Abstract: A process for producing particles of a thermoplastic polymer in spherical form involves providing at least one thermoplastic polymer in a molten state and providing an aqueous solution of at least one surface-active substance. The aqueous solution is in a temperature range from 100 to 300° C. The process also involves dispersing the thermoplastic polymer in the aqueous solution to obtain an aqueous solution containing dispersed thermoplastic polymer, which is cooled down to a temperature below the solidification point of the thermoplastic polymer to obtain a suspension containing an aqueous solution and particles of the thermoplastic polymer suspended in a solid state and in spherical form. The particles can be separated from the suspension and, optionally, dried. The particles obtained from the process have a particle size distribution having a d[4,3] value of more than 10 ?m and a d90.3 value of more than 20 ?m.

Abstract: A process for producing particles of a thermoplastic polymer in spherical form involves providing at least one thermoplastic polymer in a molten state and providing an aqueous solution of at least one surface-active substance. The aqueous solution is in a temperature range from 100 to 300° C. The process also involves dispersing the thermoplastic polymer in the aqueous solution to obtain an aqueous solution containing dispersed thermoplastic polymer, which is cooled down to a temperature below the solidification point of the thermoplastic polymer to obtain a suspension containing an aqueous solution and particles of the thermoplastic polymer suspended in a solid state and in spherical form. The particles can be separated from the suspension and, optionally, dried. The particles obtained from the process have a particle size distribution having a d[4,3] value of more than 10 ?m and a d90.3 value of more than 20 ?m.

Abstract: Optical absorber-containing thermoplastic polymer particles (OACTP particles) may be produced by methods that comprise: mixing a mixture comprising a thermoplastic polymer, a carrier fluid that is immiscible with the thermoplastic polymer, and optionally an emulsion stabilizer at a temperature greater than a melting point or softening temperature of the thermoplastic polymer and at a shear rate sufficiently high to disperse the thermoplastic polymer in the carrier fluid; cooling the mixture to below the melting point or softening temperature of the thermoplastic polymer to form solidified particles comprising the thermoplastic polymer; separating the solidified particles from the carrier fluid; and exposing the solidified particles to an optical absorber to produce the OACTP particles.

Abstract: Provided is an apparatus for producing solid polymeric microparticles, the apparatus comprising a plurality of liquid droplet generators for forming liquid droplets of a first liquid, and a nozzle for forming a jet of a second liquid, wherein the plurality of liquid droplet generators and the nozzle are arranged relative to each other such that, in use, liquid droplets from the plurality of liquid droplet generators pass through a gas into said jet of second liquid.

Abstract: Method of producing prills includes providing a hollow body rotatable about a first axis, the body having a wall rotationally symmetrical around the first axis forming an interior space, the wall including nozzles; providing a second body disposed in the hollow body such that a gap exists between the hollow body and the second body; supplying liquid to the gap; generating jets of liquid from the nozzles radially outward by driving the rotational motion of the hollow body and/or second body around the first axis of rotation using a rotary drive unit; applying a reciprocal pressure excitation on the jets of liquid by moving the hollow body and/or second body along the first axis; and decoupling the rotations of the one of the hollow body and second body and a reciprocating drive-unit.

Abstract: A respirable dry powder including acetylsalicylic acid in particles has a mass median aerodynamic diameter (MMAD) within a range of about 0.5 ?m to about 10 ?m. The respirable dry powder may contain a pharmaceutically acceptable excipient, such as a phospholipid, in an amount ranging from about 0.1% (w/w) to about 10% (w/w) of the particles.

Abstract: A process for producing polyolefin particles from a polyolefin composition, comprising the steps of: a) providing a melted composition of a polyolefin and b) providing particles from the melted composition by: b1) mixing a first flow of a supercritical fluid in the melted composition in a pressure vessel to obtain a solution saturated with the supercritical fluid and b2) passing the solution from the pressure vessel through a throttling device to a spraying tower to expand the solution to obtain the polyolefin particles in the spraying tower, wherein a second flow of a supercritical fluid is injected in the throttling device, wherein the supercritical fluid is a supercritical fluid of a substance selected from the group consisting of CO2, NH3, H2O, N2O, CH4, ethane, propane, propylene, n-butane, i-butane, n-pentane, benzene, methanol, ethanol, isopropanol, isobutanol, chlorotrifluoromethane, monofluoromethane, 1,1,1,2-Tetrafluoroethane, toluene, pyridine, cyclohexane, cyclohexanol, o-xylene, dimethyl ether an

Abstract: A cold spark fire electronic eruptive apparatus characterized in that the erupting apparatus is comprised of an ejecting unit, an activation unit, a power unit, and a storage unit, wherein, the storage unit stores a cold fireworks material for discharge, the power unit is connected to the storage unit and also is connected with a heating unit, the power unit transmitting the cold fireworks material in the storage unit to the heating unit, and the heating unit activating the cold fireworks raw material, sending it to the air removal unit for eruption.

Abstract: A cold spark waterfall machine, which comprises an accelerating unit, a heating unit, a power unit, and a storage unit. The storage unit stores a cold fireworks raw material for discharging. The power unit is connected to the storage unit wherein the storage unit is connected with the heating unit, and the power unit transmits the cold fireworks raw material in the storage unit to the heating unit. The heating unit activates the cold fireworks raw material and sends the cold fireworks raw material to the acceleration unit. The acceleration unit causes the activated material to accelerate in a downward eruption, thus forming a waterfall of low temperature sparks.

Abstract: Superabsorbent material, comprising clay-crosslinked superabsorbent polymers, obtainable by polymerizing in a spray-stream, polymerizable compounds in the presence of a polymerization initiator system, and nano-sized or individual clay particles, which are all introduced into a vessel by a spraying step in the form of a said spray-stream thereof, whereby said clay particles crosslink said polymers during polymerization. The invention also relates to such a process and absorbent articles comprising such superabsorbent material.

Abstract: In a method and apparatus for micropelletization of a polymeric material, a melt thread of the polymeric material is formed by an extruder. A flowing gas is directed to the melt thread to form Rayleigh disturbances in the melt thread and break up the melt thread into discrete microdroplets. The discrete microdroplets are then solidified to form micropellets.

Abstract: Polymer pellets are formed using air to influence the separation of polymer from a polymer melt. In accordance with one or more embodiments, a polymer material is extruded through a nozzle to form a polymer melt extending from the nozzle. A non-uniform thickness is generated in the polymer melt using a gas or gasses to apply a drag force to the polymer melt. This drag force reduces a thickness of a portion of the polymer melt adjacent the nozzle, and the polymer melt is fractured into discrete droplets at the reduced thickness. The discrete droplets are then solidified to form pellets.

Abstract: A method for formation of micro-prilled poloxamer particles is disclosed. The particles find special use in pharmaceutical formulations. The process involves use of atomizing nozzles at higher than normal pressure atomizing gas, high atomizing gas temperature, use of high feed temperatures to reduce the viscosity of the poloxamer and optionally sieving after prill formation in prilling towers. The poloxamer particles are spherical and preferably have an average nominal diameter of less than or equal to 106 microns. The process is very cost effective and rapid.

Abstract: The problem addressed by the present invention is providing a method for producing microparticles. At least two fluids to be processed, a raw material fluid that contains a raw material and a processing fluid that contains a substance for processing the raw material are mixed in a thin film fluid formed between at least two surfaces for processing that are disposed so as to face each other, that can approach and separate from each other and at least one of which rotates relative to the other, and microparticles of the raw material that is processed are obtained. At this time, the proportion of the microparticles of the raw material which has been processed that coalesces with each other is controlled by controlling the circumferential speed of the rotation in a confluence section in which the raw material fluid and processing fluid flow together.

Abstract: A method for producing fine particles, including: discharging a fine particle material liquid, where solid materials to be formed into fine particles are dissolved or dispersed in a solvent or are melted, from two or more discharge holes in a downward vertical direction, to thereby form liquid droplets; and solidifying the liquid droplets discharged to form fine particles, wherein in the discharging a fine particle material liquid, gas flow is supplied at angle of greater than 0° but 90° or smaller to the downward vertical direction, and wherein an initial discharge velocity of the liquid droplets discharged from the discharge hole located at an upstream side of the gas flow in a flowing direction thereof is equal to or higher than an initial discharge velocity of the liquid droplets discharged from the discharge hole located at a downstream side of the gas flow in the flowing direction thereof.

Abstract: A seamless capsule manufacturing apparatus (1) manufactures a seamless capsule by means of nozzles (2a-2d). A core liquid (5) and a coating liquid (6) are supplied to each of the nozzles (2a-2d) from pumps (16, 18) through distributors (21, 22). The distributors (21, 22) and the nozzles (2a-2d) are connected to each other by core liquid distributing tubes (23a-23d) and coating liquid distributing tubes (25a-25d), and each of the core liquid distributing tubes (23a-23d) and each of the coating liquid distributing tubes (25a-25d) have the same length. A vibrator (24) is mounted to the distributor (21), and the core liquid (5) is supplied to the nozzles (2a-2d) while being vibrated. Each of the distributors (21, 22) is provided with an air vent device (35), and air vent is performed appropriately.

Abstract: The present invention provides a method for making uniform, spherical, acrylic polymeric beads by jetting, the beads produced, and ion exchange resins produced from functionalizing the uniform, spherical polymeric beads.

Abstract: Provided is a glucose sensor. The glucose sensor according to the present invention includes noble metal-graphene composites, and has high sensitivity and significantly excellent current flow as compared to titanium dioxide-graphene composites. In addition, the noble metal-graphene composite manufactured by aerosol spray pyrolysis serves as an improved glucose sensor having desirable sensitivity, stability, reproducibility, and selectivity.

Abstract: A particulate production apparatus, including a droplet discharger to discharge a liquid including a particulate element which is solidified to become a particulate; and a pressure controller to feed the liquid including a particulate element to the droplet discharger at a pressure within a desired range.

Abstract: A spherical tungsten carbide powder is characterized by that the material has a microhardness higher than 3600 kgf/mm2, and that the powder has an apparent density from 9.80 to 11.56 g/cm3. A method for the manufacture of a powder comprises the steps: a) providing a chamber comprising a rotatable crucible, b) adding material into said rotatable crucible, c) melting the material using a plasma arc discharge, d) rotating the crucible to atomize the molten material to form liquid droplets, with subsequent cooling of the droplets to obtain a powder, wherein the material added into said rotatable crucible is heated to a temperature above 40% of the melting temperature of the material before it enters the crucible. It is possible to reduce the current required for melting the stock. Heat losses are decreased, and the spherical powder obtained during atomization becomes more homogeneous in its composition and structure. The cost is reduced.

Abstract: A method of producing particulate, including introducing an initial liquid including a particulate component in a lower concentration than that of a liquid including a particulate component or no concentration to a projection hole of a droplet projector so as to be projected at the start of the discharging; discharging a droplet of the liquid comprising a particulate component from the projection hole; and solidifying the droplet to form a particulate.

Abstract: The present invention provides a sonochemical irradiation-based method for the preparation of polydopamine (PDA) nanocapsules having reduced wall thickness and uniform size distribution, which may further comprise at least one payload; nanocapsules obtained by this method; and compositions thereof. Such compositions may be formulated for different purposes, e.g., as pharmaceutical compositions for various therapeutic or diagnostic purposes.

Abstract: A method of manufacturing toner is provided. In the method, toner constituents are dissolved or dispersed in an organic solvent to prepare a toner constituents liquid. The toner constituents liquid is degassed so that the toner constituents liquid includes dissolved oxygen in an amount of 3 mg/L or less. The toner constituents liquid is vibrated in a chamber having at least one nozzle to form a liquid column resonance standing wave in the toner constituents liquid. The toner constituents liquid is discharged from the nozzle disposed within an area including an antinode of the liquid column resonance standing wave to form the toner constituents liquid into liquid droplets. The liquid droplets are dried to solidify the liquid droplets into solid particles.

Abstract: Formulations of neutral retinoids, in particular fenretinide (HPR) in the form of lipid nanoparticles, solid dispersions and emulsions are disclosed. These compositions are used to treat diseases that are amenable to treatment by HPR, such as neoplastic diseases by achieving higher and more prolonged concentrations of HPR in the subject. The key steps for preparing lipid nanovesicles of HPR include mixing and sonication, sterile filtration, without or without lyophilization for long-term stable storage, and employ processes and materials that are scalable from the laboratory to the manufacturing level. The formulation are suitable for injection into human or animal patients without causing allergic or hypersensitivity responses by avoiding chemical surfactants and animal sources of phospholipids in their manufacture.

Abstract: A method for producing particles, including: bringing a compressive fluid into contact with a pressure plastic material, so as to produce a melt of the pressure plastic material; and discharging the melt of the pressure plastic material by differential pressure to a space, so as to form particles, wherein the discharging includes at least one of (A) discharging the melt of the pressure plastic material while a compressive fluid is supplied to the melt of the pressure plastic material, and (B) discharging the melt of the pressure plastic material through one or more through-holes, to which vibration is applied, so as to change the shape of the melt of the pressure plastic material from a columnar shape, through the columnar shape with constrictions, into a particle shape.

Abstract: The present invention relates to a new manufacture process for producing an iron containing phosphate adsorbent, in particular to a process for manufacturing and isolating an iron(III)-based phosphate adsorbent which exhibits valuable pharmacological properties.

Abstract: A process for obtaining compositions constituted by propolis nanoparticles is disclosed. The nanoparticles are optionally associated to a substance of interest such as active ingredients, and, optionally, substances of secondary effect such as synergists and adjuvants. The process includes preparing a fraction A, which consists of propolis extract dissolved in an organic solvent, to which stabilizer and/or emulsifier may be added, and, optionally, substances of interest and/or of secondary effect; ii) preparing a fraction B, aqueous phase, constituted by: (ii.1) water; or (ii.2) an aqueous solution or dispersion, to which stabilizer and/or emulsifier may be added; (iii) dropping the fraction A onto the fraction B or vice versa; iv) homogenizing the mixture by stifling and spontaneous formation of nanoparticles with average size from 1 to 1000 nm in a dispersion; and v) optionally (v-1) removing organic solvent and/or (v-2) drying the nanodispersion.

Abstract: Dissociation of a macroscale version of an aramid fiber leads to the nanofiber form of this polymer. Indefinitely stable dispersions of uniform high-aspect-ratio aramid nanofibers (ANFs) with diameters between 3 and 30 nm controlled by the media composition and up to 10 ?m in length are obtained. ANFs can be processed in transparent thin films using layer-by-layer assembly (LBL) with superior mechanical performance.

Abstract: In a method and system for forming concentrated volumes of microbeads, a polymer solution and/or suspension includes a polymer dissolved and/or dispersed in a medium. Streams of a focusing fluid and of the polymer solution and/or suspension flow towards a fluid bath, and into intersection with one another, so &s to focus the polymer solution and/or suspension. The polymer solution and/or suspension stream forms microbeads in the fluid bath. Some of the focusing fluid is drawn from the fluid bath, so as to concentrate the microbeads in die fluid bath. The system includes a flow focusing apparatus and a liquid-containing cell. The focusing apparatus includes polymer and focusing nozzles. The cell contains the fluid bath and has an outlet port, through which the focusing fluid is drawn from the fluid bath.

Abstract: The present invention relates to a method for the production of micro-particles of polysaccharides. The method includes preparing a feeding solution and a gelifying liquid to collect nebulized jets of the feeding solution. The feeding solution contains at least one polymer capable of forming micro-particle structures and at least one biologically active substance. The feeding solution is pressurized inside an air-less nebulizing unit and then nebulized through the unit itself so as to generate nebulized jets impacting the surface of the gelifying liquid.

Abstract: A toner manufacturing method, a toner manufacturing apparatus, and a toner are disclosed. The toner manufacturing apparatus includes a droplet generating unit that includes a thin film in which plural nozzles are formed, and an annular vibrating unit that is arranged at a perimeter of a deformable domain of the thin film for vibrating the thin film; a storage unit for storing a toner-containing liquid that includes at least a resin and a colorant, and for supplying the toner-containing liquid 10 to the droplet generating unit; and a granulating unit for solidifying droplets that are periodically breathed out from the nozzles of the droplet generating unit to form toner particles.

Abstract: Disclosed is a micro particle for a thermal control material capable of being applied as a highly thermal conductive material for thermal control, and an apparatus and a method of producing the micro particle for the thermal control material by using an ultrasonic high-temperature vibration scheme. More specifically, a Boron Nitride (BN) particle having a plate shape and an excellent thermal conductivity is coated on a PCM having a shape of a micro bead, to increase the thermal conduction to the inside PCM, so that a phase change is easily generated, and which allows an easy treatment of the PCM in a liquid state at a temperature equal to or higher than a melting point of the PCM.

Abstract: The invention relates to a process for the preparation of particles based on a thermoplastic polymer with a mean diameter of less than 1 mm. The process of the invention comprises more particularly a stage of preparation of a composition comprising the thermoplastic polymer and an additive, in the molten state, of cooling the composition and of disintegration of the thermoplastic polymer dispersion.

Abstract: Controlled geometry particles of thermoplastic polymers are prepared from compositions containing the thermoplastic polymer and two additives, in the molten state, by cooling the molten composition and disintegrating the resulting dispersion of thermoplastic polymer; powders obtained therefrom advantageously have mean particle diameters ranging from 0.1 to 800 ?m and are useful additives in, e.g., paints and coatings.

Abstract: A method of forming particles, comprises accelerating a first stream comprising a first liquid, applying a charging voltage of at most 1.5 kV to the first stream, and vibrating the first stream, to form particles.

Abstract: A particulate production apparatus, including a droplet discharger to discharge a liquid including a particulate element which is solidified to become a particulate; and a pressure controller to feed the liquid including a particulate element to the droplet discharger at a pressure within a desired range.

Abstract: A method of manufacturing toner is provided. In the method, toner constituents are dissolved or dispersed in an organic solvent to prepare a toner constituents liquid. The toner constituents liquid is degassed so that the toner constituents liquid includes dissolved oxygen in an amount of 3 mg/L or less. The toner constituents liquid is vibrated in a chamber having at least one nozzle to form a liquid column resonance standing wave in the toner constituents liquid. The toner constituents liquid is discharged from the nozzle disposed within an area including an antinode of the liquid column resonance standing wave to form the toner constituents liquid into liquid droplets. The liquid droplets are dried to solidify the liquid droplets into solid particles.

Abstract: Proppant material for hydraulic fracturing is provided. The particles of the proppant are formed by drip casting. A slurry of finely divided ceramic particles is flowed through nozzles and formed into droplets under the influence of vibration. Uniform sized, smooth surface, spherical green particles are formed. The green particles are dried and sintered to form the proppant. The proppant is used in the process of hydraulic fracturing of wells.

Abstract: Methods and systems for preparing nanocrystalline compositions using focused acoustic processing to cause and/or enhance crystal growth. A flow through system may be employed to expose sample material having a volume of greater or less than 30 mL to focused acoustic energy while flowing through a process chamber at a rate of at least 0.1 mL/min. Sample material may be processed by a suitable focused acoustic field in a cyclic fashion and/or with adjustment of processing parameters based on monitored characteristics of the sample, such as level of crystallinity. Nanocrystalline particles within the sample may have a tight particle size distribution with an average particle size between 10 nm and 1 micron. Stable nanocrystalline compositions may be reproducibly prepared using focused acoustics to have controllable morphologies and dimensions.

Abstract: A composition for pelletized bitumen and a method for preparing the same is disclosed. The composition is comprised of: between approximately 30% to approximately 40% by weight of bitumen; between approximately 15% to approximately 30% by weight of stiffening compound; between approximately 35% to approximately 45% by weight of setting compound; and approximately 0.05% by weight of water. The stiffening compound is comprised of between approximately 10% to approximately 20% by weight of ground asphalt shingles; between approximately 5% to approximately 10% by weight of vulcanized rubber; between approximately 1% to approximately 2% by weight of uintahite; and up to approximately 0.5% by weight of zeolite. And the stiffening compound may be Type II Portland cement.

Abstract: A method for producing tables made of mixtures of a plurality of materials, and a method for producing a sulfurous fertilizer. A method for producing tablets made of mixtures of a plurality of materials, particularly urea mixtures, having the following steps:—producing a liquid melt of a first material,—adding at least one further material in solid or liquid form to the melt for producing a mixture,—output of drops of the mixture onto a steel belt by means of a drop former having a rotating, perforated outer drum,—solidification of the drops of the mixture on the steel belt into tablets, wherein the at least one additional material is mixed into the liquid melt in liquid form immediately before the drop former or into the liquid melt in solid. form upstream of a two-stage heated grinding and mixing unit.

Abstract: The present invention provides spherical rubber chemicals and the method for preparing the same. The spherical rubber chemicals of the present invention include spherical antioxidants, spherical vulcanization agents, spherical processing aids, spherical reinforcing agents, or spherical adhesive agents. With the spherical rubber chemicals of the present invention, the shortcomings of powdery or semi-spherical rubber chemicals are overcome, including eliminating the dust pollution during granulation procedure and avoiding the raw material loss and the environmental pollution, while solving the quality problem of lower melting point of product caused by the presence of fine powder crystal. Furthermore, the resultant rubber chemicals has an improved smoothness of surface, which is helpful to improve the flowing and mixing behaviors of the rubber chemicals in mixing or open milling process with rubbers.

Abstract: Methods and apparatus for continuously preparing a particulate material are provided. One method of the invention includes mixing a first solution comprising a solute dissolved in a solvent, with a second solution, thereby providing a first solution-second solution mixture; and introducing the mixture into the high-energy zone of a high shear dispersion system and dispersing the first solution-second solution mixture prior to significant particulate growth, whereby the dispersed mixture forms a suspension of particles of the solute; and wherein significant particulate growth has occurred when the average equivalent spherical diameter of at least one particle in the solution is greater than 10 micrometer. Integrated apparatuses for performing methods of the invention are also provided.

Abstract: Nanofibers are fabricated by introducing a mixture of a polymer solution and inorganic precursor into a dispersion medium and shearing the mixture. Liquid strands, streaks or droplets of the mixture are spun into elongated fibers that include inorganic fibrils. The resulting composite inorganic/polymer fibers may be provided as an end product. Alternatively, the polymer may be removed to liberate the inorganic fibrils, which may be of the same or smaller cross-section as the polymer fibers and may be provided as an end product.

Abstract: The present invention relates to methods and compositions to prepare small size particles of poorly water soluble agents or drugs with surface enriched hydrophilicity.

Abstract: The current invention relates to methods of making nano-particles of a material with a narrow polydispersity. The particle materials are active agents, organic compounds, polymers, and combinations thereof.

Abstract: Proppant material for hydraulic fracturing is provided. The particles of the proppant are formed by drip casting. A slurry of finely divided ceramic particles is flowed through nozzles and formed into droplets under the influence of vibration. Uniform sized, smooth surface, spherical green particles are formed. The green particles are dried and sintered to form the proppant. The proppant is used in the process of hydraulic fracturing of wells.

Abstract: A drop pelletizing device and method for producing pellets from a low-viscosity plastic melt are provided. The drop pelletizing device can include a die plate with holes, in which the plastic melt can be subjected to a harmonic pressure oscillation such that the plastic melt emerging from the holes forms individual pellet droplets, a pressure vessel, in which prevails an overpressure above the ambient pressure, a discharge device adapted to discharge the individual pellet droplets from the pressure vessel and to reduce the overpressure, a separator adapted to separate the individual pellet droplets from the coolant; and at least one circulating device adapted to agitate the coolant to separated and unclump the individual pellet droplets in the coolant and for producing turbulence within the coolant.

Abstract: An object of the present invention is to provide a resin microparticle for a toner raw material that has a small particle diameter and a narrow particle diameter distribution and has a low odor. There are provided a resin microparticle for a toner raw material characterized in that all of the following requirements (i) to (iii) are satisfied: Requirement (i): A particle diameter of 50% volume (D50) satisfies the relationship 0.05 ?m?D50?1 ?m; Requirement (ii): A particle diameter of 10% volume (D10) and a particle diameter of 90% volume (D90) satisfy the relationship D90/D10?7; and Requirement (iii): The content of an organic solvent is not more than 70 ppm.

Abstract: Multiphasic nano-components (MPNs) having at least two phases and at least one active ingredient are provided. The MPNs can be used in various methods for medical diagnostics or with pharmaceutical, personal care, oral care, and/or nutritional compositions, for example, in oral care, hair, or skin products. The MPNs can be designed to have targeted delivery within an organism, while providing controlled release systems or combining incompatible active ingredients. Further, the MPNs can be used as biomedical coatings (such as anti-microbial coatings), or anti-corrosive coatings, bioimaging probes with combined diagnostic and therapeutic use, and fragrance release systems, among others. The MPNs can be formed by electrified jetting of polymers.