Abstract: Methods of forming structures including a substrate (e.g., ceramic) and an interface layer comprising a metal are disclosed. Structures and electrochemical cells and batteries are also disclosed. Exemplary methods include flash sintering of metal and ceramic materials. Various structures may be suitable for use as solid electrolytes in solid-state electrochemical cells, as well as for many other applications.

Abstract: A coating having a thickness between 0.1 and 2 mm is obtained from a mixture with the following composition: 10-25% by weight of micronized powder; 40-60% by weight of inorganic gravels of petrographic origin of sizes comprised between 0.063-2 mm; 10-40% by weight of a polymerisable base resin selected from polyurethane, polyester, epoxy or acrylic, with additives, and optionally pigments. The proportion of the mentioned gravel and micronized powder of the coating being up to 90% in an inner most area of interphase between coating and surface of the petrous substrate, covering one third of the thickness of the coating. The method comprises depositing the mentioned mixture on the substrate and vibrating the assembly, and subsequently proceeding to a step of curing and subsequent mechanical finishing of the surface.

Abstract: A method of forming silicon carbide by spark plasma sintering comprises loading a powder comprising silicon carbide into a die and exposing the powder to a pulsed current to heat the powder at a rate of between about 50° C./min and about 200° C./min to a peak temperature while applying a pressure to the powder. The powder is exposed to the peak temperature for between about 30 seconds and about 5 minutes to form a sintered silicon carbide material and the sintered silicon carbide material is cooled. Related structures and methods are disclosed.

Abstract: A method of binder jet printing a part includes depositing a layer of a powder on a working surface and selectively printing a binder solution comprising a binder into the layer of powder in a first pattern to generate a printed layer. The pattern is representative of a structure of a layer of the part. The method also includes selectively printing a channel support agent solution comprising a channel support agent into the layer of powder to generate a green body. The channel support agent is selectively printed in a second pattern representative of an internal channel of the part. The method further includes heating the green body part above a first temperature to remove the binder and generate a brown body part and heating the brown body part above a second temperature to sinter the powder to generate the part having the internal channel generated from removal of the channel support agent.

Abstract: A method of forming silicon carbide by spark plasma sintering comprises loading a powder comprising silicon carbide into a die and exposing the powder to a pulsed current to heat the powder at a rate of between about 50° C./min and about 200° C./min to a peak temperature while applying a pressure to the powder. The powder is exposed to the peak temperature for between about 30 seconds and about 5 minutes to form a sintered silicon carbide material and the sintered silicon carbide material is cooled. Related structures and methods are disclosed.

Abstract: The invention relates to a device for producing products having individual geometries, comprising a substrate carrier device, a material application device for applying material, preferably above the substrate carrier device, which material application device can be moved relative to the substrate carrier device, and a control device which is coupled to the material application device for signaling. According to the invention, the material application device is coupled to an input interface for signaling and for selection of a first or a second application mode, the control device and the application device being designed such as to produce, in the first application mode, a three-dimensional product on the surface of a substrate plate by way of an additive production method, said substrate plate being connected to the substrate carrier device.

Abstract: A method for producing an electrode assembly includes: obtaining a porous active material molded body by molding a constituent material containing a lithium multiple oxide in the form of particles by compression, and then performing a heat treatment at a temperature of 850° C. or higher and lower than the melting point of the used lithium multiple oxide; forming a solid electrolyte layer by applying a liquid containing a constituent material of an inorganic solid electrolyte to the surface of the active material molded body including the inside of each pore of the active material molded body, and then performing a heat treatment; and bonding a current collector to the active material molded body exposed from the solid electrolyte layer.

Abstract: A method for producing an electrode assembly includes: obtaining a porous active material molded body by molding a constituent material containing a lithium multiple oxide in the form of particles by compression, and then performing a heat treatment at a temperature of 850° C. or higher and lower than the melting point of the used lithium multiple oxide; forming a solid electrolyte layer by applying a liquid containing a constituent material of an inorganic solid electrolyte to the surface of the active material molded body including the inside of each pore of the active material molded body, and then performing a heat treatment; and bonding a current collector to the active material molded body exposed from the solid electrolyte layer.

Abstract: The invention relates to a process for producing products having a specific geometry, in particular dental prostheses or auxiliary dental parts, comprising the steps of producing a plurality of products on the surface of a substrate plate by selective curing, in particular by selective sintering or melting, wherein the material is applied in successive layers, one or a plurality of predetermined regions are selectively cured by means of high-energy radiation and joined to one or a plurality of regions of the subjacent layer after each application of a layer, wherein the predetermined regions are predetermined according to a cross-sectional geometry of the product in the respective layer.

Abstract: A method for producing a three dimensional green article includes: (a) providing a slurry composition that contains an inorganic powder, a binder, and a solvent; (b) forming a slurry layer made of the slurry composition; (c) removing the solvent of the slurry layer from an upper surface of the slurry layer so as to form the slurry layer into a green layer with a plurality of pores; (d) scanning the green layer with an energy beam having a power sufficient to vaporize or burn the binder such that the vaporized binder or the burnt binder escapes from the green layer through the pores, while leaving the inorganic powder which is not bound by the binder; and (e) repeating steps (b) to (d).

Abstract: Described herein are nanofibers and methods for making nanofibers that have a plurality of pores. The pores have of any suitable size or shape. In some embodiments the pores are “mesopores”, having a diameter between 2 and 50 nm. In some embodiments, the pores are “ordered”, meaning that they have a substantially uniform shape, a substantially uniform size and/or are distributed substantially uniformly through the nanofiber. Ordering of the pores results in a high surface area and/or high specific surface area. Ordered pores, without limitation, result in a nanofiber that is substantially flexible and/or non-brittle. The nanofibers and methods for making nanofibers may be used, without limitation, in batteries, capacitors, electrodes, solar cells, catalysts, adsorbers, filters, membranes, sensors, fabrics and/or tissue regeneration matrixes.

Abstract: There are provided a fluorine-containing photocurable resin composition and a method of preparing a mold comprising the same and more particularly, a photocurable resin composition having chemical resistance, mechanical properties and high transmittance, etc. as well as being easily wetted with and released from thermosetting or photocurable resins for pattern formation regardless of additional surface treatment, as opposed to the existing polymer resin materials used for resin molds, and a method of preparing a resin mold using the same.

Abstract: A method for integrally molding a metal and a resin and a metal-resin composite structure obtainable by the same are provided. The method comprises forming a nanopore in a surface of a metal sheet; melting a thermoplastic resin on the surface of the metal sheet formed with the nanopore; and injection molding the thermoplastic resin onto the surface of the metal sheet. The thermoplastic resin is a mixture of a main resin and a polyolefin resin, the main resin is a mixture of polyphenylene oxide and a polyamide, and the polyolefin resin has a melting point of about 65° C. to about 105° C.

Abstract: A method for integrally molding a metal and a resin and a metal-resin composite structure obtainable by the same are provided. The method comprises forming a nanopore in a surface of a metal sheet; melting a thermoplastic resin on the surface of the metal sheet formed with the nanopore; and injection molding the thermoplastic resin onto the surface of the metal sheet. The thermoplastic resin includes a mixture of a main resin and a polyolefin resin, the main resin is a polycarbonate, and the polyolefin resin has a melting point of about 65° C. to about 105° C.

Abstract: A method of making garment material, the method having the steps: applying coagulant (34) to a substrate (32); applying a foam (38) of the polymeric material to the substrate (32); allowing the coagulant (34) to coagulate some of the foam (38); and removing uncoagulated foam (38) from the substrate (32) to leave a layer of coagulated polymeric material on the substrate (32).

Abstract: This disclosure provides methods of flash sintering and compositions created by these methods. Methods for sintering multilayered bodies are provided in which a sintered body is produced in less than one minute. In one aspect, each layer is of a different composition, and may be constituted wholly from a ceramic or from a combination of ceramic and metallic particles. When the body includes a layer of an anode composition, a layer of an electrolyte composition and a layer of a cathode composition, the sintered body can be used to produce a solid oxide fuel cell.

Abstract: Disclosed herein is a method comprising disposing a first particle in a reactor; the first particle being a magnetic particle or a particle that can be influenced by a magnetic field, an electric field or a combination of an electrical field and a magnetic field; fluidizing the first particle in the reactor; applying a uniform magnetic field, a uniform electrical field or a combination of a uniform magnetic field and a uniform electrical field to the reactor; elevating the temperature of the reactor; and fusing the first particles to form a monolithic solid.

Abstract: The assemblies of the invention can comprise a fine fiber layer having dispersed within the fine fiber layer an active particulate material. Fluid that flows through the assemblies of the invention can have any material dispersed or dissolved in the fluid react with, be absorbed by, or adsorbed onto, the active particulate within the nanofiber layer. The structures of the invention can act simply as reactive, absorptive, or adsorptive layers with no filtration properties, or the structures of the invention can be assembled into filters that can filter particulate from a mobile fluid while simultaneously reacting, absorbing, or adsorbing materials from the mobile fluid.

Abstract: The current document is directed to processes for producing improved porous catalysts for the dehydrogenation of organic compounds. In one implementation, the process comprises providing a powder of metal particles, sieving the powder using vibrating-screen sieves, aligning metal particles collected from sieving under an external magnetic field, partially sintering the aligned metal particles to form a solid matrix by heating the aligned metal particles in a furnace or microwave oven, or heating the aligned metal particles using a laser sintering process with a controlled amount of external heat, to a temperature below the melting point of the metal powder, and oxidizing the matrix to produce the porous catalyst. The catalysts produced by the disclosed methods have a porous body with increased surface area, can assume various microstructures, and consist essentially of metal oxides.

Abstract: A nanoporous ceramic membrane and preparation method thereof is provided. The nanoporous ceramic membrane is prepared by halloysite nanotubes (HNTs), and its porosity is between 35% to 85%. This method comprises steps as following: HNTs and polymers with a certain ratio are dispersed in organic solvent, and HNTs/polymer composite fibers are prepared through electrospinning method; after the HNTs/polymers composite fibers are laminated, they are sintered at high temperature in a certain or vacuum atmosphere, and a nanoporous ceramic membrane is obtained. Ceramic membrane prepared by this method is corrosion resistant, thermal resistant, and have large specific surface area, it may widely applied in the field of filtration, catalyst carrier and purification of high-temperature gas, etc.

Abstract: A method of forming a graphitic carbon body employs compression and resistance heating of a stock blend of a carbon material and a binder material. During molding of the body, resistance heating is accompanied by application of mechanical pressure to increase the density and carbonization of the resulting preform body. The preform can then be subjected to a graphitization temperature to form a graphite article.

Abstract: Methods, structures, devices and systems are disclosed for fabricating and implementing nanoparticles with hollow core and sealable holes. In one aspect, a nanoparticle device can includes a shell structure including at least two layers including an internal layer and an external layer, the internal layer structured to enclose a hollow interior region and include one or more holes penetrating the internal layer, the external layer is of a porous material and formed around the internal layer and sealing the one or more holes, and a substance contained within the hollow interior region, the substance incapable of passing through the external layer.

Abstract: A composite anode active material, an anode including the composite anode active material, a lithium battery including the anode, and a method of preparing the composite anode active material. The composite anode active material includes: a shell including a hollow carbon fiber; and a core disposed in a hollow of the hollow carbon fiber, wherein the core includes a first metal nanostructure and a conducting agent.

Abstract: A nanocellular foam has pores, interconnecting ligaments, and nodes where three or more ligaments intersect. The ligament cross section thickness is less than 200 microns and the distance between nodes is less than 1000 microns. A method of fabricating a nanocellular foam comprising forming a compact with one or more powders and applying energy to cause at least one or more powders to undergo a change in state is disclosed.

Abstract: A process for curing a porous muffler preform defined by a plurality of glass fibers and a heat-curing thermoset or thermoplastic materials applied to the plurality of glass fibers is disclosed herein. The process includes the step of enclosing the muffler preform in a chamber. The process also includes the step of surrounding the muffler preform with steam. The process also includes the step of causing steam to enter the muffler preform from multiple directions.

Abstract: A method of producing gypsum building board, in which there is added, to an aqueous gypsum slurry containing a water swellable clay, a basic water-soluble polymer having preferential affinity for clay. The slurry is allowed to set so as to form a board. The basic water-soluble polymer may be, for example, a polyvinyl alcohol or a polymer consisting essentially of carbon, nitrogen and hydrogen and having amine groups (which may be primary, secondary, tertiary or quaternary) in the polymer backbone and/or in side chains thereof.

Abstract: A ceramic filter comprising: (a) from about 75% to about 95% by weight of diatomaceous earth; (b) from about 10% to about 20% by weight of a flux; and (c) from about 0.03% to about 0.4% by weight of a metallic compound; the percentages by weight being percentages by weight of the ceramic filter.

Abstract: According to one embodiment, a template manufacturing method is a method for manufacturing a template for use in an imprint processing in which a pattern having irregularities are formed on a principal surface, and the pattern is brought into contact with a resist member formed on a substrate to be processed, to transfer the pattern to the resist member, the method including implanting charged particles at least into the bottoms of concave portions of the template.

Abstract: A method of forming a filter element is disclosed comprising introducing a mixture into a feeder, the mixture comprising a plurality of susceptor particles and a plurality of polymeric binder particles. The mixture is advanced through the feeder and into a die comprising an excitation portion where eddy currents are induced in the susceptor particles by subjecting the mixture to a high-frequency electromagnetic field, the eddy currents being sufficient to elevate the temperature of the susceptor particles to cause adjacent polymeric binder particles to be heated to at least a softening point. The susceptor particles bind with the heated polymeric binder particles in the die to form a coherent mass. The coherent mass is advanced out of the die and cooled to form the filter element.

Abstract: A method of controlling power applied to an induction coil assembly used for densifying porous articles with a liquid matrix precursor. The control of applied power addresses dynamic changes in the electrical characteristics of the porous article being densified as it becomes denser. In particular, the power applied is controlled in accordance with changes in resonant frequency of the coupled system of the induction heating system and the porous article.

Abstract: Provided is a separator for a rechargeable lithium battery including a porous support including a polymer derived from polyamic acid or a polymer derived from polyimide, wherein the polyamic acid and the polyimide include a repeating unit prepared from aromatic diamine including at least one ortho-positioned functional group relative to an amine group and dianhydride.

Abstract: The invention relates to a process for manufacturing at least one elementary electrochemical cell comprising a first and a second electrode between which an electrolyte is intercalated, said first and second electrodes and said electrolyte being in the form of layers, which process is characterized in that it comprises: a) producing at least one structure comprising a layer of a powder of a first electrode material and a layer of a powder of a second electrode material between which a layer of a powder of an electrolyte material is intercalated; and b) simultaneously sintering all the powder layers by an electric field sintering. Applications: manufacture of energy- or hydrogen-producing electrochemical systems, in particular solid oxide fuel cells (SOFCs) or high temperature electrolysers cells (HTEs).

Abstract: Porous films with straight pores oriented normal to the plane of the films are produced through solution processing techniques. The production takes advantage of inorganic-surfactant or inorganic-polymer co-assembly and a patterned substrate. The patterned substrate, which is also produced via solution phase self-assembly, forces vertical orientation in a hexagonal cylinder system with no practical limits in substrate size or type. This provides a route to vertically oriented inorganic pores with a pitch ranging from 3 nm to over 15 nm and pore sizes ranging from 2 nm to over 12 nm. The size is tuned by choice the choice of organic templating agents and the deposition conditions. The pores can be produced with or without a capping layer which can be used to seal the nanopores.

Abstract: A method is provided for making a high repellency material. In one embodiment the method includes the steps of providing a polymeric material having an external surface including particle-like micron-scale topography, etching the external surface with a high energy treatment; and depositing a fluorochemical onto the etched external surface by a plasma fluorination process. The external surface may define a plurality of micro-tears proximate the micron-scale topography.

Abstract: The invention provides foams of desired cell sizes formed from metal or ceramic materials that coat the surfaces of carbon foams which are subsequently removed. For example, metal is located over a sol-gel foam monolith. The metal is melted to produce a metal/sol-gel composition. The sol-gel foam monolith is removed, leaving a metal foam.

Abstract: A composite interbody device includes superior and inferior endplates with a plastic core molded therebetween. The core includes one or more features for permitting bone growth through the core. Each endplate includes a bone interface side coated with hydroxyapatite, for promoting bone on-growth. Pores in the bone interface sides permit bone in-growth. Core interface sides of the endplates include relatively larger pores for accepting molten material from the core, for example during injection molding, to enhance bonding of the endplates with the core. Each endplate has a central barrier layer for preventing the molten core material from extruding through the core interface pores into the bone interface pores, reserving the bone interface pores for bone in-growth. A method of manufacturing the composite interbody device is also disclosed.

Abstract: A process for the preparation of thermoplastic auxetic foams comprising the steps of: a) taking conventional thermoplastic foam; b) subjecting said foam to at least one process cycle wherein the foam is biaxially compressed and heated; c) optionally subjecting the foam to at least one process cycle wherein the biaxial compression is removed and the foam mechanically agitated prior to reapplying biaxial compression and heating; d) cooling said foam to a temperature below the softening temperature of said foam; and e) removing said compression and heat.

Abstract: A method for making a porous material, includes melt-blending two or more non-miscible polymers to obtain a co-continuous melt, solidifying the melt to obtain a solid mass consisting of two co-continuous polymer phases, and selectively extracting one of the co-continuous phases thereby creating within the solid mass an essentially continuous pore network having an internal surface. The method further includes replicating the internal surface of the pore network within the solid mass by coating the internal surface with successive layers of materials, and selectively extracting the solid mass without extracting the layers of materials, to thereby yield the product porous material, formed of the layers of materials. The material has a void fraction higher than about 75%, and mainly having essentially fully interconnected sheath-like non-spherical pores and essentially non-fibrous walls.

Abstract: Disclosed herein is a method for producing a sheet including a silica aerogel, the method including (S1) gelling a water glass solution in a mixture of an alcohol and water to prepare a wet gel, (S2) hydrophobically modifying the surface of the wet gel with a non-polar organic solvent, an organosilane compound and an alcohol, (S3) dissolving the hydrophobically modified silica gel and a polymer in an aprotic organic solvent to prepare an electrospinning solution, and (S4) electrospinning the electrospinning solution to produce a fiber web including a silica aerogel, and a sheet in which a polymer and a silica aerogel coexist in the form of a fiber.

Abstract: A method and system for surfacing of particle systems is proposed to achieve high surface resolutions and low execution times, comprising partitioning particles into sub-blocks, each sub-block associated linear data arrays, sequentially accessing each array to composite the particles into a respective sub-volume using estimates of grid stencils derived from particle kernels, performing random-access into the sub-volumes, processing each linear array, and lexicographically pushing the corresponding sub-volume into a DT-Grid to convert the sub-volume to a narrow band level set. Further steps to improve the temporal coherence of resulting surface, to reduce artifacts from sparsely sampled regions of space, to enhance artistic expression, and for flexible post processing can be performed.

Abstract: An aluminum alloy-and-resin composite includes an aluminum alloy substrate and resin composition formed on the substrate. The substrate is subjected to electrochemically etched and formed with nano-pores on its surface. The resin composition integrally couples to the surface of the aluminum alloy substrate by filling the nano-pores. The resin composition contains crystalline thermoplastic synthetic resins.

Abstract: A method of drying a ceramic formed body comprising the step of performing dielectric drying on an unfired honeycomb formed body formed with a ceramic material as a main raw material under a condition that a power density is 5 to 20 [kW/kg (water)].

Abstract: Structural inorganic cellular materials with controlled open porosity are produced by foaming fine particulate-laden aqueous solutions into stable, uniform, dodecahedral froth structures which are dried and sintered by microwave energy or high voltage instant electrical discharge. Porous open cell biomedical implants such as niobium or tantalum acetabular caps with engineered osteoconductive porosity are among the products achievable.

Abstract: The invention relates to a process for obtaining a porous material made of recrystallized SiC, especially in the form of a structure for filtering a particulate-laden gas, starting from at least two powders of fine and coarse SiC particles, blended with an organic material comprising an organic pore former and/or a binder, in suitable proportions and in the presence of a sufficient amount of a solvent, such as water, so as to allow forming of said blend and firing thereof between 1600° C. and 2400° C., said process being characterized in that the difference between the percentile d90 of the coarse particle powder and the percentile d10 of the fine particle powder multiplied by the volume of organic material in the initial blend, expressed as a percentage relative to the total volume of the SiC particles, is between 250 and 1500. The invention also relates to the porous material made of recrystallized SiC that can be obtained by said process.

Abstract: A method of forming a graphitic carbon body employs compression and resistance heating of a stock blend of a carbon material and a binder material. During molding of the body, resistance heating is accompanied by application of mechanical pressure to increase the density and carbonization of the resulting preform body. The preform can then be subjected to a graphitization temperature to form a graphite article.

Abstract: A composite interbody vertebral implant for facilitating fusion of adjacent vertebrae. The implant includes a first endplate of a porous metal material and a second endplate of a porous metal material which are configured to allow bone ingrowth. The implant also includes a polymeric body positioned between and bonded to the first and second endplates such that polymeric material of the polymeric body is impregnated into pores of the first and second endplates to bond the components together. The implant may include a cavity extending through the composite implant configured to receive bone growth material to facilitate fusion between a first vertebra and a second vertebra.

Abstract: Provided are a silicon carbide-based porous article comprising silicon carbide particles as an aggregate, metallic silicon and an aggregate derived from organometallic compound particles to form pores through volume shrinkage due to decomposition/conversion by heat treatment; and a method for producing the silicon carbide-based porous article, comprising, adding organometallic compound particles to form pores through volume shrinkage due to decomposition/conversion by heat treatment to a raw-material mixture containing silicon carbide particles and metallic silicon, then forming into an intended shape, calcinating and/or firing the resultant green body, forming pores through volume shrinkage due to decomposition/conversion of the organometallic compound particles, and the decomposed/converted substance of the organometallic compound particles being present as an aggregate in the porous article.

Abstract: A honeycomb filter includes an outer wall having a substantially cylindrical shape and a central axis of the substantially cylindrical shape, first walls provided at an inner side of the outer wall and extending along the central axis, and second walls provided at the inner side of the outer wall and extending along the central axis. The first walls and the second walls substantially perpendicularly cross to define cells having a substantially square shape in a cross-section perpendicular to the central axis. A thickness of the outer wall in the cross-section at a first intersection between the outer wall and a first diameter substantially parallel to the first walls in the cross-section and a thickness of the outer wall in the cross-section at a second intersection between the outer wall and a second diameter substantially parallel to the second walls in the cross-section are largest.

Abstract: A cosmetic applicator is made of a rubber latex foam which has been solidified by microwave irradiation. The foam satisfies (i) a bubble fineness corresponding to 9 bubbles/mm2 or more, (ii) flexibility of 0.7 N/cm2 or less in initial Young's modulus indicated by 50% compressive stress, and (iii) bulk density of 0.14 g/cm3 or less.

Abstract: The invention relates to a process for fabrication of a porous refractory ceramic product made from SiC, by heat treatment and sintering at high temperature, starting from a fraction of fine particles of SiC and from a fraction of larger-sized particles of SiC, said process being characterized in that, in a step preliminary to the heat treatment and to the sintering at high temperature, the finest particles of SiC are agglomerated then, in a second step, the granules thus obtained are added to the SiC powder with particles of larger size. The invention also relates to a porous body made from recrystallized SiC in an essentially ? form, in particular a particulate filter for automobile application, obtained by such a process.