Abstract: A manufacturing method of a fiber reinforced composite member includes the steps of: forming a fabric 1 on the surface of a mandrel 10, infiltrating the formed fabric with matrix, and leaving portions 12a, 12b of the mandrel as integral with the fabric and removing the mandrel before the fabric adheres to the mandrel by matrix infiltration. Subsequently, a remaining portion of the mandrel is used as a reference surface and machining is performed. Without possibility of adhesion to the mandrel and resulting breakage, machining bases (axial center and reference surface) during machining can accurately be provided, and this can largely enhance machining precision and yield of the final product.

Abstract: A method of replicating a structured surface that includes providing a tool having a structured surface having a surface morphology of a crystallized vapor deposited material; and replicating the structured surface of the tool to form a replicated article. A replicated article includes at least one replicated surface, wherein the replicated surface includes a replica of a crystallized vapor deposited material. A replication tool includes: a tool body that includes a tooling surface; and a structured surface on the tooling surface, wherein the structured surface includes crystallized vapor deposited material or a replica of crystallized vapor deposited material.

Abstract: A method of producing an optical element forming die to form an optical element by pressing a glass material softened with heat, including a first process of producing a primary processed product having a volume resistance value Z (0<Z≦1 (&OHgr;·cm) by sintering ceramic powders; and a second process of forming the optical element forming die by processing the primary processed product.

Abstract: An apparatus and methods of manufacturing seamless gaskets using expanded intercalated graphite worms, in which an annular die cavity has a central column with a charge inlet in a perimeter wall. Expanded intercalated graphite worms communicate from a source through the charge inlet in the annular die cavity for depositing a charge of expanded intercalated graphite worms within the die cavity. An upper pusher is movable from a first position distally spaced from an open end of the die cavity to a second position within the die cavity for compressing a first charge of expanded intercalated graphite worms. A lower pusher is movable from a first position to a second position during the compressing of the first charge of expanded intercalated graphite worms in the die. The upper pusher causes the lower pusher to move to the second position, so that a second charge of expanded intercalated graphite worms is received in substantially the same volume as the first charge.

Abstract: Disclosed are methods of manufacturing electronic devices, particularly integrated circuits. Such methods include the use of low dielectric constant material prepared by using a removable porogen material.

Abstract: A resin transfer molding (RTM) process is disclosed for rapidly filling a fibrous preform and/or a rigid, porous body with high viscosity resin or pitch. The process is suitable for impregnated multiple porous bodies stacked in a single mold. The process uses a fibrous preform or rigid porous body which is placed into a mold matching the desired part geometry. A resin is injected into the mold at temperature and pressure. After cooling, the infiltrated component is removed from the mold. The mold is constructed from two halves fitted to form at least one mold cavity. A gate fitted with a nozzle is set into one of the mold halves, and a valve admits resin or pitch into the gate area. Venting or vacuum can be applied to the mold. The mold is held in a hydraulic press and an extruder, optionally fitted with an accumulator, supplies molten resin or pitch to the mold.

Abstract: A method for molding an optical disk comprises: applying a thermally insulative insert coating to at least one thermally insulative mold insert to provide at least one coated mold insert having a reduced surface roughness; positioning the coated mold insert between a thermally conductive mold form and a portion of a thermally conductive mold apparatus; injecting a molten thermoplastic material into the mold apparatus; retaining the material in the mold apparatus for a time sufficient for the molten thermoplastic material to cool below its glass transition temperature to form the optical disk; and ejecting the optical disk from the mold apparatus. In another embodiment, the mold insert is coated or laminated on the mold form with the mold insert having a coefficient of thermal expansion compatible with the coefficient of thermal expansion of the mold form. In another embodiment, the mold insert is fabricated by being applied, cured, and then removed from a release layer.

Abstract: Carbonaceous fibers having sharp ends and which are useful as an electron-emitting material, for example, in cold-cathode display devices. Carbonaceous fibers having a structure such that planes formed of carbon atoms in a condensed ring structure are concentrically grown around a fiber axis then subjected to heating at a temperature of 400-1200° C. in the presence of oxygen.

Abstract: A method for manufacturing a free-standing solid diamond microchannel plate produces a base structure, including a silicon material, having a backing and a vertical extension. A chemical vapor deposition diamond material is deposited onto the backing. The diamond material is leveled with the vertical extension of the base structure. The silicon backing is removed from the leveled base structure.

Abstract: A process for making high aspect ratio metal flakes comprises applying a multi-layer sandwich of vapor deposited metal and release coats in alternating layers to a rotating chilled drum or suitable carrier medium contained in a vapor deposition chamber. The alternating metallized layers are applied by vapor deposition and the intervening release layers are preferably solvent-soluble materials applied by suitable coating or vapor deposition sources contained in the vapor deposition chamber. The release coat materials can be a thermoplastic solvent-soluble polymer. The multi-layer sandwich built up in the vacuum chamber is removed from the drum or carrier and treated with a suitable solvent to dissolve the release coating from the metal in a stripping process that leaves the metal flakes essentially release coat free.

Abstract: This invention relates to microfabricated surgical devices made of a conformally coated polymer.

Abstract: Near net shape free standing articles can be produced by chemical vapor deposition techniques when a suitable substrate is suspended in a chemical vapor deposition zone according to the disclosed technique. By suspending such substrates from linear suspension supports such as ropes, cables and wires, multiple near net shape articles can be produced with substantial manufacturing cost savings over previously employed techniques.

Abstract: A method of removing a core from a CMC component in which the core was used to form an internal cavity. According to one embodiment of the invention, the core is removed from a fully densified CMC component by heating the component and core to a temperature at which the core deteriorates but below a temperature at which the component would melt or otherwise be damaged. According to a second embodiment of this invention, the component is only partially densified, and then impregnated with a coating material that is resistant to a leaching compound capable of removing the core. The core can then be removed using the leaching compound without damage to the internal surfaces of the component defined by the core when the component was fabricated.

Abstract: In a method for manufacturing electronic parts by laminating metal thin films and insulating thin films on a support, a mold releasing agent is applied to the support before the start of lamination. Alternatively, the mold releasing agent is applied to the surface of the laminate during the lamination step, and then lamination is resumed. Therefore, the laminate can be prevented from cracking when the laminate is separated from the support or divided into plural pieces in the lamination direction. Thus, the reliability and productivity of electronic parts improve.

Abstract: The invention provides a method for the manufacture of a dental restoration including the steps of forming a model of refractory material of a tooth, and forming, by flame spraying directly on to said refractory model, a base layer of predetermined thickness of said restoration, said refractory model being cooled during the formation of said base layer. The refractory model is subjected to burn out, and optionally hardening heat treatment, and one or more layers of dental porcelain are applied to the base layer following sintering of said base layer.

Abstract: A process for making high aspect ratio metal flakes economically and at high production rates comprises applying a multi-layer sandwich of vapor deposited metal and release coats in alternating layers to a rotating chilled drum or suitable carrier medium contained in a vapor deposition chamber. The alternating metallized layers are applied by vapor deposition and the intervening release layers are preferably solvent or water soluble materials applied by suitable coating or vapor deposition sources contained in the vapor deposition chamber. The release coat materials can be a thermoplastic solvent-soluble polymer, a water soluble inorganic salt, or a high boiling point dissolvable wax-like substance. The multi-layer sandwich built up in the vacuum chamber is removed from the drum or carrier and treated with a suitable solvent or water to dissolve the release coating from the metal in a stripping process that leaves the metal flakes essentially release coat free.

Abstract: The invention provides a method for the manufacture of a dental restoration including the steps of forming a model of refractory material of a tooth, and forming, by flame spraying directly on to said refractory model, a base layer of predetermined thickness of said restoration, said refractory model being cooled during the formation of said base layer. The refractory model is subjected to burn out, and optionally hardening heat treatment, and one or more layers of dental porcelain are applied to the base layer following sintering of said base layer.

Abstract: A method for producing a multiplicity of miniature cavities extending from a mold surface for molding a plastic product having features integrally molded with and extending from a product base, and a mold so produced. The mold cavities are formed by depositing multiple layers of plating material on a workpiece in a predetermined pattern selected to produce a desired mold cavity shape. The mold may be in the form of a roll or belt for continuous processing, or in any form for discrete injection molding. The invention is particularly applicable to the production of touch fastener products, such as those with arrays of miniature hooks.

Abstract: A process for making functional or decorative flakes or platelets economically and at high production rates comprises applying a multi-layer sandwich of vapor deposited metal and release coats in alternating layers to a rotating chilled drum or suitable carrier medium contained in a vapor deposition chamber. The alternating metallized layers are applied by vapor deposition and the intervening release layers are preferably solvent soluble thermoplastic polymeric materials applied by vapor deposition sources contained in the vapor deposition chamber. The multi-layer sandwich built up in the vacuum chamber is removed from the drum or carrier and treated with a suitable organic solvent to dissolve the release coating from the metal in a stripping process that leaves the metal flakes essentially release coat free.

Abstract: A method for molding an agglomeration of fused microspheres to create a fragrance delivery system by use of room temperature setting binders. The molded pre-glass agglomeration has an extended fragrance release time exceeding a year and a half, and uses microcapillary action to quickly uptake oils and alcohols. The molded pre-glass agglomeration provides a slow release of fragrance without the escape of any residual liquid. The molded pre-glass agglomeration may be replenished, an unlimited number of times, with fragrance containing oils and alcohols after the odor fades. The molded pre-glass agglomerations may also be colored or dyed.

Abstract: A method of producing a carbon-carbon part having a filamentized composite fiber substrate is provided. A substrate having a plurality of discontinuous filamentized fibers and a binder that binds said filaments together to form a composite substrate is provided, and carbon atoms are deposited onto the filaments at a predetermined temperature so that the binder is removed completely from the filaments and replaced with carbon atoms to from a dense carbon-carbon part.

Abstract: Disclosed are methods of manufacturing electronic devices, particularly integrated circuits. Such methods include the use of low dielectric constant material prepared by using a removable porogen material.

Abstract: A wrinkle-free organic film having a high light transmittance and a uniform film thickness is obtained by forming an organic thin film on the surface of a substrate having a contact angle of the surface to water of 90° or higher, followed by peeling the film therefrom.

Abstract: Near net shape free standing articles can be produced by chemical vapor deposition techniques when a suitable substrate is suspended in a chemical vapor deposition zone according to the disclosed technique. By suspending such substrates from linear suspension supports such as ropes, cables and wires, multiple near net shape articles can be produced with substantial manufacturing cost savings over previously employed techniques.

Abstract: A process of monolithically forming one-piece reflective pavement marker or delineator, including at least one retro reflective face. The process is based on molding the pavement marker or delineator with means to integrally form cube-corner reflective elements and internal hollow cavity air gaps simultaneously. The pavement marker also provides means to enhance agglutination to the roadway. The open ends of hollow cavities at the marker base can be sealed, thereby maximizing the base area for adhesive wetting parameter.

Abstract: A method of synthesizing an even free-standing diamond film without growth cracks is disclosed. The intrinsic tensile stress of a diamond film is compensated by an artificial compressive stress with a step down control of the deposition temperature during deposition. After a diamond film is deposited with a predetermined thickness at a deposition temperature, the deposition temperature is decreased in multiple steps during the deposition. The bending of the diamond wafer is minimized by using a tungsten substrate with higher elastic modulus than molybdenum.

Abstract: A process of producing relatively large, dense, free-standing silicon carbide articles by chemical vapor deposition is enabled by the provision of specially designed isolation devices. These devices segregate silicon carbide deposits on the intended portions of substrates, thereby alleviating the need to fracture heavy silicon carbide deposits in order to remove, or otherwise move, the substrate, with the heavy deposit thereon, from the deposition furnace. The isolation devices enable the use of more efficient vertically extended vacuum furnaces. The isolation devices also enable the commercial production of relatively dense, large, thin-walled, silicon carbide shells.

Abstract: In a method for manufacturing electronic parts by laminating metal thin films and insulating thin films on a support, a mold releasing agent is applied to the support before the start of lamination. Alternatively, the mold releasing agent is applied to the surface of the laminate during the lamination step, and then lamination is resumed. Therefore, the laminate can be prevented from cracking when the laminate is separated from the support or divided into plural pieces in the lamination direction. Thus, the reliability and productivity of electronic parts improve.

Abstract: A housingless abrasion resistance reflective pavement marker is disclosed. The marker includes a housingless, flat topped body and at least one reflective member encapsulated in the marker's body during casting. The body can be made of abrasion and impact resistant curable resinous material filled with inert additives. The reflective member can be coated with abrasive resistance diamond like carbon film to enhance durability and retain longer reflectivity. The reflective member can have an inside surface divided into light reflecting cells. The reflective cells can be further protected by a variety of impact reducing raised ridges. Disclosed is a method for making housingless reflective pavement marker in an open face mold.

Abstract: A process of producing relatively large, dense, free-standing silicon carbide articles by chemical vapor deposition is enabled by the provision of specially designed isolation devices. These devices segregate silicon carbide deposits on the intended portions of substrates, thereby alleviating the need to fracture heavy silicon carbide deposits in order to remove, or otherwise move, the substrate, with the heavy deposit thereon, from the deposition furnace. The isolation devices enable the use of more efficient vertically extended vacuum furnaces. The isolation devices also enable the commercial production of relatively dense, large, thin-walled, silicon carbide shells.

Abstract: A generally tubular device (e.g., a stent or catheter) for placement in a lumen of a patient's body is made by forming a depressed pattern in an external surface of a mold. The depressed pattern corresponds to a desired shape of the generally tubular device. A material is deposited in the depressed pattern for the material to form the generally tubular device conforming to the depressed pattern. The generally tubular device is separated from the mold.

Abstract: A solid freeform fabrication process and apparatus for making a three-dimensional object. The process includes the steps of (1) positioning a material deposition sub-system a selected distance from a target surface, (2) operating this sub-system to deposit materials onto the target surface by carrying out the sub-steps of (a) operating a multiple-channel fluid phase delivery device of the deposition sub-system for supplying multiple fluid compositions to a small region proximate the target surface and (b) operating a focused energy source to produce a phase change zone at this region, thereby inducing deposition of materials onto the target surface, and (3) during the material deposition process, moving the deposition sub-system and the target surface relative to one another in a plane defined by first and second directions and in a third direction orthogonal to this plane to form deposition materials into a three dimensional shape. These steps are preferably executed under the control of a computer system.

Abstract: A method and system are described for controlling the delivery of vapor from a bubbler containing a supply of liquid through which a carrier gas is bubbled and from which bubbler vapors are delivered in a vapor stream entrained with the carrier gas. In general, the present invention involves utilizing the pressure of the vapor leaving the bubbler as the specific characteristic monitored and controlled to ensure that the concentration level of carrier gas to vapor is maintained at the desired level throughout the manufacturing process.The present invention involves introducing a concentration detector within the flow path of the bubbler vapors from the bubbler and having the output of the concentration detector input to a concentration controller. The concentration controller compares the concentration value received from the concentration detector to a desired concentration value determined for the system.

Abstract: Methods and compositions are described that provide three-dimensional fibrillar matrices useful as, among other things, structural prosthetics and scaffolds for cells. The porous fibrillar matrices of the present invention have desirable mechanical properties suitable to a variety of applications, including platforms for in vitro cell cultivation, implants for tissue and organ engineering, implants as tendon and facia prosthetics, and product packaging.

Abstract: A method for molding high precision components is provided that allows inexpensive, rapid fabrication of components using a process involving a silicon substrate, in which the mold pattern is created using multiple mask layers, a deep reactive ion etch process and photolithographic patterning techniques.

Abstract: A bypass conduit having a desired hollow internal geometry for defining a bounded blood flow path from an open first end positioned in a heart chamber and an open second end connected to a lumen of a coronary vessel is made by forming a master having an external surface with an external geometry complementary to the desired internal geometry of the conduit. The external surface of the master is coated with pyrolytic carbon to define a pyrolytic carbon conduit of pyrolytic carbon bonded to the external surface of the master and with the pyrolytic carbon having an internal surface with a conduit geometry complementary to the external geometry of the master. The master is removed from the pyrolytic carbon conduit.

Abstract: The invention comprises devices composed of at least one microscopic hollow tube having a wall of single or multiple layers with a thickness of at st one nanometer and a diameter of at least 5 nanometers. The walls of the tubes can be formed from a wide variety of materials, some of the preferred materials include metals, polymers, carbon, ceramics, glasses. If the space between the tubes is filled, the tubes become channels in a monolithic or composite body. The channels can have a random or ordered orientation. The interior of the tube walls can be coated with a desired material such as a catalyst and also may have depressions or elevations therein that were imparted to the fibers upon which the tubes are formed. The wall layers may be porous for the purpose of removing the fiber therethrough. Microtubes and microtube devices may be interfaced with the macroscopic world in a number of ways.

Abstract: A method of fabricating a needle via conformal deposition in a two-piece mold includes the step of attaching a top mold member to a bottom mold member such that the top mold member and the bottom mold member define an enclosed, elongated needle trench with a deposition aperture. A conformal substance, such as polysilicon, is then passed through the deposition aperture such that the conformal substance is deposited within the enclosed, elongated needle trench to form a needle. The method is used to form needles with prongs, multiple channels, multiple ports, barbs, strength enhancement features, and circuitry.

Abstract: A method and apparatus for making carbon/carbon composite discs for an aircraft brake employs a continuous feeding of fiber strands into a mold. Water is then combined with the fibers and the fibers are compressed to form a moisturized mat or preform. The fibers are then needled such that the fibers within the mat or preform extend in radial, circumferential, and axial directions. The mat or preform is then subjected to densification. The resulting disc is of total carbon construction. The water introduced into the mat during the processing serves as both a sacrificial binder and a lubricant during the fabrication.

Abstract: A carbon composite structure, for example, an automotive engine piston, is made by preparing a matrix including of a mixture of non crystalline carbon particulate soluble in an organic solvent and a binder that has a liquid phase. The non crystalline particulate also contains residual carbon hydrogen bonding. An uncured structure is formed by combining the matrix mixture, for example, carbon fibers such as graphite dispersed in the mixture and/or graphite cloth imbedded in the mixture. The uncured structure is cured by pyrolyzing it in an inert atmosphere such as argon. Advantageously, the graphite reinforcement material is whiskered prior to combining it with the matrix mixture by a novel method involving passing a gaseous metal suboxide over the graphite surface.

Abstract: An apparatus is provided for synthesizing a silica glass ingot. The appartus includes a stage having a target plate thereover, the target plate being rotatable relative to the stage around a predetermined vertical axis, and a furnace for reacting material gas with combustion gas to synthesize the silica glass ingot on the target plate; the furnace having an opening at its bottom. The appratus further includes an elevation system that moves the stage in a vertical direction parallel to the predetermined vertical axis so as to vertically move the target plate through the opening of the furnace, the elevation system supporting the stage from at least one side of the stage and lacking a structure directly below the stage that would substantially interfere with the vertical movement of the stage.

Abstract: Articles having at least one precision replicated surface are formed by chemical vapor deposition on a substrate surface which has been precision shaped and finished as the converse of the desired precision surface of the article. The substrate surface is provided with a thin release coating which adheres to the substrate when the article is removed thereby allowing the substrate to be reused. The method is particularly advantageous for forming the interior surfaces of domes and asymmetrical optical surfaces of zinc sulfide.

Abstract: A conductive wire is electrically heated in a gas atmosphere, wherein a gas reacts with a constituent material of the conductive wire, under gravity-free or micro gravity state. A ceramic is formed on a surface of the wire sa an outer core through a reaction between the wire and the gas and is left by caving an inside wire by melting while maintaining controlled gas convection.

Abstract: Disclosed is a crucible of pyrolytic boron nitride (PBN) for molecular beam epitaxy for melting of the source material, with which the troubles due to adhering of the molten source material in the form of drops caused on the quality of the epitaxial layer can be greatly decreased. Namely, the inner surface of the crucible is free from pits or other irregularities responsible to the adhering of the melt when the growth plane, which can be exposed by stripping of the surface layer of 0.50 mm thickness by cleavage, has a surface roughness Ra not exceeding 2.0 .mu.m and Rmax not exceeding 18 .mu.m. Such a PBN crucible can be prepared by the CVD method to deposit PBN on the surface of a graphite core of which the surface roughness Ra does not exceed 2 .mu.m.

Abstract: There is disclosed a pyrolytic boron nitride container used for a Boat method in which material melt is retained In the container, and a crystal is grown while a temperature gradient is imparted to the material melt. The transmissivity of the pyrolytic boron nitride container with respect to light at a wave number ranging from 3700 cm.sup.-1 to 6500 cm.sup.-1 has a profile such that the transmissivity monotonously changes in the longitudinal direction of the container. The transmissivity profile is produced by imparting a pressure profile during manufacture of the container through deposition of pyrolytic boron nitride, by roughing the outer surface of the container such that the surface roughness has a profile, or by compounding pyrolytic boron nitride with a different material. It becomes possible to facilitate generation of a temperature gradient in material melt within the container and to facilitate control of a temperature profile in the container.

Abstract: Apparatus which is disclosed comprises a metal mold, a metal plunger and an annular manifold, and includes means for moving the plunger and the manifold between an open position in which the manifold surrounds the plunger and a gob of softened glass can be introduced into the mold and a closed position in which the manifold surrounds the plunger and the latter forms, with the mold and the manifold, a cavity in which a glass part can be formed. The manifold and the plunger have facing walls which are above the mold cavity, have portions which are in close fitting sliding engagement, and, thereabove, portions which diverge away from one another and form an annular space.

Abstract: Process of mixing a fugitive plasticizer, e.g., ethylene carbonate, with moist particulate polyacrylonitrile then removing the water enabling adjustment of the melt viscosity for extrusion of the polyacrylonitrile into film, fiber, pellets and shaped articles. Stretching and heating the extruded polyacrylonitrile film or fiber causes the fugitive plasticizer to exude and vaporize from the film or fiber, carrying with it any remaining acrylonitrile monomer. The resulting film or fiber exhibits substantially increased molecular weight, thus enhancing the tensile strength and barrier properties of the polyacrylonitrile product. The process also produces polyacrylonitrile foam products. A novel cross-linking agent for polyacrylonitrile, divinyloxybutane, is disclosed. Thermostabilizing agents for polyacrylonitrile, N-maleimides and stilbene derivatives, are also disclosed.

Abstract: A refractory composite structure is formed which comprises a ductile refractory metallic layer with a roughened surface which is tightly bonded to a refractory composite structural shell. The roughened surface is preferably dendritic in form and produced by chemical vapor deposition techniques. The refractory composite structural shell is preferably a carbon-carbon composite formed by applying a carbon filament preform to the roughened surface, infiltrating the preform with a carbon matrix precursor, and carbonizing the precursor.

Abstract: A process and apparatus for making a ceramic article, especially pipes and tubes of ceramic material such as silicon carbide, in which the article is formed by projecting a ceramic powder mixture comprising refractory particles and combustible particles against a smooth-surface metal former which is heated to a temperature of at least 850.degree. C. where in the presence of an oxygen-rich gas the combustible particles react exothermically to produce from the refractory particles and the reaction product of the combustible particles a coherent refractory article in the shape of the former.

Abstract: Disclosed are .[.a.]. processes and reactors for rapidly producing large diameter, high-purity polycrystalline silicon rods for semiconductor applications by the deposition of silicon from a gas containing a silane compound. The equipment includes a reactor vessel which encloses a powder catcher having a cooled surface. Also within the vessel is a cylindrical water jacket which defines multiple reaction chambers. The silicon powder generated in this process adheres to the coolest surfaces, which are those of the powder catcher, and is thereby collected. Little of the powder adheres to the walls of the reaction chambers. In some embodiments, a fan can be provided to increase gas circulation.