended quartz seed body (40) having an angle of about 35.25.degree. rotated about a X axis (20) from a +Z axis (22) to a -Y axis (24) and defining an AT-cut is provided and a quartz crystal bar (48) is grown thereupon. In each case, the subsequent quartz crystal bar (32,48) may be wafered parallel to the seed body (18,40) thereby; reducing waste (68), recovering the seed body (18,40) for reuse, producing wafers (70) without intervening seed portions, and increasing factory capacity.
    Type: Grant
    Filed: December 15, 1997
    Date of Patent: December 14, 1999
    Assignee: CTS Corporation
    Inventors: Joseph F. Balascio, Thien T. Nguyen, David J. Weary, Theodore E. Lind
  • Patent number: 5968261
    Abstract: An apparatus for growing single-polytype, single crystals of silicon carbide utilizing physical vapor transport as the crystal growth technique. The apparatus has a furnace which has a carbon crucible with walls that border and define a crucible cavity. A silicon carbide source material provided at a first location of the crucible cavity, and a monocrystalline silicon carbide seed is provided at a second location of the crucible cavity. A heat path is also provided in the furnace above the crucible cavity. The crucible has a stepped surface that extends into the crucible cavity. The stepped surface has a mounting portion upon which the seed crystal is mounted. The mounting portion of the stepped surface is bordered at one side by the crucible cavity and is bordered at an opposite side by the furnace heat path. The stepped surface also has a sidewall that is bordered at one side by and surrounds the furnace heat path.
    Type: Grant
    Filed: April 21, 1997
    Date of Patent: October 19, 1999
    Assignee: Northrop Grumman Corporation
    Inventors: Donovan L. Barrett, Raymond G. Seidensticker, deceased, Richard H. Hopkins
  • Patent number: 5964944
    Abstract: An easy and low-cost method of producing a large-size and high-purity silicon carbide (SiC) single crystal includes reacting silicon vapor directly with a carbon-containing compound gas under a heated atmosphere (growth space 14) to grow a silicon carbide single crystal (15) on a silicon carbide seed crystal (12), in which the silicon vapor generated from molten silicon (13) is used as a silicon vapor source, and a hydrocarbon gas (9) (e.g., propane gas) is used as the carbon-containing compound gas.
    Type: Grant
    Filed: March 21, 1997
    Date of Patent: October 12, 1999
    Assignee: Kabushiki Kaisha Toyota Chuo Kenkyusho
    Inventors: Naohiro Sugiyama, Atsuto Okamoto, Toshihiko Tani, Nobuo Kamiya
  • Patent number: 5962915
    Abstract: Improved commercial single crystal wafers (250), as shipped to end users form a full circle, and comprise a "stress concentration notch" (172) which accurately defines a desired cleavage plane. The stress concentration notch is introduced into the wafers in bulk by means of a properly oriented cut along the length of a single crystal ingot, after machining the ingot to the desired end product diameter, and prior to sawing the ingot into slices. The stress concentration notch uniquely defines the first and second faces of the wafer.
    Type: Grant
    Filed: October 14, 1997
    Date of Patent: October 5, 1999
    Assignee: Anerkan Xtal Technology, Inc
    Inventors: Gary Shen-Cheng Young, Shan-Xiang Zhang
  • Patent number: 5951756
    Abstract: A method of forming GaAs/AlGaAs hetero-structure. The method includes the steps of preparing a GaAs substrate having a (411)A-oriented surface and setting the GaAs substrate inside a growth container with the (411)A surface being disposed as a surface to be deposited. The pressure inside the growth chamber is reduced and the GaAs substrate is heated up to a predetermined temperature to cause epitaxial growth of Ga, Al, As on the (411)A substrate and forming a GaAs/AlGaAs hetero-structure on the (411)A-oriented GaAs substrate.
    Type: Grant
    Filed: February 13, 1996
    Date of Patent: September 14, 1999
    Assignee: Kubota Corporation
    Inventors: Satoshi Hiyamizu, Satoshi Shimomura, Yasunori Okamoto
  • Patent number: 5932002
    Abstract: In a conventional method for pulling a single crystal, in order to exclude the dislocation induced in contact of a seed crystal with a melt, a neck having a small diameter has been formed. But when a heavy single crystal having a large diameter of 12 inches or so is pulled, it is impossible to hold the single crystal, leading to the falling. When the diameter of the neck is made larger in order to prevent the falling, the dislocation cannot be excluded, leading to the propagation of the dislocation to the single crystal. In the present invention, using a seed crystal having a cylindrical body and a conical front portion, the induction of the dislocation is inhibited by making the temperature of the front portion almost the same as the temperature of the melt when the front portion of the seed crystal is brought into contact with the melt and a single crystal is pulled without forming a neck after melting part of the front portion into the melt.
    Type: Grant
    Filed: August 28, 1997
    Date of Patent: August 3, 1999
    Assignee: Sumitomo Sitix Corporation
    Inventor: Teruo Izumi
  • Patent number: 5893948
    Abstract: The invention provides a method for forming a plurality of single silicon crystals over a substrate. The method forms a plurality of nucleation sites over the substrate. An amorphous silicon layer is formed over the substrate covering the plurality of silicon nucleation sites. The amorphous silicon layer is melted by using a laser beam and then crystallized to form the plurality of single silicon crystals. Each of the plurality of single silicon crystals correspond to one of the plurality of nucleation sites.
    Type: Grant
    Filed: April 5, 1996
    Date of Patent: April 13, 1999
    Assignee: Xerox Corporation
    Inventors: Norbert H. Nickel, Gregory B. Anderson, Steven E. Ready, James B. Boyce, Ping Mei
  • Patent number: 5891240
    Abstract: A radio frequency automatic identification system detects targets which include solid resonators resonating at several frequencies, attributing information to the frequencies at which the target resonates. Preferred resonators are quartz crystals, which may be made by a process of heating quartz to soften it and cutting crystals to approximate size and resonant frequency. Resonators produced by such a process are measured to determine their actual resonant frequency, and preferably the crystals are sorted into predetermined frequency windows in accordance with their measured resonant frequency. A set of resonators having frequencies corresponding to predetermined data is selected from the sorted groups of resonators and incorporated into a target. The preferred target is an ink-like material having a plurality of resonators disposed in a matrix which is radio frequency transparent at the frequency of interest.
    Type: Grant
    Filed: April 27, 1995
    Date of Patent: April 6, 1999
    Assignee: Gordian Holding Corporation
    Inventor: Morton Greene
  • Patent number: 5885344
    Abstract: A non-Dash neck method of preparing a single crystal silicon rod, pulled in accordance with the Czochralski method. The process is characterized in that a large diameter, dislocation-free seed crystal is allowed to thermally equilibrate prior to initiation of silicon rod growth, in order to avoid the formation of dislocations resulting from thermal shock to the crystal. The process is further characterized in that a resistance heater is used to melt the lower tip of the seed crystal to form a molten cap before it is brought into contact with the melt. The process yields a single crystal silicon rod having a short, large diameter neck which is dislocation-free, and which is capable of supporting a silicon rod which weighs at least about 100 kilograms during growth and subsequent handling.
    Type: Grant
    Filed: August 8, 1997
    Date of Patent: March 23, 1999
    Assignee: MEMC Electronic Materials, Inc.
    Inventors: Kyong-Min Kim, Sadasivam Chandrasekhar
  • Patent number: 5851284
    Abstract: According to the process of the present invention for producing a garnet single crystal fiber, a crystal is grown while the direction of a seed crystal, corresponding to the direction of growth, is set in a direction having angles of at least 10.degree. from a direction equivalent to the <100> orientation, at least 20.degree. from a direction equivalent to the <110> orientation and at least 20.degree. from a direction equivalent from the <211> orientation. The resulting garnet single crystal fiber does not include a core, which is formed due to facet formation, and has an excellent optical homogeneity necessary for use in an optical device such as a laser device or an isolator.
    Type: Grant
    Filed: November 18, 1996
    Date of Patent: December 22, 1998
    Assignee: Nippon Telegraph and Telephone Corporation
    Inventors: Shigeo Ishibashi, Itaru Yokohama, Yuzo Ishida, Kazunori Naganuma
  • Patent number: 5840117
    Abstract: A method for surface flattening a crystal substrate includes (a) processing a surface of a silicon single crystal substrate, the surface deviating by 0.1.degree. or less from the (001) plane, so as to form a processed zone thereon which is an obstacle to the movement of surface steps present on the surface of the silicon single crystal substrate and which is adjacent to a preselected region having a surface to be flattened when viewed on an atomic level; (b) holding the substrate processed in step (a) in a chamber having an adjustable degree of vacuum so that the substrate has a temperature which is controlled by direct-current passage and heating; and (c) heating the substrate to move the surface steps along the substrate from the preselected region and gather the surface steps in the processed zone, thereby forming a flat surface in the preselected region of the substrate when viewed on the atomic level.
    Type: Grant
    Filed: August 23, 1996
    Date of Patent: November 24, 1998
    Assignee: Agency of Industrial Science & Technology
    Inventors: Kunihiro Sakamoto, Atsushi Ando
  • Patent number: 5833749
    Abstract: A compound semiconductor substrate having at least one compound semiconductor layer epitaxially grown on a silicon single crystal substrate, wherein the silicon single crystal substrate has a surface on which the compound semiconductor layer is epitaxially grown, the surface being inclined at an off angle of not more than 1 deg to a (100) plane of silicon crystal; and the compound semiconductor layer has a free or top surface having a roughness of 3 nm or less in terms of a mean square roughness, Rms, determined by an atomic force microscopic measurement in a view field area of 10 .mu.m.times.10 .mu.m or a roughness of 10.5 nm or less in terms of a maximum height difference, Ry.
    Type: Grant
    Filed: January 16, 1996
    Date of Patent: November 10, 1998
    Assignee: Nippon Steel Corporation
    Inventors: Akihiro Moritani, Aiji Yabe, Akiyoshi Tachikawa, Takashi Aigo
  • Patent number: 5803965
    Abstract: A method and system for manufacturing a semiconductor device having a semiconductor layer using a pulsed laser includes the steps of generating a laser beam using a solid laser source, generating a multi-harmonic wave from the laser beam using a multi-harmonic oscillator, filtering the multi-harmonic wave, and irradiating the filtered wave onto the semiconductor layer.
    Type: Grant
    Filed: August 13, 1996
    Date of Patent: September 8, 1998
    Assignee: LG Electronics, Inc.
    Inventor: Jung Kee Yoon
  • Patent number: 5792566
    Abstract: Improved commercial single crystal wafers (250), as shipped to end users form a full circle, and comprise a "stress concentration notch" (172) which accurately defines a desired cleavage plane. The stress concentration notch is introduced into the wafers in bulk by means of a properly oriented cut along the length of a single crystal ingot, after machining the ingot to the desired end product diameter, and prior to sawing the ingot into slices. The stress concentration notch uniquely defines the first and second faces of the wafer.
    Type: Grant
    Filed: July 2, 1996
    Date of Patent: August 11, 1998
    Assignee: American Xtal Technology
    Inventors: Gary Shen-Cheng Young, Shan-Xiang Zhang
  • Patent number: 5785752
    Abstract: Proposed is an improvement in the method for the preparation of a chip of an oxide garnet film epitaxially having a specific chemical composition as grown on the surface of a GGG substrate wafer having a crystallographic plane orientation of (111), which is useful as a working element in a magnetostatic wave device such as high-frequency filters, signal noise enhancers, isolators and the like with decreased temperature dependence of the properties. The epitaxially grown single crystal film is adjusted to have such dimensions that the thickness h and the smallest dimension L within the plane of the film satisfy the relationship that the ratio h/L is in the range from 0.001 to 0.25.
    Type: Grant
    Filed: December 12, 1995
    Date of Patent: July 28, 1998
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Masayuki Tanno, Toshihiko Ryuo
  • Patent number: 5779790
    Abstract: In a method of manufacturing a silicon monocrystal using the Czochralski method, a seed crystal is brought into contact with silicon melt and is then pulled such that after a neck portion is formed, a silicon monocrystal is grown below the neck portion. The crystal has a hollow portion which has an opening in a contact surface of the seed crystal to be brought into contact with the silicon melt. Alternatively, the seed crystal has a hollow portion which will have an opening in the contact surface of the seed crystal when the contact surface is brought into contact with the silicon melt. Use of such seed crystals makes it possible to increase the strength of the neck portion and to pull a heavy and long silicon monocrystal having a large diameter.
    Type: Grant
    Filed: March 10, 1997
    Date of Patent: July 14, 1998
    Assignee: Shin-Etsu Handotai Co., Ltd.
    Inventors: Toshinari Murai, Naoki Nagai
  • Patent number: 5769941
    Abstract: A seed (22) is formed to have a ?110! direction (24) that is at an angle (26) to the pull direction (23) used for growing a semiconductor ingot (36). Dislocations (34) in the ingot (36) terminate on the surface of the neck (37) of the ingot, and do not propagate into the body (38) of the ingot (36).
    Type: Grant
    Filed: May 1, 1996
    Date of Patent: June 23, 1998
    Assignee: Motorola, Inc.
    Inventor: Herng-Der Chiou
  • Patent number: 5759264
    Abstract: A method for a vapor-phase growth of a GaAs.sub.1-x P.sub.x epitaxial layer having a uniform thickness is disclosed. This method allows the GaAs.sub.1-x P.sub.x epitaxial layer (wherein x stands for an alloy composition satisfying the expression, 0.ltoreq.x.ltoreq.1) to be formed on a plurality of semiconductor single crystal substrates 1 by setting the semiconductor single crystal substrates 1 in place on a wafer holder 16 disposed inside a vapor-phase growth apparatus 30 in an amount of not less than 70% as the covering ratio of the total surface area of the substrates to the surface area of the wafer holder 16.
    Type: Grant
    Filed: March 21, 1996
    Date of Patent: June 2, 1998
    Assignee: Shin-Etsu Handotai Co., Ltd.
    Inventors: Masataka Watanabe, Tsuneyuki Kaise, Masayuki Shinohara, Masahisa Endo
  • Patent number: 5753555
    Abstract: A method is provided for forming an epitaxial silicon layer on a diffused region of a silicon substrate having an anisotropic ratio of more than 3:1 between the growth rate in the direction perpendicular to the substrate surface and the growth rate in the direction parallel to the substrate surface. The epitaxial silicon layer serves as a contact plug which does not contact an adjacent contact plug formed by the same process in order to obtain a reliable semiconductor memory device with a high throughput, which is free from short circuit failure.
    Type: Grant
    Filed: October 24, 1996
    Date of Patent: May 19, 1998
    Assignee: NEC Corporation
    Inventor: Hiromitsu Hada
  • Patent number: 5716450
    Abstract: In a method of growing a gallium nitride related compound semiconductor crystal on a single crystal substrate, the {011} plane or the {101} plane of rare earth group 13 (3B) perovskite is used as the single crystal substrate. As a result, a gallium nitride group semiconductor crystal excellent in crystallinity can be grown epitaxially.
    Type: Grant
    Filed: December 6, 1995
    Date of Patent: February 10, 1998
    Assignee: Japan Energy Corporation
    Inventors: Seiji Togawa, Hitoshi Okazaki
  • Patent number: 5714005
    Abstract: ST-cut and AT-cut quartz seed bodies (18,40) for quartz crystal synthesis and method for making the same are disclosed. An extended quartz seed body (18) having an angle of about 42.75.degree. rotated about a X axis (20) from a +Z axis (22) to a -Y axis (24) and defining a ST-cut is provided and a quartz crystal bar (32) is grown thereupon. Analogously, an extended quartz seed body (40) having an angle of about 35.25.degree. rotated about a X axis (20) from a +Z axis (22) to a -Y axis (24) and defining an AT-cut is provided and a quartz crystal bar (48) is grown thereupon. In each case, the subsequent quartz crystal bar (32,48) may be wafered parallel to the seed body (18,40) thereby; reducing waste (68), recovering the seed body (18,40) for reuse, producing wafers (70) without intervening seed portions, and increasing factory capacity.
    Type: Grant
    Filed: December 20, 1995
    Date of Patent: February 3, 1998
    Assignee: Motorola Inc.
    Inventors: Joseph F. Balascio, Thien T. Nguyen, David J. Weary, Theodore E. Lind