Utilizing Electron Arc Or Electron Beam Patents (Class 264/470)
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Patent number: 9703225Abstract: A semiconductive roller (1) is provided, which is formed from a rubber composition and has an outer peripheral surface (4) irradiated with electron radiation in a non-oxidizing atmosphere, wherein the rubber composition contains a rubber component including an epichlorohydrin rubber and a diene rubber, the epichlorohydrin rubber being present in a proportion of 50 mass % to 80 mass %, a thiourea crosslinking agent and/or a triazine crosslinking agent, and a sulfur crosslinking component.Type: GrantFiled: March 23, 2016Date of Patent: July 11, 2017Assignee: SUMITOMO RUBBER INDUSTRIES, LTD.Inventor: Kei Tajima
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Patent number: 9472391Abstract: A semiconductor device manufacturing method includes forming a thin film containing silicon, oxygen, carbon and a specified Group III or Group V element on a substrate by performing a cycle a predetermined number of times. The cycle includes: supplying a precursor gas containing silicon, carbon and a halogen element and having an Si—C bonding and a first catalytic gas to the substrate; supplying an oxidizing gas and a second catalytic gas to the substrate; and supplying a modifying gas containing the specified Group III or Group V element to the substrate.Type: GrantFiled: March 31, 2014Date of Patent: October 18, 2016Assignee: HITACHI KOKUSAI ELECTRIC INC.Inventors: Satoshi Shimamoto, Yoshiro Hirose, Atsushi Sano, Tsukasa Kamakura, Takaaki Noda
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Patent number: 9315710Abstract: The present invention generally relates to a method for manufacturing phase change material (PCM) pellets. The method includes providing a melt composition, including paraffin and a polymer. The paraffin has a melt point of between about 10° C. and about 50° C., and more preferably between about 18° C. and about 28° C. In one embodiment, the melt composition includes various additives, such as a flame retardant. The method further includes forming the melt composition into PCM pellets. The method further may include the step of cooling the melt to increase the melt viscosity before pelletizing. Further, PCM compounds are provided having an organic PCM and a polymer. Methods are provided to convert the PCM compounds into various form-stable PCMs. A method of coating the PCMs is included to provide PCMs with substantially no paraffin seepage and with ignition resistance properties.Type: GrantFiled: March 15, 2013Date of Patent: April 19, 2016Assignee: REG SYNTHETIC FUELS, LLCInventor: Ramin Abhari
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Patent number: 9120124Abstract: First a metal plate is coated with a primer layer. Next the metal plate is coated with an adhesive layer over the primer layer. Then the metal plate is coated with a compound that includes an inorganic fiber, an organic fiber, an unvulcanized fluororubber, a peroxide for vulcanization and an inorganic filler over the primer layer and the adhesive layer. Thereafter, the metal plate coated with the compound is hot pressed with the fluororubber being vulcanized.Type: GrantFiled: January 23, 2012Date of Patent: September 1, 2015Assignee: U-SUN GASKET CORPORATIONInventor: Kazuhiro Takahashi
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Publication number: 20150108693Abstract: Methods are provided for reducing one or more dimensions of individual pieces of biomass; treating biomass, such as size-reduced biomass; changing a molecular structure of a biomass material; and, optionally, subjecting the biomass to a primary process to form a product. The methods include processing biomass materials using a screw extrusion process, and treating the biomass material with a screw extrusion process in size-reduction and treating steps.Type: ApplicationFiled: December 22, 2014Publication date: April 23, 2015Inventor: Marshall Medoff
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Publication number: 20150076743Abstract: A method of continuously manufacturing a cured membrane includes continuously compounding and mixing a vulcanizable rubber composition in a mixing extruder while continuously removing gasses from the vulcanizable rubber composition during mixing with a vacuum. The vulcanizable rubber composition may be continuously extruded to form an extrudate, which may be continuously calendered to form a green membrane. The green membrane may be continuously cured, such as by a hot air conveyor curing system, to form a cured membrane.Type: ApplicationFiled: March 20, 2013Publication date: March 19, 2015Inventors: Bruce Douglas, Michael Hubbard, Hao Wang
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Publication number: 20150054202Abstract: A method to reduce or minimize the reduction in molecular weight of a stent during processing is disclosed. The stent has a scaffolding including a polymer formulation comprising PLLA and polymandelide. The polymandelide reduces the molecular weight drop during processing, particularly during sterilization. The stent scaffolding can further include one or more additional stabilizing agents that additionally reduce the molecular weight drop during processing.Type: ApplicationFiled: October 31, 2014Publication date: February 26, 2015Inventors: Byron Lambert, Yunbing Wang, James Oberhauser
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Publication number: 20140294917Abstract: In one embodiment, this invention is directed to a method of preparing a thermoset or thermoplastic polymer fiber comprising the following sequential steps: (i) providing a monomeric or oligomeric mixture, wherein said monomeric or oligomeric mixture comprises monomers or oligomers which polymerize by radiation; (ii) optionally heating or cooling said monomeric or oligomeric mixture for obtaining optimal viscosity; (iii) pumping said monomeric or oligomeric mixture through a spinneret, die or any other nozzle type; and (iv) radiating said monomeric or oligomeric mixture with a radiation source under room temperature, wherein said thermoset or thermoplastic polymer fibers are formed.Type: ApplicationFiled: November 26, 2012Publication date: October 2, 2014Inventors: Oleg PALCHIK, Valery Palchik
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Publication number: 20140251532Abstract: A method includes premixing an anti-static additive and a first crosslinker to form an anti-static intermediate mixture where the anti-static additive is dispersed in the first crosslinker. The method also includes compounding the anti-static intermediate mixture and at least a portion of the first fluoropolymer to form a first compounded mixture. The method further includes extruding the first compounded mixture to form a layer.Type: ApplicationFiled: May 12, 2014Publication date: September 11, 2014Applicants: Eaton Corporation, AGC Chemicals Americas, Inc.Inventors: Soumayajit Sarkar, Javed Mapkar, Edward Hummelt, Kenneth Phaneuf, Robert Michael Lefere, Joseph David Proof, Gregory James Chapman
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Patent number: 8703038Abstract: Methods of fabricating an implantable medical devices such as stents made from biodegradable polymers are disclosed that reduce or minimize chain scission and monomer generation during processing steps. The method includes processing a poly(L-lactide) resin having an number average molecular weight between 150 to 200 kD in an extruder in a molten state. A poly(L-lactide) tube is formed from the processed resin and a stent is fabricated from the tube. The number average molecular weight of the poly(L-lactide) of the stent after sterilization is 70 to 100 kD.Type: GrantFiled: July 19, 2013Date of Patent: April 22, 2014Assignee: Abbott Cardiovascular Systems Inc.Inventors: Yunbing Wang, James Oberhauser
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Patent number: 8696974Abstract: An adhesive composition comprising 100 parts by weight of a fluorine-containing polymer and 2 to 30 parts by weight of an unsaturated compound containing at least one polar group selected from the group consisting of an epoxy group and a carboxyl group, wherein the fluorine-containing polymer has been graft-modified with the polar group-containing unsaturated compound by irradiation of ionizing radiation, a production process thereof, and formed products such as a heat-shrinkable tube equipped with a layer composed of the adhesive composition.Type: GrantFiled: August 26, 2010Date of Patent: April 15, 2014Assignee: Sumitomo Electric Fine Polymer, Inc.Inventors: Kiyoaki Moriuchi, Hiroshi Hayami, Shinya Nishikawa
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Patent number: 8678804Abstract: An apparatus for the continuous modification of polymers in the flowable state by electron radiation, includes a device configured for converting polymers into the flowable state, a forming device and at least one irradiation device structured and arranged to provide electron radiation in a region of irradiation. Additionally, the apparatus includes at least one cooling device, a radiation guard and supply and discharge lines inside the radiation guard. The supply and discharge lines realize a continuous transport of the polymers in the flowable state at least through the radiation guard into the region of irradiation. Additionally, the supply and discharge lines realize a continuous transport of one of polymers remaining in the flowable state and modified at least inside the radiation guard and solid formed and modified polymers out of the region of the irradiation.Type: GrantFiled: September 5, 2006Date of Patent: March 25, 2014Assignee: Leibniz-Institut fuer Polymerforschung Dresden E.V.Inventors: Michael Stephan, Gert Heinrich, Helmut Dorschner
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Publication number: 20130300034Abstract: Methods of fabricating an implantable medical devices such as stents made from biodegradable polymers are disclosed that reduce or minimize chain scission and monomer generation during processing steps. The method includes processing a poly(L-lactide) resin having an number average molecular weight between 150 to 200 kD in an extruder in a molten state. A poly(L-lactide) tube is formed from the processed resin and a stent is fabricated from the tube. The number average molecular weight of the poly(L-lactide) of the stent after sterilization is 70 to 100 kD.Type: ApplicationFiled: July 19, 2013Publication date: November 14, 2013Inventors: Yunbing Wang, James OBERHAUSER
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Patent number: 8552084Abstract: A process for preparing a pressure sensitive adhesive using a modified planetary roller extruder is described. The process in accordance with one aspect of the invention is a continuous process that includes introducing primary raw materials comprising a non-thermoplastic elastomer into a planetary roller extruder, introducing a heat-activatable crosslinker into the planetary roller extruder for mixing with the primary raw materials, and compounding the primary raw materials and the heat activatable crosslinker to form an adhesive composition while maintaining the temperature of the adhesive composition between about 25° C. and about 100° C. The non-thermoplastic elastomer is masticated during compounding and at least some of the heat-activatable crosslinker remains generally unactivated and is available for later activation.Type: GrantFiled: December 27, 2011Date of Patent: October 8, 2013Assignee: Intertape Polymer Corp.Inventors: John Kinch Tynan, Jr., Richard Walter St. Coeur, David Michael Kovach, Thomas Lombardo
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Patent number: 8496865Abstract: Methods of fabricating an implantable medical devices such as stents made from biodegradable polymers are disclosed that reduce or minimize chain scission and monomer generation during processing steps. The method includes processing a poly(L-lactide) resin having an number average molecular weight between 150 to 200 kD in an extruder in a molten state. A poly(L-lactide) tube is formed from the processed resin and a stent is fabricated from the tube. The number average molecular weight of the poly(L-lactide) of the stent after sterilization is 70 to 100 kD.Type: GrantFiled: October 15, 2010Date of Patent: July 30, 2013Assignee: Abbott Cardiovascular Systems Inc.Inventors: Yunbing Wang, James Oberhauser
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Patent number: 8431065Abstract: Methods for making a crosslinked elastomeric composition and articles made of the same are provided. In at least one specific embodiment, an elastomeric composition comprising at least one propylene-based polymer is blended with at least one component selected from the group consisting of multifunctional acrylates, multifunctional methacrylates, functionalized polybutadiene resins, functionalized cyanurate, and allyl isocyanurate; and blended with at least one component selected from the group consisting of hindered phenols, phosphites, and hindered amines. The propylene-based polymer can include propylene derived units and one or more dienes, and have a triad tacticity of from 50% to 99% and a heat of fusion of less than 80 J/g. The blended composition can then be extruded and crosslinked. The extruded polymer can be crosslinked using electron beam radiation having an e-beam dose of about 100 KGy or less. The crosslinked polymers are particularly useful for making fibers and films.Type: GrantFiled: April 13, 2012Date of Patent: April 30, 2013Assignee: ExxonMobil Chemical Patents Inc.Inventor: Sunny Jacob
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Publication number: 20130072633Abstract: A flexible tubing material includes a radiation crosslinked blend of a first elastomeric polymer including a styrenic thermoplastic elastomer, an ethylene vinyl acetate elastomer, a polylefin elastomer with a second elastomeric polymer including a polyolefin elastomer, a diene elastomer, or combination thereof, with the proviso that the first elastomeric polymer and the second elastomeric polymer are different. In an embodiment, a method of making a material includes providing the first elastomeric polymer, providing the second elastomeric polymer, blending the first elastomeric polymer and the second elastomeric polymer, extruding or injection molding the blend, and crosslinking the blend with radiation.Type: ApplicationFiled: October 4, 2012Publication date: March 21, 2013Inventors: Yoshitaka Kawamoto, Sridhar Krishnamurthi Siddhamalli
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Patent number: 8257637Abstract: A method is provided for removing a resin layer of a resin-coated metal tube. The resin layer is removed with a laser beam. More particularly, the resin layer of a desired range is burned out by focusing the laser beam into a pinpoint without defocusing the sectional shape of the laser beam in the axial direction o the resin-coated metal tube.Type: GrantFiled: January 14, 2005Date of Patent: September 4, 2012Assignee: Usui Kakusai Sangyo Kaisha LimitedInventor: Atsushi Okada
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Patent number: 8202467Abstract: A method for extruding transparent and/or translucent article is provided. In one embodiment, the method comprises providing a propylene-based polymer comprising propylene derived units and one or more dienes, the propylene-based polymer having a triad tacticity of from 50% to 99% and a heat of fusion of less than 80 J/g, extruding the propylene-based polymer in the absence of processing oil into an article; and then crosslinking the extruded article.Type: GrantFiled: July 24, 2007Date of Patent: June 19, 2012Assignee: ExxonMobil Chemical Patents Inc.Inventors: Abdelhadi Sahnoune, Sunny Jacob
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Patent number: 8178031Abstract: Methods for making a crosslinked elastomeric composition and articles made of the same are provided. In at least one specific embodiment, an elastomeric composition comprising at least one propylene-based polymer is blended with at least one component selected from the group consisting of multifunctional acrylates, multifunctional methacrylates, functionalized polybutadiene resins, functionalized cyanurate, and allyl isocyanurate; and blended with at least one component selected from the group consisting of hindered phenols, phosphites, and hindered amines. The propylene-based polymer can include propylene derived units and one or more dienes, and have a triad tacticity of from 50% to 99% and a heat of fusion of less than 80 J/g. The blended composition can then be extruded and crosslinked. The extruded polymer can be crosslinked using electron beam radiation having an e-beam dose of about 100 KGy or less. The crosslinked polymers are particularly useful for making fibers and films.Type: GrantFiled: December 3, 2010Date of Patent: May 15, 2012Assignee: ExxonMobil Chemical Patents Inc.Inventors: Sunny Jacob, Alistair D. Westwood, Tonson Abraham
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Publication number: 20120091633Abstract: Methods of fabricating an implantable medical devices such as stents made from biodegradable polymers are disclosed that reduce or minimize chain scission and monomer generation during processing steps. The method includes processing a poly(L-lactide) resin having an number average molecular weight between 150 to 200 kD in an extruder in a molten state. A poly(L-lactide) tube is formed from the processed resin and a stent is fabricated from the tube. The number average molecular weight of the poly(L-lactide) of the stent after sterilization is 70 to 100 kD.Type: ApplicationFiled: October 15, 2010Publication date: April 19, 2012Inventors: Yunbing Wang, James Oberhauser
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Patent number: 8110612Abstract: A process for preparing a pressure sensitive adhesive using a modified planetary roller extruder is described. The process in accordance with one aspect of the invention includes introducing primary raw materials including a non-thermoplastic elastomer into a feeding section of the modified planetary roller extruder, conveying the raw materials from the feeding section to a compounding section of the modified planetary roller extruder, continuously mixing the primary raw materials in the compounding section to produce a homogeneous adhesive composition. The adhesive composition may be applied to a web-form material. The compounding section of the modified planetary roller extruder includes a main spindle surrounded by and intermeshed with a plurality of planetary spindles at least one of which is a double transversal mixing spindle having a plurality of back-cut helical flights.Type: GrantFiled: February 5, 2007Date of Patent: February 7, 2012Assignee: Intertape Polymer Corp.Inventors: John Kinch Tynan, Jr., Richard Walter St. Coeur, David Michael Kovach, Thomas Lombardo
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Publication number: 20110277867Abstract: Provided is an in-tank tube excellent in pressure-resisting performance. The in-tank tube is an in-tank tube (1) for an automotive fuel of a monolayer structure, the in-tank tube (1) for an automotive fuel being installed in a fuel tank (2) and having a construction that absorbs displacement of the fuel tank (2) and vibration of a fuel pump (5). Further, the in-tank tube (1) for an automotive fuel is formed into a monolayer structure formed of a resin material using an aliphatic polyamide resin as a main component, and has the following pressure-resisting characteristic (X): (X) when silicone oil is charged as a pressurizing medium into the in-tank tube immersed in a test liquid (Fuel C:methanol=85:15 (volume basis)) at 80° C. for 168 hours, both ends of the in-tank tube are each blocked with a test pipe, and a pressure test is performed at a rate of pressure increase of 1.0 MPa/min and room temperature, a pressure (burst pressure) at which the in-tank tube bursts or the test pipe disconnects is 2.Type: ApplicationFiled: July 28, 2011Publication date: November 17, 2011Applicant: TOKAI RUBBER INDUSTRIES, LTD.Inventors: Kazutaka Katayama, Koji Mizutani, Keita Asai, Tokunori Kobayashi
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Patent number: 8022112Abstract: A plasticized ceramic-forming mixture and a method for stiffening the mixture, the mixture comprising a combination of inorganic powder, one or more plasticizing organic binders, a radiation-curable monomer, a photoinitiator, and water, and the method comprising stiffening the surfaces of extruded shapes of the mixture by applying electromagnetic energy to the surfaces following extrusion.Type: GrantFiled: November 29, 2007Date of Patent: September 20, 2011Assignee: Corning IncorporatedInventors: Michelle Dawn Fabian, Edward John Fewkes, Kevin Robert McCarthy
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Publication number: 20110217653Abstract: A belt member for intermediate transfer, including a crosslinked product of a thermoplastic resin; and an electroconductive particulate material, wherein the belt member satisfies the following formulae (I) and (ii): 6?log(?v200)?10??(i) 0?log(?v10)?log(?v1,000)?2??(ii) wherein ?v200, ?v10 and ?v1,000 represent volume resistivities when the belt member is applied with biases of 200 V, 10 V and 1,000 V, respectively.Type: ApplicationFiled: February 3, 2011Publication date: September 8, 2011Inventors: Akira Izutani, Makoto Matsushita
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Publication number: 20110152810Abstract: Embodiments of the disclosure include elastomeric stretch fibers containing an anti-tack agent, methods of preparing the fiber, methods of using this fiber, articles including this fiber, and the like.Type: ApplicationFiled: December 16, 2010Publication date: June 23, 2011Applicant: INVISTA North America S.a.r.l.Inventors: James Michael LAMBERT, Young D. Nguyen, Robert O. Waldbauer, JR., Hong Liu
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Publication number: 20110101572Abstract: Disclosed is a method of manufacturing a charging roller useable in an electrophotographic image forming apparatus and a charging roller manufactured according to the method. The method includes introducing a conductive agent and a mixture of a rubber-based material and polyolefin-based resin into an extruder, extruding the conductive agent and the mixture to obtain an extrudate, crosslinking the extrudate by electron beam irradiation, and polishing the crosslinked extrudate. The method results in an environmentally friendly and simplified manufacturing processes, and/or in the reduction of the manufacturing costs.Type: ApplicationFiled: July 8, 2010Publication date: May 5, 2011Applicant: Samsung Electronics Co., LtdInventors: Tae-hyun KIM, Jong-moon Eun, Yong-hoon Lee
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Patent number: 7910795Abstract: A technique for imparting latent elasticity to components of an absorbent article is provided. More specifically, a latent elastic film that contains a crosslinkable semi-crystalline polyolefin is initially incorporated into an absorbent article. The film is not highly elastic prior to crosslinking and is thus dimensionally stable. Consequently, the film need not be maintained in a mechanically stretched condition during attachment to other components of the absorbent article, which provides for greater freedom in the location and manner in which the components are attached together. Once incorporated into the absorbent article, the semi-crystalline polyolefin is crosslinked to form a three-dimensional network having elastic memory. The film may also be heat activated, either through crosslinking or an additional step, to cause the film to shrink and further improve its stretch characteristics.Type: GrantFiled: March 9, 2007Date of Patent: March 22, 2011Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Oomman P. Thomas, C. Allen Smith, James Austin
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Patent number: 7867433Abstract: Methods for making a crosslinked elastomeric composition and articles made of the same are provided. In at least one specific embodiment, an elastomeric composition comprising at least one propylene-based polymer is blended with at least one component selected from the group consisting of multifunctional acrylates, multifunctional methacrylates, functionalized polybutadiene resins, functionalized cyanurate, and allyl isocyanurate; and blended with at least one component selected from the group consisting of hindered phenols, phosphites, and hindered amines. The propylene-based polymer can include propylene derived units and one or more dienes, and have a triad tacticity of from 50% to 99% and a heat of fusion of less than 80 J/g. The blended composition can then be extruded and crosslinked. The extruded polymer can be crosslinked using electron beam radiation having an e-beam dose of about 100 KGy or less. The crosslinked polymers are particularly useful for making fibers and films.Type: GrantFiled: May 30, 2008Date of Patent: January 11, 2011Assignee: ExxonMobil Chemical Patents Inc.Inventors: Sunny Jacob, Alistair D. Westwood, Tonson Abraham
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Publication number: 20100324207Abstract: Relates to mono-backsheets for photovoltaic modules. These mono-backsheets are produced or producible from a molding compound, this molding compound being based on at least one polyamide. The photovoltaic module mono-backsheet according to the invention is characterized in that the at least one polyamide is synthesized from linear and/or branched aliphatic and/or cycloaliphatic monomers, which have an average of at least 8 and at most 17 carbon atoms. The monomers are selected from the group which comprises diamines, dicarboxylic acids, lactams, and amino carboxylic acids, as well as mixtures thereof. The polyamides PA 610 and PA 612 are excluded from the present invention, and the polyamides based on lactams and amino carboxylic acids are cross-linked.Type: ApplicationFiled: June 17, 2010Publication date: December 23, 2010Applicant: EMS-PATENT AGInventors: André STURZEL, Georg STOEPPELMANN, Dietmar ETZEL, Botho HOFFMANN
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Publication number: 20100139226Abstract: In accordance with the invention there are devices and processes for making ceramic nanofiber mats and ceramic filters for use in high temperature and in corrosive environments. The process for forming a ceramic filter can include electrospinning a preceramic polymer solution into a preceramic polymer fiber having a diameter from about 10 nm to about 1 micron and forming a preceramic polymer fiber web from the preceramic polymer fiber onto a collector. The process can also include pyrolyzing the preceramic polymer fiber web to form a ceramic nanofiber mat having a diameter less than the diameter of the preceramic polymer fiber, the ceramic nanofiber mat comprising one or more of an oxide ceramic and a non-oxide ceramic such that the ceramic fiber mat can withstand temperature greater than about 1000° C.Type: ApplicationFiled: March 12, 2008Publication date: June 10, 2010Applicant: University of Florida Research Foundation, Inc.Inventors: Wolfgang M. Sigmund, Vasana Maneeratana, Paolo Colombo, Chang-Yu Wu, Hyoungjun Park, Qi Zhang
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Patent number: 7678841Abstract: A method of increasing the gas transmission rate of a packaging film comprises providing a packaging film that comprises at least about 0.001 weight % of fullerene material selected from spherical fullerenes, bowl-shaped fullerenes, multi-walled carbon nanotubes, carbon nanocones, and carbon nano-onions. The packaging film is exposed to an amount of radiation energy effective to increase the oxygen transmission rate of the packaging film by at least about 100 cc (STP)/m2. day (1 atm, 0% RH, 23° C.).Type: GrantFiled: August 19, 2005Date of Patent: March 16, 2010Assignee: Cryovac, Inc.Inventor: Michael D. Grah
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Patent number: 7645415Abstract: An elastic film, particularly for hygiene articles, has at least one layer that is produced extrusion of an elastomer polymer composition and subsequently cross-linked. The elastomer polymer composition contains a mixture of 40 to 90 parts by weight of a styrene block copolymer, 5 to 50 parts by weight of a plasticizer oil, and up to 10 parts by weight of a thermoplastic polymer. The layer of the elastomer polymer composition is cross-linked by treatment with electron beams. The elastomer polymer composition additionally contains 2 to 20 parts by weight of a reactive plasticizer that has a mole mass of less than 10,000 kg/kmol, is compatible with soft segments of the styrene block copolymer, and has functional acrylate groups.Type: GrantFiled: August 24, 2007Date of Patent: January 12, 2010Assignee: Nordenia Technologies GmbHInventor: Maik Hach
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Publication number: 20090319031Abstract: Various embodiments of the present invention include implantable medical devices such as stents manufactured from polymers, and more particularly, biodegradable polymers including biodegradable polyesters. Other embodiments include methods of fabricating implantable medical devices from polymers. The devices and methods utilize one or more stabilizers, where each stabilizer may be chosen from the following categories: free radical scavengers, peroxide decomposers, catalyst deactivators, water scavengers, and metal scavengers.Type: ApplicationFiled: June 19, 2008Publication date: December 24, 2009Inventors: Yunbing Wang, Stephen D. Pacetti, Carina V. Harold
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Patent number: 7608216Abstract: Methods for preparing a shaped rubber article, comprising admixing at least one thermoplastic material and at least one elastomer material to provide a processable and dimensionally stable rubber composition, shaping the composition, and irradiating the composition to form the shaped rubber article. The dimensional stability of the uncured composition may be provided by partial dynamic vulcanization, high performance reinforcing fillers, fractional curing, or combinations thereof. The elastomer material is present in an amount greater than about 65% by weight based on the total weight of the thermoplastic and elastomer materials present in the admixture.Type: GrantFiled: December 27, 2006Date of Patent: October 27, 2009Assignee: Freudenberg-Nok General PartnershipInventors: Edward H. Park, Francis Joseph Walker
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Publication number: 20080317990Abstract: A high strength, flexible crosslinked polyethylene (PEX) material is provided wherein the base polymer is intermixed with a polymer modifier which affects the amorphous region of the polymer, leaving the crystalline portion of the base polymer virtually unaffected. Consequently, the amorphous region's density is lowered, resulting in a more flexible final product, while the crosslinked molecular structure and/or crystalline portion of the polymer, which controls the strength of the base polymer, remains strong. The polymer modifier can comprise a hydrocarbon fluid such as PAO, Group III basestocks, or a gas-to-liquid hydrocarbon. A method for producing the plastic material is also provided. The plastic material has particular utility in the production of tubing, piping, and conduits for transporting gases, liquids, and the like, as well as wire and cable coatings such as jacketing and insulation.Type: ApplicationFiled: June 18, 2008Publication date: December 25, 2008Applicants: EXXONMOBIL CHEMICAL COMPANY INC., ZURN PEX, INC.Inventors: Gary Lee Runyan, Bruce A. Harrington, Bryan R. Chapman, David B. Dunaway, Gerd Arthur Allermann, Robert G. Russell, Rodney Mize
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Patent number: 7241817Abstract: The present invention relates to a process for grafting an unsaturated monomer onto a fluoropolymer, having the steps of: a) melt blending the fluoropolymer with the unsaturated monomer; b) forming the blend obtained in a) into films, sheets, granules or powder; c) exposing the products from step b), in the absence of air, to photon (?) or electron (?) irradiation with a dose of between 1 and 15 Mrad; and d) optionally treating the product obtained at c) in order to remove all or part of the unsaturated monomer that has not been grafted onto the fluoropolymer. Structures made with these materials are barriers to many fluids and in particular to petrol and to air-conditioning fluids and may be formed into bottles, tanks, containers, pipes, hoses and vessels of all sorts. They may also be converted into films with which packaging is made.Type: GrantFiled: June 2, 2004Date of Patent: July 10, 2007Assignee: Arkema FranceInventors: Anthony Bonnet, Barbara Ramfel, Fabrice Chopinez, Karine Triballier, Michael Werth, Thierry Pascal
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Patent number: 7217472Abstract: A support member is useful for supporting membranes such as solid polymer electrolyte ion exchange membranes such as those used in electrochemical cell applications. The support member has a first lattice pattern on a first side of a single piece of material. A second lattice pattern on a second side of the single piece of material cooperates with the first lattice pattern to establish a plurality of flow passages across the material. Each lattice pattern has a corresponding plurality of recesses that extend partway through the material and overlapping portions of the recesses define the flow passages. In a disclosed example, the monolithic support member lattice patterns are established using chemical etching.Type: GrantFiled: December 18, 2003Date of Patent: May 15, 2007Assignee: Hamilton Sundstrand CorporationInventor: Andrei Leonida
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Patent number: 7008589Abstract: A process produces cling-fastener parts with a large number of interlocking members (24) from a formulation encompassing radiation-crosslinkable prepolymers. The prepolymer is molded, cast, and/or compression molded into the shape of a large number of interlocking members (24) together with a cling-fastener base (21), and is then radiation-cured. The apparatus producing the cling fasteners encompasses a feed (32, 10) for the formulation (14) of radiation-crosslinkable, in particular acrylic, prepolymers, at least one shaping roll (11) and one backing roll (12). The shaping roll (11) has a large number of radial cutouts (17). A source of UV radiation (19), or an electron-beam source, provides radiation curing of the molded radiation-curable formulation.Type: GrantFiled: January 22, 2000Date of Patent: March 7, 2006Assignee: Binder Kletten-Haftverschluss-Systeme GmbHInventor: Konstantinos Poulakis
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Patent number: 6913824Abstract: A method for making agglomerate particles from a composition comprising at least a radiation curable binder and solid particulates. The method comprises the steps of forcing the composition through a perforated substrate to form agglomerate precursor particles which then separate from the perforated substrate. Then, the particles are irradiated to form soldified, handleable agglomerate particles before being collected.Type: GrantFiled: July 2, 2003Date of Patent: July 5, 2005Assignee: 3M Innovative Properties CompanyInventors: Scott R. Culler, James L. McArdle, Jeffrey W. Nelson, John T. Wallace
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Patent number: 6824729Abstract: A method of preparing a nonwoven web that has substantially continuous synthetic fine fiber includes preparing an aqueous amide crosslinked polymer solution. The solution is extruded through a die having a plurality of orifices to form a plurality of threadlines. The threadlines are then attenuated with a primary gaseous source under conditions sufficient to permit the viscosity of each threadline to increase incrementally with increasing distance from the die, at a rate sufficient to provide fibers having a desired attenuation and mean fiber diameter without significant fiber breakage.Type: GrantFiled: March 4, 2002Date of Patent: November 30, 2004Assignee: Kimberly-Clark Worldwide, Inc.Inventors: Jian Oin, Yong Li, Wendy Lynn Van Dyke, Anthony John Wisneski, Palani Raj Ramaswami Wallajapet, Hannong Rhim
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Publication number: 20040070104Abstract: The invention concerns a method which consists in: a) forming by extrusion an extruded thermoplastic tube (20) having, when coming out of the extruder, a diameter D1; b) then subjecting said extruded tube of diameter D1 to a radiation treatment, so as to produced a cross-linked tube (21); c) after bringing said cross-linked tube (21) to a temperature not less than a temperature substantially equal to the melting point of its crystalline phase, subjecting it, in displacement, to a radial monoaxial expansion for form an expanded tube (22) of diameter D2, then cooling it down to a temperature, typically room temperature, at which it can be cut into tube portions (23) with length substantially equal to the height of said caps (1); and e) assembling or forming a head (10, 100, 101, 102, 103) on said tube portion (23), so as to obtain a cap or top (1), with heat-shrinkable skirt, economical and having a homogeneous skirt (11, 12) free of axial connection line.Type: ApplicationFiled: May 19, 2003Publication date: April 15, 2004Inventor: Jacques Granger
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Patent number: 6620214Abstract: Methods for making ceramic aggregate particles comprising forming a plurality of ceramic aggregate precursor particles from a composition by forcing the composition through at least one orifice in a substrate, at least partially curing the ceramic aggregate precursor particles, and heating the ceramic aggregate precursor particles to provide ceramic aggregate particles wherein solid particulates are bonded together by ceramic binder.Type: GrantFiled: October 5, 2001Date of Patent: September 16, 2003Assignee: 3M Innovative Properties CompanyInventors: James L. McArdle, Jeffrey W. Nelson, Scott R. Culler, John T. Wallace
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Patent number: 6602457Abstract: The present invention relates to high dielectric non-woven fabrics and their synthetic process and more particularly, relates to a process for preparing high dielectric non-woven fabrics including the steps of (a) mix-spinning polyvinylidene fluoride (PVDF) and polypropylene (PP) to prepare a fiber, (b) polarizing the fiber prepared in the step (a) to improve the dielectric constant of the fiber, and (c) manufacturing non-woven fabrics from the fiber having improved dielectric constant, prepared in the step (b), and non-woven fabrics prepared according to the mentioned process.Type: GrantFiled: September 7, 2000Date of Patent: August 5, 2003Assignee: Clean Air Technology Co.Inventors: Choong-Joong Lee, Soon-Kyu Chung, Jin-Soo Joo
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Patent number: 6540953Abstract: A method of producing a microporous membrane comprising the steps of: extruding a polymer at a temperature of from (polymer melting point +10° C.) to (polymer melting point +100° C.); drawing the extruded polymer at a rate of 5˜120 m/min in 10˜150° C. to obtain a polymer film; annealing the polymer film at a temperature of from (polymer melting point −100° C.) to (polymer melting point −5° C.) for 10 seconds to 1 hour; irradiating both surfaces of the annealed polymer film with an ion-particle amount of 102˜1020 ion/cm2 energized at 10−2˜107 KeV, at an irradiating distance of 5˜100 cm under a vacuum of 10−2˜10−[torr; cold stretching the irradiated polymer film at a temperature of from −20° C. to (polymer melting point −40° C.); hot stretching the cold stretched polymer film at a temperature of from (polymer melting point −40° C.) to (polymer melting point −5° C.Type: GrantFiled: May 17, 2000Date of Patent: April 1, 2003Assignee: LG Chemical Ltd.Inventors: Sang-Young Lee, Myung-Man Kim, Heon-Sik Song
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Patent number: 6506333Abstract: The present invention provides a method for fabricating a medical tubing. The method includes the steps of: (1) providing a material selected from the group consisting of ethylene homopolymers and ethylene copolymers, wherein the ethylene copolymers are obtained by copolymerizing ethylene with a comonomer selected from the group consisting of lower alkyl olefins, lower alkyl esters of a carboxylic acid and lower alkene esters of a carboxylic acid, the lower alkyl and lower alkene each have from 3-18 carbons, or blends thereof; (2) providing an extruder with an extrusion die; (3) extruding the material into a medical tubing; (4) providing a surface modifier solution; (5) preheating the surface modifier solution to a temperature within the range of 50-80° C.; and (6) applying the preheated solution onto the tubing at it exits the extrusion die when the tubing is in a molten state or a semi-molten state.Type: GrantFiled: September 3, 1999Date of Patent: January 14, 2003Assignee: Baxter International Inc.Inventors: Chuan Qin, Patrick T. Ryan, Michael T. K. Ling, Donna L. Rostron, Yuanpang S. Ding, Lecon Woo, Susan R. Mizener, Birendra K. Lal
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Patent number: 6485665Abstract: Polyurethane elastomer fibers with superior mechanical and heat distortion properties are obtained by a method in which (a) a segmented polyurethane polymer is produced on the basis of a macro-diol, an aliphatic diisocyanate, and a chain extender with at least two hydroxy and/or amino groups, where the polymer has a molar excess of isocyanate groups over the hydroxy and/or amino groups from the macro-diol and chain extender; (b) the polyurethane polymer is melt-extruded to form a fiber; and (c) The extruded fiber is subjected to a post-treatment. Steps (a) and (b) are carried out under temperature conditions and within a time interval where essentially no allophanate will be formed, while step (c) is performed under temperature conditions and within a time interval in which the polyurethane polymer is cross-linked through the formation of allophanate.Type: GrantFiled: July 19, 2000Date of Patent: November 26, 2002Assignee: Rhodianyl S.N.C.Inventors: Frank Hermanutz, Peter Hirt, Oliver Oess, Wilhelm Oppermann
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Patent number: 6287505Abstract: Self-tuning materials which can efficiently emit or receive radio waves in spite of being simple in their construction and small in their dimension, and are applied to patch antenna, wave directors or the like. Metallic chips containing two or more kinds of ingredients which are distributed in a layered, net-like or needle-shaped configuration, and an organic or inorganic bonding material which is small in dissipation of electric power under radio waves of high frequencies are mixed with each other, and are pressurized under a high pressure while being highly electrified in the direction perpendicular to the pressurizing direction to mold the metallic chips and the bonding material in a plate-shaped configuration while being heated.Type: GrantFiled: July 6, 1999Date of Patent: September 11, 2001Assignee: Suisaku LimitedInventor: Etsuko Kaitani
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Patent number: 6241937Abstract: A polyolefin shaped article having high strength and high modulus is efficiently manufactured without a need to accompany a process of removing a flow modifier or the like. A method is characterized as including the steps of melt forming a composition principally containing 100 parts by weight of high-density polyolefin, such as high-density polyethylene, and 1-30 parts by weight of a polymerizable monomer or oligomer having a preferred affinity for the high-density polyolefin into a sheet or film, calendering and stretching the sheet or film, and then polymerizing the polymerizable monomer or oligomer incorporated in the sheet or film.Type: GrantFiled: April 27, 1999Date of Patent: June 5, 2001Assignee: Sekisui Chemical Co., Ltd.Inventors: Masanori Nakamura, Satoru Yamamoto
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Publication number: 20010000547Abstract: Touch fasteners with different portions having different material properties, and methods and apparatus for making such a product. In one embodiment, the fastener includes a cross-linkable polymer, and a first portion of the fastener is cross-linked and a second portion of the fastener is not cross-linked or is cross-linked to a degree less than said first portion. In another embodiment, the fastener is made in a continuous process on a rotating mold roll having a plurality of fastener element mold cavities extending into the mold roll from its outer circumferential surface.Type: ApplicationFiled: December 13, 2000Publication date: May 3, 2001Applicant: Velcro Industries, B.V.Inventors: Ernesto S. Tachauer, Brian J. VanBenschoten