Automatic Temperature And/or Pressure Control Patents (Class 202/160)
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Patent number: 6224716Abstract: A system for dehydrating lubricating and hydraulic fluids includes a heating circuit and circuitry for creating a vacuum. The heating circuitry introduces a stream of heated fluid into a vacuum chamber in which a partial vacuum is drawn by the vacuum circuit. Aqueous components of the fluid stream are flashed in the vacuum chamber by virtue of the elevated temperature and reduced pressure. Dehydrated fluid is then collected and evacuated from the vacuum chamber. Vapor from the vacuum chamber, including the aqueous components of the fluid stream are collected, condensed and separately evacuated. The heating circuit limits surface temperature of a heating element in a closed-loop manner to avoid degradation of the fluid. The fluid stream is introduced into the vacuum chamber or is recirculated through the heating circuit to maintain a desired level of fluid temperature in a closed-loop manner.Type: GrantFiled: March 18, 1998Date of Patent: May 1, 2001Assignee: Oilquip, Inc.Inventor: Perry D. Yoder
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Patent number: 6200428Abstract: Wastewater treatment apparatus having a fluid receiving vessel for collecting and heating wastewater to a temperature below boiling, a superheated vaporizing chamber and at least one spray head to spray wastewater into the vaporizing chamber for conversion of the wastewater to vapor to be withdrawn from the apparatus, with the contaminants in the wastewater collected in the apparatus for separate removal.Type: GrantFiled: March 31, 1998Date of Patent: March 13, 2001Inventor: Raymond E. VanKouwenberg
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Patent number: 6193849Abstract: A fractionator has a fractionation vessel, a reactor effluent vapors inlet, a vapor feed contacting zone, a baffled contacting section above the vapor feed contacting zone, a tops section above the baffled contacting section, a heavy bottoms liquid hold-up pool section below the vapor feed contacting zone, a bottoms outlet, a bottoms recycle system with a heat exchanger. Recycled, cooled bottoms is fed back to the fractionation vessel at the heavy bottoms liquid hold-up pool section and above the vapor feed contacting zone. The improvements involve providing a separation tray and downpipe for separating cooler bottoms liquid from hotter product vapors within the fractionation vessel: to avoid condensation and absorption of product vapors by the liquid pool; to have more rapid and uniform quenching of hot liquid entering the pool; and substantially reduce costly onstream maintenance to clean fouled bottoms recycle exchangers.Type: GrantFiled: April 21, 1995Date of Patent: February 27, 2001Inventor: William Lockett, Jr.
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Patent number: 6159344Abstract: The invention relates to a distillation and reaction device having a reaction section and a distillation-reaction section. The distillation-reaction section has a distillation zone with at least one device for circulation of the effluent from the reaction section to the distillation zone. Effluent from the reaction section is circulated to the distillation zone. The distillation-reaction section also has at least one distillation-reaction zone having at least one catalyst bed. The distillation-reaction zone is distinct from the distillation zone and provides at least partly the reflux of the distillation zone. The distillation-reaction section can also have at least one complementary reaction zone containing at least one catalyst bed. The invention further relates to a process for preparing at least one aliphatic monoalcohol, generally in excess, and at least one olefin.Type: GrantFiled: July 25, 1997Date of Patent: December 12, 2000Assignee: Institut Francais du PetroleInventors: Marie-Claire Marion, Alain Forestiere, Christophe Thille, Jean-Charles Viltard
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Patent number: 6159345Abstract: A method and apparatus for recycling and recovering potentially explosive solvents includes providing a contaminated solvent to a distillation tank, vaporizing the solvent in the distillation tank, thereby producing solvent vapor, condensing the solvent vapor, and adding a free radical scavenger substance to the distillation tank during the heating step. The vapor is then condensed and collected in a clean solvent tank where additional free radical scavenger substance is added to the clean solvent tank. Preferably, contaminated solvent is introduced into the solvent recovery system by providing contaminated solvent into contaminated solvent tank which is connected to the distillation tank, and an oxygen displacer substance is provided to the contaminated solvent tank and the clean solvent tank so as to minimize the amount of free oxygen in the tanks.Type: GrantFiled: November 6, 1998Date of Patent: December 12, 2000Assignee: Mitsubishi Chemical America, Inc.Inventors: John C. Donnelly, Guerry L. Grune, Gregory A. Frick, Kenneth L. Marsh
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Patent number: 6117275Abstract: Process and apparatus for regenerating a contaminated solvent wherein said solvent is first separated from higher-boiling contaminants in an evaporator, and then contaminants having a lower boiling point than said solvent are separated out in a condenser in which the temperature of said lower-boiling contaminants coming out of said condenser and the temperature of said solvent coming out of said condenser are separately controlled.Type: GrantFiled: April 14, 1998Date of Patent: September 12, 2000Assignee: Didda Maria Janina BaumannInventor: Walter Baumann
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Patent number: 6110325Abstract: An apparatus and method are provided in which a vaporizer vaporizes a liquid feed for introduction to a feed conversion unit such as a steam active reformer. A condenser condenses vaporized feed from the vaporizer when introduction of feed to the feed conversion unit is stopped. Condensed, liquid feed is passed back into the vaporizer and is conserved rather than going to flare.Type: GrantFiled: July 8, 1997Date of Patent: August 29, 2000Assignee: Krupp UHDE GmbHInventor: Martin K. Lyons
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Patent number: 6088630Abstract: Automatic control systems, and corresponding processes, for controlling either an anode adjuster in a chlor/alkali cell or at least one average middle temperature of a distillation column wherein the combination of feedback control from at least one real unit operation variable and an embedded real-time dynamic simulation of that variable are used.Type: GrantFiled: November 9, 1998Date of Patent: July 11, 2000Assignee: Olin CorporationInventor: David W. Cawlfield
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Patent number: 6063242Abstract: An evaporation system for separation of a fluid mixture into its component parts, especially for the reclamation of solvents, has a vacuum pump connected to the evaporator, especially a rotation evaporator, with at least one separator being connected to the suction side of the vacuum pump and at least one secondary condenser being connected at the pressure side of the vacuum pump. A fine regulating valve (8) is installed in the connecting pipe (7) between the rotation evaporator (2) and the separator (9), which is connected in front of the vacuum pump (10), for regulation of the boiling pressure.Type: GrantFiled: August 31, 1998Date of Patent: May 16, 2000Assignee: KNF Neuberger GmbHInventor: Erwin Hauser
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Patent number: 6030504Abstract: A distiller control circuit includes a power bus with first and second lines and a fan circuit connected across the lines and having a fan motor and a fan thermostat in series. There is also a heater circuit connected across the lines and having a heater and a heater thermostat in series. The fan thermostat is normally open, closes at an elevated temperature and automatically re-opens when the temperature subsides. The heater thermostat is normally closed, opens at an elevated temperature and must be manually reset to the closed position.The raw water vessel has a reset mechanism with a pivot-mounted bar and a contact surface on the bar. When the contact surface is depressed, the bar is urged to the second position for resetting the heater thermostat. The heater circuit terminates in a two-stud male connector and the platform has a two-slot female connector. The studs slide into electrically-conductive engagement with the slots when the raw water vessel is inserted into the condensing platform.Type: GrantFiled: March 18, 1997Date of Patent: February 29, 2000Assignee: The West Bend CompanyInventors: David C. Belongia, Robert V. Myszka
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Patent number: 5968320Abstract: A system for transporting and burning under negative pressure in a boiler a raw coke oven gas to produce steam energy. The system has the usual battery of coke ovens and corresponding ascension pipes connected to a collector main. Flushing liquor is sprayed into the hot coke oven gases to effect cooling in the collector main. A transport main delivers the cooled raw coke oven gases and flushing liquor to a burner of a steam producing boiler where the transport main includes a downcomer for separating the raw coke oven gas from the flushing liquor. The coke oven gas is burned in the boiler where a suction fan is provided at the exhaust of the boiler to develop a negative pressure in the system where the boiler has reinforced walls to withstand the negative pressure. A change in negative pressure in the system is detected and monitored by a controller system which varies draw of the suction fan in response to a detected change in negative pressure in the system.Type: GrantFiled: February 7, 1997Date of Patent: October 19, 1999Assignee: Stelco, Inc.Inventor: Hugh H. Sprague
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Patent number: 5928477Abstract: A method and apparatus permits concentration of a water-miscible organic liquid in a mixture of such liquid and water, with recovery of a desired concentrate of the water-miscible organic liquid and water, and a relatively clean water containing only a very low content of the water-miscible organic liquid which enables disposal of the water in sewage systems, the method and apparatus thus enhancing the ability to satisfy environmental concerns; the method has particular application to the recovery of a reusable glycol/water mixture from diluted spent aircraft deicer fluid (ADF).Type: GrantFiled: January 7, 1998Date of Patent: July 27, 1999Assignee: Inland Technologies Inc.Inventors: Peter Henry Firth Gammon, Gary James Dinn, John Joseph Whitten
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Patent number: 5925223Abstract: A process and apparatus for improving the thermal efficiency of a steam turbine power generating plant while simultaneously desalinating seawater or brine and purifying water which contains minerals, salts, and other dissolved solids. Exhaust gases from a power plant is heat exchanged against water in a secondary ecomomizer which circulates water at a temperature near, or slightly above the dewpoint of the combustion exhaust of the high-pressure boiler. The heated water is flashed to produce low-pressure steam. The low-pressure steam is condensed against the last effect of a multi-effect desalinization unit. Steam from the first effect of the desalination unit is condensed against steam condensate from the power plant turbine to preheat the condensate and thereby recover heat from the power plant's exhaust gas. Salinous water is fed to the multi-effect desalinization unit to produce fresh water and a concentrated brine.Type: GrantFiled: April 1, 1997Date of Patent: July 20, 1999Inventors: Gary D. Simpson, Karl Lin
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Patent number: 5906714Abstract: A method of separating water from an aqueous emulsion using a minimum of energy includes heating the aqueous emulsion in a sump, conveying concentrated emulsion from the sump to a heat exchanger so as to pass therethrough back to the sump, circulating water vapor and non-condensable gases from the sump through a compressor to raise its temperature and passing the heated water vapor and non-condensable gases through the heat exchanger to condense and heat the concentrated emulsion therein and evaporate water therefrom, a thermostat filled with water and water vapor, together with first and second pressure switches respectively communicating with the sump and the external atmosphere and the heat exchanger and the external atmosphere, maintaining a temperature differential between 0.5.degree. and 3.degree. C. between the aqueous emulsion in the sump and the temperature of the compressed water vapor and noncondensable gases.Type: GrantFiled: October 15, 1996Date of Patent: May 25, 1999Assignees: Agro Milj.o slashed. A/S, OHM Electric Co., Ltd.Inventors: Asger Gramkow, Jeppe Christian Bastholm, Finn Erik Christensen
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Patent number: 5893271Abstract: A cooling system with super heating control for a vapor degreasing apparatus is provided. The cooling system consists of a single condenser receiving a substantially gaseous refrigerant and producing a substantially liquid refrigerant. A first chilling coil evaporates at least a portion of the substantially liquid refrigerant which results in heat absorption by the first chilling coil at a first absorption rate. A second chilling coil evaporates at least a portion of the substantially liquid refrigerant resulting in heat absorption by the second chilling coil at a second absorption rate, and a desuperheating system, connected to the first and second chilling coils and the condenser, controlling the temperature of the substantially gaseous refrigerant generated by the first and second chilling coils and received by the condenser.Type: GrantFiled: July 30, 1997Date of Patent: April 13, 1999Assignee: Detrex CorporationInventor: Christopher J. Brink
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Patent number: 5879516Abstract: Improved kugelrohr or apparatus for distilling or separating liquids. It includes a rugged, reliable air oven and drive unit with numerous safety features. One or more external guards eliminate burn hazard and risk of accidental contact. A thermal isolation support isolates the oven from its rest surface. A grounded heating element eliminates shock hazards. The oven is fitted with a grommet or bushing to support a flask connected to one or more additional flasks in a series. The outlet of the last flask in the series is connected to a drive tube via a flexible coupling. The drive tube is connected to a rotary bearing assembly mounted on a drive unit. The oven and the flasks may include impellers for circulating air to enhance heating efficiency.Type: GrantFiled: February 29, 1996Date of Patent: March 9, 1999Inventor: David H. Kasman
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Patent number: 5876567Abstract: A distillation solvent recycling system is provided which is characterized by improved safety features, modular construction, a double insulated solvent reservoir, electronic control and display of system parameters, and self diagnosis of system malfunctions. The components of the system are assembled into a compact unitized structure so as to maximize safety, efficiency, portability, convenience and ease of operation and maintenance. An outer insulative and protective safety casing shields the operator from process hazards while the system is in operation. An inner lid is provided with improved sealing mechanisms for preventing the escape of toxic solvent vapors. An outer safety lid shields the operator from heat and trace vapors in the vicinity of the solvent reservoir.Type: GrantFiled: April 28, 1995Date of Patent: March 2, 1999Inventors: Soichiro Yamamoto, Jean-Pierre Pepin
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Patent number: 5853671Abstract: An improved condenser system for condensing vapor containing liquid or solid particles to minimize contamination of the condenser system by such particles and to increase the efficiency of liquid processing systems, including extracting particles from the vapor producing processing and cool down of the liquid and returning the particles to the processing container without fouling the condenser system or losing product.Type: GrantFiled: November 4, 1994Date of Patent: December 29, 1998Inventor: Kai Lieberam
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Patent number: 5827402Abstract: An improved drinking water apparatus is provided which utilizes a microcomputer to detect water level to automatically control water intake and heating. The apparatus includes a heating tank having a heater at the bottom side, a first cooling pipe at the top of the heating tank, a distilled water tank, and a second cooling pipe located at the top of the distilled water tank and connected to the first cooling pipe. The cooling pipes are each provided with a cooling fan for cooking the steam generated by boiling water into distilled water. The temperature of the distilled water is lowered to a degree suitable for drinking purposes.Type: GrantFiled: April 25, 1997Date of Patent: October 27, 1998Inventor: Ben-Mo Liao
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Patent number: 5817217Abstract: The invention relates to a machine for confining a primary fluid by means of a secondary fluid whose boiling temperature is lower than that of the primary fluid. The machine includes, in particular, primary vapor cooling means comprising a heat exchanger (11) for exchanging heat between the primary vapor and the secondary fluid (12), which means are provided with orifices (15) for exhausting the secondary vapor into the inside of the tank (4) so that the hat exchanger ensures that the primary vapor condenses and that the secondary fluid vaporizes, thereby making it possible to obtain thermal self-stabilization inside the tank.Type: GrantFiled: June 7, 1996Date of Patent: October 6, 1998Inventor: Jean-Paul Garidel
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Patent number: 5792428Abstract: An apparatus for oligomerization of C.sub.4 and C.sub.5 isoolefins or the etherification thereof with C.sub.1 to C.sub.6 alcohols wherein the reactants are contacted first in a partial liquid phase reactor (boiling point reactor) with a fixed bed acid cation exchange resin catalyst at an LHSV of 5 to 20, pressure of 0 to 400 psig and temperature of 120.degree. to 300.degree. F., at a pressure to maintain the reaction mixture at its boiling point whereby at least a portion but less than all of the reaction mixture is vaporized and the entire reaction stream is directed to a catalytic distillation column reactor for further reaction of the reactants, where the improvement is having a decoupling drum between the boiling point reactor and the catalytic distillation column reactor. The addition of a decoupler drum allows the reactors to operate at a pressure independent of each other.Type: GrantFiled: May 20, 1996Date of Patent: August 11, 1998Assignee: Chemical Research & Licensing CompanyInventors: Amarjit S. Bakshi, Timothy P. McGuirk, J. C. Gupta, Thomas Koval
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Patent number: 5783047Abstract: A monotube or multitube 2 is coupled to a body shell 1 via tube plates 3a and 3b at both ends, so that a tube interior 4 and a tube exterior 5 of the monotube or multitube 2 are isolated from each other. A difference is made in operating pressure between the tube interior 4 and the tube exterior 5, so that one of the tube interior 4 and the tube exterior 5 is used as a lower-pressure column and the other is used as a higher-pressure column. A wall of the tube is used as a heat transfer surface, so that heat is transferred from the higher pressure side (higher temperature side) to the lower pressure side (lower temperature side).Type: GrantFiled: April 24, 1996Date of Patent: July 21, 1998Assignees: Kimura Chemical Plants Co., Ltd., Kansai Chemical Engineering Co., Ltd., Maruzen Petrochemical Co., Ltd.Inventors: Kazumasa Aso, Hiroshi Matsuo, Hideo Noda, Tomoaki Takada, Nobuyuki Kobayashi
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Patent number: 5770019Abstract: When waste liquid is concentrated using a radiant heat section and a heat absorbent section of a heat pump circuit, in the proper place of the heating region of the heat pump circuit, a detector for detecting the pressure and/or temperature of the heat transfer medium is provided, or a detector for detecting the value of an electric current flowing through or the amount of electric power consumed in a system which includes a compressor for the heat pump circuit, is provided, and by the provision of a control system which can halt the concentration operation when the detected value exceeds a set value, both with a liquid in which the concentration of the non-volatile component is low so that a comparatively long time is required for the concentration operation, and, conversely, with a liquid in which the concentration of the non-volatile component is high so that the concentration operation is completed in a comparatively short time, the concentration operation has good efficiency, and can always be halted atType: GrantFiled: December 13, 1994Date of Patent: June 23, 1998Assignees: Konica Corporation, The Tokyo Electric Power Company, Incorporated, Sanyo Electric Co., Ltd.Inventors: Masayuki Kurematsu, Satoshi Yuzawa, Shoichi Kuroda, Souichiro Shibata, Noriyuki Shimamura, Toshiaki Kawada, Yuio Yoshiokaya
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Patent number: 5733417Abstract: A regenerating system, for the removal of water and potentially harmful organic constituents from a dehydration fluid used to dehydrate gas. The system includes apparatus for converting all the organic constituents to a gaseous phase; and utilizing the gaseous organic constituents in the separation of the water from the dehydration fluid.Type: GrantFiled: November 4, 1996Date of Patent: March 31, 1998Assignee: Gas Research InstituteInventor: Adolph J. Foral
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Patent number: 5720856Abstract: A process and apparatus for the production of a beverage distills aqueous influent into a forerun overhead fraction that is the first result of a distillation operation, a distillate, and a bottom products fraction that is left over from the aqueous influent without being distilled. The forerun overhead fraction is removed, the distillate is sterilized and remineralized into the beverage, and the bottom products fraction is removed so the process can begin again with more aqueous influent.Type: GrantFiled: February 23, 1995Date of Patent: February 24, 1998Inventor: Bruno Pirone
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Patent number: 5705036Abstract: A water distilling apparatus includes a preheat tank having an inlet and an outlet for storing water from a water source via the inlet, a boiling tank formed of a conductive casing connected to a ground potential and having an inlet in connection with the outlet of the preheat tank, a heater located within the boiling tank to boil water thereby generating steam, and an outlet flue extending from the boiling tank through the preheat tank as to condense the steam and preheat the water within the preheat tank, a heat dissipation coil connected with the outlet flue out of the preheat tank, a fan blowing air against the heat dissipation coil, a cool water tank connected with the heat dissipation coil for storing condensed water therefrom, an electrode vertically extending into the boiling tank, electrically isolated from the case of the boiling tank and connected to a positive voltage source, a control circuit electrically connected to each of the electrode, the fan, and the heater for disconnecting the fan and thType: GrantFiled: February 6, 1996Date of Patent: January 6, 1998Inventors: Yueh-feng Wu, Mu-huo Chen
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Patent number: 5679274Abstract: The disclosure involves a countertop distiller for home use. Such distiller is of the type including a condensing coil and an electrically-powered water heater. A method for controlling power flow to the heater includes the steps of activating a timer circuit to energize the heater, increasing the temperature of the coil and bypassing the timer circuit when the coil temperature increases to a predetermined value. The heater is de-energized when the water in the raw water container is substantially depleted and the heater temperature increases to a predetermined value because of such depletion. A new electrical circuit for a countertop distiller is also disclosed.Type: GrantFiled: May 13, 1996Date of Patent: October 21, 1997Assignee: The West Bend CompanyInventor: Michael A. Mahood
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Patent number: 5647961Abstract: A system for decontaminating and separating individual refrigerants from a mixture of refrigerants contaminated with solids, liquids and non-condensible gasses, includes three stages. In the first stage, solid and liquid contaminants are removed. In the second stage, the mixture of refrigerants passes through a condensation column where successive condensation stages remove individual refrigerants from the mixture of refrigerants. The remaining mixture of refrigerants passes through a third stage where non-condensible gas contaminants are removed.Type: GrantFiled: March 17, 1995Date of Patent: July 15, 1997Assignee: Tom NicolInventor: Spencer G. Lofland
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Patent number: 5643419Abstract: In the method of optimizing the control of the mass transfer zone in distillation columns by their characteristic areas which are dependent on pressure and heating steam, the temperature is measured on two different theoretical plates in the mass transfer zone of the column. The measured values are compared with one of the characteristic curves of the characteristic areas, which represent the nominal values for the temperature and the distance between the points where the thermometers are installed in the column.Type: GrantFiled: June 7, 1995Date of Patent: July 1, 1997Assignee: Hoechst AktiengesellschaftInventor: Hermann Rathert
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Patent number: 5624530Abstract: Spray drying system for drying a liquid feed which is made up of a solution or suspension of particles in a fluid medium. The system enables the spray drying of wet material and converting the material into powder by evaporation of a liquid medium at reduced pressure or at a vacuum. The system includes a heating chamber and an evacuation device, communicating with the interior of the heating chamber. This provision enables creation of reduced pressure within the chamber, accompanied by evaporation of the fluid medium at temperatures lower than needed for evaporation at normal pressure, and evacuation of the moisture vapor generated during evaporation.Type: GrantFiled: April 21, 1994Date of Patent: April 29, 1997Assignee: Ultrasonic Dryer, Ltd.Inventors: Akper Sadykhov, Raphael Semiat
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Patent number: 5591310Abstract: An apparatus for distillation of a liquid near or above its critical point wherein the liquid contains a dissolved solid. The apparatus includes a separation section wherein the liquid may be separated into a vapor and a liquid residue separated by a liquid surface. The apparatus includes a pump for pumping liquid into the apparatus so as to establish and maintain the liquid and vapor in the separation section at a desired pressure and a heat source for heating the liquid and vapor so as to establish a rising temperature profile in the separation section. The pump and heat source are cooperatively controllable for regulating the position of the liquid surface so that liquid residue can be discharged from immediately below the liquid surface.Type: GrantFiled: December 8, 1993Date of Patent: January 7, 1997Assignee: Grundfos International A/SInventor: Henrik G. Olrik
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Patent number: 5575894Abstract: A regenerating system, for the removal of water and potentially harmful organic constituents from a dehydration fluid used to dehydrate gas. The system includes apparatus for converting all the organic constituents to a gaseous phase, and utilizing the gaseous organic constituents in the separation of the water from the dehydration fluid.Type: GrantFiled: January 25, 1995Date of Patent: November 19, 1996Assignee: Gas Research InstituteInventor: Adolph J. Foral
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Patent number: 5569357Abstract: A vortex evaporator having a holder for holding at least one container presents a chamber wherein liquid is evaporated from a liquid and solid solution in a container. The vortex evaporator also includes a drive mechanism, coupled to the holder, for moving each container in an orbital motion within the chamber to cause the solution in the container to form a vortex configuration. The vortex evaporator further includes a gas supply system for directing gas into the container to increase the evaporation rate of the liquid and a control system for controlling operation of the vortex evaporator. In an alternative embodiment, a vacuum supply system may be utilized instead of the gas supply system. Further, the vortex evaporator will preferably include a heater, at least one liquid level sensor, a heat sensor and a motion dampening assembly all located within the chamber.Type: GrantFiled: April 28, 1994Date of Patent: October 29, 1996Assignee: Labconco CorporationInventors: Lowell L. Kuhn, James F. Ptacek, Gary P. Roepke
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Patent number: 5536375Abstract: A distiller for producing potable water employs a metal boiler tray having a cover member in which there is an inlet for raw water and which together form a steam chamber having an outlet for steam. The boiler tray bottom has a plurality of steps including a highest, an intermediate and a lowest level step which are all covered with water at the beginning of a distillation cycle. The temperature of the highest level step is monitored with a sensor. A rise in the temperature of the highest level step by a predetermined amount above the boiling temperature of water indicates that the highest and intermediate level steps have become dry. This results in a signal to a controller to open a valve and admit replenishment raw water whose amount is dependent on valve open time. Steam evolved from the boiler tray is conducted through a first check valve in the cover member to demister chamber when the mist or carryover water in the steam impinges on a baffle and is separated from the steam as condensate.Type: GrantFiled: September 29, 1994Date of Patent: July 16, 1996Assignee: Emerson Electric Co.Inventor: Jonathan C. Vogelman
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Patent number: 5535877Abstract: A method and apparatus for removing water from a solution of water and glycol solution. The apparatus finds application in recycling of glycol wherein a water and glycol solution having as much as a 95% water content when introduced to the apparatus leaves the apparatus with a water content in the order of 40% to 60%. The glycol concentrator has a packing medium made from glass shards that provide a labyrinth through which air is circulated in one direction and thin streams of glycol are circulated in generally the opposite direction. It is believed that mixing of the thin streams of solution and air flow steams in the labyrinth results in a thin film evaporation process. The glycol concentrator apparatus has reduced energy requirements when compared with a distilling process.Type: GrantFiled: February 28, 1994Date of Patent: July 16, 1996Inventors: Peter d. Eastcott, Nicole A. Truman, Peter Truman
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Patent number: 5494556Abstract: A method of separating a liquid mixture wherein the liquid mixture is heated; the heated liquid mixture is supplied to a pervaporation membrane module to separate a permeable component of the liquid; a portion of non-permeated liquid is circulated through a circulation pipe into a liquid mixture feeding pipe before a heater, and the remaining portion of the non-permeated liquid is extracted to the outside of the system, and wherein the temperature of the liquid in the liquid mixture feeding pipe in which the non-permeated liquid has been mixed with the liquid mixture or in the circulation pipe for the non-permeated liquid, is measured, and when the measured temperature is out of a predetermined range, new supply of the liquid mixture and/or extraction of the non-permeated liquid is stopped.Type: GrantFiled: November 28, 1994Date of Patent: February 27, 1996Assignees: Mitsubishi Chemical Corporation, Mitsubishi Kasei Engineering CompanyInventors: Masaaki Mita, Masumi Hino, Moriyoshi Kudo
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Patent number: 5487815Abstract: A method of optimizing the control of the mass transfer zone in distillation columns. Distillation columns are control optimized by controlling the steam feed, reflux, or pressure by determining the deviation from nominal values of characteristic curves of characteristic areas determined by measuring two different theoretical plates in the mass transfer zone of the column.Type: GrantFiled: February 2, 1994Date of Patent: January 30, 1996Assignee: Hoechst AktiengesellschaftInventor: Hermann Rathert
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Patent number: 5464504Abstract: In a distillation column, which for control purposes cannot tolerate the inherent dead time between analysis of consecutive samples in chromatograph analyzers, the chromatograph output is frequently corrected by inferring a dynamic correction based on the temperature change of a selected tray in the column. The dynamic correction applied to the distillation analyzer essentially eliminates the inherent dead time for obtaining a chromatograph analysis, and accordingly increased the rapidity of response of the column controls which rely on chromatograph analysis.Type: GrantFiled: December 2, 1993Date of Patent: November 7, 1995Assignee: Phillips Petroleum CompanyInventor: Martin H. Beauford
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Patent number: 5451300Abstract: A process and apparatus for stripping a volatile component from a liquid. The volatile component is destroyed by exothermic reaction with an active component in the gas phase, typically over a catalyst. Heat generated by the reaction of the volatile and active components is transferred to a fluid contact zone in which the organic component is stripped from the liquid stream by a stripping gas. Transfer of heat to the fluid contact zone increases the equilibrium partial pressure of the volatile component in the gas phase and thus increases the driving force for mass transfer in the stripping operation. Preferably, the volatile component is reacted with the active component in a regenerative heat transfer reaction system.Type: GrantFiled: June 1, 1993Date of Patent: September 19, 1995Assignee: Monsanto CompanyInventors: Yurii S. Matros, David E. McCombs
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Patent number: 5443695Abstract: The invention relates to an improved method and a novel apparatus for the concentration, separation, and purification of contaminated chemical compounds, wherein the chemical compound is less volatile than the contaminant. The distillation is performed using constant, predetermined distillation parameters.Type: GrantFiled: February 26, 1993Date of Patent: August 22, 1995Assignee: Athens CorporationInventor: Wallace I. Yuan
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Patent number: 5368699Abstract: A method of controlling concentrations in process technology operations--preferentially in thermal separation technology--using a non-linear, pressure-compensated temperature as control signal. The method can be used flexibly within a wide operating range.Type: GrantFiled: February 3, 1993Date of Patent: November 29, 1994Assignee: Bayer AktiengesellschaftInventors: Franz F. Rhiel, Gunther Weymans, Said Mahiout
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Patent number: 5368698Abstract: A water distillation apparatus includes a cylindrical housing with a first cover thereon, a pair of spaced apart funnel-shaped partitions, a second cover on the uppermost partition and a skirt extending downwardly from the periphery of the cover and the uppermost partition to a location above the bottom of the housing, the partitions and skirt dividing the interior of the housing into an inlet reservoir chamber for cold water above the first partition, a lower boiling chamber beneath the second partition and an inclined condensation passage between the partitions. Cold water is introduced through a pipe and solenoid valve into the bottom of the reservoir chamber for overflow through an opening in the second cover into the boiling chamber. A heater in the boiling chamber heats the water to produce steam which rises, passing into the condensation passage and flowing downwardly to a central drain for discharge into a distilled water reservoir beneath the housing.Type: GrantFiled: March 11, 1994Date of Patent: November 29, 1994Assignee: Big Iron Drilling Ltd.Inventors: George R. Field, Wallace B. Bolte, Norman N. Pepin
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Patent number: 5348623Abstract: An automatic water heating and distilling apparatus is provided having a hot water reservoir, an evaporator tank, a condenser, a distilled water reservoir and a control mechanism. Water is boiled within the evaporator tank generating steam which is condensed in the condenser to form distilled water. The heat rejected during condensation is transferred into the hot water reservoir. The distilled water reservoir has an input coupled to the condenser, an output for distilled water, and an overflow so that excess distilled water is returned to the evaporator tank. The control mechanism automatically regulates the operation of a heater within the evaporator to maintain the water in the hot water reservoir within a selected operating range. Various alternative embodiments are also described including a hot water heating apparatus utilizing an enclosed heat transfer device partially filled with liquid having a boiling point above the selected temperature for the water to be heated.Type: GrantFiled: September 30, 1992Date of Patent: September 20, 1994Assignee: Terrill Designs, Inc.Inventor: Michael E. Salmon
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Patent number: 5334291Abstract: An apparatus for removing non-volatile residues and impurities from a used solvent includes a self-scrubbing heating distillation subassembly for separating purified solvent for reuse and a controlled waste collector subassembly for overflowing concentrated residues and impurities stripped from the used solvent into an easy-to-service container. The apparatus may be disposed in a parallel in-line relationship with a circulating solvent flow circuit, such as in a dry cleaning operation, to continuously withdraw and purify aliquot portions of the circulating solvent stream, returning good solvent back to the flow circuit and concentrating non-volatile residues and impurities to a removable, environmentally sound serviceable container.Type: GrantFiled: July 9, 1993Date of Patent: August 2, 1994Assignee: Safety-Kleen Corp.Inventors: Gilbert Gavlin, William M. Langdon, deceased, Boris Goltsin, Gunther Erlebacher, Douglas A. Larson
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Patent number: 5314587Abstract: A method and apparatus are disclosed wherein a standpipe mounted in an accumulator outside the operating zone of a distillation column is used in conjunction with a liquid level controller to measure condensate collected in the accumulator and to change the amount of energy provided to the distillation column in response to changes in the level of condensate collected in the accumulator.Type: GrantFiled: January 13, 1993Date of Patent: May 24, 1994Assignee: Union Carbide Chemicals & Plastics Technology CorporationInventor: Gerald L. Smith
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Patent number: 5306397Abstract: The apparatus is located almost completely under the surface of the sea. The vacua in the de-aeration and the evaporation chambers are generated by a vacuum pump and are maintained by the effects of a pressure reduction device at the inlet for warm seawater and a lifting pump at the outlet for brine. The de-aerator and the evaporator are laid out as heat exchangers and penetrated by heating tubes, which are flowed through passively by warm seawater. The immersion tube forming the steam compartment which is suspended vertically in the sea serves as a condenser. The condenser is cooled passively by cold seawater. The attachment to the bottom of the sea is performed by a single point mooring construction via an anchor chain at an anchor weight. The elevation of the water production unit is controlled automatically by means of an air chamber and an air compressor.Type: GrantFiled: October 28, 1992Date of Patent: April 26, 1994Assignee: PI Praktische Informatik GmbHInventor: Edgar Schmidt
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Patent number: 5304286Abstract: To provide a balanced supply of distilled water and undistilled hot water for a household, a condenser coil communicates at one end with a steam generator located above a hot water heater and at its other end well the holding tank of a distilled water system, with a condenser entering the hot water heater near the bottom. The steam generator power input matches the power needed to meet the recovery rate to satisfy undistilled hot water demand under normal conditions. The condenser includes a plurality of loops grouped together so a line drawn from top to bottom through them is no longer than 5 inches. The length of the loops is at least 6 inches and the tubes have inside diameters between 1/4 inch and 5 inches and a total area of at least 25 square inches. Near the outlet of the condenser, the tube bends upwardly by approximately a diameter to create a water holding portion in the lower most loop of the condenser to restrain condensate and maximize heat transfer.Type: GrantFiled: November 1, 1989Date of Patent: April 19, 1994Inventor: David G. Palmer
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Patent number: 5302253Abstract: A method and apparatus for automatically measuring the acidity of overhead water in an oil refinery, and dispensing a neutralizing agent into the refinery system at a rate responsive to that measurement. A sample of overhead water is collected and passed through a filter and cation exchange resin. The acid concentration of the sample is then automatically measured and a signal generated based on the concentration. The signal goes to a controller which controls the dispensation rate of neutralizing agent into the refinery system, thus reducing the acidity of the overhead water and limiting the corrosive effects of such acidity.Type: GrantFiled: April 13, 1992Date of Patent: April 12, 1994Assignee: Nalco Chemical CompanyInventors: Ronald B. Lessard, Paul Fearnside
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Patent number: 5296103Abstract: A method for the fractional distillation of a mixture of at least two compounds with different boiling points, a rising flow of vapor is brought into intimate contact with a descending flow of liquid obtained within a column (1) by the partial condensation of the flow of vapor itself by heat exchange with a cooled surface which extends through a filling (37).Type: GrantFiled: May 13, 1992Date of Patent: March 22, 1994Assignee: T.I.I. Tecnologie Industriali Innovative S.n.c. di Rosa Corigliano e.C.Inventor: Gianclaudio Masetto
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Patent number: 5286351Abstract: A water distiller is provided which is used in conjunction with a hot water heater where normally wasted energy is used to preheat the hot water heater inlet. The distiller includes a heat storage tank, an evaporator tank having a water inlet, a heater and a steam outlet, and a first and second heat exchanger located within the heat storage tank. Steam generated in the evaporator tank passes through the first heat exchanger and condenses, forming distilled water. The heat rejected during condensation is absorbed within the heat storage tank. The second heat exchanger is used to preheat the water flowing to the hot water heater inlet by passing the water through the second heat exchanger on an as needed basis where it absorbs heat from the heat storage tank.Type: GrantFiled: May 15, 1991Date of Patent: February 15, 1994Assignee: Terrill Designs, Inc.Inventor: Michael E. Salmon