Methods Patents (Class 250/424)
  • Publication number: 20140256122
    Abstract: Methods and apparatus for a carbon ion source head. An ionization chamber is configured to receive a process gas containing carbon and a noble carrier gas; a cathode is disposed in the ionization chamber and configured to emit electrons in thermionic emission; a graphite coating is provided on at least a portion of the cathode; and an outlet on the ionization chamber is configured to output carbon ions. A method for ion implantation of carbon is disclosed. Additional alternative embodiments are disclosed.
    Type: Application
    Filed: March 8, 2013
    Publication date: September 11, 2014
    Inventors: Yi-Jiun Lee, Cheng-Hung Hu, Yh-Hsiu Hsiao, Kan Hwa Chang, Ming-Te Chen
  • Patent number: 8829468
    Abstract: The present invention provides an inductively coupled, magnetically enhanced ion beam source, suitable to be used in conjunction with probe-forming optics to produce an ion beam without kinetic energy oscillations induced by the source.
    Type: Grant
    Filed: April 2, 2012
    Date of Patent: September 9, 2014
    Assignee: FEI Company
    Inventors: John Keller, Noel Smith, Roderick Boswell, Lawrence Scipioni, Christine Charles, Orson Sutherland
  • Patent number: 8829467
    Abstract: An IMS or other analytical instrument has a corona discharge needle (20) to ionize sample gases or vapours. A gate (3) is opened or closed to admit or prevent entry of the ions produced by the corona discharge to a drift chamber (4). The operation of the corona discharge needle (20) and the gate (3) are controlled such that the gate is open during at least two discharges, to admit faster ions produced by the most recent discharge together with slower ions produced by an earlier discharge.
    Type: Grant
    Filed: December 23, 2005
    Date of Patent: September 9, 2014
    Assignee: Smiths Group PLC
    Inventors: Alastair Clark, John Patrick Fitzgerald, Stephen John Taylor, Robert Brian Turner
  • Publication number: 20140246577
    Abstract: Described herein are methods and systems related to the use of the pre-existing ion injection pathway of a mass spectrometer to perform beam-type collision-activated dissociation, as well as other dissociation methods. The methods can be practiced using a wide range of mass spectrometer configurations and allows MSn experiments to be performed on very basic mass spectrometers, even those without secondary mass analyzers and/or collision cells. Following injection and selection of a particular ion type or population, that population can be fragmented via beam-type collision-activated dissociation (CAD), as well as other dissociation methods, using the pre-existing ion injection pathway or inlet of a mass spectrometer. For CAD applications, this is achieved by transmitting the ions back along the ion injection pathway with a high degree of kinetic energy. As the ions pass into the higher pressure regions located in or near the atmospheric pressure inlet, the ions are fragmented and then trapped.
    Type: Application
    Filed: March 5, 2014
    Publication date: September 4, 2014
    Inventors: Joshua J. COON, Graeme C. MCALISTER
  • Patent number: 8822947
    Abstract: A particle beam generating device includes at least one accelerator unit for generating a particle beam and at least one emission unit for the output of the at least one particle beam onto a workpiece. The device is configured to release at least two particle beams including hadronic particles with at least one of a different mass or a different charge.
    Type: Grant
    Filed: May 26, 2011
    Date of Patent: September 2, 2014
    Assignee: GSI Helmholzzentrum fuer Schwerionenforschung GmbH
    Inventors: Gerhard Kraft, Nami Saito, Dieter Schardt
  • Patent number: 8822948
    Abstract: A method of and apparatus for controlling the temperature of an inductively coupled or microwave induced plasma for optical emission spectrometry or mass spectrometry in which the intensities of two spectral lines of radiation emitted by the plasma are measured, and the power provided to sustain the plasma is adjusted so that the ratio of the intensities remains substantially constant.
    Type: Grant
    Filed: November 8, 2013
    Date of Patent: September 2, 2014
    Assignee: Thermo Electron Manufacturing Limited
    Inventor: Stephen Hartwell
  • Publication number: 20140239191
    Abstract: The uninterrupted production of an ion beam with self-cleaning of a discharge chamber and extractor system, including extraction aperture(s), of an ion implantation device. The method increases the time of continuous operation of the ion implantation device, and therefore, increases total implantation time without reducing intensity. As a result, the time integrated output of the ion implantation device is increased. The method includes feeding a working molecule comprising at least two boron atoms and a strong oxidizer into an ion implantation device and removing gaseous compounds from the ion implantation device, wherein said working molecule provides upon fragmentation a polyatomic boron-containing ion, and the strong oxidizer which reacts with solid products of decomposition of the working molecule to form said gaseous compounds. A working molecule including at least two boron atoms and at least one strong oxidizer is also disclosed.
    Type: Application
    Filed: July 20, 2012
    Publication date: August 28, 2014
    Inventors: Ady Itzchak Hershcovitch, Oleg Alexeyenko, Timur Kulevoy, Rostislav Kuibeda, Efim Oks, Vasiliy Gushenets, Pavel Storozhenko, Ella Gurkova, Sergey Dugin, Gennady Kropachev, Dimitri Seleznev
  • Publication number: 20140231669
    Abstract: A microwave ion source includes a plasma chamber, a magnetic field generator that generates a magnetic field in the plasma chamber, and a control unit that controls the magnetic field generator to apply an initial magnetic field for plasma ignition to the plasma chamber and change the initial magnetic field to a normal magnetic field after the plasma ignition. The plasma chamber may have a vacuum window that receives a microwave, and an ion extraction opening. The initial magnetic field may have a flat magnetic field distribution from the vacuum window to the ion extraction opening.
    Type: Application
    Filed: February 18, 2014
    Publication date: August 21, 2014
    Applicant: SUMITOMO HEAVY INDUSTRIES, LTD.
    Inventors: Nobuaki Takahashi, Hirohiko Murata
  • Patent number: 8809803
    Abstract: A wide ion beam source includes a plurality of RF windows arranged in a predetermined relationship, a single plasma chamber disposed on a first side of the plurality of RF windows, a plurality of RF antennas, each RF antenna of the plurality of RF antennas disposed on a second side of a respective RF window of the plurality of RF windows, the second side being opposite the first side, and a plurality of RF sources, each RF source coupled to a respective RF antenna of the plurality of RF antennas, wherein a difference in frequency of a first RF signal produced by a first RF source coupled to a first RF antenna from that of a second RF signal produced by a second RF source coupled to an RF antenna adjacent to the first RF antenna is greater than 10 kHz.
    Type: Grant
    Filed: August 7, 2013
    Date of Patent: August 19, 2014
    Assignee: Varian Semiconductor Equipment Associates, Inc.
    Inventors: Costel Biloiu, Joseph C. Olson, Edward W. Bell, Manny Sieradzki
  • Patent number: 8809800
    Abstract: An ion source and method of cleaning are disclosed. One or more heating units are placed in close proximity to the inner volume of the ion source, so as to affect the temperature within the ion source. In one embodiment, one or more walls of the ion source have recesses into which heating units are inserted. In another embodiment, one or more walls of the ion source are constructed of a conducting circuit and an insulating layer. By utilizing heating units near the ion source, it is possible to develop new methods of cleaning the ion source. Cleaning gas is flowed into the ion source, where it is ionized, either by the cathode, as in normal operating mode, or by the heat generated by the heating units. The cleaning gas is able to remove residue from the walls of the ion source more effectively due to the elevated temperature.
    Type: Grant
    Filed: July 31, 2009
    Date of Patent: August 19, 2014
    Assignee: Varian Semicoductor Equipment Associates, Inc.
    Inventors: Bon-Woong Koo, Christopher R. Campbell, Craig R. Chaney, Robert Lindberg, Wilhelm P. Platow, Alexander S. Perel
  • Publication number: 20140224983
    Abstract: A collision cell for a mass spectrometer arranged to receive ions for fragmentation in a chamber and comprising an activation ion generator configured to irradiate the received ions with activation ions of the same polarity as the received ions. The activation ion generator is preferably a plasma generator, configured to generate a plasma comprising the activation ions.
    Type: Application
    Filed: March 15, 2013
    Publication date: August 14, 2014
    Inventors: Konstantin CHINGIN, Roman ZUBAREV
  • Patent number: 8803112
    Abstract: A novel composition, system and method thereof for improving beam current during silicon ion implantation are provided. The silicon ion implant process involves utilizing a first silicon-based co-species and a second species. The second species is selected to have an ionization cross-section higher than that of the first silicon-based species at an operating arc voltage of an ion source utilized during generation and implantation of active silicon ions species. The active silicon ions produce an improved beam current characterized by maintaining or increasing the beam current level without incurring degradation of the ion source when compared to a beam current generated solely from SiF4.
    Type: Grant
    Filed: August 28, 2013
    Date of Patent: August 12, 2014
    Assignee: Praxair Technology, Inc.
    Inventors: Ashwini K. Sinha, Lloyd Anthony Brown, Serge Marius Campeau
  • Publication number: 20140218729
    Abstract: A liquid sampling, atmospheric pressure, glow discharge (LS-APGD) device as well as systems that incorporate the device and methods for using the device and systems are described. The LS-APGD includes a hollow capillary for delivering an electrolyte solution to a glow discharge space. The device also includes a counter electrode in the form of a second hollow capillary that can deliver the analyte into the glow discharge space. A voltage across the electrolyte solution and the counter electrode creates the microplasma within the glow discharge space that interacts with the analyte to move it to a higher energy state (vaporization, excitation, and/or ionization of the analyte).
    Type: Application
    Filed: February 4, 2014
    Publication date: August 7, 2014
    Applicants: Clemson University, Pacific Northwest National Laboratory, Lawrence Berkeley National Laboratory
    Inventors: R. Kenneth Marcus, Charles Derrick Quarles, JR., Richard E. Russo, David W. Koppenaal, Charles J. Barinaga, Anthony J. Carado
  • Patent number: 8796639
    Abstract: Provided is an ion beam treatment apparatus. The treatment apparatus includes a target for generating positive ions including a thin film for generating positive ions and nanowires disposed on at least one side of the thin film for generating positive ions, and a laser for emitting a laser beam incident on nanowires to project positive ions to a tumor region of a patient by generating the positive ions from the thin film for generating positive ions. Each of the nanowires may include a metal nanocore and a polymer shell surrounding the metal nanocore. The laser beam incident on the nanowires forms surface plasmon resonance, a near field having an intensity enhanced more than an intensity of the laser beam is formed by the surface plasmon resonance, and the positive ions are emitted from the thin film for generating positive ions by the near field.
    Type: Grant
    Filed: June 17, 2013
    Date of Patent: August 5, 2014
    Assignee: Electronics and Telecommunications Research Institute
    Inventors: Moon Youn Jung, Hyeon-Bong Pyo, Dong-Ho Shin, Seunghwan Kim
  • Patent number: 8791410
    Abstract: A mass spectrometry system based on the general principle of accelerator mass spectrometry (AMS) is disclosed. An ion source (10) generates a beam (B) of ions having a negative charge state. A first mass analyzer (20) transmits only ions having a predetermined mass. The ions are passed through a stripper target (80) comprising helium and/or hydrogen as a stripping gas to change the charge state of said ions from negative to positive charge and to dissociate molecular ions by collisions. A second mass analyzer (110, 130) transmits ions in charge state 1+ having the predetermined mass, which are detected by a detector (140). By using helium and/or hydrogen gas and detecting ions in charge state 1+, it becomes possible to use kinetic energies below 200 keV without excessive transmission losses due to angular straggling. At sufficiently low energies, no additional acceleration is required after ions have been extracted from the ion source.
    Type: Grant
    Filed: April 7, 2011
    Date of Patent: July 29, 2014
    Assignee: Eth Zürich, Eth Transfer
    Inventors: Hans-Arno Synal, Tim Schulze-König, Martin Suter
  • Patent number: 8785889
    Abstract: An ion implantation system and process, in which the performance and lifetime of the ion source of the ion implantation system are enhanced, by utilizing isotopically enriched dopant materials, or by utilizing dopant materials with supplemental gas(es) effective to provide such enhancement.
    Type: Grant
    Filed: March 15, 2013
    Date of Patent: July 22, 2014
    Assignee: Advanced Technology Materials, Inc.
    Inventors: Robert Kaim, Joseph D. Sweeney, Anthony M. Avila, Richard S. Ray
  • Patent number: 8785843
    Abstract: A sampling cone of a mass spectrometer is disclosed having a metallic boride coating such as titanium diboride.
    Type: Grant
    Filed: June 20, 2013
    Date of Patent: July 22, 2014
    Assignee: Micromass UK Limited
    Inventors: Gordon A. Jones, David S. Douce, Amir Farooq
  • Patent number: 8785881
    Abstract: An ionic liquid ion source can include a microfabricated body including a base and a tip. The body can be formed of a porous material compatible with at least one of an ionic liquid or room-temperature molten salt. The body can have a pore size gradient that decreases from the base of the body to the tip of the body, such that the at least one of an ionic liquid or room-temperature molten salt is capable of being transported through capillarity from the base to the tip.
    Type: Grant
    Filed: November 1, 2013
    Date of Patent: July 22, 2014
    Assignee: Massachusetts Institute of Technology
    Inventors: Paulo C. Lozano, Steven Mark Arestie
  • Publication number: 20140197333
    Abstract: A mass analyzer includes a desolvation chamber into which an upstream gas is injected to provide a counter-flow to said downstream flow in the chamber. The counter-flow may slow the downstream flow of solvated ionized particles in the chamber, while allowing lighter desolvated ions to travel toward an outlet aperture of the desolvation chamber.
    Type: Application
    Filed: January 14, 2013
    Publication date: July 17, 2014
    Applicant: Ionics Mass Spectrometry Group Inc.
    Inventors: Charles Jolliffe, Lisa Cousins, Gholamreza Javahery
  • Patent number: 8779354
    Abstract: A mass spectrometer is disclosed comprising an Electron Transfer Dissociation cell. Positive analyte ions are fragmented into fragment ions upon colliding with singly charged negative reagent ions with the cell. The cell comprises a plurality of ring electrodes which form a spherical trapping volume. Ions experience negligible RF heating over the majority of the trapping volume which enables the kinetic energy of the analyte and reagent ions to be reduced to just above thermal temperatures. An Electron Transfer Dissociation cell having an enhanced sensitivity is thereby provided. Fragment ions created within the cell may be cooled and may be transmitted onwardly to an orthogonal acceleration Time of Flight mass analyser enabling a significant improvement in the resolution of the mass analyser to be obtained.
    Type: Grant
    Filed: April 23, 2012
    Date of Patent: July 15, 2014
    Assignee: Micromass UK Limited
    Inventors: Martin Green, Jason Lee Wildgoose, Jeffrey Mark Brown
  • Patent number: 8779383
    Abstract: Isotopically enriched silicon precursor compositions are disclosed, as useful in ion implantation to enhance performance of the ion implantation system, in relation to corresponding ion implantation lacking such isotopic enrichment of the silicon precursor composition. The silicon dopant composition includes at least one silicon compound that is isotopically enriched above natural abundance in at least one of 28Si, 29Si, and 30Si, and may include a supplemental gas including at least one of a co-species gas and a diluent gas. Dopant gas supply apparatus for providing such silicon dopant compositions to an ion implanter are described, as well as ion implantation systems including such dopant gas supply apparatus.
    Type: Grant
    Filed: May 21, 2013
    Date of Patent: July 15, 2014
    Assignee: Advanced Technology Materials, Inc.
    Inventors: James J. Mayer, Richard S. Ray, Robert Kaim, Joseph D. Sweeney
  • Patent number: 8779395
    Abstract: An ion implantation system for improving performance and extending lifetime of an ion source is disclosed whereby the selection, delivery, optimization and control of the flow rate of a co-gas into an ion source chamber is automatically controlled.
    Type: Grant
    Filed: December 1, 2011
    Date of Patent: July 15, 2014
    Assignee: Axcelis Technologies, Inc.
    Inventors: Neil K. Colvin, Tseh-Jen Hsieh
  • Patent number: 8772710
    Abstract: The present invention generally relates to a low temperature plasma probe for desorbing and ionizing at least one analyte in a sample material and methods of use thereof. In one embodiment, the invention generally relates to a low temperature plasma probe including: a housing having a discharge gas inlet port, a probe tip, two electrodes, and a dielectric barrier, in which the two electrodes are separated by the dielectric barrier, in which application of voltage from a power supply generates a low temperature plasma, and in which the low temperature plasma is propelled out of the discharge region by the electric field and/or the discharge gas flow.
    Type: Grant
    Filed: August 26, 2013
    Date of Patent: July 8, 2014
    Assignee: Purdue Research Foundation
    Inventors: Zheng Ouyang, Jason Harper, Nicholas Charipar, Robert Graham Cooks
  • Publication number: 20140183376
    Abstract: An ion source for use in a radiation generator tube includes a back passive cathode electrode, a passive anode electrode downstream of the back passive cathode electrode, a magnet adjacent the passive anode electrode, and a front passive cathode electrode downstream of the passive anode electrode. The front passive cathode electrode and the back passive cathode electrode define an ionization region therebetween. At least one ohmically heated cathode is configured to emit electrons into the ionization region. The back passive cathode electrode and the passive anode electrode, and the front passive cathode electrode and the passive anode electrode, have respective voltage differences therebetween, and the magnet generating a magnetic field, such that a Penning-type trap is produced to confine the electrons to the ionization region. At least some of the electrons in the ionization region interact with an ionizable gas to create ions.
    Type: Application
    Filed: December 27, 2012
    Publication date: July 3, 2014
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventor: Luke Perkins
  • Publication number: 20140183349
    Abstract: An ion source for use in a radiation generator tube includes a back passive cathode electrode, a passive anode electrode downstream of the back passive cathode electrode, a magnet adjacent the passive anode electrode, and a front passive cathode electrode downstream of the passive anode electrode. The front passive cathode electrode and the back passive cathode electrode define an ionization region therebetween. At least one Spindt cathode is configured to emit electrons into the ionization region. The back passive electrode electrode and the passive anode electrode, and the front passive cathode electrode and the passive anode electrode, have respective voltage differences therebetween, and the magnet generates a magnetic field, such that a Penning-type trap is produced to confine the electrons to the ionization region. At least some of the electrons in the ionization region interact with an ionizable gas to create ions.
    Type: Application
    Filed: December 27, 2012
    Publication date: July 3, 2014
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Jonna Flores, Luke Perkins
  • Publication number: 20140183348
    Abstract: An ion source for use in a particle accelerator includes at least one cathode. The at least one cathode has an array of nano-sized projections and an array of gates adjacent the array of nano-sized projections. The array of nano-sized projections and the array of gates have a first voltage difference such that an electric field in the cathode causes electrons to be emitted from the array of nano-sized projections and accelerated downstream. There is a ion source electrode downstream of the at least one cathode, and the at least one cathode and the ion source electrode have the same voltage applied such that the electrons enter the space encompassed by the ion source electrode, some of the electrons as they travel within the ion source electrode striking an ionizable gas to create ions.
    Type: Application
    Filed: December 27, 2012
    Publication date: July 3, 2014
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Jani Reijonen, Luke Perkins, Harold Pfutzner
  • Patent number: 8765072
    Abstract: Superior hydroxyls are provided which have effects on organic and inorganic compounds and/or pollutants over substantial periods of time and/or at substantial distances from where the superior hydroxyls are generated. Also provided is a hydroxyl generator, in which UV-lamps are positioned such that the coronas which they produce when emitting UV-radiation fill substantially all of the interior space of the hydroxyl generator. The coronas overlap each other by a maximum amount of between 5% and 25% of the radius of each corona.
    Type: Grant
    Filed: August 31, 2012
    Date of Patent: July 1, 2014
    Assignee: HGI Industries, Inc.
    Inventor: Guy J. E. Morneault
  • Publication number: 20140175301
    Abstract: A ion source comprises: a chamber (45), an injection to inject matter into the chamber, wherein said matter comprises at least a first species, a tip with an apex located in the chamber, wherein the apex has a surface made of a metallic second species, a generator to generate ions of said species, and a regulation system adapted to set operative conditions of the chamber to alternatively generate ions from the gaseous first species, and ions from the non-gaseous metallic second species.
    Type: Application
    Filed: June 5, 2012
    Publication date: June 26, 2014
    Applicants: UNIVERSITE LYON 1 CLAUDE BERNARD, CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE -CNRS
    Inventors: Jacques Gierak, Nicolas Allemandou, Klaus Hasselbach, Jean-Paul Leggeri, Guillaume Donnier-Valentin, Stephen Purcell, Pauline Gavand
  • Patent number: 8760054
    Abstract: A method and apparatus is provided for generating a plasma electron flood using microwave radiation. In one embodiment, a microwave PEF apparatus is configured to generate a magnetic field that rapidly decays over a PEF cavity, resulting in a static magnetic field having a high magnetic field strength near one side (e.g., “bottom”) of the PEF cavity and a low magnetic field strength (e.g., substantially zero) near the opposite side (e.g., “top”) of the PEF comprising an elongated extraction slit. In one particular embodiment, the one or more permanent magnets are located at a position that is spatially opposed to the location of the elongated extraction slit to achieve the rapidly decaying magnetic field. The magnetic field results in an electron cyclotron frequency in a region of the cavity equal to or approximately equal to a microwave radiation frequency so that plasma is generated to diffuse through the extraction apertures.
    Type: Grant
    Filed: January 21, 2011
    Date of Patent: June 24, 2014
    Assignee: Axcelis Technologies Inc.
    Inventors: William DiVergilio, Bo Vanderberg
  • Patent number: 8759766
    Abstract: Provided is an air supply tube including an inlet port that takes in air, an outlet port that is arranged opposite a portion of an elongated target structure in a longitudinal direction, to which air taken in from the inlet port is to be supplied, and has an elongated opening shape, a channel portion in which a channel space for allowing air to flow between the inlet port and the outlet port is formed, and plural suppressing portions that suppress the flow of air, wherein the plural suppressing portions include at least a most downstream suppressing portion, a first upstream suppressing portion that is provided in a part initially located on the upstream side in the air flow direction, and a gap regulating portion that forms an extended gap at the same interval.
    Type: Grant
    Filed: April 5, 2012
    Date of Patent: June 24, 2014
    Assignee: Fuji Xerox Co., Ltd.
    Inventors: Yasunori Momomura, Kazuki Inami, Yuki Nagamori, Koji Otsuka, Masafumi Kudo
  • Patent number: 8759788
    Abstract: In one embodiment an ion source includes an arc chamber and an emitter having a surface disposed in the arc chamber, where the emitter is configured to generate a plasma in the arc chamber. The ion source further includes a repeller having a repeller surface positioned opposite the emitter surface, and a hollow cathode coupled to the repeller and configured to provide a feed material into the arc chamber.
    Type: Grant
    Filed: March 11, 2013
    Date of Patent: June 24, 2014
    Assignee: Varian Semiconductor Equipment Associates, Inc.
    Inventor: Neil Bassom
  • Publication number: 20140166870
    Abstract: An ion source includes a cathode to emit electrons, a cathode grid downstream of the cathode, a reflector electrode downstream of the cathode grid, reflector grid radially inward of the reflector electrode, and an extractor electrode downstream of the reflector electrode, the extractor electrode and cathode grid defining an ionization region therebetween. The cathode and the cathode grid have a first voltage difference such the electrons are accelerated through the cathode grid and into the ionization region on a trajectory toward the extractor electrode. The reflector grid and the extractor electrode have a second voltage difference less than the first voltage difference such that the electrons slow as they near the extractor electrode and are repelled on a trajectory toward the reflector electrode. The reflector electrode has a negative potential such that the electrons are repelled away from the reflector electrode and into the ionization region.
    Type: Application
    Filed: December 19, 2012
    Publication date: June 19, 2014
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Jani Reijonen, Irina Molodetsky, Kenneth E. Stephenson
  • Publication number: 20140166872
    Abstract: An ion source includes a cathode emitting primary electrons, a cathode grid downstream of the cathode, a reflector electrode downstream of the cathode grid, a reflector grid radially inward of the reflector electrode, and an extractor electrode downstream of the reflector electrode. The cathode and the cathode grid have a voltage difference such that the electric field accelerates the primary electrons on a trajectory toward the extractor electrode. The reflector grid and the extractor electrode have a voltage difference such that the electric field repels the primary electrons on a trajectory away from the extractor electrode and toward the reflector electrode. The cathode and reflector electrode have a voltage difference such that some primary electrons strike the reflector electrode, creating secondary electrons. The reflector grid has a positive potential such that the electric field attracts the primary and secondary electrons into the ionization region where they interact with ionizable gas.
    Type: Application
    Filed: December 19, 2012
    Publication date: June 19, 2014
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Jani Reijonen, Irina Molodetsky, Kenneth E. Stephenson
  • Patent number: 8754383
    Abstract: A closed plasma channel (“CPC”) superconductor which, in a first embodiment, is comprised of an elongated, close-ended vacuum conduit comprising a cylindrical wall having a longitudinal axis and defining a transmission space for containing an ionized gas of vapor plasma (hereinafter “plasma components”), the plasma components being substantially separated into regionalized channels parallel to the longitudinal axis in response to a static magnetic field produced within the transmission space. Each channel is established along the entire length of the transmission space. At least one channel is established comprised primarily of free-electrons which provide a path of least resistance for the transmission of energy therethrough. Ionization is established and maintained by the photoelectric effect of a light source of suitable wavelength to produce the most conductive electrical transmission medium.
    Type: Grant
    Filed: February 5, 2013
    Date of Patent: June 17, 2014
    Assignee: Glenn Lane Family Limited Liability Limited Partnership
    Inventor: Glenn E. Lane
  • Patent number: 8754365
    Abstract: The present invention is directed to a method and device to desorb an analyte using heat to allow desorption of the analyte molecules, where the desorbed analyte molecules are ionized with ambient temperature ionizing species. In various embodiments of the invention a current is passed through a mesh upon which the analyte molecules are present. The current heats the mesh and results in desorption of the analyte molecules which then interact with gas phase metastable neutral molecules or atoms to form analyte ions characteristic of the analyte molecules.
    Type: Grant
    Filed: March 12, 2013
    Date of Patent: June 17, 2014
    Assignee: Ionsense, Inc.
    Inventors: Jordan Krechmer, Brian D. Musselman
  • Patent number: 8748845
    Abstract: Ion sources, systems and methods are disclosed.
    Type: Grant
    Filed: January 24, 2012
    Date of Patent: June 10, 2014
    Assignee: Carl Zeiss Microscopy, LLC
    Inventors: Billy W. Ward, John A. Notte, Louis S. Farkas, Randall G. Percival, Raymond Hill, Klaus Edinger, Lars Markwort, Dirk Aderhold, Ulrich Mantz
  • Publication number: 20140151573
    Abstract: In a multi-energy ion implantation process, an ion implanting system having an ion source, an extraction assembly, and an electrode assembly is used to implant ions into a target. An ion beam having a first energy may be generated using the ion source and the extraction assembly. A first voltage may be applied across the electrode assembly. The ion beam may enter the electrode assembly at the first energy, exit the electrode assembly at a second energy, and implant ions into the target at the second energy. A second voltage may be applied across the electrode assembly. The ion beam may enter the electrode assembly at the first energy, exit the electrode assembly at a third energy, and implants ions into the target at the third energy. The third energy may be different from the second energy.
    Type: Application
    Filed: February 5, 2014
    Publication date: June 5, 2014
    Applicant: Advanced Ion Beam Technology, Inc.
    Inventor: Zhimin Wan
  • Patent number: 8742363
    Abstract: The invention relates to a method for ionizing and identifying gases, wherein the gases to be identified are ionized in a reaction chamber and the product ions are measured, wherein the measurement of the product ions takes place via electrical fields acting on the product ions and the detection is performed with a detector for ions. It is provided that ionization takes place via UV radiation, and that simultaneously or sequentially ionization by electrons takes place. The invention further relates to a device for ionizing and identifying gases, which includes an ion source chamber having an ion source and an ion mobility spectrometer. For this purpose, a partition between the ion source chamber and the ion mobility spectrometer has a UV-transparent window and a window permeable for electrons, wherein UV radiation and electron radiation can be generated in the ion source chamber with the ion source.
    Type: Grant
    Filed: August 11, 2011
    Date of Patent: June 3, 2014
    Assignee: Airsense Analytics GmbH
    Inventors: Wolf Münchmeyer, Bert Ungethüm, Andreas Walte
  • Patent number: 8729494
    Abstract: An ion source is disclosed wherein a sample is introduced into the sample chamber of the ion source in the gas phase via a sample introduction capillary tube. The sample is directed onto a heated surface coated with an oxidizing reagent such as copper oxide. Carbon in the sample is oxidized to form carbon dioxide. The resulting carbon dioxide molecules are then ionised by electron impact ionization with an electron beam and the resulting ions are passed to a mass analyzer for mass analysis.
    Type: Grant
    Filed: July 16, 2009
    Date of Patent: May 20, 2014
    Assignee: Micromas UK Limited
    Inventor: Robert Harold Bateman
  • Patent number: 8729495
    Abstract: Suspended nanotubes are used to capture and ionize neutral chemical units, such as individual atoms, molecules, and condensates, with excellent efficiency and sensitivity. Applying a voltage to the nanotube(s) (with respect to a grounding surface) creates an attractive potential between a polarizable neutral chemical unit and the nanotube that varies as 1/r2, where r is the unit's distance from the nanotube. An atom approaching the nanotube with a sub-threshold angular momentum is captured by the potential and eventually spirals towards the nanotube. The atom ionizes as in comes into close proximity with a sidewall of the nanotube, creating an ion whose polarity matches the polarity of the electric potential of the nanotube. Repulsive forces eject the ion, which can be detected more easily than a neutral chemical unit. Suspended nanotubes can be used to detect small numbers of neutral chemical units (e.g., single atoms) for applications in sensing and interferometry.
    Type: Grant
    Filed: March 24, 2011
    Date of Patent: May 20, 2014
    Assignee: President and Fellows of Harvard College
    Inventors: Lene V. Hau, Jene A. Golovchenko, Anne Goodsell
  • Patent number: 8729496
    Abstract: In various embodiments of the invention, a cargo container can be monitored at appropriate time intervals to determine that no controlled substances have been shipped with the cargo in the container. The monitoring utilizes reactive species produced from an atmospheric analyzer to ionize analyte molecules present in the container which are then analyzed by an appropriate spectroscopy system. In an embodiment of the invention, a sorbent surface can be used to absorb, adsorb or condense analyte molecules within the container whereafter the sorbent surface can be interrogated with the reactive species to generate analyte species characteristic of the contents of the container.
    Type: Grant
    Filed: March 15, 2013
    Date of Patent: May 20, 2014
    Assignee: Ionsense, Inc.
    Inventor: Brian D. Musselman
  • Patent number: 8723110
    Abstract: An apparatus for generating ions includes an Electrospray ionization source configured to provide a spray of charged droplets from a sample solution during operation of the apparatus; an atmospheric pressure chemical ionization (APCI) source including a corona discharge needle configured to produce a corona discharge that further ionizes the spray during operation of the apparatus; and a gas delivery system configured to deliver a gas flow to the corona discharge needle during operation of the apparatus, wherein the gas flow comprises a reagent ion gas which facilitates ionization of the spray by the corona discharge.
    Type: Grant
    Filed: August 26, 2011
    Date of Patent: May 13, 2014
    Assignees: PerkinElmer Health Sciences, Inc., Chem-Space Associates, Inc.
    Inventors: Craig M. Whitehouse, Thomas P. White, Ross C. Willoughby, Edward William Sheehan
  • Patent number: 8723143
    Abstract: A focused ion beam (FIB) system is disclosed, comprising an inductively coupled plasma ion source, an insulating plasma chamber containing the plasma, a conducting source biasing electrode in contact with the plasma and biased to a high voltage to control the ion beam energy at a sample, and a plurality of apertures. The plasma within the plasma chamber serves as a virtual source for an ion column comprising one or more lenses which form a focused ion beam on the surface of a sample to be imaged and/or FIB-processed. The plasma is initiated by a plasma igniter mounted near or at the column which induces a high voltage oscillatory pulse on the source biasing electrode. By mounting the plasma igniter near the column, capacitive effects of the cable connecting the source biasing electrode to the biasing power supply are minimized. Ion beam sputtering of the apertures is minimized by proper aperture materials selection.
    Type: Grant
    Filed: October 19, 2011
    Date of Patent: May 13, 2014
    Assignee: FEI Company
    Inventors: Anthony Graupera, Sean Kellogg, Tom Miller, Dustin Laur, Shouyin Zhang, Antonius Bastianus Wilhelmus Dirriwachter
  • Patent number: 8716675
    Abstract: An alternating current electrospray mass spectrometry device includes an electrospray device having at least one emitter providing a passageway for transmission of an analyte sample. At least one conductive element is in electrical communication with the at least one emitter. A power source generates an alternating current electric field to form a liquid cone at a tip of the emitter and ionizes the analyte sample present in the liquid cone. The frequency of the electric field entrains low mobility ions in the liquid cone. The AC electric field causes the emitter to discharge the liquid cone as a liquid aerosol drop, and a mass spectrometry device analyzes the ionized analyte sample to determine the composition of the contained analyte sample.
    Type: Grant
    Filed: April 27, 2011
    Date of Patent: May 6, 2014
    Assignee: University of Notre Dame du Lac
    Inventors: Nishant Chetwani, Catherine Cassou, David Go, Hsueh-Chia Chang
  • Patent number: 8716681
    Abstract: In one embodiment, a sample processing method includes placing a sample on a sample placing module, and setting first processing boxes on one side of slice formation scheduled regions of the sample, and second processing boxes on the other side thereof. The method includes processing the sample by performing a primary scan which sequentially scans the first processing boxes with a continuously generated ion beam, and a secondary scan which sequentially scans the second processing boxes with a continuously generated ion beam, to form slices of the sample. The primary and secondary scans are performed so that a first scanning condition for scanning first regions within the first and second processing boxes is set different from a second scanning condition for scanning second regions between the first processing boxes and between the second processing boxes, to allow frame portions of the sample to remain in the second regions.
    Type: Grant
    Filed: August 30, 2013
    Date of Patent: May 6, 2014
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Hitomi Kawaguchiya, Mitsuo Koike
  • Patent number: 8716673
    Abstract: A single column inductively coupled plasma source with user selectable configurations operates in ion-mode for FIB operations or electron mode for SEM operations. Equipped with an x-ray detector, energy dispersive x-ray spectroscopy analysis is possible. A user can selectively configure the ICP to prepare a sample in the ion-mode or FIB mode then essentially flip a switch selecting electron-mode or SEM mode and analyze the sample using EDS or other types of analysis.
    Type: Grant
    Filed: November 29, 2011
    Date of Patent: May 6, 2014
    Assignee: FEI Company
    Inventor: Brian Roberts Routh, Jr.
  • Patent number: 8710456
    Abstract: A multi-sectional linear ionizing bar with at least four elements is disclosed. First, disclosed bars may include at least one ionization cell with at least one axis-defining linear ion emitter for establishing an ion cloud along the length thereof. Second, disclosed bars may include at least one reference electrode. Third, disclosed bars may include a manifold for receiving gas or air from a source and for delivering same past the linear emitter(s) such that substantially none of the gas/air flows into the ion cloud. Fourth, disclosed bars may include means for receiving the ionizing voltage and for delivering same to the linear emitter(s) to thereby establish the ion cloud. In this way, disclosed ionizing bars may transport ions from the plasma region toward a charge neutralization target without inducing substantial vibration of the linear emitter and without substantial contaminants from the gas/air flow reaching the linear emitter.
    Type: Grant
    Filed: July 22, 2013
    Date of Patent: April 29, 2014
    Assignee: Illinois Tool Works Inc.
    Inventors: Aleksey Klochkov, Peter Gefter, Steven Bernard Heymann, Leslie W. Partridge, Greenberry Bedford Brown, Matthew T. Antonelli
  • Patent number: 8710457
    Abstract: The process of the present application facilitates the production of electric energy by the excitation and capture of electrons from atoms, molecules and ions from ground or water sources, or any other form of matter that can be passed along the surface or through the electron extraction assembly. The electrons are captured, collected, isolated and controlled for distribution as electric energy. It is an energy efficient process for the capture of electrons and for the production of electric energy. These results are accomplished by the excitation and capture of electrons from the object particles by electrically charged components in an electric field. It can operate continuously without interruption. Through the subject process, electric energy can be supplied individually to each structure, community or demand location allowing independence from any other energy source.
    Type: Grant
    Filed: July 10, 2013
    Date of Patent: April 29, 2014
    Inventor: Eugene B. Pamfiloff
  • Patent number: 8710473
    Abstract: A droplet generation and detection device may include: a droplet generation unit for outputting a charged droplet; at least one droplet sensor including a magnetic circuit including a coil configured of an electrically conductive material, the magnetic circuit being disposed such that the charged droplet passes around the magnetic circuit, and a current detection unit for detecting current flowing in the coil and outputting a detection signal; and a signal processing circuit for detecting the charged droplet based on the detection signal.
    Type: Grant
    Filed: October 28, 2011
    Date of Patent: April 29, 2014
    Assignee: Gigaphoton Inc.
    Inventors: Hakaru Mizoguchi, Kouji Kakizaki, Osamu Wakabayashi, Masahiro Inoue
  • Publication number: 20140110598
    Abstract: Various embodiments provide an ion source device and a method for providing the ion source. An exemplary ion source device can include an arc chamber, a filament, a reflector, a slit outlet, a source gas inlet, and/or a cleaning gas inlet. The filament can be configured to generate thermo-electrons in the arc chamber. The reflector can be configured to reflect the thermo-electrons back to the arc chamber. The slit outlet can be configured to exit a gaseous material out of the arc chamber. The source gas inlet and the cleaning gas inlet can be located on a same sidewall of the arc chamber configured to respectively introduce an ion source gas and an inert cleaning gas into the arc chamber.
    Type: Application
    Filed: December 3, 2013
    Publication date: April 24, 2014
    Applicant: Semiconductor Manufacturing International (Shanghai) Corporation
    Inventors: LULEI WU, LEON SHAN, CHUNRONG DONG