Compressed Vapor As Heat Source Patents (Class 203/24)
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Publication number: 20030132097Abstract: A desalination device includes a saltwater input line and a desalinator having a water input connected to the input line, a fresh water output and a brine output. A fuel cell generates electricity and is connected to an energy source for the desalinator. A heat exchanger transfers waste heat from the fuel cell to desalinator.Type: ApplicationFiled: January 15, 2002Publication date: July 17, 2003Inventors: Brian Kenet, Pedro Joaquin Sanchez Belmar
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Publication number: 20030132095Abstract: A method for distilling water includes the steps of entering brine to be distilled into a sub-atmospheric boiler having a brine section with a brine output and a water vapor output; concentrating brine in the brine section to a concentration of at least 250 grams of salt or contaminants per liter; stirring the brine in the brine section; and exiting the brine through the brine output. A distiller with a subatmospheric boiler having a stirring device is also provided.Type: ApplicationFiled: January 15, 2002Publication date: July 17, 2003Inventors: Brian Kenet, Pedro Joaquin Sanchez Belmar
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Patent number: 6551466Abstract: A method and apparatus for removing a contaminant from a fluid feed stream containing the contaminant. The method includes the steps of providing a feed stream and heating it in a first step to at least partially remove some of the contaminants and recover energy from a concentrate and distillate generated. Further heating the feed stream in a second heating step in a heated separator generates a saturated vapor fraction and a concentrated liquid contaminant fraction. The vapor fraction may be compressed to generate a temperature differential in the reboiler exchanger with the vapor fraction being passed into contact with a reboiler exchanger to provide a stream of condensed vapor from the reboiler. The stream may be circulated through the reboiler exchanger and the heated separator to maintain from about 1% to about 50% by mass vapor in the stream.Type: GrantFiled: December 22, 1999Date of Patent: April 22, 2003Assignee: Aqua Pure Ventures Inc.Inventors: Steve Kresnyak, Edward Warchol, Robert Becker
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Patent number: 6482297Abstract: The present invention relates to an improved process for distilling ammonia from a mixture, more particular from a mixture resulting from the reaction between aminonitrile and water (which reaction is also called cyclizing hydrolysis). The process for distilling the ammonia contained in an aqueous caprolactam solution, uses a column with a bottom temperature less than or equal to 160° C. and at an absolute pressure less than or equal to 5 bar, the ammonia distilled at the top of the column being compressed to a pressure greater than or equal to 10 bar and then condensed at a temperature of 25° C. to 60° C.Type: GrantFiled: June 6, 2001Date of Patent: November 19, 2002Assignee: Rhodia Fiber & Resin IntermediatesInventors: GĂ©rald Bocquenet, Patrick Houssier
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Publication number: 20020092759Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020092758Abstract: A distillation unit (10) employs counterflow-heat-exchanger modules (102, 104, 106, 108, and 110) to use the heat from water that has come from a rotary heat exchanger (32) to heat feed water that is being sent to it for distillation. In one of the modules the feed water is heated only by concentrate that results from the distillation process, whereas only condensate heats the feed water in the other modules. By thus employing four different flows in two sets of heat-exchanger modules rather than three flows in a single set, the distillation unit can employ relatively simple counterflow-heat-exchanger modules and easily adjust flows to achieve a desired output concentration in response to different expected feed concentrations while maintaining optimum feed flows.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020092762Abstract: A distillation unit (10) includes a filter (116) through which feed water passes before it is introduced into a rotary heat exchanger (32) for evaporation and subsequent condensation. During a normal mode of operation, liquid that has not evaporated as a result of passage through the rotary heat exchanger's evaporation chambers (56) is recirculated for reintroduction into those chambers, together with a minor amount of feed liquid from the filter to make up for evaporation. At the same time, some filtered feed water is fed into one side of a transfer pump (166), where it slowly accumulates. Periodically, though, during short flushing-mode periods, the erstwhile recirculating liquid is redirected at a relatively high flow rate through the filter (116) in the reverse direction, thereby flushing it.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Patent number: 6402897Abstract: A combination liquid distillation unit and heater, where the distilled liquid is heated to an elevated temperature to effect distillation, and then stored and maintained at an elevated temperature in a hot liquid tank. Thermal communication between the distillation unit portion and the storage tank allow heat from the distillation unit to be recovered in the hot distilled liquid in the tank to be transferred back to the feed water and/or to help maintain the hot distilled liquid in the tank at an appropriate elevated temperature. A start-up chamber in the distillation unit stores a reservoir of feed liquid during periods of inactivity, and allows the hot distilled liquid in the tank to preheat this feed liquid so that the feed liquid boils more quickly upon start-up.Type: GrantFiled: October 24, 1997Date of Patent: June 11, 2002Inventor: Charles L. Gunn
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Publication number: 20020053507Abstract: A water distiller comprises a sub-atmospheric boiler having a non-recirculating brine section, an input, a brine output and a vapor output, the input for water to be distilled, the brine output for brine, and the vapor output for water vapor, a compressor connected to the vapor output for heating the water vapor, and an heated vapor line connected to an output of the compressor, the heated vapor line heating the brine section. Also provided is a method for distilling water comprising the steps of entering water to be distilled into a sub-atmospheric boiler, a part of the water to be distilled boiling immediately and a part entering a brine section of the boiler; raising a temperature of water vapor exiting the boiler so as to form a heated water vapor; passing the heated water vapor by the brine section so as to heat the brine section; and removing brine from the brine section when the brine reaches a predetermined salinity.Type: ApplicationFiled: January 10, 2002Publication date: May 9, 2002Inventor: Pedro Joaquin Sanchez Belmar
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Patent number: 6375803Abstract: A method and apparatus for removing a contaminant from a fluid feed stream containing the contaminant. The method includes the steps of providing a feed stream (10) and heating it in a first step (18) to at least partially remove some of the contaminants and recover energy from a concentrate and distillate generated. Further heating the feed stream in a second heating step (20) in a heated separator generates a saturated vapor fraction (30) and a concentrated liquid contaminant fraction. The vapor fraction (30) may be compressed (32) to generate a temperature differential in the reboiler exchanger (34) with the vapor fraction being passed into contact with a reboiler exchanger (34) to provide a stream of condensed vapor from the reboiler. The stream may be circulated through the reboiler exchanger (34) and the heated separator to maintain from about 1% to about 50% by mass vapor in the stream.Type: GrantFiled: January 14, 2000Date of Patent: April 23, 2002Assignee: Aqua-Pure Ventures Inc.Inventors: Minoo Razzaghi, Robert Spiering
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Patent number: 6365005Abstract: An improved design of a vapor compression distiller which makes use of a rapid, highly turbulent flow through the heat-of-evaporation recovery, or primary, heat exchanger. The distiller may also include the use of turbulators to increase turbulence and mixing within the primary heat exchanger. The increased level of turbulence and mixing dramatically reduces fouling inside the primary heat exchanger and increases the heat transfer efficiency. The improvements in the distiller are maximized by recirculating the liquid to be evaporated at a high multiple of the flow rate of the liquid feed to the distiller. The distiller may also include a feed circulation loop with a secondary heat exchanger to increase the efficiency of heat-of-evaporation recovery in the evaporation/condensation cycle. Applications of the vapor compression distiller include purification of waste liquids, concentration of dilute liquid mixtures, and separation of liquid/liquid, liquid/gas, and liquid/solid mixtures.Type: GrantFiled: February 9, 1999Date of Patent: April 2, 2002Inventor: James W. Schleiffarth
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Patent number: 6355145Abstract: A method for removing a contaminant from a fluid feed stream containing the contaminant. The method includes the steps of providing a feed stream and heating it in a first step to at least partially remove some of the contaminants and recover energy from a concentrate and distillate generated. Further heating the feed stream in a second heating step in a heated separator generates a saturated vapor fraction and a concentrated liquid contaminant fraction. The vapor fraction may be compressed to generate a temperature differential in the reboiler exchanger with the vapor fraction being passed into contact with a reboiler exchanger to provide a stream of condensed vapor from the reboiler. The stream may be circulated through the reboiler exchanger and the heated separator to maintain from about 1% to about 50% by mass vapor in the stream. The apparatus includes a unique configuration of a vapor compressor, heated separator in combination with a forced circulation circuit to generate the decontamination result.Type: GrantFiled: January 14, 1998Date of Patent: March 12, 2002Assignee: Aqua-Pure Ventures, Inc.Inventors: Steve Kresnyak, Minoo Razzaghi, Robert Spiering
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Patent number: 6280578Abstract: Essence of the invention is a: a liquid, whose saturated vapour pressure is not less than the pressure at the top of a rectification column, is delivered into the nozzle of a liquid-gas jet apparatus as a motive liquid; the pressure maintained in a separator represents from 1.1 to 160 times the pressure of a vapor phase at the inlet of the liquid-gas jet apparatus; condensation of easy-condensable components of the vapor phase in the motive liquid and forming of a liquid-vapor mixture take place after mixing of the vapor phase with the motive liquid; the liquid-vapor mixture is separated in the separator into a compressed gaseous component and a liquid medium. The introduced method results in an increase in efficiency of a pumping-ejector system for the distillation of a liquid product.Type: GrantFiled: December 21, 1998Date of Patent: August 28, 2001Inventor: Serguei A. Popov
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Patent number: 6261419Abstract: The invention relates to an improved evaporator and condenser unit for use in distilling a liquid such as water. The evaporator and condenser unit includes a plurality of stacked, spaced-apart plates disposed within a housing. The plates are horizontally arranged around a common, vertical axis for rotation. Adjacent plates define spaces between their oppositely facing surfaces, which are alternating configured as evaporating and condensing chambers. An outlet tube transfers vapor generated within the housing to a compressor and an inlet tube delivers compressed vapor to the condensing chambers. A sump containing the liquid to be distilled is located at a lower portion of the housing. A rotating element extends into the sump and forces liquid to be distilled up a stationary feed pipe where it is discharged into the evaporating chambers which are open at both their inner and outer ends.Type: GrantFiled: February 8, 1999Date of Patent: July 17, 2001Assignee: Ovation Products CorporationInventor: William H. Zebuhr
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Patent number: 6238524Abstract: The invention relates to an improved evaporator and condenser unit for use in distilling a liquid such as water. The evaporator and condenser unit includes a plurality of stacked, spaced-apart plates disposed within a housing. The plates are horizontally arranged around a common, vertical axis for rotation. Adjacent plates define spaces between their oppositely facing surfaces, which are alternating configured as evaporating and condensing chambers. An outlet tube transfers vapor generated within the housing to a compressor and an inlet tube delivers compressed vapor to central receiving space within the stack of plates. A sump containing the liquid to be distilled is located at a lower portion of the housing. Each plate includes a plurality of ports for distributing liquid to be distilled and for extracting a condensate.Type: GrantFiled: December 14, 1998Date of Patent: May 29, 2001Assignee: Ovation Products CorporationInventor: William H. Zebuhr
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Patent number: 6120651Abstract: A method permits concentration of a water-miscible organic liquid in a mixture of such liquid and water, with recovery of a desired concentrate of the water-miscible organic liquid and water, and a relatively clean water containing only a very low contest of the water-miscible organic liquid which enables disposal of the water in sewage systems, the method thus enhancing the ability to satisfy environmental concerns; the method has particular application to the recovery of a reusable glycol/water mixture from diluted spent aircraft deicer fluid (ADF).Type: GrantFiled: May 20, 1999Date of Patent: September 19, 2000Assignee: Inland Technologies Inc.Inventors: Peter Henry Firth Gammon, Gary James Dinn, John Joseph Whitten
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Patent number: 5968321Abstract: Distillation system having an evaporator/condenser core with heat transfer plates welded together along their edges to form alternate boiling and condensing chambers. Feed liquid is supplied to the boiling chambers through a pair of heat exchangers which preheats the liquid and a steam stripper utilizing ceramic pieces to remove gasses from the liquid. Vapor from the boiling chambers is compressed and delivered to the condensing chambers where it is condensed and gives up its heat to the liquid in the boiling chambers. Pumps positioned between the two heat exchangers draw the condensed product and unvaporized feed liquid containing dissolved solids from the evaporator/condenser and circulate them through the heat exchangers to transfer heat to the feed liquid.Type: GrantFiled: February 13, 1996Date of Patent: October 19, 1999Assignee: Ridgewood WaterPure CorporationInventor: Stephan B. Sears
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Patent number: 5928477Abstract: A method and apparatus permits concentration of a water-miscible organic liquid in a mixture of such liquid and water, with recovery of a desired concentrate of the water-miscible organic liquid and water, and a relatively clean water containing only a very low content of the water-miscible organic liquid which enables disposal of the water in sewage systems, the method and apparatus thus enhancing the ability to satisfy environmental concerns; the method has particular application to the recovery of a reusable glycol/water mixture from diluted spent aircraft deicer fluid (ADF).Type: GrantFiled: January 7, 1998Date of Patent: July 27, 1999Assignee: Inland Technologies Inc.Inventors: Peter Henry Firth Gammon, Gary James Dinn, John Joseph Whitten
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Patent number: 5925223Abstract: A process and apparatus for improving the thermal efficiency of a steam turbine power generating plant while simultaneously desalinating seawater or brine and purifying water which contains minerals, salts, and other dissolved solids. Exhaust gases from a power plant is heat exchanged against water in a secondary ecomomizer which circulates water at a temperature near, or slightly above the dewpoint of the combustion exhaust of the high-pressure boiler. The heated water is flashed to produce low-pressure steam. The low-pressure steam is condensed against the last effect of a multi-effect desalinization unit. Steam from the first effect of the desalination unit is condensed against steam condensate from the power plant turbine to preheat the condensate and thereby recover heat from the power plant's exhaust gas. Salinous water is fed to the multi-effect desalinization unit to produce fresh water and a concentrated brine.Type: GrantFiled: April 1, 1997Date of Patent: July 20, 1999Inventors: Gary D. Simpson, Karl Lin
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Patent number: 5906714Abstract: A method of separating water from an aqueous emulsion using a minimum of energy includes heating the aqueous emulsion in a sump, conveying concentrated emulsion from the sump to a heat exchanger so as to pass therethrough back to the sump, circulating water vapor and non-condensable gases from the sump through a compressor to raise its temperature and passing the heated water vapor and non-condensable gases through the heat exchanger to condense and heat the concentrated emulsion therein and evaporate water therefrom, a thermostat filled with water and water vapor, together with first and second pressure switches respectively communicating with the sump and the external atmosphere and the heat exchanger and the external atmosphere, maintaining a temperature differential between 0.5.degree. and 3.degree. C. between the aqueous emulsion in the sump and the temperature of the compressed water vapor and noncondensable gases.Type: GrantFiled: October 15, 1996Date of Patent: May 25, 1999Assignees: Agro Milj.o slashed. A/S, OHM Electric Co., Ltd.Inventors: Asger Gramkow, Jeppe Christian Bastholm, Finn Erik Christensen
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Patent number: 5738761Abstract: A waste water treatment system includes a preliminary first stage separator for separating an aqueous phase from other materials. A pressure vessel sedimentation follows for removing most of the remaining solids from the waste material. The liquid and a minor fraction of the solids then pass on to an evaporation vessel where the water vapor is removed, compressed and passed through a condenser inside the evaporator vessel to recycle heat in the evaporator. The condenser is a stacked plate heat exchanger of unique design with the plates separated by steam gaskets and water gaskets to provide a very high heat transfer surface area to volume ratio. The condensate from the condenser passes through a second heat exchanger that heats the liquid flowing into the evaporator. The effluent water is purified by the evaporation. The residual solids may be heat treated to evaporate residual moisture and to sterilize the solids using a steam-jacketed auger. The resultant solids may be used as fertilizer.Type: GrantFiled: January 18, 1996Date of Patent: April 14, 1998Assignee: Haron Research CorporationInventor: Ronald B. Fletcher
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Patent number: 5599429Abstract: The water distillation system according to the invention recaptures and utilizes the inherent heat of transformation in converting from the vapor to the liquid states. The water distillation system efficiently removes volatile gases and impurities from the distillate and recaptures and reuses the heat from the impurities. A water seal is created to seal the drive shaft aperture of the compression housing and the rotating drive shaft of the compression rotor. In addition, the compression rotor is assembled of ultra-light, strong member in such a manner to significantly reduce the manufacturing and maintenance costs of the compression rotor drive mechanism.Type: GrantFiled: March 16, 1994Date of Patent: February 4, 1997Assignee: Martinstill CorporationInventors: David L. Martin, Robert C. Martin
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Patent number: 5597453Abstract: A vapor compression distillation/product concentration device includes an evaporator/condenser core, with alternating boiling and condensing chambers with edge manifolds such that substantially the entirety of each plate surface is used as a heat transfer surface. Seals are conveniently formed between adjacent plates by laying a bead of liquid gasketing material such that as the plates are laid atop each other and cured, a waffle-like seal is formed surrounding the contact points between adjacent plates which interlocks the seal with the plates. A truly perpendicular fluid flow is achieved between the alternating boiling chambers and condensing chambers as each fluid traverses the entirety of each chamber in a unidirectional flow as it passes through the evaporator/condenser core.Type: GrantFiled: October 16, 1992Date of Patent: January 28, 1997Assignee: Superstill Technology, Inc.Inventor: Stephan B. Sears
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Patent number: 5591310Abstract: An apparatus for distillation of a liquid near or above its critical point wherein the liquid contains a dissolved solid. The apparatus includes a separation section wherein the liquid may be separated into a vapor and a liquid residue separated by a liquid surface. The apparatus includes a pump for pumping liquid into the apparatus so as to establish and maintain the liquid and vapor in the separation section at a desired pressure and a heat source for heating the liquid and vapor so as to establish a rising temperature profile in the separation section. The pump and heat source are cooperatively controllable for regulating the position of the liquid surface so that liquid residue can be discharged from immediately below the liquid surface.Type: GrantFiled: December 8, 1993Date of Patent: January 7, 1997Assignee: Grundfos International A/SInventor: Henrik G. Olrik
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Patent number: 5587054Abstract: A vapor compression distillation system including a boiler/condenser assembly wherein a portion of the condensate is redirected back to the condenser inlet to extract superheat from the compressed vapor and transfer it to the liquid in the boiler. The vapor entering the condenser is reduced to a saturation condition to prevent heat build up in the condenser to improve heat transfer efficiency. When the temperature of the incoming feed water is within the operating range of the boiler/condenser assembly, the system is operated under vacuum sufficient to match the boiler temperature with the temperature of the incoming feed water so that no preheater or waste heat recovery exchanges are required.Type: GrantFiled: October 11, 1994Date of Patent: December 24, 1996Assignee: Grano Environmental CorporationInventor: Robert C. Keith
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Patent number: 5512142Abstract: A process and device for purifying organically polluted waste water utilizing a primary system and a closed secondary system. The primary system includes a first heat exchanger, a second heat exchanger and a cyclone located between the two heat exchangers. The first heat exchanger evaporates the waste water into a waste water vapor and a waste water sump solution. The heat for evaporating the waste water in the first heat exchanger is obtained primarily from raw water in the secondary system. A second heat exchanger in the primary system condenses the waste water vapor and in the process causes evaporation of raw water in the secondary system. The level of waste water in the primary system is monitored as is an operational parameter in the secondary system. With the data obtained from this monitoring, the drawing off of the waste water sump solution is controlled.Type: GrantFiled: July 14, 1994Date of Patent: April 30, 1996Inventor: Jakob Hoiss
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Patent number: 5366514Abstract: This invention relates to an evaporative salt plant installation including methods of operation and apparatus which produce high purity salt economically and in high yield comprising the combination of a gas turbine which drives a vapor compressor, whose exhaust gases are used to produce steam to drive a topping steam turbine generator, which in turn generates the electrical energy requirements of the plant, and wherein the discharge vapors from the steam turbine are combined with the discharge vapors from the vapor compressor, which is in turn in combination with a vapor compression evaporator and a purge evaporator, whereby both evaporators produce salt, and where the overhead vapors of the purge evaporator are used in a brine cooled condenser to preheat input cold brine, thereby producing water condensate which is recovered, along with evaporator steam chest condensate streams, and used in solution mining underground salt, thereby allowing for both the productive use and recovery of substantially all the rType: GrantFiled: December 30, 1992Date of Patent: November 22, 1994Assignee: Texas Brine CorporationInventors: Lawrence F. Becnel, Jr., John E. Currey, Raymond W. Ver Hoeve
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Patent number: 5300197Abstract: A distillation apparatus includes a distillation unit for distilling feed water. The distillation unit includes an evaporation part, a condensation part and a hydrophobic porous membrane interposed between the evaporation part and the condensation part, which are integrated with one another. A heating unit for heating the feed water and a cooling portion for cooling distillate produced by distillation of the feed water are provided apart from the distillation unit. One or both of the heating unit and the cooling unit are provided with a heat pump. With this construction, an additional heater does not need to be provided, and the distillation unit and both of the heating unit and the cooling unit can be changed in size and performance independently of each other, so that the overall size of the distillation apparatus can be reduced.Type: GrantFiled: December 10, 1990Date of Patent: April 5, 1994Assignee: Hitachi, Ltd.Inventors: Kenji Mitani, Akira Ashida, Katsuya Ebara, Hideaki Kurokawa
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Patent number: 5232556Abstract: A water desalination apparatus which is constructed of a main housing which includes a condensation chamber and a vapor chamber located above the condensation chamber. Brackish water is to be supplied into the vapor chamber with this brackish water to produce a vapor which is to be removed by a centrifugal compressor arrangement into the condensation chamber. The condensed brackish water from the vapor chamber is to flow through a mass of thin-walled tubes to be eventually discharged into the ambient. The exterior wall of these tubes is located within the condensation chamber and it is on the walls of these tubes that the distilled water vapor is to collect and condense and flow from the condensation chamber to a collection source.Type: GrantFiled: September 30, 1991Date of Patent: August 3, 1993Inventor: Frank J. Passarelli
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Patent number: 5227027Abstract: A water distillation system and process capable of high efficiency operation used in combination with a heat pump system wherein the water distillation apparatus includes a water pre-heating device positioned within the feed water to heat the feed water to approximately 150 degrees Fahrenheit to facilitate operation of a water evaporator device which vaporizes the water by boiling thereof. Contaminants are removed from this pure water vapor which is at approximately 215 degrees Fahrenheit. The water vapor is passed to a water condenser to provide high purity water at approximately 180 degrees Fahrenheit. The heat pump system provides for refrigerant condensing at approximately 225 degrees Fahrenheit to facilitate boiling of the water in the adjacent water evaporator and includes refrigerant vaporization adjacent the water condenser to facilitate absorbing and reclaiming of the latent heat of the distillate.Type: GrantFiled: November 7, 1991Date of Patent: July 13, 1993Inventor: Robert T. Topper
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Patent number: 5171455Abstract: Small quantities of one or more liquids having a low boiling point dispersed with a large quantity of one or more immiscible liquids having a higher boiling point are separated in a rapid and efficient manner. A non-reactive gas (nitrogen, helium, air, or combinations thereof) is heated by recycled energy and make-up energy to a temperature above the boiling point of at least one liquid but below that of at least one other liquid. The heated gas is combined with the unheated or preheated liquid-liquid mixture to be separated, and the liquid-gas blend is mixed, heated and distributed by an improved heat exchanger having thermal conductive gas tubing, metal wools and fins) and nebulizer, forming a mist inside a vessel containing a pool liquid of at least one liquid having a boiling point higher than that of at least one other liquid, which pool liquid has been heated with at least a heat pump means to a temperature above the boiling point of at least one liquid but below the pool liquid's own boiling point.Type: GrantFiled: July 10, 1992Date of Patent: December 15, 1992Assignee: International Environmental Systems, Inc.Inventors: Lawrence K. Wang, Roland E. Weber, John J. Pavlovich
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Patent number: 5156706Abstract: A vertical tube evaporation process for the concentration of saline water and other liquids, including the addition of an anionic mono-molecular dispersant thereto which interacts with materials precipitated during concentration and inhibits the formation of scale or fouling depositions on evaporator surfaces, and wherein the additive is incorporated into the precipitated materials and improves their removal during the descaling or defouling of evaporator surfaces by rendering such precipitates redispersable in fresh water or in a non-saturated liquid used for descaling or defouling of evaporator surfaces.Type: GrantFiled: April 29, 1988Date of Patent: October 20, 1992Inventor: Hugo H. Sephton
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Patent number: 4954223Abstract: A distillation apparatus including a pair of vertical lower vessels each open at its upper end, and a pair of elongate upper vessels each having an open lower end, slidably mounted in a respective one of the lower vessels. A heat exchanger is mounted in each of the upper vessels, with the upper end of one upper vessel being connected to the inlet of the heat exchanger in the other vessel, and vice versa. A reciprocating drive mechanism drives the two upper vessels up and down in opposite directions so as to simultaneously effect compression in the space above the liquid level in the downwardly moving vessel while expanding the space above the liquid in the other vessel, driving vapor from the downwardly moving vessel into the heat exchanger in the other vessel, where it condenses.Type: GrantFiled: July 29, 1988Date of Patent: September 4, 1990Inventors: Joseph E. Leary, Edward L. Parr
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Patent number: 4830711Abstract: A method of and system for recovering a solvent from a mixture of solvent and hydrocarbons, the system comprising at least two evaporation flasks successively fed with a charge consisting of said mixture to be separated, at least one steam generator performing the condensation of the solvent, a circuit for conveying the evaporated solvent and connecting the flasks to the generator and a circuit of an intermediate fluid in gaseous phase including a compressor for raising the condensation temperature of this fluid, the latter circuit connecting the generator to heat exchangers arranged upstream of each flask.Type: GrantFiled: June 4, 1987Date of Patent: May 16, 1989Assignee: Compagnie Francaise d'Etudes et de Construction "Technip"Inventors: Patricia Delbourgo, Michel Coupard, Jean-Jacques Delorme
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Patent number: 4778001Abstract: There is disclosed a method and apparatus for exchanging heat between a first fluid and a second fluid immiscible with said first fluid comprising the step of presenting one of said fluids in finely divided form for direct contact with the others. One fluid may be a molten metal which is sprayed or bubbled through the other.Type: GrantFiled: November 4, 1986Date of Patent: October 18, 1988Assignee: Shirley InstituteInventor: Colin M. Reed
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Patent number: 4713089Abstract: A system and method is disclosed for removing dissolved organic impurities, such as gasoline or other hydrocarbons, from groundwater. The contaminated water is fed into a stripper column, operated under a deep vacuum, to enable the water to enter the column at its boiling point. Steam, as a vaporizing gas, strips the impurities out of the water and the overhead vapor phase is compressed to boost it to a higher pressure, so it can be condensed to vaporize part of the bottoms stream from the column. Since the bottoms stream is mostly water, the vapor generated is the steam used to strip impurities from the water.Type: GrantFiled: July 18, 1986Date of Patent: December 15, 1987Assignee: The Dow Chemical CompanyInventor: Lanny A. Robbins
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Patent number: 4710272Abstract: An apparatus for distilling a source liquid which utilizes a substantially vertical liquid column. The liquid column is contained by a tubular container closed at the top and open at the bottom. The open bottom of the tubular container is submerged within a source liquid reservoir. The height of the tubular container is greater than the maximum obtainable height for the given density of the portion of source liquid contained within the column. A vacuum is located within the tubular container above the surface of the portion of source liquid contained in the column. In the area of the vacuum, there is located a centrifugal compressor which is to function to move vapor from the vacuum section of the tubular container and compress such along with the transfer of heat to the point that the vapor becomes liquid. This now product liquid is to be removed from the apparatus.Type: GrantFiled: March 20, 1986Date of Patent: December 1, 1987Inventors: Frank J. Passarelli, George A. Matsukas, Charles P. Caspary
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Patent number: 4698136Abstract: A process for the continuous production of boiler feed water from process waters in the oil extraction industry during which salts and hydrocarbons are removed from the water, without Fe.sup.++ precipitating. The heavy hydrocarbons are mechanically separated, the volatile hydrocarbons are separated from the water, by means of a thermal degassing, and the low boiling and the non-condensable hydrocarbons are separated in a shower evaporation step with downstream vapor compression, wherein the low boiling non-condensable hydrocarbons are evaporated with the waste water within the shower evaporator and the non-condensable hydrocarbons then are drawn off from a downstream separator. A salt-free oxygen-free pure water is removed from a separator.Type: GrantFiled: May 23, 1985Date of Patent: October 6, 1987Assignee: Fried Krupp GmbHInventor: Mohammed El-Allawy
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Patent number: 4668345Abstract: Desalination apparatus comprising a vessel, an evaporation surface for receiving saline water in the vessel, a condensation chamber arranged in the vessel beneath the evaporation surface, an evaporation chamber arranged in the vessel above the evaporation surface, a fresh water tank for containing a reservoir of fresh water and fresh water vapor thereabove, a first conduit connecting the fresh water tank and the condensation chamber, a pump for compressing in the condensation chamber fresh water and fresh water vapor to maintain a pressure-temperature differential between the condensation chamber and the evaporation chamber at the evaporation surface, a second conduit connecting the evaporation chamber and the fresh water tank for removal of fresh water vapor from the evaporation chamber and its delivery to the reservoir of fresh water, and valves and conduits for conveying saline water to the evaporation surface and for taking off fresh water accumulated in the fresh water tank.Type: GrantFiled: February 26, 1985Date of Patent: May 26, 1987Inventor: Thomas B. Warren
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Patent number: 4636284Abstract: A process for the separation of water from a water-containing mixture of azeotrope, with an extractant which removes water from the mixture or azeotrope, recovery of the non aqueous portion of the mixture or azeotrope as a product, and regeneration of the extractant for reuse by the removal of water therefrom. A feature thereof is that residual water can be removed from the extractant, and the extractant regenerated for reuse by contacting the heated extractant with a portion of the same product from which the water has been removed; or, the extractant can be regenerated in the process by contact with an inert gas which has been dried in the process. The water-containing mixture or azeotrope is preferably contacted with a portion of the vaporous product to recover the heat of condensation for use in the process.Type: GrantFiled: May 18, 1984Date of Patent: January 13, 1987Inventors: John C. English, John A. Ondrey, Jason M. Voyce
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Patent number: 4594131Abstract: A water purification process is described for the removal of ammonia and optionally one or more acid gases from wastewaters such as coke-plant or coal conversion wastewaters. The process involves adding alkali to these wastewaters in amounts sufficient to react with fixed ammonia salts present in the wastewater and to enable substantial amounts of the ammonia to be evolved upon distillation, and subjecting the thus treated wastewater to distillation to remove substantial amounts of the ammonia and acid gases present from the wastewater. This process is achieved by two separate and successive distillations. In this process, the vapor streams being withdrawn from the first and/or second distillations are subjected to an impurity removal process to thereby produce a vapor stream substantially reduced in impurities, and useful as a stripping vapor in this process, and then reusing this vapor stream as a stripping vapor in the process.Type: GrantFiled: August 13, 1984Date of Patent: June 10, 1986Assignee: United States Steel CorporationInventor: Edward E. Maier
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Patent number: 4587370Abstract: A fractionation method is disclosed for the recovery of product alkylaromatic hydrocarbons produced by the alkylation of aromatic hydrocarbons. Three fractionation columns are employed in series. Aromatic feed hydrocarbons are recycled from the overhead of the first column, which is reboiled by the overhead vapor of the second column. The product alkylaromatic is recovered from the condensate produced in using the second column overhead as a heat source. The product alkylaromatic is also present in the bottoms of the second column which flows into a low pressure stripping column. The entire overhead vapor of the stripping column is compressed and passed into the lower portion of the second column.Type: GrantFiled: June 5, 1985Date of Patent: May 6, 1986Assignee: UOP Inc.Inventor: Richard R. DeGraff
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Patent number: 4585524Abstract: Demineralized crude water is distilled during flow along a first path which is defined by stationary parts. Such water is evaporated and thereafter cooled and condensed by a heat transfer medium which is circulated along an endless second path. Evaporation of crude water results in condensation of the medium, and condensation of resulting water vapors into distillate results in evaporation of the medium. The medium is caused to pass through a heat pump which raises its pressure and temperature before the thus heated medium exchanges heat with and evaporates crude water in the first path. The medium and/or the distillate can be used for preheating crude water upstream of the evaporating station, and the vapors are preferably purified by one or more cyclones, by an electrostatic filter and/or by ultrasonic waves intermediate the evaporating and condensing stations.Type: GrantFiled: June 22, 1983Date of Patent: April 29, 1986Inventor: Jakob Hoiss
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Patent number: 4575405Abstract: A process for the rectification of binary liquid mixtures is disclosed wherein one component of the mixture is more volatile than the other component. A rectification column is employed having rectification, intermediate and depletion stages, with a working fluid comprised of the components to be separated being employed to furnish energy for the rectification process.Type: GrantFiled: December 9, 1982Date of Patent: March 11, 1986Assignee: Cie Electro MecaniqueInventor: Jacques Sterlini
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Patent number: 4561941Abstract: A highly efficient essence recovery process associated with a continuous process which utilizes mechanical vapor recompression for concentrating fruit juices. In one embodiment of this invention the essence is extracted from a juice by introducing feed juice to an evaporator and heating the feed juice within the evaporator sufficiently to boil off essence bearing vapor, by mechanically compressing the essence bearing vapor, the compression raising the condensing temperature of the essence bearing vapor, utilizing the compressed and heated essence bearing vapor to evaporates the feed juice within the evaporator, a substantial portion of the compressed and heated vapor condensing out as it evaporates the feed juice, and collecting the excess vapor as the essence with or without further concentration. By utilizing the method outlined above, it is possible to use the excess heat of the mechanical vapor recompression system to produce an outflow of essence enriched vapors.Type: GrantFiled: November 26, 1982Date of Patent: December 31, 1985Assignee: APV Equipment, IncorporatedInventors: Derek F. Dinnage, George F. Worrall
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Patent number: 4537039Abstract: A vapor compression distilling device (10) includes a first chamber (30) adapted to contain liquid (32) to be distilled. A compressor (70) is interconnected to the first chamber (30) for withdrawing vapor from the liquid (32) in the first chamber (30). The compressor (70) also functions to compress the vapor. A second chamber (12) is adapted to receive the compressed vapor from the compressor (70) such that the compressed vapor is condensed in the second chamber (12) into a liquid condensate. A device (16) is disposed in the second chamber (12) for boiling, concentrating and circulating the liquid (32) to be distilled. The device (16) is provided with circulating flow connections (18, 36) to the first chamber (30) and extends into the second chamber (12), such that the exterior of the device (16) is exposed to the compressed vapor generated by the compressor (70).Type: GrantFiled: June 6, 1983Date of Patent: August 27, 1985Inventor: Robert E. Fearon
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Patent number: 4525243Abstract: A tank for receiving water to be desalinated supports a vacuum pump at the upper end thereof. The inlet of the pump communicates with the tank for reducing the interior of the tank to a subatmospheric pressure and the outlet of the pump communicates with heat transfer coils submerged just below a water level in the tank. The vacuum pump has an outer casing defining a heating area which traps the heat generated by operation of the pump. An inlet for water to be desalinated leads through the heated area around the pump and is discharged above the water level at the heat transfer coils for vaporization of the incoming water. The heat transfer coils communicate with condensing coils leading downwardly in the tank. The heat transfer coils are supported on a float and have an inlet and outlet arrangement providing for even distribution of vapor.Type: GrantFiled: March 5, 1984Date of Patent: June 25, 1985Assignee: J. Stanley Miller CorporationInventor: Stanley Miller
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Patent number: 4461675Abstract: A process for vaporizing a working liquid and condensing the vapors thereof is provided wherein the heat of compression is used in vaporizing the liquid. In the process, the working liquid is compressed to a high pressure thereby adding heat of compression thereto. This heat of compression is transferred from the working liquid to a still as a result of which the liquid is vaporized and contains sensible heat. The fluid containing this sensible heat is passed to an evaporator and substantially all sensible heat over that used to boil-up said liquid is removed by heat transfer contact between the fluid containing the sensible heat through use of an auxiliary condensing coil, so that thermal balance is maintained.Type: GrantFiled: April 26, 1982Date of Patent: July 24, 1984Assignee: Allied CorporationInventors: Harry F. Osterman, George C. Nylen
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Patent number: 4444576Abstract: A method for the distillative separation of a feed stream containing light hydrocarbons and acid gas components in a distillative column into an enriched overhead product, such as a carbondioxide fraction, and an enriched bottom product of C.sub.2 + and hydrogen sulfide, the method which comprises: introducing a liquid alkane additive into the column, to provide a relatively uniform, constant temperature zone in the column above the point of feed inlet of the feed stream; extracting heat from the upper portion of the low-temperature zone; and introducing heat into the lower portion of the temperature zone approximately at or above the feed inlet of the feed stream, to reduce the energy requirement of the distillation.Type: GrantFiled: November 1, 1982Date of Patent: April 24, 1984Assignee: Koch Process Systems, Inc.Inventors: James M. Ryan, John V. O'Brien
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Patent number: 4440601Abstract: A method and apparatus for high volume distillation of impure liquid, particularly of binary mixtures of relatively low boiling organic substances and water, comprises fractionally distilling the impure liquid to form a vapor of a low boiling organic substance; compressing the vapor; passing at least a portion of the compressed vapor through a vapor composition adjustment zone wherein the organic substance may catalytically or otherwise react or merely stabilize following compression; compressing the vapor exiting the adjustment zone to form a recompressed vapor; cooling the recompressed vapor in heat transfer relation with the impure liquid whereby the vapor at least partially condenses, transferring sufficient heat to the impure liquid for evaporating the liquid and to form the aforementioned low boiling organic vapor; and collecting the condensed low boiling organic vapor.Type: GrantFiled: January 15, 1981Date of Patent: April 3, 1984Inventors: Jerome Katz, Sidney J. Fogel