Abstract: A method for heat treating a powder metallurgy nickel-base alloy article comprises placing the article in a furnace at a start temperature in the furnace that is 80° C. to 200° C. below a gamma prime solvus temperature, and increasing the temperature in the furnace to a solution temperature at a ramp rate in the range of 30° C. per hour to 70° C. per hour. The article is solution treated for a predetermined time, and cooled to ambient temperature.

Abstract: A method of additively manufacturing is provided. The method may include successively depositing and fusing together layers of a superalloy powder mixture comprised of a base material powder and a eutectic powder, to build up an additive portion, which eutectic powder has a solidus temperature lower than the solidus temperature of the base material powder. The method may also include heat treating the additive portion at a temperature greater than 1200° C. to heal cracks and/or fill pores and to homogenize the alloy of which the additive portion is comprised. The additive portion alloy has a chemistry defined by the superalloy powder mixture. The base material powder may be formed of a nickel-base superalloy with an aluminum content by weight of at least 1.5%. The eutectic powder may be a nickel-base alloy including by weight about 6% to about 11% chromium, about 5% to about 9% titanium, and about 9% to about 13% zirconium, with balance nickel as its primary components.

Abstract: Disclose is a copper alloy for a laser cladding valve seat. the copper alloy may include an amount of about 15.0 to 25.0 wt % of Ni, an amount of about 1.0 to 4.0 wt % of Si, an amount of about 0.5 to 1.0 wt % of B, an amount of about 1.0 to 2.0 wt % of Cr, an amount of about 5.0 to 15.0 wt % of Co, an amount of about 2.0 to 20.0 wt % of Mo, an amount of about 0.1 to 0.5 wt % of Ti and the balance Cu, all the wt % based on the total weight of the copper alloy. Particularly, the copper alloy may not include Fe, and may include Ti silicacide. Further disclosed is a laser cladding valve seat including the copper alloy, which does not generate cracks and is excellent in wear resistance.

Abstract: Heat treatment of an Alloy 282 which has been subjected to an initial solution annealing followed by cooling can be heat treated by heating the Alloy 282 to a temperature between 954° C. and 1010° C. until the gamma prime (??) phase is sufficiently dissolved, and cooling the Alloy 282 to a temperature a sufficiently low temperature, and at a sufficiently high cooling rate, to suppress gamma prime precipitation. A component such as a turbine exhaust case and a gas turbine engine made of said alloy can be heat treated in the above manner.

Abstract: The disclose relates to ordered Alloy 690 comprising: a matrix that includes a short range order (SRO) in a state in which nickel (Ni) is enriched, and chromium (Cr) and iron (Fe) are depleted, and the ordered Alloy 690 is characterized by having excellent resistance to stress corrosion cracking and improved thermal conductivity due to agglomeration of nickel (Ni) atoms, as compared with the unordered Alloy 690.

Abstract: The present invention relates to a method for manufacturing Alloy 690 ordered alloy to be used in a steam generator tube serving as a heat exchanger in a nuclear power plant (hereinafter, referred to as NPP), and Alloy 690 ordered alloy manufactured thereby, and provides a method for manufacturing Alloy 690 ordered alloy with improved thermal conductivity, and Alloy 690 ordered alloy manufactured thereby, the method comprising the steps of: solution-annealing Alloy 690; cooling the solution-annealed Alloy 690 to a first temperature of 200° C./min or less; and ordering the cooled Alloy 690 in the temperature range of 410-520° C.

Abstract: A method for recycling a Ni-based single crystal superalloy part or unidirectionally solidified superalloy part provided with a thermal barrier coating containing at least a ceramic on a surface of a Ni-based single crystal superalloy substrate or Ni-based unidirectionally solidified superalloy substrate, in which the method including the steps of: melting and desulfurizing a Ni-based single crystal superalloy part or Ni-based unidirectionally solidified superalloy part at a temperature of the melting point or more of the Ni-based single crystal superalloy or Ni-based unidirectionally solidified superalloy and less than the melting point of the ceramic; heating a casting mold for a recycled Ni-based single crystal superalloy part or casting mold for a recycled Ni-based unidirectionally solidified superalloy part to a temperature of the melting point or more of the Ni-based single crystal superalloy or Ni-based unidirectionally solidified superalloy; pouring the desulfurized melted Ni-based single crystal supe

Abstract: Methods for processing bonded dual alloy rotors are provided. In one embodiment, the method includes obtaining a bonded dual alloy rotor including rotor blades bonded to a hub disk. The rotor blades and hub disk are composed of different alloys. A minimum processing temperature (TDISK_PROCESS_MIN) for the hub disk and a maximum critical temperature for the rotor blades (TBLADE_MAX) is established such that TBLADE_MAX is less than TDISK_PROCESS_MIN. A differential heat treatment process is then performed during which the hub disk is heated to processing temperatures equal to or greater than TDISK_PROCESS_MIN, while at least a volumetric majority of each of the rotor blades is maintained at temperatures below TBLADE_MAX. Such a targeted differential heat treatment process enables desired metallurgical properties (e.g., precipitate hardening) to be created within the hub disk, while preserving the high temperature properties of the rotor blades and any blade coating present thereon.

Abstract: The present invention relates to ordered Alloy 690 with improved thermal conductivity. By maintaining Alloy 690 in a temperature range of 350-570° C. for a proper amount of time, the atomic arrangement is controlled to properly form the ordered phases. The ordered phases formed in the ordered Alloy 690 increases its thermal conductivity due to a low thermal scattering effect of the ordered phase as observed in pure metals.

Abstract: A heat treatment technique may include heating an alloy component to a temperature above a transition temperature of the alloy or heating an alloy component to a temperature below the transition temperature of the alloy. The heat treatment technique further may include cooling a first portion of the alloy component at a first cooling rate, and cooling a second portion of the alloy component at a second cooling rate different than the first rate. The first cooling rate may result in formation of a plurality of first precipitate phase domains comprising a first average size in the first portion, and the second cooling rate may result in formation of a plurality of second precipitate phase domains comprising a second average size in the second portion. The average size of the first precipitate phase domains may be different than the average size of the second precipitate phase domains.

Abstract: A pre-weld heat treatment of the nickel based superalloy including heating a nickel based superalloy (e.g., IN939) casting to 2120° F. at a rate of 2° F. per minute, and then soaking the casing for one hour at 2120° F. The casting is then cooled in stages including slowly cooling the casting at a rate of 1° F. per minute to about 1900° F. and holding at that temperature for about 10 minutes. Then the casting is further slowly cooled at a rate of 1° F. per minute to about 1800° F. and holding at that temperature for about 10 minutes, and further slowly cooled to a temperature range of 1650° F. to 1450° F., and then fast cooled to room temperature. The pre-weld heat treatment may optionally include a step of heating the casting to about 1850° F. at a rate of 50° F. per minute before slowly heating to 2120° F.

Abstract: A method of in-situ reconditioning a heat exchanger includes the steps of: providing an in-service heat exchanger comprising a precipitate-strengthened alloy wherein at least one mechanical property of the heat exchanger is degraded by coarsening of the precipitate, the in-service heat exchanger containing a molten salt working heat exchange fluid; deactivating the heat exchanger from service in-situ; in a solution-annealing step, in-situ heating the heat exchanger and molten salt working heat exchange fluid contained therein to a temperature and for a time period sufficient to dissolve the coarsened precipitate; in a quenching step, flowing the molten salt working heat-exchange fluid through the heat exchanger in-situ to cool the alloy and retain a supersaturated solid solution while preventing formation of large precipitates; and in an aging step, further varying the temperature of the flowing molten salt working heat-exchange fluid to re-precipitate the dissolved precipitate.

Abstract: Methods of forming dual microstructure components include consolidating a powder material comprising an alloy to form a billet, the billet having a first grain structure, inductively heating the billet at an inductive heat treat temperature above a gamma prime solvus temperature of the alloy and subjecting the billet to a subsolvus heat treat temperature that is below the gamma prime solvus temperature of the alloy, waiting a period of time for the first grain structure in an outer portion of the billet to transform into a second grain structure that is coarser than the first grain structure, after the steps of inductively heating and subjecting the billet to the subsolvus heat treat temperature. The methods also include dividing the billet into at least two sections, and machining a final shape into one or more of the at least two sections to form the dual microstructure component.

Abstract: A single crystal casting having substantially improved high-temperature oxidation resistance, hot corrosion (sulfidation) resistance, and resistance to creep under high temperature and high stress is characterized by an as-cast composition comprising a maximum sulfur content of 0.5 ppm by weight, a maximum phosphorus content of 20 ppm by weight, a maximum nitrogen content of 3 ppm by weight, a maximum oxygen content of 3 ppm by weight, and a combined yttrium and lanthanum content of 5-80 pm by weight. It has been discovered that careful control of the deleterious impurities, particularly sulfur, phosphorus, nitrogen and oxygen, in combination with a carefully controlled addition of yttrium and/or lanthanum provides unexpected improvements in corrosion and oxidation resistance, while also enhancing high-temperature, high-stress resistance to creep, without any detrimental effects on other mechanical properties, processing or producability, particularly castability.

Abstract: A coated article having an improved coating oxidation life includes a superalloy substrate material having a composition which includes sulfur, herein the sulfur is present in an amount less than 1 ppm; and an overlay coating formed over a surface of the substrate material.

Abstract: A nickel-titanium-rare earth (Ni—Ti-RE) alloy comprises nickel at a concentration of from about 35 at. % to about 65 at. %, a rare earth element at a concentration of from about 1.5 at. % to about 15 at. %, boron at a concentration of up to about 0.1 at. %, with the balance of the alloy being titanium. In addition to enhanced radiopacity compared to binary Ni—Ti alloys and improved workability, the Ni—Ti-RE alloy preferably exhibits superelastic behavior. A method of processing a Ni—Ti-RE alloy includes providing a nickel-titanium-rare earth alloy comprising nickel at a concentration of from about 35 at. % to about 65 at. %, a rare earth element at a concentration of from about 1.5 at. % to about 15 at. %, the balance being titanium; heating the alloy in a homogenization temperature range below a critical temperature; and forming spheroids of a rare earth-rich second phase in the alloy while in the homogenization temperature range.

Abstract: A method of extending the useable life of a gas turbine component fabricated from a cobalt-based alloy is disclosed. The method includes applying a rejuvenation process to the alloy where the alloy is placed in a protected atmosphere and heated to three different elevated temperatures and held at the elevated temperatures for approximately four hours each. Application of the rejuvenation process allows gas turbine components to be returned to service for at least one more service interval of approximately 24,000 operating hours.

Abstract: A powder metallurgical article and process are disclosed. The article is a repaired or enlarged powder metallurgical article. The repaired or enlarged powder metallurgical article includes a formed article including a first alloy and a material including a second alloy. The material is welded to the formed article to form the repaired or enlarged powder metallurgical article. The repaired or enlarged powder metallurgical article includes a substantially uniform grain structure.

Abstract: Processes for fabricating components to have two or more regions with different grain structures, and components produced by such processes. First and second preforms are fabricated to comprise interface surfaces at which the preforms can be joined together. The first and second preforms are formed of first and second precipitation-strengthened alloys, respectively, and the first alloy differs from the second alloy by having a higher solvus temperature or a higher grain refiner content. The preforms are joined together to form an article comprising first and second portions formed by the first and second preforms, respectively, and corresponding to first and second regions of the component, respectively, and the interface surfaces of the preforms form a joint between the first and second portions of the article. A supersolvus heat treatment is performed on the article so that greater grain growth occurs in the second portion than in the first portion.

Abstract: A slurry and slurry coating process for forming a diffusion aluminide coating on a substrate, including internal surfaces within the substrate. The process involves preparing a slurry of a powder containing a metallic aluminum alloy having a melting temperature higher than aluminum, an activator capable of forming a reactive halide vapor with the metallic aluminum, and a binder containing an organic polymer. The slurry is applied to surfaces of the substrate, which is then heated to burn off the binder, vaporize and react the activator with the metallic aluminum to form the halide vapor, react the halide vapor at the substrate surfaces to deposit aluminum on the surfaces, and diffuse the deposited aluminum into the surfaces to form a diffusion aluminide coating. The process can be tailored to selectively produce an inward or outward-type coating. The binder burns off to form an ash residue that can be readily removed.

Abstract: A method for manufacturing a nonlinear superelastic file comprising the steps of: providing a superelastic file having a shaft and a file axis; providing a fixture including a file groove being defined by one or more displacement members, the file groove configured for receiving the shaft; inserting at least a portion of the shaft into the fixture along the file groove, the portion of the shaft including a first portion of the shaft; contacting the first portion of the shaft with a first displacement member of the one or more displacement members such that the first portion of the shaft is displaced from the file axis thereby forming a first offset portion of the shaft; heating the portion of the shaft while inserted in the fixture to a temperature of at least about 300° C. for a time period of at least about 1 minute to shape-set the portion of the shaft thereby forming a shape-set nonlinear file.

Abstract: Disclosed are a high-strength Ni-base alloy, a method of producing the Ni-base alloy, and a method of recovering a member made of a degraded Ni-base alloy. It contains not more than 0.1 wt % C, not more than 50 wt % Fe, not more than 30 wt % Cr, Ti, and at least one of Nb and Al. It has been strengthened by precipitates of a ?? phase (Ni3Al) and/or a ?? phase (Ni3Nb). It contains also a ? phase (Ni3Ti) which is thermodynamically stable in a temperature range of 800° C. to 900° C. When observed a cross-section of the Ni-base alloy, a plurality of nodes exist along each segment connecting two meeting points each of which point is defined by adjacent three crystal grains, and precipitates of the ?? phase and/or the ?? phase in each of crystal grains of the Ni-base alloy have an average particle size of not more than 100 nm.

Abstract: This document describes a process/strategy for age hardening nickel based alloys to create desirable properties with reduced energy expenditure. The inventive process introduces isolated atom nucleation sites to accelerate the nucleation rate by approximately 36 times, thereby permitting age hardening to occur in significantly less time and with significantly less energy expenditure.

Abstract: An alloy comprising 5 at %?Al<16 at %, about 0.05 at % to 1 at % of a reactive element selected from the group consisting of Hf, Y, La, Ce, Zr, and combinations thereof, and Ni, wherein the alloy composition has a predominately ?-Ni+??-Ni3Al phase constitution.

Abstract: A pre-weld heat treatment of the nickel based superalloy including heating a nickel based superalloy (e.g., IN939) casting to 2120° F. at a rate of 2° F. per minute, and then soaking the casing for one hour at 2120° F. The casting is then cooled in stages including slowly cooling the casting at a rate of 1° F. per minute to about 1900° F. and holding at that temperature for about 10 minutes. Then the casting is further slowly cooled at a rate of 1° F. per minute to about 1800° F. and holding at that temperature for about 10 minutes, and further slowly cooled to a temperature range of 1650° F. to 1450° F., and then fast cooled to room temperature. The pre-weld heat treatment may optionally include a step of heating the casting to about 1850° F. at a rate of 50° F. per minute before slowly heating to 2120° F.

Abstract: A method of heat treating a superalloy article is disclosed. The method includes hot-working an article comprising an superalloy to produce a hot-worked microstructure throughout the article; solution treating the article at a temperature and for a time sufficient to form a partially recrystallized warm-worked microstructure throughout the article; and cooling the article. The method also includes precipitation aging the article at a first precipitation aging temperature of about 1300° F. to about 1400° F. for a first duration of about 4 hours to about 12 hours; cooling the article to a second precipitation aging temperature; precipitation aging the article at a second precipitation aging temperature of about 1150° F. to about 1200° F. for a second duration of about 4 hours to about 12 hours; and cooling the article from the second precipitation aging temperature to an ambient temperature.

Abstract: A nickel powder with an average particle size of 0.05 to 1.0 ?m, which is composed of nickel particles having an oxidized surface layer and containing sulfur, wherein the sulfur content with respect to the total weight of the powder is 100 to 2000 ppm, and the intensity of a peak identified to sulfur bonded to nickel in surface analysis by ESCA of the nickel particles varies in a direction toward the center from the surface of the particles, and this intensity has its maximum at a location deeper than 3 nm from the particle outermost surface. This nickel powder is manufactured by bringing a nickel powder containing sulfur and dispersed in a non-oxidizing gas atmosphere into contact with an oxidizing gas at a high temperature.

Abstract: A heat treatment technique may include heating an alloy component to a temperature above a transition temperature of the alloy or heating an alloy component to a temperature below the transition temperature of the alloy. The heat treatment technique further may include cooling a first portion of the alloy component at a first cooling rate, and cooling a second portion of the alloy component at a second cooling rate different than the first rate. The first cooling rate may result in formation of a plurality of first precipitate phase domains comprising a first average size in the first portion, and the second cooling rate may result in formation of a plurality of second precipitate phase domains comprising a second average size in the second portion. The average size of the first precipitate phase domains may be different than the average size of the second precipitate phase domains.

Abstract: An intermetallic compound having excellent mechanical properties at high temperatures is provided. An intermetallic compound of the present invention contains greater than 5 at % and not greater than 13 at % of Al, not less than 9.5 at % and less than 17.5 at % of V, not less than 0 at % and not greater than 3.5 at % of Ti, not less than 0 weight ppm and not greater than 1000 weight ppm of B, and the remaining portion consisting of Ni and inevitable impurities, and having a dual multi-phase microstructure comprising a primary L12 phase and an (L12+D022) eutectoid microstructure.

Abstract: A method for controlling microbial growth in potable water stored in a vessel having a metallic surface includes heating the metallic surface to a temperature between about 480° C. (900° F.) and about 870° C. (1600° F.), exposing the metallic surface to oxygen during heating to oxidize potential reduction sites on the metallic surface and charging potable water containing silver ions to the vessel. A vessel having a metallic surface is prepared for long-term storage of potable water containing silver ions by heating the metallic surface to a temperature between about 480° C. (900° F.) and about 870° C. (1600° F.) and exposing the metallic surface to oxygen during heating to oxidize electropositive metals on the metallic surface or by treating the metallic surface with an aqueous solution containing on oxidizing agent to oxidize potential reduction sites on the metallic surface.

Abstract: A method for manufacturing a probed for an electrical test includes producing by a deposition technique a deposit including a probe main body portion made of a nickel-boron alloy and a probe tip portion projecting downward from the probe main body portion and made of a different conductive material from the probe main body portion. The method further includes annealing the deposit. The average grain diameter of the nickel-boron alloy is between 97 ? and 170 ?. The contained amount of boron is from 0.02 wt % to 0.20 wt %.

Abstract: Disclosed herein is a method of treating a component comprising solution treating the component for a period of about 4 to about 10 hours at a temperature of about 1750 to about 1850° F.; cooling the component to a temperature of about 1490 to about 1520° F. at an average rate of 1° F./min to about 25° F./min; stabilizing the component at about 1450 to about 1520° F. for a period of from about 1 to about 10 hours; cooling the component to room temperature; precipitation aging the component by heating the component to a first precipitation aging temperature of about 1275 to about 1375° F. for about 3 to about 15 hours; cooling the component at an average rate of 50 to about 150° F./hour to a second precipitation aging temperature of about 1100 to about 1200° F. for a time period of about 2 to about 15 hours; and cooling the component.

Abstract: Disclosed herein is a method of treating a component comprising solution treating the component for a period of about 4 to about 10 hours at a temperature of about 1750 to about 1850°F.; cooling the component to a temperature of about 1580 to about 1650°F. at an average rate of 1°F./min to about 25°F./min; stabilizing the component at about 1580 to about 1650°F. for a period of about 1 to about 10 hours; cooling the component to room temperature; precipitation aging the component at a first precipitation aging temperature of about 1275 to about 1375°F. for about 3 to about 15 hours; cooling the component at an average rate of 50 to about 150°F./hour to a second precipitation aging temperature of about 1100 to about 1200°F. for a time period of about 2 to about 15 hours; and cooling the component.

Abstract: A friction stir processing tool is formed from a Ni-based dual multi-phase intermetallic compound alloy containing rhenium(Re). The Ni-based dual multi-phase intermetallic compound alloy is preferably formed by casting, while gradually cooling, a melt containing all the components of the composition and is preferably heat treated after casting. Moreover, in a method for friction stir processing, a work is softened by friction heat generated when the friction stir processing tool, while rotating, is pressed against the work to be processed. The friction stir processing tool includes the Ni-based dual multi-phase intermetallic compound alloy, and therefore further high hardness is exhibited to improve abrasion resistance, so that even a long period of friction stir processing can be endured.

Abstract: A process and alloy for producing a turbine blade whose properties enable the blade to operate within a steam turbine at maximum operating temperatures of greater than 1300° F. (about 705° C.). The process includes casting the blade from a gamma prime-strengthened nickel-base superalloy having a composition of, by weight, 14.25-15.75% cobalt, 14.0-15.25% chromium, 4.0-4.6% aluminum, 3.0-3.7% titanium, 3.9-4.5% molybdenum, 0.05-0.09% carbon, 0.012-0.020% boron, maximum 0.5% iron, maximum 0.2% silicon, maximum 0.15% manganese, maximum 0.04% zirconium, maximum 0.015% sulfur, maximum 0.1% copper, balance nickel and incidental impurities, and an electron vacancy number of 2.32 maximum. The casting then undergoes a high temperature solution heat treatment to promote resistance to hold-time cracking. The blade exhibits a combination of yield strength, stress rupture properties, environmental resistance, and cost in steam turbine applications to 1400° F. (about 760° C.).

Abstract: The present invention provides a heat-resistant bearing characterized in that it is formed of an Ni3(Si,Ti)-based intermetallic compound alloy, the Ni3(Si,Ti)-based intermetallic compound alloy containing 25 to 500 ppm by weight of B with respect to a weight of an intermetallic compound having a composition of 100% by atom in total consisting of 10.0 to 12.0% by atom of Si, 1.5% by atom or more but less than 7.5% by atom of Ti, more than 2.0% by atom but 8.0% by atom or less of Ta and a balance made up of Ni excepting impurities, the Ni3(Si,Ti)-based intermetallic compound alloy having a microstructure composed of an L12 phase and of one or both of an Ni solid solution phase and a second phase dispersion containing Ni and Ta, or a microstructure composed of an L12 phase.

Abstract: A nickel-titanium-rare earth (Ni—Ti-RE) alloy comprises nickel at a concentration of from about 35 at. % to about 65 at. %, a rare earth element at a concentration of from about 1.5 at. % to about 15 at. %, boron at a concentration of up to about 0.1 at. %, with the balance of the alloy being titanium. In addition to enhanced radiopacity compared to binary Ni—Ti alloys and improved workability, the Ni—Ti-RE alloy preferably exhibits superelastic behavior. A method of processing a Ni—Ti-RE alloy includes providing a nickel-titanium-rare earth alloy comprising nickel at a concentration of from about 35 at. % to about 65 at. %, a rare earth element at a concentration of from about 1.5 at. % to about 15 at. %, the balance being titanium; heating the alloy in a homogenization temperature range below a critical temperature; and forming spheroids of a rare earth-rich second phase in the alloy while in the homogenization temperature range.

Abstract: A method for heat treating a nickel base alloy includes the steps of: a. heating a nickel base alloy to at least its delta (?) phase solvus temperature, and lower than its incipient melting temperature for a predetermined time sufficient to dissolve substantially all of the nickel base alloy's delta (?) phase, and b. cooling the nickel base alloy to a temperature below the gamma prime (?) precipitation temperature at a rate sufficient to precipitate the alloy's chromium carbide and gamma prime (?) in a serrated grain boundary.

Abstract: A process for heat treating a component formed of an alloy. The process includes manipulating uniaxial strain test data of the alloy using a triaxiality factor to determine an equivalent multiaxial stress state. Conditions are then applied to the multiaxial stress state to identify a cooling path for the component. The cooling path includes boundaries for heat treatment temperatures and cooling rates that do not exceed predetermined stresses or strains and/or avoid predetermined residual stress patterns in the alloy. The component is then heated to a heat treatment temperature and quenched according to the cooling path identified in the applying step.

Abstract: A heat treatment method for desensitizing a nickel-based alloy with respect to environmentally-assisted cracking, the alloy having the following composition in percentages by weight: C?0.10%; Mn?0.5%; Si?0.5%; P?0.015%; S?0.015%; Ni?40%; Cr=12%-40%; Co?10%; Al?5%; Mo=0.1%-15%; Ti?5%; B?0.01%; Cu?5%; W=0.1%-15%; Nb=0-10%; Ta?10%; the balance being Fe, and inevitable impurities that result from processing, characterized in that the alloy is held at 950° C.-1160° C. in an atmosphere of pure hydrogen or containing at least 100 ppm of hydrogen mixed with an inert gas. A part made of a nickel-based alloy having the composition and that has been subjected to the heat treatment.

Abstract: A method for heat treating a 718-type nickel-base comprises heating a 718-type nickel-base alloy to a heat treating temperature, and holding the alloy at the heat treating temperature for a heat treating time sufficient to form an equilibrium or near-equilibrium concentration of ?-phase grain boundary precipitates within the nickel-base alloy and up to 25 percent by weight of total ??-phase and ??-phase. The 718-type nickel-base alloy is air cooled. The present disclosure also includes a 718-type nickel-base alloy comprising a near-equilibrium concentration of ?-phase grain boundary precipitates and up to 25 percent by weight of total ??-phase and ??-phase precipitates. Alloys according to the disclosure may be included in articles of manufacture such as, for example, face sheet, honeycomb core elements, and honeycomb panels for thermal protection systems for hypersonic flight vehicles and space vehicles.

Abstract: Shape Memory Alloy tube is protected from damage during drawing, caused by galling-type interaction between the tube and high-carbon dies, by forming an oxide surface layer. This invention protects the tube internal diameter from oxidation while allowing the tube outside diameter to be oxidized, by using an oxygen getter located within the tube during the oxidation step. The method yields a higher quality internal diameter and improves productivity.

Abstract: In a process for producing a large single-crystal component or directionally solidified component made of a nickel-based superalloy, the component is first cast into shape in a known manner to form a microstructure comprising dendrites, and then solution annealing for homogenizing the cast microstructure of the component and two-stage precipitation heat treatment are carried out. In order to avoid chemical inhomogeneities and internal stresses caused thereby, a HIP process with a pressure of higher than 160 MPa is carried out following the solution annealing.

Abstract: The present invention provides an Ni-base dual multi-phase intermetallic compound alloy which has a dual multi-phase microstructure including: a primary precipitate L12 phase and an (L12+D022) eutectoid microstructure, and which comprises more than 5 atomic % and up to 13 atomic % of Al; at least 9.5 atomic % and less than 17.5 atomic % of V; between 0 atomic % and 5.0 atomic % inclusive of Nb; more than 0 atomic % and up to 12.5 atomic % of Ti; more than 0 atomic % and up to 12.5 atomic % of C; and a remainder comprising Ni.

Abstract: A metallic material is made from at least one refractory metal or an alloy based on at least one refractory metal. The metallic material has an oxygen content of about 1,000 to about 30,000 ?g/g and the oxygen is interstitial.

Abstract: A method of heat treating an Ni-base superalloy article is disclosed. The method includes hot-working an article comprising an NiCrMoNbTi superalloy comprising, in weight percent, at least about 55 Ni to produce a hot-worked microstructure; solution treating the article at a temperature of about 1600° F. to about 1750° F. for about 1 to about 12 hours to form a partially recrystallized warm-worked microstructure; and cooling the article. The method also includes precipitation aging the article at a first precipitation aging temperature of about 1300° F. to about 1400° F. for a first duration of about 4 hours to about 12 hours; cooling the article to a second precipitation aging temperature; precipitation aging the article at a second precipitation aging temperature of about 1150° F. to about 1200° F. for a second duration of about 4 hours to about 12 hours; and cooling the article from the second precipitation aging temperature to an ambient temperature.

Abstract: A method of improving the properties of a component of a medical device entails constraining the component, which comprises about 45-55 at. % Ni, about 45-55 at. % Ti, and about 0.3 at. % Cr, into a predetermined configuration. The component also includes at least about 35% cold work. The component is heated during the constraining at a temperature of between about 425° C. and about 500° C. for a time duration of between about 5 minutes and about 30 minutes, thereby improving the superelastic and mechanical properties of the component. A medical device includes a superelastic component for use in a body vessel that comprises about 45-55 at. % Ni, about 45-55 at. % Ti, and about 0.3 at. % Cr, where the component has an upper plateau strength of at least about 75 ksi, a residual elongation of about 0.1% or less, and an austenite finish temperature (Af) of about 30° C. or less.

Abstract: A first-stage turbine that is adapted for receiving high energy air directly from a combustion chamber in a gas turbine engine auxiliary power unit includes a disk formed from a first alloy and having an outer surface, and a unitary blade wheel formed from a second alloy that is different than the first alloy. The unitary blade wheel includes an annular member having an inner surface that is joined to the disk, and blades that are integrally formed with the annular member.

Abstract: The disclosure provides bearing sleeves or bushings made of memory shape material, and processes for installing such bearing sleeves or bushings. In one process, inner and outer surfaces of a bearing sleeve, made of a memory shape material, may be compressed at least one first temperature. A bearing may be inserted in a cavity of the bearing sleeve, and the bearing sleeve may be disposed adjacent to a surface of a structure, while the bearing sleeve is at the at least one first temperature. The inner and outer surfaces of the bearing sleeve may be expanded, at least one second temperature, to abut against the bearing and the surface of the structure.

Abstract: An Ni3Al-based intermetallic compound of the present invention comprises greater than 5 at % and not greater than 13 at % of Al, not less than 9.5 at % and less than 17.5 at % of V, not less than 0 at % and not greater than 5 at % of Nb, not less than 50 weight ppm and not greater than 1000 weight ppm of B, and the remaining portion consisting of Ni and inevitable impurities, and has a dual multi-phase microstructure comprising a primary L12 phase and an (L12+D022) eutectoid microstructure.