Abstract: A distillation column for separating a multicomponent mixture into at least three fractions. The distillation column has at least one separating wall and at least one material exchange element (1) above the at least one separating wall. A device (10) for mixing the steam flows flowing upwards to the left and the right of the at least one separating wall is arranged between the at least one separating wall and the at least one material exchange element (1). The use of the distillation column for purifying isocyanates, in particular for toluene diisocyanate (TDI), is also described.

Abstract: Fractionation systems utilizing a single rectifying column with a stripping column housed in the same vessel and having a uniform diameter are described. Methods of separating feed streams using the fractionation systems are also described.

Abstract: One exemplary embodiment can be a process for treating a hydroprocessing fraction. The process can include obtaining a bottom stream from a fractionation zone, and passing at least a portion of the bottom stream to a film generating evaporator zone for separating a first stream containing less heavy polynuclear aromatic compounds than a second stream.

Abstract: The present invention provides a method and an apparatus for recovery of spent lubricating oil. The evaporation of hydrocarbon fractions from spent lubricating oil is carried out in three steps. The first step is at approximately 150-1030 mbar and between 70-240° C. in which is greater than 99% water, greater than 99% of ethylene glycol and greater than 50% of hydrocarbon molecules with normal boiling point up to 310° C. are evaporated from spent oil. The second step is operated at 6-30 mbar and 200-2900 C in which predominantly gasoil and light vacuum gasoil fractions are evaporated. The third step is operated at 250-320° C. and 0.5-15 mbar in which mainly heavy vacuum gasoil (boiling range of 425 to 570° C. on ASTM D-1160 test) is evaporated from spent oil.

Abstract: The present invention discloses a horizontal multi-stage distillation system. The system comprises a feed stream, a distillate stream, a residue stream, a group of vessels, a plurality of vapour non-return valves (NRVs), a plurality of plurality of pumps, a plurality of liquid recycle NRVs, a liquid stream, a vapour stream, a plurality of liquid recycle streams, a plurality of level transmitters, a plurality of flow control valves (FCVs) and a plurality of liquid non-return valves (NRVs). Each vessel is connected to the adjacent vessel. The group of vessels comprises a condenser vessel, a reboiler vessel, a feed vessel, at-least one rectification vessel and at-least one stripping vessel. The present invention provides a horizontal multi-stage distillation system with higher efficiency and operational flexibility compared with equivalent vertical distillation columns. The present invention also avoids the interstage backflow of the liquid and vapours.

Abstract: A process for recovering liquefied petroleum gas from tail gas includes recovering a tail gas stream from a pressure swing adsorption zone and contacting the tail gas stream with a sponge liquid such as an unstabilized reformate liquid stream in order to recover C3+ hydrocarbons from the tail gas stream. The C3+ hydrocarbons may be recovered from the sponge liquid as liquefied petroleum gas.

Abstract: A process and apparatus provides for blending a heavy naphtha stream with a diesel stream to increase the yield of diesel. The diesel stream is recovered separately from a kerosene stream to leave the kerosene stream undiminished. The blended diesel provides a valuable composition.

Abstract: The present invention concerns a method for lowering the water dew point subsea in a produced multiphase hydrocarbon fluid stream containing water, the method comprising the steps of: separating (10) the hydrocarbon fluid stream (1) into a liquid phase (3) and a first gas phase (2); cooling (20) the first gas phase in a controlled manner to knock out water or condensing water and optionally other condensates while keeping the fluid above a hydrate formation temperature thereof; separating off condensed liquids (6) and a second gas phase; wherein the second gas phase (8) has a water dew point which is lower than that of the initial multiphase hydrocarbon fluid stream. The invention also concerns a system for lowering the water dew point subsea.

Abstract: Pitch is obtained, in a reactor configured for the atmospheric process, from a feedstock of oil hydrocarbons consisting of a feedstock_of decanted oil. In the process, the feedstock is subjected to heating stages in reflux and distillation conditions with removal of volatile products generated, wherein the gaseous products are eliminated at each stage and the successively generated residual products comprise a final residue recovered as a predominantly isotropic pitch.

Abstract: A method of reducing residual hydrocarbon accumulation during processing can comprise forming a permeable body (608) of a comminuted hydrocarbonaceous material within an enclosure (602). A primary liquid collection system (610) is located in a lower portion of the permeable body. The primary liquid collection system (610) has an upper surface for collecting and removing liquids. Comminuted hydrocarbonaceous material below the primary liquid collection system (610) forms a non-production zone (616). At least a portion of the permeable body (608) is heated to a bulk temperature above a production temperature sufficient to remove hydrocarbons therefrom within a production zone (614), where conditions in the non-production zone (616) are maintained below the production temperature.

Abstract: A method for improving yield of petroleum hydrocarbon distillate in a distillation tower (6) comprises: preheating raw oil of petroleum hydrocarbon ready for fractionation; feeding it to a vaporization section (11) through a pressure feed system (3) under a pressure 100-1000 kPa higher than the vaporization section (11) of the distillation tower (6) for simultaneous atomizing and vaporizing; then feeding it to a fractionation section (13) for distillation-separation; and finally, discharging distillate product from the top and/or side of the tower and unvaporized heavy oil from the bottom. A distillation tower (6) for improving yield of petroleum hydrocarbon distillate comprises a vaporization section (11) and a fractionation section (13), and further comprises a pressure feed system (3) for feeding the raw oil of petroleum hydrocarbon ready for fractionation under a pressure 100-1000 kPa higher than that in the vaporization section (11) of the distillation tower (6).

Abstract: Systems and methods for extracting recoverable materials from source materials are provided. According to one embodiment, a plasma furnace includes an open-faced tray, a pair of arc rods, Faraday coils and a smooth interior surface. The open-faced tray carries tar sands from one end of the plasma furnace to another. The arc rods are disposed above the open-faced tray and are operable to generate a plasma energy field for vaporizing bitumen contained within the tar sands. The Faraday coils are positioned underneath the open-faced tray to create a magnetic field proximate to the tar sands and cause the plasma energy field to penetrate and heat the tar sands to a temperature sufficient to release a bond between the bitumen and the tar sands by focusing and drawing the plasma energy field through the tar sands. Vaporized bitumen condenses on the smooth interior surface from which it is collected.

Abstract: A method is disclosed for treating the effluent from a hydrocarbon pyrolysis process unit to recover heat and remove tar therefrom. The method comprises passing the gaseous effluent to at least one primary heat exchanger, thereby cooling the gaseous effluent and generating high pressure steam. Thereafter, the gaseous effluent is passed through at least one secondary heat exchanger having a heat exchange surface maintained at a temperature such that part of the gaseous effluent condenses to form in situ a liquid coating on said surface, thereby further cooling the remainder of the gaseous effluent to a temperature at which tar, formed by the pyrolysis process, condenses. The condensed tar is then removed from the gaseous effluent in at least one knock-out drum.

Abstract: A process is provided for cracking hydrocarbon feedstock containing resid comprising: heating the feedstock, mixing the heated feedstock with a fluid and/or a primary dilution steam stream to form a mixture, optionally further heating the mixture, flashing the mixture within a flash/separation vessel to form a vapor phase and a liquid phase, partially condensing the vapor phase by contacting with a condenser within the vessel, to condense at least some coke precursors within the vapor while providing condensates which add to the liquid phase, removing the vapor phase of reduced coke precursors content as overhead and the liquid phase as bottoms, heating the vapor phase, cracking the vapor phase in a radiant section of a pyrolysis furnace to produce an effluent comprising olefins, and quenching the effluent and recovering cracked product therefrom. An apparatus for carrying out the process is also provided.

Abstract: An apparatus for reducing the coke dust in the decoking effluents of the hydrocarbon cracking ovens according to the invention provides means for the condensation of the effluent, means for collecting a liquid condensate, means for filtering said liquid condensate, and means for washing the residual vapours and gases that cannot be condensed by using the same condensate suitably filtered from coke, the filtered condensate being evaporated for the following discharge to the atmosphere by using the thermal content of the input decoking gases. A process for reducing the coke dust in the decoking effluents of the hydrocarbon cracking ovens according to the invention consists in that the solid content in the gaseous effluent from the decoking is removed by filtration of the condensate from said gaseous effluent and by washing of gases and vapours contained therein that cannot be condensed.

Abstract: A method and apparatus for re-refining used oil, in which the used oil is processed in at least one cyclonic vacuum evaporator comprising a void evaporation chamber (4) into which feedstock is tangentially injected, and in which a fraction of the feedstock is condensed in a spray condenser (7) communicating with the evaporation chamber (4).

Abstract: A fractionator for yielding petroleum products in association with a delayed coking process includes a bottom having a pool of petroleum residue and recycle liquid, a flash zone above the pool, an inlet line for conveying to the flash zone product vapors which are relatively warm with respect to the pool, and a baffle positioned between the flash zone and the pool to isolate the relatively warm product vapors from the pool and, thereby, reduce condensation of the product vapors. The fractionator also includes a wash zone, above the flash zone, in which the product vapors condense, and a downwardly pointed frustoconical element, an annular trough and an arrangement of conduits for conducting the condensed recycle liquid from the wash zone to the pool, out of contact with the product vapors in the flash zone.

Abstract: An internal draw tray is added to the flash zone of a coker fractionator below the coker vapor inlet to collect condensed coke drum overhead components and to keep the condensed material separate from the fresh feed to the coker furnace.

Abstract: A novel process for the purification of used oil comprising removing the ash-forming components, then subjecting the oil to vacuum fractionation. A novel vacuum fractionation column is also disclosed.

Abstract: A solvent extraction coal conversion process is provided wherein the effluent slurry product is subjected to vacuum distillation to yield distillate and extrudable still bottoms. The latter are removed from the vacuum still by means of an extrusion screw which is operatively associated with the still.

Abstract: A method and apparatus for re-refining used oil, in which the used oil is processed in at least one cyclonic vacuum evaporator comprising a void evaporation chamber (4) into which feedstock is tangentially injected, and in which a fraction of the feedstock is condensed in a spray condenser (7) communicating with the evaporation chamber (4).