Flammability Testing Patents (Class 374/8)
  • Patent number: 11579103
    Abstract: Embodiments described herein provide for the flameless premixed combustion of the pyrolysis gases of a milligram-sized sample of solid material in a microscale fire calorimeter (MFC) at high temperatures of combustion and under precisely controlled fuel-to-oxygen ratios. The microscale fire calorimeter (MFC) device and techniques set out herein provide for the generation of fuel gases from solids and the mixing of those fuel gases with oxygen under controlled conditions to obtain precise fuel/oxygen ratios during combustion. Combustion is conducted under flameless, premixed conditions in a rapid test that can generate soot and other products of incomplete combustion, which may then be analyzed to determine their type and nature. This allows for microscale, accurate, and convenient techniques for the generation and determination of the type and nature of combustion species produced over the full range of fire stages from early stage (over-ventilated) fires to late-stage (under-ventilated/high-toxicity) fires.
    Type: Grant
    Filed: April 6, 2020
    Date of Patent: February 14, 2023
    Assignee: The United States of America, as represented by the Administrator of the Federal Aviation Administration
    Inventors: Richard E. Lyon, Louise Speitel, Richard N. Walters
  • Patent number: 11387507
    Abstract: An apparatus and method for initiating thermal runaway in a battery cell are provided. The apparatus and method may be used in safety research of battery cells and packs to initiate thermal runaway. The apparatus comprises a resistive heating element for positioning in thermal contact with the battery cell for transferring heat to a region of the battery cell. An energy source is electrically coupled to the resistive heating element. A switch selectively forms a circuit to send a current pulse through the resistive heating element to generate a power pulse at the resistive heating element to heat the region of the battery cell for initiating thermal runaway. Alternatively, the heating element is heated and held at a predetermined temperature until thermal runaway is initiated. The heat generation rate may be designed to be comparable to that of an internal short circuit within a cell, which is much faster than many existing slow heating methods used to initiate thermal runaway.
    Type: Grant
    Filed: January 18, 2018
    Date of Patent: July 12, 2022
    Assignee: National Research Council of Canada
    Inventors: Steven Recoskie, Dean MacNeil, Giulio Torlone, Oltion Kodra, Joel Perron
  • Patent number: 10520456
    Abstract: Provided is a combustion experiment device, which includes a reaction tube into which a sample fluid flows and to which a temperature gradient in which a temperature rises toward a downstream side is imparted, and a burner part that is configured to flow a combustible gas along and around the reaction tube from the downstream side to an upstream side of the reaction tube and to maintain a flame surrounding the reaction tube from the outside in a radial direction of the reaction tube.
    Type: Grant
    Filed: November 9, 2016
    Date of Patent: December 31, 2019
    Assignees: TOHOKU UNIVERSITY, IHI CORPORATION
    Inventors: Takuya Tezuka, Hisashi Nakamura, Kaoru Maruta, Soichiro Kato, Shintaro Ito
  • Patent number: 8950934
    Abstract: Device for measuring the flash point of liquids and solids includes a measurement chamber (formed by a measurement basin and a lid) and which is provided with means for heating the liquid or the solid in the basin, an electrical igniter having a spark gap, temperature sensors, a pressure measuring apparatus and a press-on device for tightly connecting the measurement basin and the lid. A control device is provided in order to control the heating means, the igniter and the press-on device and to collect the measured values of the temperature sensors and the pressure measuring apparatus. The control device is formed by a computer designed as an embedded system, which is connected to the heating means, the igniter, the press-on device, the temperature sensors and the pressure measuring apparatus by means of an interface device. The measurement chamber and the control device are arranged in a common housing.
    Type: Grant
    Filed: May 10, 2011
    Date of Patent: February 10, 2015
    Assignee: Grabner Instruments Messtechnik GmbH
    Inventors: Nicolas Haas, Klaus Hense
  • Publication number: 20140241394
    Abstract: A rechargeable battery is externally heated to induce thermal runaway, and material expelled from the battery is analyzed.
    Type: Application
    Filed: February 24, 2014
    Publication date: August 28, 2014
    Applicant: The Boeing Company
    Inventor: Nels A. Olson
  • Patent number: 8540421
    Abstract: Systems for analyzing effects of cargo fire on primary aircraft structure are provided. A particular system includes a processor and a memory accessible to the processor. The memory includes instructions executable by the processor to access a thermal profile of a suppressed fire in a physical model of a cargo compartment of an aircraft. The instructions are also executable to analyze heat transfer resulting from applying the thermal profile of the suppressed fire to a structure of the aircraft surrounding the cargo compartment to determine a predicted temperature reached by one or more parts of the structure surrounding the cargo compartment as a result of the suppressed fire. The instructions are also executable to generate an output including the predicted temperature reached by the one or more parts of the structure surrounding the cargo compartment.
    Type: Grant
    Filed: December 18, 2009
    Date of Patent: September 24, 2013
    Assignee: The Boeing Company
    Inventors: Mark F. Ahlers, Mel Eshghi, Daniel F. Lewinski, Richard J. Mazzone
  • Publication number: 20130235898
    Abstract: In a combustion experimental apparatus to obtain the positions of flames formed inside a tube (1), it is possible to adjust a temperature gradient in a longitudinal direction applied to the tube, by including a temperature-adjusting fluid supply device (2) to cause a temperature-adjusting fluid to flow along the tube.
    Type: Application
    Filed: November 18, 2011
    Publication date: September 12, 2013
    Inventors: Kaoru Maruta, Hisashi Nakamura, Soichiro Kato, Naoki Oikawa
  • Patent number: 8480295
    Abstract: The invention relates to a method and a device for testing the fire hazard of a material. According to one embodiment of the method, a plane region of the surface of a specimen made of the material is brought in contact for at most a predetermined contact time with a glow wire, which has been heated to a predetermined temperature. Image data of the specimen are furthermore acquired by at least a first camera at least while the specimen is in contact with the glow wire. Image processing of the acquired image data of the specimen is furthermore carried out, preferably in realtime, ignition of the specimen by the glow wire being detected if applicable. A first duration is then determined, which corresponds to the length of time between the application of the tip of the glow wire on the specimen and the ignition of the specimen.
    Type: Grant
    Filed: December 19, 2008
    Date of Patent: July 9, 2013
    Assignee: UL LLC
    Inventors: Bahman Sarabi, Martin Behrendt
  • Publication number: 20130136150
    Abstract: Device for measuring the flash point of liquids and solids includes a measurement chamber (formed by a measurement basin and a lid) and which is provided with means for heating the liquid or the solid in the basin, an electrical igniter having a spark gap, temperature sensors, a pressure measuring apparatus and a press-on device for tightly connecting the measurement basin and the lid. A control device is provided in order to control the heating means, the igniter and the press-on device and to collect the measured values of the temperature sensors and the pressure measuring apparatus. The control device is formed by a computer designed as an embedded system, which is connected to the heating means, the igniter, the press-on device, the temperature sensors and the pressure measuring apparatus by means of an interface device. The measurement chamber and the control device are arranged in a common housing.
    Type: Application
    Filed: May 10, 2011
    Publication date: May 30, 2013
    Applicant: GRABNER INSTRUMENTS MESSTECHNIK GMBH
    Inventors: Nicolas Haas, Klaus Hense
  • Publication number: 20130128915
    Abstract: A temperature control element for a measuring device for controlling the temperature of a measurement sample, comprising first and second heating elements delivering thermal energy to the measurement sample, and control means for controlling the heating of the measurement sample, wherein the first and second heating elements heat the measurement sample until a limit temperature has been reached, and wherein thermal resistivity between the first and second heating elements is increased starting at the limit temperature, and the control means disconnects the contact between the first and second heating elements when the limit temperature is reached. A cooling element withdraws thermal energy, and the control means controls cooling of the measurement sample, wherein thermal energy is withdrawn from measurement sample by bringing the cooling element closer to the shut-off of the first heating element, and interrupting the contact between the cooling element and the shut-off of the first heating element.
    Type: Application
    Filed: August 3, 2011
    Publication date: May 23, 2013
    Inventors: Roland Aschauer, Ernst Hamann, Philipp Jordan, Andreas Schwarzmann
  • Patent number: 8434935
    Abstract: A heating furnace for testing middle and long span structures including a modular partition structure to adjust an inner volume of the heating furnace, effectively performing a load-coupled heating test of full scale members such as a beam, a short column, a slab, a conjunction frame, and a deck plate. The heating furnace for testing middle and long span structures includes a partition unit formed of a refractory material and partitioning a heating space in a main body to block transfer of heat generated from one space to the other space. A test sample is installed in the heating space of the main body partitioned by the partition unit according to a size of the test sample, and then, heat and a compression force are applied to the test sample to perform a fireproof performance test. The fireproof performance test of structure members having various lengths of 4 m, 6 m and 10 m can be performed, and consumption of various utilities consumed during the test can be optimized.
    Type: Grant
    Filed: November 8, 2010
    Date of Patent: May 7, 2013
    Assignee: Korea Institute of Construction Technology
    Inventors: Heung Youl Kim, Bong Jae Lee, Hyung Jun Kim
  • Patent number: 8292496
    Abstract: In one general aspect, a sample area is energized. A thermal energy status of the sample area is monitored. The thermal energy status including at least one of a radiant energy and a temperature. A thermal signature of a region included in the sample area is determined based on the thermal energy status of the region. The thermal signature is analyzed to determine whether explosive particles are included in the region.
    Type: Grant
    Filed: November 14, 2007
    Date of Patent: October 23, 2012
    Assignee: L-3 Communications CyTerra Corporation
    Inventors: David H. Fine, Edward E. A. Bromberg, Sean C. Christiansen, Steven Bullock, Ravi K. Konduri, Geoffrey Solomon
  • Publication number: 20110228808
    Abstract: A system and method are disclosed for collecting and analyzing the measurements and observations required during flammability testing of materials. The system may include one or more input devices for electronically providing one or more timing signals related to a timing sequence of a specified flammability test and one or more attribute signals related to selected attributes of a test specimen. Additionally, a timing device may be coupled to the one or more input devices. The timing device may be configured to perform one or more time interval measurements based on the one or more timing signals. Further, a computing device may be coupled to the timing device. The computing device may be configured to analyze the one or more time interval measurements and the one or more attribute signals to determine a flammability classification for the test specimen in accordance with the specified flammability test.
    Type: Application
    Filed: March 19, 2010
    Publication date: September 22, 2011
    Applicant: TICONA LLC
    Inventors: Frank Ayotte, Wendy Sterling, Elizabeth Kelly
  • Patent number: 7862227
    Abstract: An apparatus (A) for testing an associated construction material sample includes a housing (20) having an internal chamber (22) divided by a wall portion (30) into first and second portions (24, 26). A support in the housing is dimensioned to mount an associated construction material sample therein. A first burner (60) communicates with first portion of the housing for supplying a flame thereto. A second burner (80) communicates with the second portion of the housing for preheating the first portion. The testing method of an associated construction material sample includes installing the sample in the housing, preheating the housing, introducing a flame toward the sample, monitoring the flame as combustion progresses longitudinally along the sample, and recording data regarding the flame progression.
    Type: Grant
    Filed: March 28, 2008
    Date of Patent: January 4, 2011
    Inventors: Richard A. West, Michael R. Rosecrans
  • Publication number: 20100164125
    Abstract: A method of evaluating the flame retardancy of a sealing resin comprises a step of fusion cutting a heating element by causing the heating element to generate heat by the passage of electric current to a test sample of a molded body of the sealing resin including the heating element therein; a step of igniting the sealing resin by continuing the passage of electric current even after the heating element is fusion-cut; and a step of measuring voltage and/or current applied in a period from when the heating element is fusion-cut to the ignition of the sealing resin. The test sample is used in the method of evaluating the flame retardancy and provided with a heating wire; conducting terminals made of metal having an electric resistance lower than the heating wire and connected to both ends of the heating wire; and a sealing resin layer covering the outer periphery of the heating wire.
    Type: Application
    Filed: December 17, 2009
    Publication date: July 1, 2010
    Applicant: KABUSHIKI KAISHA TOSHIBA
    Inventors: Kizashi Tanioka, Masanori Okamoto, Akiko Suda
  • Publication number: 20100098131
    Abstract: Systems for analyzing effects of cargo fire on primary aircraft structure are provided. A particular system includes a processor and a memory accessible to the processor. The memory includes instructions executable by the processor to access a thermal profile of a suppressed fire in a physical model of a cargo compartment of an aircraft. The instructions are also executable to analyze heat transfer resulting from applying the thermal profile of the suppressed fire to a structure of the aircraft surrounding the cargo compartment to determine a predicted temperature reached by one or more parts of the structure surrounding the cargo compartment as a result of the suppressed fire. The instructions are also executable to generate an output including the predicted temperature reached by the one or more parts of the structure surrounding the cargo compartment.
    Type: Application
    Filed: December 18, 2009
    Publication date: April 22, 2010
    Applicant: The Boeing Company
    Inventors: Mark F. Ahlers, Mel Eshghi, Daniel F. Lewinski, Richard J. Mazzone
  • Patent number: 7690837
    Abstract: Embodiments provide systems and methods for analyzing effects of cargo fire on primary aircraft structure. A thermal profile of a suppressed fire in a cargo compartment of an aircraft is developed. The thermal profile is applied to a heat transfer model of structure of an aircraft, and structural integrity of the modeled structure is analyzed. The thermal profile may be developed by introducing a fire in a physical model of a cargo compartment instrumented with temperature sensors and determining profiles of temperature versus time. A heat transfer model of aircraft structure is built, boundary conditions are input into the heat transfer model, and the model is run. When analysis of the modeled structure determined structural integrity to be insufficient to satisfy flight certification requirements, structural parameters are modified, the thermal profile is applied to a heat transfer model of the modified structure, and the analysis is repeated.
    Type: Grant
    Filed: March 7, 2006
    Date of Patent: April 6, 2010
    Assignee: The Boeing Company
    Inventors: Mark F. Ahlers, Mel Eshghi, Daniel F. Lewinski, Richard J. Mazzone
  • Patent number: 7671717
    Abstract: The present invention relates to an unrecoverable line-type temperature sensitive detector having short-circuit fault alarm function, comprises a detecting cable comprising at least two detecting conductors disposed in parallel and a fusible insulation layer, a resistor, and a resistance signal measuring device, wherein the detecting cable further comprises a semiconductor layer, and wherein the semiconductor layer and the fusible insulation layer are disposed between the detecting conductors so as to space the detecting conductors apart. The detector of the present invention may distinguish short-circuit fault from short circuit caused by fire, and thus overcome the disadvantage of not distinguishing short-circuit fault from short-circuit due to fire in the conventional detector. Therefore, the problem of lack of short-circuit fault alarm function in the prior art is resolved. Accordingly, the present invention improves the reliability of unrecoverable line-type temperature sensitive detector.
    Type: Grant
    Filed: September 13, 2007
    Date of Patent: March 2, 2010
    Assignee: Sureland Industrial Fire Safety Limited
    Inventors: Weishe Zhang, Gangjin Li
  • Patent number: 7645069
    Abstract: A method of detecting energetic materials, such as explosives, includes energizing a sample area that contains particles of energetic materials. In the method, temperature characteristics from the sample area are monitored, and a temperature released from exothermic decomposition of the particles is detected. The method further includes analyzing the detected temperature to determine the presence of the exothermic compound which caused the decomposition.
    Type: Grant
    Filed: July 27, 2006
    Date of Patent: January 12, 2010
    Assignee: L-3 Communications Cyterra Corporation
    Inventors: David H. Fine, Herbert Duvoisin, III, Edward E. A. Bromberg, Steven Bullock, David P. Lieb, C. Andrew Helm, Sean C. Christiansen, Eric Moy
  • Patent number: 7632012
    Abstract: A method for measuring the differential emissivity between two sites on the surface of a body and the temperature of the two sites. The method includes a plurality of measurements of the infrared radiation arising from each of the two sites under a number of different conditions. Some of the measurements include irradiation by external infrared radiation at a known wavelength and intensity. The infrared radiation arising from each of the sites may include emitted radiation, reflected ambient radiation, and reflected external radiation. Additionally, the temperature determined using the method described can be used to calibrate infrared imaging devices used to inspect the entire body.
    Type: Grant
    Filed: September 1, 2005
    Date of Patent: December 15, 2009
    Assignee: Siemens Energy, Inc.
    Inventor: Michael Twerdochlib
  • Patent number: 7570042
    Abstract: The present invention relates to a method for evaluating the effect of an electric discharge on an aircraft structure through the evaluation of the damage caused by the effect of the thermal heating generated by the mentioned discharge on the structure, including the steps of: applying an electric discharge on the material of the aircraft structure using an intensity generator; distributing in an electric mesh with resistive electric elements the material of the aircraft structure; calculating the intensities running through the electric mesh of the material of the aircraft structure from the intensity introduced in the generators; calculating with the previous intensities the heat which is dissipated in each of the elements of the electric mesh of the material of the aircraft structure; calculating the distribution of temperatures in each of the elements of the electric mesh of the material of the aircraft structure; determining the elements of the electric mesh of the material of the aircraft structure whic
    Type: Grant
    Filed: May 30, 2007
    Date of Patent: August 4, 2009
    Assignee: Airbus Espana, S.L.
    Inventors: Valentín García Martínez, José Ignacio López-Reina Torrijos, Raúl Fernández Recio
  • Publication number: 20090168833
    Abstract: The invention relates to a method and a device for testing the fire hazard of a material. According to one embodiment of the method, a plane region of the surface of a specimen made of the material is brought in contact for at most a predetermined contact time with a glow wire, which has been heated to a predetermined temperature. Image data of the specimen are furthermore acquired by at least a first camera at least while the specimen is in contact with the glow wire. Image processing of the acquired image data of the specimen is furthermore carried out, preferably in realtime, ignition of the specimen by the glow wire being detected if applicable. A first duration is then determined, which corresponds to the length of time between the application of the tip of the glow wire on the specimen and the ignition of the specimen.
    Type: Application
    Filed: December 19, 2008
    Publication date: July 2, 2009
    Applicants: BAYER MATERIAL SCIENCE AG
    Inventors: Bahman SARABI, MARTIN BEHRENDT
  • Patent number: 7438467
    Abstract: An assembly and method for testing the fire performance of sheet piling sections which includes: a first wall formed from sheet piling sections; a second wall substantially parallel to the first wall; a base plate; and a pair of end sections extending between the opposing ends of the two walls. The first and second walls and the end sections are attached to, and extend upwardly from, the base plate to form a cavity, which can be filled with materials. The assembly also includes two top sections, which are attached to the first and second walls and joined together by at least one connector. The sheet piling sections of the first wall are exposed to a heat source to certify compliance with fire codes and regulations.
    Type: Grant
    Filed: October 4, 2006
    Date of Patent: October 21, 2008
    Assignee: Skyline Steel, LLC
    Inventor: David Borger
  • Publication number: 20080084910
    Abstract: An assembly and method for testing the fire performance of sheet piling sections which includes: a first wall formed from sheet piling sections; a second wall substantially parallel to the first wall; a base plate; and a pair of end sections extending between the opposing ends of the two walls. The first and second walls and the end sections are attached to, and extend upwardly from, the base plate to form a cavity, which can be filled with materials. The assembly also includes a two top sections, which are attached to the first and second and joined together by at least one connector. The sheet piling sections of the first wall are exposed to a heat source to certify compliance with fire codes and regulations.
    Type: Application
    Filed: October 4, 2006
    Publication date: April 10, 2008
    Inventor: David Borger
  • Patent number: 7329043
    Abstract: An apparatus for testing properties of a product comprising a thermal barrier layer comprises an ignition source, a test stand that extends a sample of the product over the ignition source, and a means for measuring thermal transfer across the sample. The apparatus may further comprise a means for measuring thermal transfer across each layer of the sample. A method for testing properties of a product comprising a thermal barrier layer comprises supporting a sample of the product over an ignition source, heating the sample via the ignition source, and determining a thermal differential across the sample. The method may further comprise determining a thermal differential across each layer of the sample.
    Type: Grant
    Filed: November 4, 2004
    Date of Patent: February 12, 2008
    Assignee: L&P Property Management Company
    Inventors: Steven E. Ogle, Kenneth C. Thompson, D. Patrick Steagall, James Eric DeBord
  • Patent number: 6991365
    Abstract: A flammability test apparatus comprises a chamber, an inlet, an ignition source, a heater, and pressure and temperature sensors. In one embodiment, the chamber includes a horizontally-oriented, cylindrically-shaped section. The inlet allows a fluid to be introduced into the chamber. The ignition source ignites the fluid within the chamber, and the heater adjusts the temperature of the fluid within the chamber. The test apparatus includes a sparger for dispersing the fluid within the chamber, and the sparger disposed within the chamber and attached to the inlet. The test apparatus also includes a relief system for exhausting the chamber after the pressure of the fluid in the chamber exceeds a preset pressure.
    Type: Grant
    Filed: May 17, 2002
    Date of Patent: January 31, 2006
    Assignee: Baker Engineering and Risk Consultants, Inc.
    Inventor: Adrian Pierorazio
  • Patent number: 6536943
    Abstract: Methods and apparatus for testing flammability properties of cellular plastics are described. Heat is applied to the underside of a heat-conductive plate on which is placed a specimen of the cellular plastic. A plurality of spaced-apart heat sensing devices are positioned below the specimen and in direct or close contact with the plate, one such heat sensing device being centrally positioned relative to the plate and serving as the setpoint sensor. A plurality of spaced-apart heat sensing devices are also disposed above the specimen and in direct or close contact with the top surface of the specimen, one such heat sensing device being centrally positioned relative to the top of the specimen. The sensing devices are adapted to provide signals convertible into information regarding the temperatures at their respective locations.
    Type: Grant
    Filed: October 17, 2001
    Date of Patent: March 25, 2003
    Assignee: Albemarle Corporation
    Inventor: Elbert F. Feske
  • Patent number: 6471507
    Abstract: The WSL Gas Igniter is, in essence, a small, reuasable gas bomb intended to be used in the testing of fire suppression systems. The device has two main parts. The main parts are the control box and the igniter head. The control box controls all aspects of operation. It controls the flow of all gases, as well as, the electrically powered ignition system. The igniter head contains an accumulation/combustion chamber in which a combustible mixture of gases is introduced. Also, the combustion chamber contains a small spark generating means. A control signal initiates a spark system and the flow of gases into the combustion chamber simultaneously. At the desired moment of ignition, the control signal is removed, which ceases the gas flow and ignites the combustible mixture of gases in the combustion chamber. The explosion produced by the invention is intended to ignite a test subject for the purpose of testing fire suppression capability.
    Type: Grant
    Filed: November 2, 1999
    Date of Patent: October 29, 2002
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: David Eugene Hall
  • Patent number: 6377348
    Abstract: A smoke chamber for determining the amount of visible smoke emitted by a foundry core/mold resin system is composed of an elongate chamber having a proximal end, a distal end, and sides. The chamber is fitted with air inlet at its proximal end, a smoke outlet at its distal end, and a sample station disposed between the air inlet and the smoke outlet. The sample station includes a sample holder and furnace for heating a sample placed in the sample holder. The chamber also includes a light assembly disposed along one side of the chamber from the sample station to the smoke outlet. A light detection assembly is disposed on a chamber side opposite the light assembly for detecting light emitted from the light assembly. The chamber also includes fan for drawing smoke from a heated sample placed in the sample holder to the smoke outlet. The corresponding method for determining the amount of visible smoke emitted by a foundry core/mold resin system includes placing a sample in the sample holder.
    Type: Grant
    Filed: August 7, 2000
    Date of Patent: April 23, 2002
    Assignee: Ashland, Inc.
    Inventor: James Thurston Schneider
  • Patent number: 6312155
    Abstract: An apparatus for assessing burn injury to underlying tissue from a flammable material. The apparatus includes an artificial human tissue and a plurality of temperature sensors located at predetermined locations in the artificial human tissue to measure temperature of the artificial human tissue during a flammability test. The apparatus further includes a heat sink device for simulating the heat sink properties of a human body. The apparatus further includes a heat exchange tank for maintaining the artificial human tissue at a regulated temperature, the heat exchange tank being filled with a fluid. The apparatus further includes a heat exchanger for exchanging heat with the fluid in the heat exchange tank. The apparatus further includes a water supply device for supplying water to the interior of the heat exchanger. The apparatus also includes a data acquisition system attached to the plurality of temperature sensors for recording the temperature of the artificial human tissue.
    Type: Grant
    Filed: October 7, 1999
    Date of Patent: November 6, 2001
    Assignee: Risk Analysis & Management
    Inventors: Daniel Stool, Merrill Zavod, Scott Milkovich, Eugene D. Rider
  • Patent number: 5932796
    Abstract: An apparatus for determining the flashpoint of a substance, including a test cup adapted to contain the substance, a heating element which heats the substance, a tube and a needle valve which produce a calibrated flame, a temperature sensor which measures the temperature of the substance, and an optical detector, having at least one optical fiber, which detects variations in the light intensity from the flame, or from the ignited vapor emitted by the substance.
    Type: Grant
    Filed: October 1, 1997
    Date of Patent: August 3, 1999
    Assignee: Elf Antar France
    Inventors: Didier Arthaud, Alain Piquemal, Frederic Tort
  • Patent number: 5869343
    Abstract: The invention describes a method and an apparatus for the automated testing of the flash point and can be used for determining the flash point of flammable liquids. In particular, the inventive method makes is possible to automate the phase of preparing and changing the samples. The apparatus described is characterized in that the whole of the test equipment (1) consists of a stationary simultaneous function head (2) and a mobile test insert (3), which can be separated completely from the simultaneous function head (2), the test insert (3), pre-installed, having the temperature sensor (4) and the flash point indicator (5) and contacting elements (6) for producing the electrical connection to the temperature sensor (4) and to the flash point indicator (5) and at least one coupling element (10) for producing the mechanical connection between a stirrer driving mechanism (7) and the stirrer (8) being disposed at the simultaneous function head (2).
    Type: Grant
    Filed: February 27, 1997
    Date of Patent: February 9, 1999
    Assignee: Petrotest Instruments GmbH & Co. KG
    Inventors: Bernhard Handschuck, Helmut Eilers
  • Patent number: 5182940
    Abstract: Apparatus is provided for continually monitoring the flash point temperature of a liquid pertoleum product flowing through a pipeline. The apparatus is located adjacent the pipeline for periodically drawing product samples therefrom and for testing the samples to determine the respective flash point temperatures. The apparatus includes a microprocessor, which is programmed to control the operation of the apparatus, a testing chamber and a Wheatstone bridge circuit for measuring the Lower Explosive Limit (LEL) of a combustible gas-air mixture which is drawn through the testing chamber. The gas-air mixture ignites on the surface of an active resistive filament, thereby increasing its temperature and resistance, which causes a current to flow within the magnitude bridge circuit. The magnitude of the current is directly proportional to the change of resistance of the active filament and the LEL of the vapor-air mixture.
    Type: Grant
    Filed: October 17, 1991
    Date of Patent: February 2, 1993
    Assignee: Automated Pipeline Instruments Incorporated
    Inventors: Kenneth M. Bailey, Rex L. Mitchener, Timothy J. Wehking, Craig P. Reith
  • Patent number: 5176449
    Abstract: The present invention is related to a device and method for determining the flash point of a liquid or solid material to be tested by measuring the pressure obtained in the measuring chamber after an ignition. According to the invention, a liquid or solid is placed into a measuring vessel and the measuring vessel is heated. The measuring vessel is tightly closed with a cover. At a given temperature the generated vapor-air-mixture is ignited and the pressure increase occurring due to the temperature increase is taken as a measure for the size of the flame for determining the flash point. The pressure increase is preferably measured with a piezoresistive pressure transducer. The temperature of the heated cover is measured with the temperature sensor and the sample temperature with the temperature sensor.
    Type: Grant
    Filed: November 20, 1991
    Date of Patent: January 5, 1993
    Inventor: Werner Grabner
  • Patent number: 5110214
    Abstract: An apparatus and method for determining the propensity of a polymer to emit smoke by measuring the smoke emitted when the polymer is melted and extruded. The polymer is heated to a molten state and extruded under controlled time conditions into a receptacle from which gaseous samples can be collected, then the gaseous samples from the receptacle are analyzed for smoke content to determine the propensity of the polymer to emit smoke.
    Type: Grant
    Filed: July 9, 1990
    Date of Patent: May 5, 1992
    Assignee: Phillips Petroleum Company
    Inventors: David R. Battiste, Kenneth W. Willcox, Tommy J. Morgan
  • Patent number: 5052817
    Abstract: An apparatus for testing ignitability of an initiator includes a body having a central cavity, initiator holder for holding the initiator over the central cavity of the body, an ignition material holder disposed in the central cavity of the body and having a cavity facing the initiator holder which receives a measured quantity of ignition material to be ignited by the initiator and a chamber in communication with the cavity of the ignition material and the central cavity of the body, and a measuring system for analyzing pressure characteristics generated by ignition of the ignition material by the initiator. The measuring system includes at least one transducer coupled to an oscillograph for recording pressure traces generated by ignition.
    Type: Grant
    Filed: October 4, 1990
    Date of Patent: October 1, 1991
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Laurence J. Bement, James W. Bailey, Morry L. Schimmel
  • Patent number: 4990312
    Abstract: In the preferred embodiment of the promoted combustion chamber disclosed herein, a thick-walled tubular body that is capable of withstanding extreme pressures is arranged with removable upper and lower end closures to provide access to the chamber defined within the body. A bracket is arranged in the chamber for dependently supporting a test sample of a material being evaluated in the chamber. To facilitate the real-time analysis of a test sample, several pressure-tight viewing ports capable of withstanding the simulated environmental conditions are arranged in the walls of the tubular body for observing the test sample during the course of a test. A replaceable heat-resistant tubular member and replaceable flame-resistant internal liners are arranged to be fitted inside of the chamber for protecting the interior wall surfaces of the combustion chamber during the evaluation tests.
    Type: Grant
    Filed: July 18, 1989
    Date of Patent: February 5, 1991
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Michelle A. Rucker, Joel M. Stoltzfus
  • Patent number: 4831559
    Abstract: Apparatus for automatically monitoring the flash point of a liquid passing through a conduit which includes a closed equilibrator vessel into which a sample stream of the liquid is confined and volatile vapors therefrom are allowed to saturate air introduced into the vessel, and a combustible gas sensor for measuring the percent lower flammable limit of the resulting gas mixture. The system further includes suitable computing means for automatically calculating the Tag closed cup flash point of the sample liquid based on the temperature of the liquid and on the measured percent lower flammable limit, and controlling the operation of the apparatus. A method of determining the flash point of such a liquid is also disclosed.
    Type: Grant
    Filed: July 25, 1986
    Date of Patent: May 16, 1989
    Assignee: Phillips Petroleum Company
    Inventor: Neil C. Miller
  • Patent number: 4809190
    Abstract: A calorimetry systems for the continuous measurement of the heating value of coal, which provides heating value data used to control coal-fired furnaces. The system has apparatus for pulverizing the coal, a gravimetric feeder for providing pulverized coal at a measured mass feed rate, an initiating self-sustained combustion of the coal therein without the need for further supporting fuel gases. Instrumentation measures the flow rates of the cooling air, primary and secondary combustion air as well as the mass flow rates of the coal into the combustor. A computer is provided which is responsive to the measuring instruments (thermocouples and pressure gauges) for controlling the feeding of the coal and fuel gases during initiation of combustion and for computing the heating value of the coal. The computer has a memory with storage for specific heat values of the constituents of the products of combustion of various ranks of coal (bituminous, subbituminous, lignite, etc.
    Type: Grant
    Filed: April 8, 1987
    Date of Patent: February 28, 1989
    Assignee: General Signal Corporation
    Inventors: John C. Homer, Shahriar Nowshiravani, Steven L. Ross, Gilbert F. Lutz
  • Patent number: 4671674
    Abstract: The present invention relates to a process for the detection and recording of the weak points or defects on hot semifinished iron and steel industry products, by application of the flame of an oxygen-supplied blowtorch to the surface to be examined, displacing the application point along the surface, picking up the image of the application point by video camera, and transmitting the image to a remote location. An observer viewing this screen can make a map of the surface examined, recording thereon the weak points or defects detected both by their dimensions and by their type. This process finds application in the hot treatment of the slabs, blooms, and steel rods, when the casting, defect repair and rolling operations are to be carried out continuously.
    Type: Grant
    Filed: December 20, 1985
    Date of Patent: June 9, 1987
    Assignee: Somafer
    Inventor: Michel Detronde
  • Patent number: 4637735
    Abstract: A bench-scale apparatus for measuring the heat-release rate of pyrolysis vapors of a material sample includes an oven having a heated chamber for receiving the sample, a flue and at least one entry port, a radiometer having a radiation sensor disposed in relation to the flue of the oven such that an area into which burning pyrolysis vapors are directed from the flue is adjacent to the radiation sensor, a fuel-gas control valve in communication with the entry port of the oven, and an electronic flow meter for measuring the amount of fuel-gas passing through the control valve, wherein signals from the radiometer operate the fuel-gas control valve to provide an amount of fuel-gas sufficient to maintain a flame of the vapors at a predetermined height, and wherein the meter measures the amount of fuel-gas such that the measurement of the meter is used to indicate the heat-release rate of the pyrolysis vapors.
    Type: Grant
    Filed: January 27, 1986
    Date of Patent: January 20, 1987
    Assignee: Factory-Mutual Research Corporation
    Inventors: John de Ris, George H. Markstein
  • Patent number: 4561784
    Abstract: Test apparatus for determining ignition characteristics of various metal in oxidizer environments simulating operating conditions for materials, the test apparatus has a chamber (6) through which the oxidizing agent flows, and means for mounting a stationary test sample (36) therein, a powered, rotating shaft (E) in the chamber rigidly mounts a second test sample (35). The shaft is axially movable to bring the samples into frictional engagement and heated to the ignition point. Instrumentation 16, 32, 48, 49, 50, 51, 52, 53, 54 connected to the apparatus provides for observation of temperatures, pressures, loads on and speeds of the rotating shaft, and torques whereby components of stressed oxygen systems can be selected which will avoid accidental fires under working conditions.
    Type: Grant
    Filed: January 17, 1984
    Date of Patent: December 31, 1985
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Frank J. Benz, Randall C. Shaw, David S. Dixon
  • Patent number: 4551092
    Abstract: Decontaminating an object such as a vehicle, is achieved by subjecting the bject to an elevated temperature for a time sufficient to achieve the desired temperature. The heat source is preferably a jet engine which is supported for universal movement. The temperature of the surface of the object under treatment is determined by sensing the infrared radiation emanating from the surface of the object. In response to the attainment of a predetermined level of infrared radiation, an electric control member is used to regulate the movement of said heat source. Thus heating is caused to be directed at selected regions of the object under treatment for the time period necessary to attain the desired temperature level.
    Type: Grant
    Filed: November 14, 1983
    Date of Patent: November 5, 1985
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventor: William M. Sayler
  • Patent number: 4549815
    Abstract: Ignition delay of distillate fuels is measured by heating a block to an elevated temperature and injecting samples into a cavity in the block as it cools. The time between each injection and ignition of the fuel is measured. This measurement of ignition delay is used to determine the cetane number of the distillate fuel.
    Type: Grant
    Filed: November 21, 1983
    Date of Patent: October 29, 1985
    Assignee: Mobil Oil Corporation
    Inventors: Chaya Venkat, Dennis E. Walsh
  • Patent number: 4519716
    Abstract: A device which simulates the burning of an elongated smoking product such as a cigarette, for testing the combustability of an article. The device includes a rod-shaped resistive heating element, the length and cross section of which are the same as those of the product whose burning characteristics are to be simulated. The heating element may be divided into a plurality of longitudinally aligned heat insulated segments. A plurality of lead wires are successively spaced along the length of the heating element so as to respectively uniformly heat the respective portions of the heating element between the adjacent lead wires when an electric current is applied separately thereto. Circuitry is provided for applying an electric current to successively adjacent portions of the heating element through the lead wires for predetermined periods of time, beginning at one end of the heating element and ending at the other, thereby simulating the burning of a cigarette.
    Type: Grant
    Filed: April 9, 1984
    Date of Patent: May 28, 1985
    Inventor: Shigeru Suga
  • Patent number: 4333333
    Abstract: An apparatus is provided for determining the burning and/or glowing rate of a smokable article. The apparatus comprises a sensor for sensing the incandescent zone of the smokable article and a drive apparatus for moving the sensor along a path parallel to the direction of burning and glowing of the smokable article.
    Type: Grant
    Filed: November 24, 1980
    Date of Patent: June 8, 1982
    Assignee: B.A.T. Cigaretten-Fabriken GmbH
    Inventor: Dirk Pangritz
  • Patent number: H441
    Abstract: The hot spall tester comprises a tube furnace portion adapted for retaining a magazine portion for containment of a plurality of steel ball bearings which are heated and individually dropped through a feed tube member to a programmed or manually operated carrousel portion having a plurality of sample cups for receiving and containing individual solid propellant samples to be spall tested in accordance with the method. A torque rod is employed to facilitate rotation of the magazine portion and carrousel portion in a vertically aligned relationship with the magazine portion so that the heated steel ball is delivered by gravity through a feed tube to a sample cup of the carrousel portion positioned below the magazine portion. In operation the magazine portion and carrousel portion are aligned and vertically positioned to provide a calculated transit time for the steel ball bearing to drop by gravity to the propellant in the sample cup. Subsequent rotation of the carrousel of about 22.
    Type: Grant
    Filed: September 4, 1987
    Date of Patent: March 1, 1988
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Robert W. Milton, Lawrence B. Thorn