Abstract: A rotary evaporator is described utilizing a magnetically driven fluorocarbon cylinder, operating within a solvent container, to create a thin solvent film for rapid evaporation without the usual requirement for rotating the entire solvent container assembly. Infra-red heating is employed for efficient evaporation rates. Solvent heating is controlled during evaporation by a single temperature probe, turning the infra-red heater on and off on demand of the probe. Over heating of the product is prevented by maintaining a solvent residue at or near the conclusion of an evaporation.

Abstract: A heat transfer apparatus for processing a liquid continuously has a positive mechanical drive for a set of vertical whip rods each disposed in a vertical heat transfer tube. Each whip rod is free-standing on its lower end and is sufficiently flexible to conform closely to the inner surface of the tube as it orbits. The orbital drive propels the whip rod directly through a pair of horizontal, vertically spaced plates that engage the rods in loose openings that serve as fluid inlets from the drive plate. A motor rotates a drive shaft coupled to at least one of the drive plates through at least one eccentric crank. Each plate can be an opposed pair of plates with a separate eccentric drives 180.degree. out of phase with one another for a self balancing. Another form of drive plate uses a rigid circular ring that mounts rod-engaging sleeves via a network of wires supported by the ring.

Abstract: A rotary evaporator for laboratory scale solvent evaporative procedures is described. A magnetically driven fluorocarbon coated rotor, being open at its base and closed at its top, operating within a container for solvents, creates a thin film for rapid solvent evaporation without the usual requirement for rotating the entire solvent assembly. Rotary seals are eliminated, increased control over bubbling and foaming at higher vacuum is obtained, and continuous solvent addition is simplified.

Abstract: A rotary evaporator for laboratory scale solvent evaporative procedures is described. A magnetically driven fluorocarbon coated rotor, operating within a container for solvents, creates a thin film for rapid solvent evaporation without the usual requirement for rotating the entire solvent container assembly. Rotary seals are eliminated, increased control over bubbling and foaming at higher vacuum is obtained, and continuous solvent addition is simplified.

Abstract: Spinning band fractionating column apparatus is disclosed having a spinning band formed with a magnet embedded in its bottom end in the manner of a magnetic stirring vane for rotation by a rotating external magnetic field at the bottom of the apparatus. Reflux is controlled by an angled drip edge on a rotatable condenser column that passes a portion of dripped condensate to a collecting spout with the portion varying as rotation of the condenser column brings the drip from said edge closer or further from center opposition with the spout.