Iron Group Metal (iron, Cobalt, Nickel) Patents (Class 252/513)
  • Patent number: 11655345
    Abstract: Microelectronics and the manufacture of microelectronic components for an integrated circuit operating at a high frequency are disclosed. Production of micro-inductors having a high induction density and high quality factor, in particular at a usage frequency greater than 1 GHz, or even greater than 5 GHz, is disclosed. A nanocomposite 1 including magnetic alloy nanoparticles 10 at least partially includes a soft magnetic alloy, an insulating matrix 20, and insulating nanoparticles 30, the nanoparticles being supported in the matrix and the soft magnetic alloy nanoparticles being encapsulated by insulating nanoparticles.
    Type: Grant
    Filed: May 2, 2017
    Date of Patent: May 23, 2023
    Assignee: COMMISSARIAT A L'ENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
    Inventor: Bernard Viala
  • Patent number: 11557562
    Abstract: An anisotropic conductive film can reduce the conduction resistance of an anisotropic conductively connected connection structure, and can reliably suppress the occurrence of short-circuits. The film has a structure wherein insulating particle-including conductive particles, wherein insulating particles adhere to the surfaces of conductive particles, are distributed throughout an insulating resin layer. In the insulating particle-including conductive particles, a number of insulating particles in contact with the conductive particles with respect to a film thickness direction is lower than with respect to a film planar direction. Preferably, a number of the insulating particles overlapping with the conductive particles when one of a front and rear film surface of the anisotropic conductive film is viewed in plan view is lower than a number of the insulating particles overlapping with the conductive particles when the other of the film surfaces is viewed in plan view.
    Type: Grant
    Filed: October 18, 2017
    Date of Patent: January 17, 2023
    Assignee: DEXERIALS CORPORATION
    Inventors: Takeshi Miyake, Reiji Tsukao, Tatsurou Fukaya
  • Patent number: 11309101
    Abstract: The present invention relates to a conductive paste for a solar cell electrode, including a metal powder, a glass frit, an organic binder, a silicone-based additive and a solvent, wherein the silicone-based additive includes trimethylsiloxy-terminated polydimethylsiloxane, whereby an electrode formed using the conductive paste can be improved in aspect ratio, that is, line width and line height, thus increasing conductivity, and a solar cell having high power generation efficiency can be provided by enlarging the light-receiving surface through decreasing the line width of the electrode.
    Type: Grant
    Filed: October 18, 2017
    Date of Patent: April 19, 2022
    Assignee: LS-NIKKO COPPER INC.
    Inventors: Chung Ho Kim, Hwa Young Noh, Mun Seok Jang, Tae Hyun Jun, In Chul Kim, Min Soo Ko
  • Patent number: 11211598
    Abstract: A nanofiber based micro-structured material including metal fibers with metal oxide coatings and methods are shown. In one example, nanofiber based micro-structured material is used as an electrode in a battery, such as a lithium ion battery, where the nanofibers of micro-structured material form a nanofiber cloth with free-standing, core-shell structure.
    Type: Grant
    Filed: November 16, 2016
    Date of Patent: December 28, 2021
    Assignee: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
    Inventors: Cengiz S. Ozkan, Mihrimah Ozkan, Jeffrey Bell, Rachel Ye
  • Patent number: 11094936
    Abstract: Disclosed is a tungsten-doped lithium manganese iron phosphate-based particulate for a cathode of a lithium-ion battery. The particulates include a composition represented by a formula LixMn1-y-z-fFeyMzWfPaO4a±pC, wherein x, y, z, f, a, p, and M are as defined herein. Also disclosed is a powdery material including the particulates, and a method for preparing the powdery material.
    Type: Grant
    Filed: December 17, 2019
    Date of Patent: August 17, 2021
    Assignee: HCM CO., LTD.
    Inventors: Chien-Wen Jen, Hsin-Ta Huang, Chih-Tsung Hsu, Yi-Hsuan Wang
  • Patent number: 11031151
    Abstract: The devices and methods described herein push forward the resolution limits of directed self-assembly (DSA) technology for advanced device applications. Specifically described herein, are compositions of bioinspired DSA materials and methods using these bioinspired DSA materials to form sub-7 nm line-space patterns and to achieve functional nanoscopic structures, e.g., conducting nanowires on a substrate.
    Type: Grant
    Filed: February 27, 2020
    Date of Patent: June 8, 2021
    Assignee: THE UNIVERSITY OF NORTH CAROLINA AT GREENSBORO
    Inventors: Daniel J. C. Herr, Hemali Rathnayake, Kristen Dellinger
  • Patent number: 10984921
    Abstract: Provided is a conductive paste which makes it possible to form a conductive layer having excellent conductivity even when spherical copper powder having a small particle diameter is used. Disclosed is a conductive paste containing a conductive filler and a binder resin.
    Type: Grant
    Filed: June 28, 2018
    Date of Patent: April 20, 2021
    Assignee: SEKISUI CHEMICAL CO., LTD.
    Inventors: Masahiro Ishii, Akira Nakasuga, Shoji Nozato, Shigekatsu Ohnishi
  • Patent number: 10822511
    Abstract: An ink composition for photonic sintering and a method or producing the ink composition, the ink composition includes: metal nanoparticles comprising a first metal satisfying interaction formula 1; an organic non-aqueous binder; and a non-aqueous solvent. Interaction formula 1 is A1/A2?0.2, where A1/A2 is a ratio, in the x-ray photoelectron spectrum on the surface of the first metal, in which first metal 2p3/2 peak area of the oxide of the first metal (A1) is divided by first metal 2p3/2 peak area of the first metal (A2).
    Type: Grant
    Filed: October 20, 2016
    Date of Patent: November 3, 2020
    Assignee: KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
    Inventors: Su Yeon Lee, Young Min Choi, Sun Ho Jeong, Beyong Hwan Ryu, Tae Gon Kim, Sang Jin Oh, Eun Jung Lee, Ye Jin Jo
  • Patent number: 10813224
    Abstract: A device including an electrically conducting track arranged on a support includes a step of supply of the support, and a step of formation of the electrically conducting track on the support including a step of supply of a solution intended to be deposited on the support, a step of deposition of the solution by printing on the support. The step of supply of the solution is such that the solution supplied includes a mixture of a solvent, of a set of metal particles and of a metallic material having a melting point below that of the metal particles of the set of metal particles, and the method includes a step of melting of the metallic material which results in the formation of a solder of metallic material between metal particles of the set of metal particles.
    Type: Grant
    Filed: June 9, 2017
    Date of Patent: October 20, 2020
    Assignee: Commissariat a l'energie atomique et aux energies alternatives
    Inventors: Mohammed Benwadih, Abdelkader Aliane
  • Patent number: 10749146
    Abstract: An example of a thermal composite includes a substrate, a primer layer, a first adhesive layer, a blanket layer, a second adhesive layer, and a metal layer. The blanket layer includes basalt fibers or glass fibers. The thermal composite may be incorporated into a battery pack as a battery enclosure.
    Type: Grant
    Filed: December 28, 2016
    Date of Patent: August 18, 2020
    Assignee: GM GLOBAL TECHNOLOGY OPERATIONS LLC
    Inventors: Elisabeth J. Berger, Kestutis A. Sonta
  • Patent number: 10620121
    Abstract: Disclosed herein are methods comprising illuminating a first location of a plasmonic substrate with electromagnetic radiation, wherein the electromagnetic radiation comprises a wavelength that overlaps with at least a portion of the plasmon resonance energy of the plasmonic substrate. The plasmonic substrate can be in thermal contact with a liquid sample comprising a plurality of particles, the liquid sample having a first temperature. The methods can further comprise generating a confinement region at a location in the liquid sample proximate to the first location of the plasmonic substrate, wherein at least a portion of the confinement region has a second temperature that is greater than the first temperature such that the confinement region is bound by a temperature gradient. The methods can further comprise trapping at least a portion of the plurality of particles within the confinement region.
    Type: Grant
    Filed: April 19, 2017
    Date of Patent: April 14, 2020
    Assignee: BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM
    Inventors: Yuebing Zheng, Linhan Lin, Xiaolei Peng
  • Patent number: 10550291
    Abstract: Oxidation-resistant electrically-conductive metal particles (ORCMP) are disclosed. ORCMPs are comprised of a base-metal core, an oxidation-resistant first shell, and an optional conductive second shell. ORCMPs are low cost alternatives to silver particles in metal fillers for low-temperature, electrically-conductive adhesives. Adhesives including ORCMPs, organic vehicles, and optional conductive metal particles such as silver were formulated to yield conductive films upon curing at low temperatures. Such films can be used in many electronic devices where low-temperature, low cost films are needed.
    Type: Grant
    Filed: August 22, 2016
    Date of Patent: February 4, 2020
    Assignee: Hitachi Chemical Co., Ltd.
    Inventors: Brian E. Hardin, Stephen T. Connor, Craig H. Peters
  • Patent number: 10428216
    Abstract: Golf ball having CoR of at least 0.700 and compression of at least 50 and comprising a layer of a mixture of thermoset or thermoplastic composition and a plurality of conductive nanoshelled structures such as conductive hollow nanoshells and/or nanorice particles. Conductive nanoshelled structures may be included in amount of from about 2 wt % to greater than 50 wt. % of total weight of mixture. Diameter of each conductive nano shelled structure at widest cross-section may be up to 1000 nm. Each conductive hollow nanoshell may have shell thickness to longitudinal diameter ratio of from about 1:3 to about 1:100. Each nanorice particle may have longitudinal diameter of up to 1000 nm. Shell thickness can be from 1 nm to 100 nm and may be controlled. A layer consisting of mixture may have specific gravity that differs from specific gravity of a layer consisting of the thermoset or thermoplastic composition portion of mixture.
    Type: Grant
    Filed: August 28, 2017
    Date of Patent: October 1, 2019
    Assignee: Acushnet Company
    Inventors: Michael J. Sullivan, Brian Comeau, Erin C. McDermott
  • Patent number: 10323157
    Abstract: The present disclosure provides plated particles for use in silver/silver chloride ink for making medical devices. The plated particles include a plurality of silver coated inert particles. The silver coating of each silver coated inert particle is about 10 to 50% by weight of the silver coated inert particle. The silver/silver chloride ink includes a plurality of silver coated inert particles and a plurality of silver chloride particles. A medical device includes a backing layer, a silver/silver chloride ink layer and a conductive adhesive layer.
    Type: Grant
    Filed: August 22, 2016
    Date of Patent: June 18, 2019
    Assignee: Parker-Hannifin Corporation
    Inventors: Jesse A. Hagar, Nicholas Pascucci
  • Patent number: 10276277
    Abstract: An object of the present invention is to provide a resin composition suitable for copper pastes, which can be cured in an ambient atmosphere and has a viscosity within an appropriate range and a low specific resistance after curing. This resin composition includes (A) a copper powder, (B) a thermosetting resin, (C) a fatty acid, (D) an amine, and (E) 4-aminosalicylic acid. Preferably, the (B) component is resol-type phenolic resin. More preferably, the (C) component is at least one selected from oleic acid, linoleic acid, linolenic acid, stearic acid, palmitic acid, lauric acid, butyric acid, and propionic acid.
    Type: Grant
    Filed: July 27, 2016
    Date of Patent: April 30, 2019
    Assignee: NAMICS CORPORATION
    Inventor: Tomoyuki Takahashi
  • Patent number: 10243127
    Abstract: Discussed herein are half-Heusler thermoelectric materials including niobium, iron, antimony, and titanium that are formed by ball-milling and hot-pressing the ball-milled power to obtain various thermoelectric properties and an average grain size above 1 ?m.
    Type: Grant
    Filed: August 29, 2017
    Date of Patent: March 26, 2019
    Assignee: UNIVERSITY OF HOUSTON SYSTEM
    Inventors: Zhifeng Ren, Ran He
  • Patent number: 10141576
    Abstract: There is provided an electrode for a lithium secondary battery. The electrode include a current collector; nanoparticles distributed on a surface of the current collector, each of the nanoparticles including a transition metal or an oxide of the transition metal; and an active material layer disposed on a surface of the current collector having the nanoparticles distributed thereon. This electrode may be employed as a negative electrode for the lithium second battery, to improve a capacity of the lithium second battery.
    Type: Grant
    Filed: January 19, 2016
    Date of Patent: November 27, 2018
    Assignee: Research & Business Foundation Sungkyunkwan University
    Inventors: Su-Jeong Seo, Young-Il Song, Jung-Kab Park, Tae-Yoo Kim, Hwa-Jin Son, Jin-Ha Shin, Jungwoo Lee, Youngil Na, Younglae Cho, Jung-Ho Park, Seung-Bin Baeg, Byung-Wook Ahn, Sook-Young Yun
  • Patent number: 10134503
    Abstract: A semi-conductive crosslinked layer produced from a polymer composition includes at least one polymer A having at least one epoxy function. A cross-linking agent B includes at least one reactive function that can react with the epoxy function of said polymer A in order to allow the cross-linking of said polymer A. The polymer composition also has an electrically conductive filler having a specific surface area BET of at least 100 m2/g according to the ASTM standard D 6556.
    Type: Grant
    Filed: November 12, 2015
    Date of Patent: November 20, 2018
    Assignee: NEXANS
    Inventors: Anthony Combessis, Laurent Keromnes, Melek Maugin, Lucile Carteron
  • Patent number: 10085343
    Abstract: A thin-film capacitor includes a pair of electrode layers composed of a first electrode layer configured to store positive charges and a second electrode layer configured to store negative charges; and a dielectric layer sandwiched between the pair of electrode layers along a lamination direction. The first electrode layer includes a first main electrode layer in contact with the dielectric layer. The second electrode layer includes a second main electrode layer and a second sub-electrode layer, both of which are formed of different metallic materials. The second sub-electrode layer is sandwiched between the dielectric layer and the second main electrode layer along the lamination direction. The second main electrode layer is formed of a material having a melting point lower than both a melting point of a material of the first electrode layer, or the first main electrode layer, and that of a material of the second sub-electrode layer.
    Type: Grant
    Filed: November 6, 2017
    Date of Patent: September 25, 2018
    Assignee: TDK CORPORATION
    Inventors: Hitoshi Saita, Yoshihiko Yano
  • Patent number: 9929411
    Abstract: A carbon-based material according to the present invention contains dopant atoms of metal and non-metal such as nitrogen. In a radial distribution function obtained by Fourier transform of a K-edge EXAFS of the metal, a ratio of “A” to “B” is equal to or more than 4.0, wherein “A” denotes an intensity of the highest one of peaks around a distance equal to a coordinate bond length between atoms of the metal and the non-metal and “B” denotes an intensity of the highest one of peaks around a distance equal to a metallic bond length between atoms of the metal. Note that when the metal is platinum, in a radial distribution function obtained by Fourier transform of an LIII-edge EXAFS of the platinum, a ratio of “A” to “B” is equal to or more than 4.0.
    Type: Grant
    Filed: July 4, 2013
    Date of Patent: March 27, 2018
    Assignee: Panasonic Intellectual Property Management Co., Ltd.
    Inventors: Ryo Kamai, Shuji Nakanishi, Yuya Suzuki, Yuuki Kitade, Takao Hayashi
  • Patent number: 9847534
    Abstract: Methods of forming a metal-alloy graphene nanocomposites are provided. The methods include providing a graphene substrate and forming a conducting polymer layer on a first major surface of the graphene substrate. The methods also include pyrolyzing the conducting polymer layer to form a nitrogen-doped graphene substrate and dispersing a plurality of metal-alloy nanoparticles on a first surface of the nitrogen-doped graphene substrate to form the nanocomposite.
    Type: Grant
    Filed: August 8, 2012
    Date of Patent: December 19, 2017
    Assignee: INDIAN INSTITUTE OF TECHNOLOGY MADRAS
    Inventors: Ramaprabhu Sundara, Vinayan Bhaghavathl Parambath, Rupali Nagar, Rajalakshmi Natarajan
  • Patent number: 9844134
    Abstract: A device comprises a base element and a metallization layer over the base element. The metallization layer comprises pores and has a varying degree of porosity, the degree of porosity being higher in a portion adjacent to the base element than in a portion remote from the base element.
    Type: Grant
    Filed: January 29, 2015
    Date of Patent: December 12, 2017
    Assignee: Infineon Technologies AG
    Inventors: Martin Mischitz, Markus Heinrici, Stefan Schwab
  • Patent number: 9809501
    Abstract: A method of preparing a fine powder of calcium lanthanoid sulfide is disclosed. The method includes spraying soluble calcium and lanthanoid salts into at least one precipitating solution to form a precipitate comprising insoluble calcium and lanthanoid salts, optionally, oxidizing the precipitate comprising insoluble calcium and lanthanoid salts, and sulfurizing the optionally oxidized precipitate to form a fine powder of calcium lanthanoid sulfide. An alternative method for forming the powder is by flame pyrolysis. The calcium lanthanoid sulfide powder produced by either method can have an impurity concentration of less than 100 ppm, a carbon concentration of less than 200 ppm, a BET surface area of at least 50 m2/g, and an average particle size of less than 100 nm.
    Type: Grant
    Filed: January 21, 2010
    Date of Patent: November 7, 2017
    Assignee: The United States of America, as represented by the Secretary of the Navy
    Inventors: Shyam S. Bayya, Woohong Kim, Jasbinder S. Sanghera, Guillermo R. Villalobos, Ishwar D. Aggarwal
  • Patent number: 9777197
    Abstract: Illustrative embodiments of anisotropic conductive adhesive (ACA) and associated methods are disclosed. In one illustrative embodiment, the ACA may comprise a binder curable using UV light and a plurality of particles suspended in the binder. Each of the plurality of particles may comprise a ferromagnetic material coated with a layer of electrically conductive material. The electrically conducting material may form electrically conductive and isolated parallel paths when the ACA is cured using UV light after being subjected to a magnetic field.
    Type: Grant
    Filed: October 13, 2014
    Date of Patent: October 3, 2017
    Assignee: SUNRAY SCIENTIFIC, LLC
    Inventor: S. Kumar Khanna
  • Patent number: 9723715
    Abstract: An anisotropic conductive film, which contains a crystalline resin, an amorphous resin, and conductive particles, wherein the anisotropic conductive film is an anisotropic conductive film configured to anisotropic conductively connect a terminal of a first electronic part and a terminal of a second electronic part, and wherein the crystalline resin contains a crystalline resin containing a bond characterizing a resin, which is identical to a bond characterizing a resin contained in the amorphous resin.
    Type: Grant
    Filed: September 10, 2013
    Date of Patent: August 1, 2017
    Assignee: DEXERIALS CORPORATION
    Inventors: Yasunobu Yamada, Naoya Uesawa, Kazuhisa Aoki
  • Patent number: 9610452
    Abstract: One aspect provides a method of attaching a feedthrough to a titanium housing of an implantable medical device. The method includes applying a sinter paste onto a surface of the housing about a perimeter of an opening through the housing, the sinter paste including a biocompatible bonding material, and placing an insulator of the feedthrough onto the sinter paste so as to cover the opening. The sinter paste is then heated to a temperature less than a beta-transus temperature the titanium of the housing and to a temperature less than a melting point of the biocompatible bonding material for a desired duration to form, from the sinter paste, a sinter joint which bonds the feedthrough to the housing and hermetically seals the opening.
    Type: Grant
    Filed: December 12, 2013
    Date of Patent: April 4, 2017
    Assignee: Heraeus Deutschland GmbH & Co. KG
    Inventors: Jacob Markham, Ulrich Hausch
  • Patent number: 9595814
    Abstract: A connection portion connecting a center electrode and a terminal metal fixture together in a through hole of the insulator includes a resistor and a magnetic substance structure including a magnetic substance and a conductor and being disposed on a leading end side or a rear end side of the resistor while being positioned away from the resistor. The connection portion further includes a first conductive sealing portion, a second conductive sealing portion and a third conductive sealing portion. The first conductive sealing portion is disposed on a leading end side of a first member and is in contact therewith. The second conductive sealing portion is disposed between the first member and a second member and is in contact with the first and second members. The third conductive sealing portion is disposed on a rear end side of the second member and is in contact therewith.
    Type: Grant
    Filed: December 25, 2014
    Date of Patent: March 14, 2017
    Assignee: NGK SPARK PLUG CO., LTD.
    Inventors: Takashi Kasashima, Katsuya Takaoka, Kazuhiro Kurosawa, Kuniharu Tanaka, Toshitaka Honda, Hirokazu Kurono, Haruki Yoshida, Hironori Uegaki
  • Patent number: 9574273
    Abstract: Disclosed herein is a method for preparing a multilayer metal complex having excellent surface properties. Specifically, the present invention relates to a method for preparing a multilayer metal complex having a low cost metal-core/noble metal-shell structure, which has a high mass fraction of noble metals and exhibits excellent surface properties and dispersity.
    Type: Grant
    Filed: September 12, 2014
    Date of Patent: February 21, 2017
    Assignee: OCI COMPANY LTD.
    Inventors: Ki-Hoon Kim, Sung-Koo Kang, Min-Kyung Oh, Hyung-Rak Kim
  • Patent number: 9530554
    Abstract: Disclosed herein is a multilayer coil component including a copper-nickel mixture for an internal electrode, in which a nickel content in the internal electrode is adjusted to thereby optimize the area ratio of nickel to copper while the copper-nickel mixture is used for a material for the internal electrode of the multilayer coil component, thereby preventing deterioration in characteristics of the multilayer coil component, so that ferrite characteristics of the multilayer coil component, such as, impedance (Z), inductance (L), and the like, can be improved.
    Type: Grant
    Filed: November 19, 2013
    Date of Patent: December 27, 2016
    Assignee: SAMSUNG ELECTRO-MECHANICS CO., LTD.
    Inventors: Soo Hwan Son, Jin Woo Hahn, Byeong Cheol Moon
  • Patent number: 9511320
    Abstract: The present invention relates to a polyimide-based macromolecular compound which is produced by using DOCDA and one or more diamines selected from the group consisting of MDA, ODA, PDA, TDA, TrMPD, TeMPD and MBCA; and a gas-separation asymmetrical hollow-fiber membrane comprising the same. The polyimide-based macromolecular compound according to the present invention can advantageously be used in the production of a gas-separation hollow-fiber membrane having an asymmetrical structure since the said compound is highly viscous due to a high molecular weight in addition to having outstanding gas permeability and high selectivity while having excellent high heat resistance, chemical resistance, and mechanical properties and being outstandingly soluble in polar organic solvents.
    Type: Grant
    Filed: April 15, 2015
    Date of Patent: December 6, 2016
    Assignee: KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
    Inventors: Jeong Hoon Kim, Hee Moon Park, Bong Jun Chang, Mihye Yi, Eun-Hee Kim, Chae Young Park
  • Patent number: 9447301
    Abstract: Fusing nanowire inks are described that can also comprise a hydrophilic polymer binder, such as a cellulose based binder. The fusing nanowire inks can be deposited onto a substrate surface and dried to drive the fusing process. Transparent conductive films can be formed with desirable properties.
    Type: Grant
    Filed: September 9, 2015
    Date of Patent: September 20, 2016
    Assignee: C3Nano Inc.
    Inventors: Ying-Syi Li, Xiqiang Yang, Yu Kambe, Xiaofeng Chen, Hua Gu, Steven Michael Lam, Melanie Mariko Inouye, Arthur Yung-Chi Cheng, Alex Da Zhang Tan, Christopher S. Scully, Ajay Virkar
  • Patent number: 9412977
    Abstract: An electro-optical panel product comprises a collection of distinct light-emitting elements formed on a substrate. The product may be a display or lighting apparatus, and each electro-optical element may be an OLED. Distinct local seals are formed below respective individual electro-optical elements or groups of electro-optical elements. Some embodiments combine a metal foil substrate and glass local seals in a flexible bottom-emitting product. The local seal may be used in conjunction with a continuous thin film encapsulation structure. Optical functions can be provided by each local seal, including refraction, filtering, color shifting, and scattering. Each local seal is formed by depositing a low melting temperature glass powder suspension or paste using inkjet technology in openings formed in a starter substrate; the glass powder is fused using a scanning laser beam having a tailored beam profile. The lower encapsulation substrate incorporating local window seals may be wholly or partially pre-formed.
    Type: Grant
    Filed: May 3, 2015
    Date of Patent: August 9, 2016
    Assignee: Global OLED Technology LLC
    Inventor: Rajeev Rohatgi
  • Patent number: 9373839
    Abstract: A negative electrode active material and a secondary battery including the same are provided. More particularly, the present disclosure relates to a negative electrode active material including a Si-metal alloy including Si, the Si being present in the Si-metal alloy in an amount of 66 at % or less, and at least a portion of the Si being crystalline Si. The negative active material can provide a high-capacity battery, which can retain high capacity due to little volumetric expansion during charging and discharging, thereby demonstrating an excellent life characteristic of the secondary battery. The negative electrode active material may include a Si-metal alloy including crystalline Si having a crystal grain size of 30 nm or less. Methods of preparing a negative electrode active material and methods of preparing a secondary battery including the same are also disclosed.
    Type: Grant
    Filed: January 31, 2012
    Date of Patent: June 21, 2016
    Assignee: Samsung SDI Co., Ltd.
    Inventors: Changui Jeong, Chungyoo Lee, Sungwan Moon, Jaehyuk Kim, Yury Matulevich, Seunguh Kwon, Yohan Park, Jongseo Choi
  • Patent number: 9364820
    Abstract: An oxygen reduction catalyst of an embodiment includes: a stack of single-layer graphenes; and a phosphorus compound, wherein some of carbon atoms of the graphenes are replaced by nitrogen atoms, and the phosphorus compound has a peak of phosphorus 2p orbital of 133.0 to 134.5 eV in X-ray photoelectron spectrum.
    Type: Grant
    Filed: February 20, 2013
    Date of Patent: June 14, 2016
    Assignee: KABUSHIKI KAISHA TOSHIBA
    Inventors: Katsuyuki Naito, Yoshihiko Nakano, Norihiro Yoshinaga, Shigeru Matake, Yoshihiro Akasaka
  • Patent number: 9236155
    Abstract: This invention relates to a copper thick film paste composition paste comprising copper powder, a Pb-free, Bi-free and Cd-free borosilicate glass frit, a component selected from the group consisting of ruthenium-based powder, copper oxide powder and mixtures thereof and an organic vehicle. The invention also provides methods of using the copper thick film paste composition to make a copper conductor on a substrate. Typical substrates are selected from the group consisting of aluminum nitride, aluminum oxide and silicon nitride.
    Type: Grant
    Filed: February 4, 2013
    Date of Patent: January 12, 2016
    Assignee: E I DU PONT DE NEMOURS AND COMPANY
    Inventor: Marc Henry Labranche
  • Patent number: 9183968
    Abstract: Fusing nanowire inks are described that can also comprise a hydrophilic polymer binder, such as a cellulose based binder. The fusing nanowire inks can be deposited onto a substrate surface and dried to drive the fusing process. Transparent conductive films can be formed with desirable properties.
    Type: Grant
    Filed: July 31, 2014
    Date of Patent: November 10, 2015
    Assignee: C3Nano Inc.
    Inventors: Ying-Syi Li, Xiqiang Yang, Yu Kambe, Xiaofeng Chen, Hua Gu, Steven Michael Lam, Melanie Mariko Inouye, Arthur Yung-Chi Cheng, Alex Da Zhang Tan, Christopher S. Scully, Ajay Virkar
  • Patent number: 9163152
    Abstract: A UV photoactivatable curable paint formation for providing a cured paint coating of a desired appearance on a substrate by UV irradiation, comprises a UV curable film-forming compound; a UV photoinitiator; a particulate UV reflective material in an effective rate of curing enhancing amount without affecting the resultant desired appearance of the cured paint coating.
    Type: Grant
    Filed: June 29, 2010
    Date of Patent: October 20, 2015
    Assignee: Honda Motor Co., Ltd.
    Inventor: Nirupama Karunaratne
  • Patent number: 9039943
    Abstract: According to example embodiments, a conductive paste includes a conductive component that contains a conductive powder and a titanium (Ti)-based metallic glass. The titanium-based metallic glass has a supercooled liquid region of about 5K or more, a resistivity after crystallization that is less than a resistivity before crystallization by about 50% or more, and a weight increase by about 0.5 mg/cm2 or less after being heated in a process furnace at a firing temperature. According to example embodiments, an electronic device and a solar cell may include at least one electrode formed using the conductive paste according to example embodiments.
    Type: Grant
    Filed: February 24, 2012
    Date of Patent: May 26, 2015
    Assignee: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Se Yun Kim, Eun-Sung Lee, Sang-Soo Jee, Do-Hyang Kim, Ka-Ram Lim
  • Patent number: 9039940
    Abstract: A conductive paste may include a conductive component and an organic vehicle. The conductive component may include an amorphous metal. The amorphous metal may have a lower resistivity after a crystallization process than before the crystallization process, and at least one of a weight gain of about 4 mg/cm2 or less and a thickness increase of about 30 ?m or less after being heated in a process furnace at a firing temperature.
    Type: Grant
    Filed: March 9, 2012
    Date of Patent: May 26, 2015
    Assignee: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Suk Jun Kim, Eun Sung Lee, Se Yun Kim, Sang Soo Jee, Jeong Na Heo
  • Patent number: 9023253
    Abstract: The present invention provides a conductive paste characterized by a crystal-based corrosion binder being combined with a glass frit and mixed with a metallic powder and an organic carrier. Methods for preparing each components of the conductive paste are disclosed including several embodiments of prepare Pb—Te—O-based crystal corrosion binder characterized by melting temperatures in a range of 440° C. to 760° C. and substantially free of any glass softening transition upon increasing temperature. Method for preparing the conductive paste includes mixture of the components and a grinding process to ensure all particle sizes in a range of 0.1 to 5.0 microns. Method of applying the conductive paste for the formation of a front electrode of a semiconductor device is presented to illustrate the effectiveness of the crystal-based corrosion binder in transforming the conductive paste to a metallic electrode with good ohmic contact with semiconductor surface.
    Type: Grant
    Filed: March 7, 2013
    Date of Patent: May 5, 2015
    Assignee: Soltrium Technology, Ltd
    Inventors: Xiaoli Liu, Ran Guo, Delin Li
  • Patent number: 9005485
    Abstract: The present invention relates to a composition for a one-part die attach adhesives material useful for packaging semi-conductors including HB-LED. The composition of the present invention includes a thermal and electrical conductive filler, a polymer matrix and a solvent which form a material with high thermal conductivity, low curing temperature and high self-life temperature. The present invention also relates to a method of preparing said composition by mixing a size-selected and surface-modified filler formulation, a polymer matrix and a non-reactive organic solvent together followed by curing the mixture at a low temperature.
    Type: Grant
    Filed: March 22, 2012
    Date of Patent: April 14, 2015
    Assignee: Nano and Advanced Materials Institute Limited
    Inventors: Chenmin Liu, Dong Lu, Xianxin Lang, Bo Wang, Zhiying Li
  • Patent number: 9005483
    Abstract: Nanoparticle paste formulations can be configured to maintain a fluid state, promote dispensation, and mitigate crack formation during nanoparticle fusion. Such nanoparticle paste formulations can contain an organic matrix and a plurality of metal nanoparticles dispersed in the organic matrix, where the plurality of metal nanoparticles constitute about 30% to about 90% of the nanoparticle paste formulation by weight. The nanoparticle paste formulations can maintain a fluid state and be dispensable through a micron-size aperture. The organic matrix can contain one or more organic solvents, such as the combination of one or more hydrocarbons, one or more alcohols, one or more amines, and one or more organic acids. Optionally, the nanoparticle paste formulations can contain about 0.01 to about 15 percent by weight micron-scale metal particles or other additives.
    Type: Grant
    Filed: February 11, 2013
    Date of Patent: April 14, 2015
    Assignee: Lockheed Martin Corporation
    Inventors: Alfred A. Zinn, Andrew Fried, Tim Stachowiak, Jerome Chang, Randall Mark Stoltenberg
  • Publication number: 20150098165
    Abstract: A conductive paste that includes a (meth)acrylic resin serving as a binder resin, an organic solvent, and a metal powder. The (meth)acrylic resin has a glass transition point Tg in the range of ?60° C. to 120° C., a hydroxyl group content in the range of 0.01% to 5% by weight per molecule, an acid value in the range of 1 to 50 mgKOH/g, and a weight-average molecular weight in the range of 10,000 to 350,000 Mw.
    Type: Application
    Filed: December 15, 2014
    Publication date: April 9, 2015
    Inventors: Toshihiro Suzuki, Naoaki Ogata, Masahito Ishikawa
  • Publication number: 20150083961
    Abstract: Electrically and/or thermally conductive polymer composites and methods of preparing same are provided. In some embodiments, a method for preparing an electrically and/or thermally conductive polymer composite may include (1) mixing a polymer, a conductive particulate filler, and a solvent compatible with the polymer to form a non-conductive polymer solution or melt; (2) processing, the non-conductive polymer solution or melt to form a non-conductive polymer network composition; wherein the presence of solvent during three-dimensional network formation manipulates the polymer network structure; and (3) removing the solvent from the non-conductive polymer network composition to form an electrically and/or thermally conductive polymer composite. The altered polymer chain structure present in the non-conductive polymer network composition is maintained in the composite, and offsets the impact of particulate filler addition including increased modulus, decreased elasticity, and decreased elongation at break.
    Type: Application
    Filed: September 26, 2013
    Publication date: March 26, 2015
    Applicant: U.S. Army Research Laboratory ATTN: RDRL-LOC-I
    Inventors: Randy A. Mrozek, Joseph L. Lenhart
  • Patent number: 8987586
    Abstract: A conductive paste including a conductive powder, a metallic glass, and an organic vehicle, wherein the metallic glass has a resistivity that is decreased when the metallic glass is heat treated at a temperature that is higher than a glass transition temperature of the metallic glass.
    Type: Grant
    Filed: August 10, 2011
    Date of Patent: March 24, 2015
    Assignee: Samsung Electronics Co., Ltd.
    Inventors: Sang-Soo Jee, Eun-Sung Lee, Se-Yun Kim, Sang-Mock Lee, Jun Ho Lee, Do-Hyang Kim, Ka Ram Lim
  • Patent number: 8980139
    Abstract: A method of manufacturing a metal paste for an internal electrode according to the present invention includes preparing each of a metal powder and an organic vehicle; preparing a ceramic inhibitor powder in which a nano glass added with a rare-earth element is mixed; manufacturing a primary mixture by mixing the metal powder of 70 to 95 wt % and the ceramic inhibitor powder of 5 to 30 wt % when each of the metal powder, the organic vehicle, and the ceramic inhibitor powder in which the nano glass added with the rare-earth element is mixed is prepared; manufacturing a secondary mixture by mixing the primary mixture of 50 to 70 wt % and the organic vehicle of 30 to 50 wt % when the primary mixture is manufactured; and manufacturing the metal paste for the internal electrode by filtering the secondary mixture when the secondary mixture is manufactured.
    Type: Grant
    Filed: March 12, 2013
    Date of Patent: March 17, 2015
    Assignee: Samhwa Capacitor Co., Ltd.
    Inventors: Young Joo Oh, Jung Rag Yoon
  • Publication number: 20150070818
    Abstract: An inkjet ink that contains a functional particle having a BET-equivalent particle diameter of 50 to 1000 nm, a rheology-controlling particle having a BET-equivalent particle diameter of 4 to 40 nm, and an organic vehicle. The ink has a viscosity of 1 to 50 mPa·s at a shear rate of 1000 s?1. At a shear rate of 0.1 s?1, the ink has a viscosity equal to or higher than a viscosity ? calculated using the following equation: ?=(D)2×?/104/2+80 [where ? is the viscosity (mPa·s) at a shear rate of 0.1 s?1, D is the BET-equivalent particle diameter (nm) of the functional particle, and ? is the specific gravity of the functional particle].
    Type: Application
    Filed: November 18, 2014
    Publication date: March 12, 2015
    Inventors: Akihiro Tsuru, Taketsugu Ogura, Naoaki Ogata
  • Patent number: 8974703
    Abstract: A conductive paste may include a conductive powder, a metallic glass including a first element having a heat of mixing value with the conductive powder of less than 0, and an organic vehicle, and an electronic device and a solar cell may include an electrode formed using the conductive paste.
    Type: Grant
    Filed: October 26, 2011
    Date of Patent: March 10, 2015
    Assignees: Samsung Electronics Co., Ltd., Industry-Academic Cooperation Foundation, Yonsei University of Yonsei Unversity
    Inventors: Se Yun Kim, Eun Sung Lee, Sang Soo Jee, In Yong Song, Sang Mock Lee, Do-Hyang Kim, Ka Ram Lim
  • Publication number: 20150060739
    Abstract: Provided is a process for preparing an electrode comprising an iron active material. The process comprises first fabricating an electrode comprising an iron active material, and then treating the surface of the electrode with water to thereby create an oxidized surface. The resulting iron electrode is preconditioned prior to any charge-discharge cycle to have the assessable surface of the iron active material in the same oxidation state as in discharged iron negative electrodes active material.
    Type: Application
    Filed: September 5, 2014
    Publication date: March 5, 2015
    Applicant: Encell Technology, Inc.
    Inventors: Randy Gene OGG, Michael RODERS, Michael MEESE
  • Publication number: 20150060740
    Abstract: Provided is a process for preparing an electrode comprising an iron active material. The process comprises first fabricating an electrode comprising an iron active material, and then treating the surface of the electrode with an oxidant solution to thereby create an oxidized surface. The resulting iron electrode is thereby preconditioned prior to any charge-discharge cycle to have the assessable surface of the iron active material in the same oxidation state as in discharged iron negative electrodes active material.
    Type: Application
    Filed: September 5, 2014
    Publication date: March 5, 2015
    Applicant: ENCELL TECHNOLOGY, INC.
    Inventors: Randy Gene OGG, Michael RODERS, Michael MEESE