Mechanical Blending Patents (Class 419/32)
  • Publication number: 20130011293
    Abstract: The present invention provides a producing method of a rare earth sintered magnet which is suitable as a producing method of a high performance rare earth sintered magnet which can reduce the number of steps for reusing defective molded bodies generated in a wet molding step of the rare earth sintered magnet, and which has a small content amount of oxygen. The invention also provides a slurry recycling method used for the producing method, and a slurry recycling apparatus. Each of the methods includes a crushing step of crushing, in mineral oil and/or synthetic fluid, a molded body in which slurry formed from alloy powder for a rare earth sintered magnet and mineral oil and/or synthetic fluid is wet molded in magnetic field, and recycling the crushed molded body into slurry.
    Type: Application
    Filed: March 28, 2011
    Publication date: January 10, 2013
    Applicant: HITACHI METALS, LTD.
    Inventor: Mitsuaki Mochizuki
  • Patent number: 8329093
    Abstract: A method for preparing metal-matrix composites including cold-process isostatic compaction of previously mixed powders and hot-process uniaxial pressing of the resulting compact is disclosed. The method enables metal-matrix composites with improved properties to be obtained. A device for implementing isostatic compaction comprising a latex sheath into which the mixture of powders is poured, a perforated cylindrical container in which the latex sheath is arranged, and means for sealed insulation of the mixture of powders contained in the sheath is also disclosed.
    Type: Grant
    Filed: March 14, 2006
    Date of Patent: December 11, 2012
    Assignee: Forges de Bologne
    Inventor: Jacques Tschofen
  • Patent number: 8318082
    Abstract: A composition containing: about 45 to about 75 volume % of cubic boron nitride (CBN), where the CBN has finer and coarser particles having two different average particle sizes, the range of the average particle size of the finer particles being about 0.1 to about 2 ?m, the range of the average particle size of the coarser particles being about 0.3 to about 5 ?m, the ratio of the content of the coarser CBN particles to the finer CBN particles being 50:50 to 90:10; a secondary hard phase containing a nitride or carbonitride of a Group 4, 5 or 6 transition metal or a mixture or solid solution thereof, and a binder phase.
    Type: Grant
    Filed: October 28, 2005
    Date of Patent: November 27, 2012
    Assignee: Element Six Abrasives S.A.
    Inventors: Nedret Can, Stig Ake Andersin
  • Patent number: 8287804
    Abstract: In the method for recovering a metal from a target that contains a metal and a metal oxide, the target contains a sintered body of the metal oxide after being heated under a condition of melting the metal without melting or decomposing the metal oxide. The target is heated in an upper crucible of a two-level crucible that includes the upper crucible with a through hole-formed in a bottom surface thereof, and a lower crucible disposed below the through hole, the size of the through hole being set such that it does not allow the sintered body of the metal oxide contained in the target to pass therethrough, and the melted metal is caused to flow into the lower crucible, so that the metal is separated from the metal oxide.
    Type: Grant
    Filed: December 8, 2009
    Date of Patent: October 16, 2012
    Assignee: Tanaka Holdings Co., Ltd
    Inventors: Toshiya Yamamoto, Takanobu Miyashita, Kiyoshi Higuchi, Yasuyuki Goto
  • Publication number: 20120212119
    Abstract: An electrode material may be used in spark plugs and other ignition devices including industrial plugs, aviation igniters, glow plugs, or any other device that is used to ignite an air/fuel mixture in an engine. In one embodiment, the electrode material has one or both of iridium (Ir) or ruthenium (Ru), and has rhenium (Re).
    Type: Application
    Filed: February 22, 2012
    Publication date: August 23, 2012
    Applicant: FEDERAL-MOGUL IGNITION COMPANY
    Inventor: Shuwei Ma
  • Publication number: 20120207640
    Abstract: High strength aluminum alloys and methods for producing them. The alloys consist essentially of about 9.0 to 10.3 wt. % zinc, about 2.5 to 3.5 wt. % magnesium, about 1.5 to 3.0 wt. % copper and less than about 0.05 wt. % of any other alloying constituent. The balance consists of aluminum. These alloys are compatible with ceramic reinforcements used in metal matrix composites.
    Type: Application
    Filed: February 14, 2011
    Publication date: August 16, 2012
    Applicant: Gamma Technology, LLC
    Inventor: William C. Harrigan, JR.
  • Patent number: 8182739
    Abstract: A concentric-circular-gradient functional material for biogenic use is produced using first, second, third and forth cylindrical partitions, and a cylindrical dice which are concentrically stood on a supporting stand. Ti powder (A) fills the first cylindrical partition. A first mixed powder including Ti powder (A) and biogenic material powder (B) fills between the first and second cylindrical partitions. A second mixed powder including a smaller amount of Ti powder (A) than the first mixed powder fills between the second and third cylindrical partitions. A third mixed powder including a smaller amount of Ti powder (A) than the second mixed powder fills between the third and fourth cylindrical partitions. The biogenic material powder (B) fills between the fourth cylindrical partition and the dice. The first to fourth partitions are pulled out. The dice is capped using a punch. The powders are sintered using a discharge plasma sintering machine.
    Type: Grant
    Filed: June 13, 2008
    Date of Patent: May 22, 2012
    Assignee: Nihon University
    Inventors: Michiharu Okano, Hiroshi Izui
  • Patent number: 8119203
    Abstract: A method of treating a substrate by applying a layer of at least one metal to the substrate to form an applied metal layer on the substrate and followed by curing of the applied metal layer at sub-atmospheric pressure to form a metal protective layer. A method of treating a substrate by applying a layer of at least one metal to a substrate of an unassembled component of a reactor system to form an applied metal layer on the substrate of the unassembled component and curing the applied metal layer on the substrate of the unassembled component to form a metal protective layer. A method of treating a substrate by applying a layer of at least one metal to the substrate to form an applied metal layer, curing the applied metal layer at a first temperature and pressure for a first period of time, and curing the applied metal layer at a second temperature and pressure for a second period of time, wherein the curing forms a metal protective layer.
    Type: Grant
    Filed: May 30, 2006
    Date of Patent: February 21, 2012
    Assignee: Chevron Phillips Chemical Company LP
    Inventors: Robert L. Hise, Geoffrey E. Scanlon, Joseph Bergmeister, III, Daniel B. Knorr
  • Patent number: 8083831
    Abstract: The present invention relates to a lightweight, anti-scratch and fracture resistant material for use in manufacture of jewelry prepared by sintering a powered mixture consisting essentially of 20% by weight of titanium carbide, 25% by weight of tungsten carbide, 35% by weight of titanium nitride, and balance being a binder consisting essentially of nickel, molybdenum and cobalt.
    Type: Grant
    Filed: March 4, 2010
    Date of Patent: December 27, 2011
    Assignee: BTR Limited
    Inventor: Zhijian Xia
  • Patent number: 8075661
    Abstract: An ultra-hard composite material and a method for manufacturing the same, including mixing a metal carbide powder and a multi-element high-entropy alloy powder to form a mixture, green compacting the mixture, and sintering the mixture to form the ultra-hard composite material. The described multi-element high-entropy alloy consists of five to eleven principal elements, with every principal element occupying a 5 to 35 molar percentage of the alloy.
    Type: Grant
    Filed: April 25, 2008
    Date of Patent: December 13, 2011
    Assignee: Industrial Technology Research Institute
    Inventors: Chi-San Chen, Chih-Chao Yang, Jien-Wei Yeh, Chin-Te Huang
  • Publication number: 20110284792
    Abstract: The present invention features a steel-base sintering alloy having a high wear-resistance for a valve seat of an engine. In preferred embodiments, the steel-base sintering alloy may include a chief element of Ferrum (Fe); and a powder-alloy which are composed of Carbon (C) of 0.6˜1.2 wt %, Nickel (Ni) of 1.0˜3.0 wt %, Cobalt (Co) of 15.0˜25.0 wt %, Chrome (Cr) of 3.0˜9.0 wt %, Molybdenum (Mo) of 8.0˜15.0 wt %, Tungsten (W) of 1.0˜4.0 wt %, Manganese (Mn) of 0.5˜2.0 wt %, and Calcium (Ca) of 0.1˜0.5 wt %.
    Type: Application
    Filed: October 18, 2010
    Publication date: November 24, 2011
    Applicants: KOREA SINTERED METAL CO., LTD., HYUNDAI MOTOR COMPANY
    Inventors: Jong Myung Kim, Ki Bum Kim, Dong Jin Kang, Hyung Oh Ban, Hong Kil Baek, Won-Seog Koo, Jong-Kwan Park, Sung-Tae Choi
  • Patent number: 8025710
    Abstract: Provided are an ancillary material, used for shape processing, which is capable of shortening a processing time, avoiding a reduction in quality of a shape provided to a workpiece material, and allowing a relatively low manufacturing cost; a processing method using the ancillary material; and a method of manufacturing the ancillary material. The tungsten alloy grains (1) comprise: tungsten of greater than or equal to 80% by mass and less than or equal to 98% by mass; nickel; at least one kind of metal selected from the group consisting of iron, copper, and cobalt; and an inevitable impurity, a maximum diameter thereof is greater than or equal to 0.1 mm and less than or equal to 5.00 mm, and a specific surface area thereof is less than or equal to 0.02 m2/g. The tungsten alloy grains (1, 10), the workpiece material (30), an abrasive (20) are blended in a container (100) and the container is rotated, thereby processing the shape of the workpiece material (30).
    Type: Grant
    Filed: November 20, 2006
    Date of Patent: September 27, 2011
    Assignee: A.L.M.T. Corp.
    Inventors: Shinji Kikuhara, Hitoshi Inoue, Noboru Uenishi, Satoshi Umemoto
  • Patent number: 7993577
    Abstract: The invention relates to manufacture of titanium articles from sintered powders. The cost-effective initial powder: 10-50 wt % of titanium powder having ?500 microns in particle size manufactured from underseparated titanium sponge comprising ?2 wt % of chlorine and ?2 wt % of magnesium; 10-90 wt % of a mixture of two hydrogenated powders A and B containing different amount of hydrogen; 0-90 wt % of standard grade refined titanium powder, and/or 5-50 wt % of alloying metal powders. The method includes: mixing powders, compacting the blend to density at least 60% of the theoretical density, crushing titanium hydride powders into fine fragments at pressure of 400-960 MPa, chemical cleaning and refining titanium powders by heating to 300-900° C. and holding for ?30 minutes, heating in vacuum at 1000-1350° C., holding for ?30 minutes, and cooling.
    Type: Grant
    Filed: June 11, 2007
    Date of Patent: August 9, 2011
    Assignee: Advance Materials Products, Inc.
    Inventors: Volodymyr A. Duz, Orest M. Ivasishin, Vladimir S. Moxson, Dmitro G. Savvakin, Vladislav V. Telin
  • Patent number: 7976775
    Abstract: Disclosed is a binary aluminum alloy powder sintered material which comprises aluminum and iron, which has a completely crystalline microstructure comprising an aluminum matrix and an ?-Al phase and at least any one phase of an Al6Fe phase or an Al13Fe4 phase mixed in the aluminum matrix as nanocrystalline phases, and which has an extremely high strength and a well-balanced high ductility, though being free from any rare earth element.
    Type: Grant
    Filed: March 25, 2008
    Date of Patent: July 12, 2011
    Assignee: National Institute for Materials Science
    Inventors: Taisuke Sasaki, Kazuhiro Hono, Toshiji Mukai
  • Publication number: 20110103994
    Abstract: A method of forming a metal alloy from a powder composition comprising first particles in a range of approximately 20-90% by weight of the powder composition, the remainder of the powder composition comprising approximately 95% by weight of second particles and 5% by weight of third particles, wherein the method includes the step of using rapid thermal processing (RTP) to sinter the powder composition.
    Type: Application
    Filed: August 9, 2010
    Publication date: May 5, 2011
    Applicant: Automotive Parts and Accessory Systems R&D Centre Limited
    Inventors: June-Sang SIAK, Chan Hung Shek, Chi Yuen Chung, Wai-Lam Ralph Ip, Tik Lam Cheung
  • Publication number: 20110064600
    Abstract: A composite is produced by the steps of (a) blending a first mixture of metallic powders; (b) compacting the blended first mixture of metallic powders to a plurality of discretely shaped articles; (c) blending a second mixture of metallic powders; (d) mixing the plurality of discretely shaped articles with the blended second mixture of metallic powders to form a precursor blend; (e) compacting the precursor blend; and (f) sintering the precursor blend. The composite has a metallic matrix with embedded shapes dispersed throughout the matrix where the embedded shapes have an incipient liquid phase sintering temperature less than an incipient liquid phase sintering temperature of the matrix.
    Type: Application
    Filed: November 23, 2010
    Publication date: March 17, 2011
    Applicant: Aerojet-General Corporation
    Inventors: Timothy J. Brent, Michael T. Stawovy
  • Publication number: 20110052440
    Abstract: Dehydration and drying of a silicon alloy argil which uses water as a principal binder are carried out by a freeze-drying process, a microwave irradiation process, or a combination thereof. In the freeze-drying process, the shaped compact is put into a cooling medium within 5 minutes after completion of shape forming, retained therein for at least 5 minutes to quick-freeze water within the compact while the water is still in a finely-dispersed condition. The compact is exposed to a pressure below the triple point pressure of water. In the microwave irradiation process, the shaped compact is put into a container exposed to continuous microwave irradiation at 2.450 GHz for at least 5 minutes while under a reduced pressure below atmospheric pressure.
    Type: Application
    Filed: August 30, 2010
    Publication date: March 3, 2011
    Applicant: ISMAN J CORPORATION
    Inventors: TOSHIYUKI WATANABE, MASAFUMI MATSUSHITA, TOSHITAKA SAKURAI, KAZUYA SATO, YOKO MATSUSHITA, TAKAYOSHI MISAKI, SETSUKO SHINDO, AYUMI SHINDO, YUMIKO KUBOTA, AKIKO MATSUSHITA, KUNIO SAITO, TAKUMI SHITARA, FUTOSHI YANAGINO, TAKASHI YOSHIDA, TAKASHI MIZUSHIMA, OSAMU MATSUZONO, KOUKI SHIMIZU
  • Patent number: 7892314
    Abstract: The present invention provides powder metal compositions and methods of making and using the same. Powder metal compositions according to the invention include base metal particles, a lubricant that transforms from a solid phase material to a viscous, liquid phase material during pressing, and a micronized deformable solid material. The micronized deformable solid material fills at least a portion of the void space between the base metal particles during pressing, which allows at least a portion of the lubricant to migrate as a viscous liquid phase material to the interface between the surface of the green compact and the wall of the mold cavity to provide lubrication that reduces the ejection force necessary to remove the green compact from the mold cavity.
    Type: Grant
    Filed: August 26, 2005
    Date of Patent: February 22, 2011
    Assignee: Apex Advanced Technologies, LLC
    Inventor: Dennis L Hammond
  • Patent number: 7867438
    Abstract: A method of manufacturing a powdered composition or starting material used in producing a CBN compact which comprises CBN, a secondary hard phase and a binder phase includes two steps of attrition milling. First, the attrition milling of the secondary hard phase and the binder phase. Second, adding CBN particles to the fine particle mixture of the first attrition milling and then attrition milling this mixture.
    Type: Grant
    Filed: October 28, 2005
    Date of Patent: January 11, 2011
    Inventors: Nedret Can, Stig Ake Andersin, Robert Fries, Iain Patrick Goudemond
  • Publication number: 20110002804
    Abstract: The present invention includes consolidated hard materials, methods for producing them, and industrial drilling and cutting applications for them. A consolidated hard material may be produced using hard particles such as B4C or carbides or borides of W, Ti, Mo, Nb, V, Hf, Ta, Zr, and Cr in combination with an iron-based, nickel-based, nickel and iron-based, iron and cobalt-based, aluminum-based, copper-based, magnesium-based, or titanium-based alloy for a binder material. Commercially pure elements such as aluminum, copper, magnesium, titanium, iron, or nickel may also be used for the binder material. The mixture of the hard particles and the binder material may be consolidated at a temperature below the liquidus temperature of the binder material using a technique such as rapid omnidirectional compaction (ROC), the CERACON™ process, or hot isostatic pressing (HIP). After sintering, the consolidated hard material may be treated to alter its material properties.
    Type: Application
    Filed: September 13, 2010
    Publication date: January 6, 2011
    Applicant: BAKER HUGHES INCORPORATED
    Inventors: Jimmy W. Eason, James C. Westhoff, Roy Carl Lueth
  • Publication number: 20110001594
    Abstract: A magnetic article comprises, in total, elements in amounts capable of providing at least one (La1-aMa) (Fe1-b-cTbYc)13-dXe phase and less than 0.5 Vol % impurities, wherein 0?a?0.9, 0?b?0.2, 0.05?c?0.2, ?1?d?+1, 0?e?3, M is one or more of the elements Ce, Pr and Nd, T is one or more of the elements Co, Ni, Mn and Cr, Y is one or more of the elements Si, Al, As, Ga, Ge, Sn and Sb and X is one or more of the elements H, B, C, N, Li and Be. The magnetic article comprises a permanent magnet.
    Type: Application
    Filed: September 30, 2009
    Publication date: January 6, 2011
    Applicant: Vacuumschmelze GmbH & Co. KG
    Inventors: Matthias Katter, Joachim Gerster, Ottmar Roth
  • Patent number: 7863221
    Abstract: For producing the superconducting material MgB2, a shapeable master alloy containing Mg and B, as well as at least one additional constituent, an LiMgB alloy is.1 The process permits the production of shaped elements of MgB2, for example by forging, casting, drawing, etc.
    Type: Grant
    Filed: March 4, 2002
    Date of Patent: January 4, 2011
    Assignee: Eidenossische Technische Hochschule Zurich
    Inventors: Juan Matias Reinoso, Frank Ottinger, Michael Woerle, Reinhard Nesper
  • Publication number: 20100330386
    Abstract: A brazing product includes a compacted solid and rigid material formed of a brazing flux and a filler metal as a mixture, which has mechanical strength sufficient to make it extrudable under a press with a flux mass proportion from 3 to 20%. The invention also provides a method for manufacturing a brazing product by mixing particles of filler metal and brazing powder in order to form metal particles coated with the flux, and compacting filler metal particles coated with the brazing flux.
    Type: Application
    Filed: November 16, 2009
    Publication date: December 30, 2010
    Applicant: FP SOUDAGE
    Inventors: Philippe Schmitt, Boris Bosi
  • Publication number: 20100310406
    Abstract: The present invention provides a method for producing a powder mixture for powder metallurgy, which allows production of a green compact having both high density and high lubricity (low demolding force). The method, according to the present invention, for producing a powder mixture for powder metallurgy including an iron-base powder, a mechanical characteristic-improving powder and a lubricant, the method includes the steps of: mixing the iron-base powder and/or the mechanical characteristic-improving powder with an amide-based lubricant solution; removing a solvent in the solution; and coating the surface of the iron-base powder and/or the mechanical characteristic-improving powder with an amide-based lubricant.
    Type: Application
    Filed: May 24, 2010
    Publication date: December 9, 2010
    Inventors: Takayasu Fujiura, Yoshihiro Ito
  • Publication number: 20100278682
    Abstract: Disclosed is a binary aluminum alloy powder sintered material which comprises aluminum and iron, which has a completely crystalline microstructure comprising an aluminum matrix and an ?-Al phase and at least any one phase of an Al6Fe phase or an Al13Fe4 phase mixed in the aluminum matrix as nanocrystalline phases, and which has an extremely high strength and a well-balanced high ductility, though being free from any rare earth element.
    Type: Application
    Filed: March 25, 2008
    Publication date: November 4, 2010
    Inventors: Taisuke Sasaki, Kazuhiro Hono, Toshiji Mukai
  • Publication number: 20100247367
    Abstract: A method of producing a rare-earth magnet containing a rare-earth compound having a first rare-earth element and a second rare-earth element different from the first rare-earth element includes: a mixing step of mixing rare-earth compound powder including the first rare-earth element and subjected to a process based on hydrogenation disproportionation desorption recombination with a diffusion material including the second rare-earth element; a molding step of molding the mixed powder into a compact in a magnetic field; and a heating step of heating the compact to diffuse the second rare-earth element into the rare-earth compound powder.
    Type: Application
    Filed: March 29, 2010
    Publication date: September 30, 2010
    Applicant: TDK Corporation
    Inventors: Hideki Nakamura, Noaki Mori, Hirofumi Nakano, Kouji Tanabe
  • Publication number: 20100233014
    Abstract: A powder metallurgical combination is provided comprising an iron-based powder A comprising core particles of iron to which core particles nickel is diffusion alloyed and wherein said nickel diffusion alloyed to said core particles comprises 4-7% (preferably 4.5-6%) by weight of said iron-based powder A, and a powder B substantially consisting of particles of pure iron. Further a method is provided for preparing a powder metallurgical combination.
    Type: Application
    Filed: July 10, 2008
    Publication date: September 16, 2010
    Applicant: HOGANAS AB (PUBL)
    Inventor: Mats Larsson
  • Publication number: 20100206724
    Abstract: Provided is a method of producing a sintered compact including the steps of mixing raw material powders respectively composed of a chalcogenide element and a Vb group element or raw material powders of an alloy of two or more elements including a chalcogenide element and a Vb group element, and hot pressing the mixed powder under conditions that satisfy the following formula: P(pressure)?{Pf/(Tf?T0)}×(T?T0)+P0(Pf: final pressure, Tf: final temperature, P0: atmospheric pressure, T: heating temperature, T0: room temperature, and temperatures in Celsius). This method is able to produce a high-density, high-strength and large-diameter sintered compact containing a chalcogenide element (A) and a Vb group element (B) or containing the element (A) and (B) and additionally a IVb group element (C) and/or an additive element (D) which is free from cracks even when it is assembled and used as a sputtering target-backing plate assembly.
    Type: Application
    Filed: July 17, 2008
    Publication date: August 19, 2010
    Applicant: NIPPON MINING AND METALS CO., LTD.
    Inventor: Hideyuki Takahashi
  • Patent number: 7771649
    Abstract: Disclosed herein is a method of producing an ultrafine crystalline TiN/TiB2 composite cermet. In the method, titanium nitride (TiN)/titanium boride (TiB2)/stainless steel composite nanopowder is produced through a reaction milling process using titanium (Ti), boron nitride (BN), and stainless steel powders as raw material powders, and the resulting composite nanopowder is liquid-phase sintered. The method comprises a first step of mixing titanium powder and boron nitride powder at a molar ratio of 3:2, a second step of mixing 5-60 wt % stainless steel powder and the powder mixture, a third step of feeding the powder mixture along with a ball having a predetermined diameter into a jar and conducting a high energy ball milling process to produce titanium nitride/titanium boride/stainless steel composite nanopowder, and a fourth step of shaping and sintering the resulting composite nanopowder.
    Type: Grant
    Filed: November 19, 2007
    Date of Patent: August 10, 2010
    Assignee: Korea Institute of Science and Technology
    Inventors: Jae Hyeok Shim, Ji Woo Kim, Young Whan Cho
  • Publication number: 20100170463
    Abstract: A powder metal rocker arm is provided. The rocker arm may be connected to a cylinder head of an engine to assist in transferring motion between engine components. The rocker arm includes a pivot aperture formed therein to facilitate pivoting of the rocker arm with respect to the cylinder head. The rocker arm is formed of a metal alloy powder. The metal alloy powder is compacted to form an intermediate member. Secondary features, such as apertures and other weight reducing features may be formed in the intermediate member. The intermediate member is then sintered to form the rocker arm.
    Type: Application
    Filed: November 9, 2009
    Publication date: July 8, 2010
    Inventor: Jose Correa Neto
  • Patent number: 7749429
    Abstract: A ceramic particle group dispersed in a solvent in a state of primary particles of single crystal, a method for production thereof and a use thereof are disclosed. In one embodiment a method is disclosed for producing a sintered particle (ceramic particle) group of hydroxyapatite (HAp), which includes a step of subjecting a system wherein calcium carbonate is present between primary particles of hydroxyapatite (HAp) to sintering and then dissolving calcium carbonate with water to remove calcium carbonate. A hydroxyapatite (HAp) sintered particle group produced by the above method is a nanometer size particle group having a particle diameter of about 70 to about 120 nm, and is a particle group having a uniform particle diameter (coefficient of variation: 12%), and further 96% of the particle group is dispersed as a single crystal particle.
    Type: Grant
    Filed: September 13, 2005
    Date of Patent: July 6, 2010
    Assignee: Japan Science and Technology Agency
    Inventors: Tsutomu Furuzono, Masahiro Okada
  • Patent number: 7713468
    Abstract: Method of producing a sintered body comprising the steps of mixing one or more powders forming hard constituents with powders forming a binder phase comprising cobalt powder where the cobalt powder comprises cobalt having mainly a fcc-structure defined as the peak height ratio between the Co-fcc(200)/Co-hcp(101) being greater than or equal to about 3/2, as measured between the baseline and maximum peak height, measured by XRD with a 2?/? focusing geometry and Cu-K? radiation. The present invention also relates to a ready-to-press powder comprising cobalt having mainly a fcc-structure and where the cobalt powder has a grain size (FSSS) of from about 0.2 to about 2.9 ?m. The present invention also relates to sintered bodies made according to the method. The sintered bodied according to the present invention have reduced porosity and less crack formation.
    Type: Grant
    Filed: November 19, 2007
    Date of Patent: May 11, 2010
    Assignee: Sandvik Intellectual Property AB
    Inventors: Jeanette Persson, Leif Dahl, Gerold Weinl, Ulf Rolander
  • Patent number: 7666247
    Abstract: A method for spherically granulating and agglomerating metal particles such as tantalum and/or niobium powders is described in the present invention, which includes the steps of: a). comminuting the metal particles to form fine particles having D50 less than 50 ?m; b). granulating the comminuted metal particles comprising volatile liquid, for example, tantalum and/or niobium particles comprising volatile liquid, to form wet spherical particles; c). still drying the wet spherical particles and removing volatile liquid to form flowable pre-agglomerated particles with increased bulk density; d). heat treating the pre-agglomerated particles; e). screening the heat treated powder to obtain the flowable agglomerated particles. The present invention provides a flowable spherical agglomerated metal particles, and especially tantalum and/or niobium particles having improved properties. The present agglomerated tantalum powder have a flow rate of at least about 2.0 g/sec, a BET surface area of from about 0.
    Type: Grant
    Filed: February 17, 2006
    Date of Patent: February 23, 2010
    Assignee: Ningxia Orient Tantalum Industry Co., Ltd.
    Inventors: Jilin He, Luntao Pan, Aiguo Zheng, Yuewei Cheng, Yuezhong Ma, Hongdong Liu, Guoqi Yang, Chunxiang Wang, Yanping Wang, Shiping Zheng
  • Publication number: 20100034688
    Abstract: There is provided a method of manufacturing a permanent magnet having extremely high orientation by arranging such that the crystal fractures of alloy raw meal powder having more equal crystal orientational relationship are combined in magnetic field. In this invention, alloy raw meal powder is filled into a cavity and, while agitating the alloy raw meal powder inside the cavity, is oriented in the magnetic field. This oriented body is then compression molded in the magnetic field into a predetermined shape.
    Type: Application
    Filed: November 19, 2007
    Publication date: February 11, 2010
    Inventors: Hiroshi Nagata, Yoshinori Shingaki
  • Publication number: 20100026432
    Abstract: There is provided a method of manufacturing a permanent magnet which has an extremely high coercive force and high magnetic properties is manufactured at high productivity There are executed: a first step of causing at least one of Dy and Tb to adhere to at least part of a surface of iron-boron-rare-earth based sintered magnet; and a second step of diffusing, through heat-treatment at a predetermined temperature, at least one of Dy and Tb adhered to the surface of the sintered magnet into grain boundary phase of the sintered magnet.
    Type: Application
    Filed: December 19, 2007
    Publication date: February 4, 2010
    Inventors: Hiroshi Nagata, Kyuzo Nakamura, Takeo Katou, Atsushi Nakatsuka, Ichirou Mukae, Masami Itou, Ryou Yoshiizumi, Yoshinori Shingaki
  • Publication number: 20100028194
    Abstract: A method for protecting powder metallurgy alloy elements from oxidation and/or hydrolyzation during sintering. The method includes (1) coating the admixed alloy elements in an inert (e.g., nitrogen) atmosphere with a hydrophobic lubricant that is capable of becoming mobile during pressing, the amount of lubricant being at least 45% of the total volume of all components to be added to the base metal powder; (2) mixing the lubricant-coated admixed alloy elements with the base metal powder to form a mixture; (3) pressing the mixture to form a pre-sintered part having a green density that is from about 95% to about 98% of a calculated pore-free density; and (4) sintering the part.
    Type: Application
    Filed: August 4, 2009
    Publication date: February 4, 2010
    Applicant: APEX ADVANCED TECHNOLOGIES, LLC
    Inventors: Dennis L. Hammond, Richard Phillips
  • Patent number: 7622072
    Abstract: Methodology for constructing composite particles from ingredients comprising two or more particulate components. The resultant particles are usefully incorporated into powder coating compositions. The approach also finds utility in other applications, including but not limited to the food, drug, and cosmetics industry. Fluidized particles are subjected to an intense, but relatively brief heating event. This causes associated particles to fusingly assemble into fused composite clusters.
    Type: Grant
    Filed: January 12, 2006
    Date of Patent: November 24, 2009
    Assignee: Valspar Sourcing, Inc.
    Inventors: Walter J. Blatter, James A. Heck, Lowell G. Lindquist
  • Publication number: 20090274403
    Abstract: Disclosed is a composition for a bush-type bearing, a bush-type bearing manufactured using the composition, and a method of manufacturing the bush-type bearing. The bearing has excellent friction characteristics with a shaft made of iron (Fe) based material, and thus is able to increase the lubrication cycle of a lubricant. Further, the bearing has excellent hardness, and thus is able to prevent plastic deformation under high contact pressure.
    Type: Application
    Filed: November 20, 2007
    Publication date: November 5, 2009
    Applicant: DOOSAN INFRACORE CO., LTD.
    Inventors: Dong-Seob Shim, Chung-Rea Lee
  • Publication number: 20090252637
    Abstract: The present invention discloses a process for sintering particles using a sintering aid. The sintering aid can be brought into contact with a plurality of particles to be sintered such that a mixture of the particles and the sintering aid is provided. The mixture of particles and the sintering aid is heated and at least part of the sintering aid is vaporized. Sintering of the particles to form a sintered component followed by cooling of the sintered component can complete the process, or in the alternative, a subsequent heating step or steps can be included whereby additional vaporization of the sintering aid can occur.
    Type: Application
    Filed: March 24, 2009
    Publication date: October 8, 2009
    Applicant: Energy & Environmental Research Center Foundation
    Inventors: John Hurley, Carsten Heide
  • Publication number: 20090238712
    Abstract: A sputter target material which is of a sintered material, wherein the sputter target material consists of 0.5 to 50 atomic % in total of at least one metal element (M) selected from the group of Ti, Zr, V, Nb and Cr, and the balance of Mo and unavoidable impurities, and has a microstructure seen at a perpendicular cross section to a sputtering surface, in which microstructure oxide particles exist near a boundary of each island of the metal element (M), and wherein the maximum area of the island, which is defined by connecting the oxide particles with linear lines so as to form a closed zone, is not more than 1.0 mm2.
    Type: Application
    Filed: June 5, 2009
    Publication date: September 24, 2009
    Applicant: HITACHI METALS, LTD.
    Inventors: Keisuke Inoue, Tsuyoshi Fukui, Shigeru Taniguchi, Norio Uemura, Katsunori Iwasaki, Kazuya Saitoh
  • Publication number: 20090226340
    Abstract: A method of making a degradable alloy includes adding one or more alloying products to an aluminum or aluminum alloy melt; dissolving the alloying products in the aluminum or aluminum alloy melt, thereby forming a degradable alloy melt; and solidifying the degradable alloy melt to form the degradable alloy. A method for manufacturing a product made of a degradable alloy includes adding one or more alloying products to an aluminum or aluminum alloy melt in a mould; dissolving the one or more alloying products in the aluminum or aluminum alloy melt to form a degradable alloy melt; and solidifying the degradable alloy melt to form the product. A method for manufacturing a product made of a degradable alloy includes placing powders of a base metal or a base alloy and powders of one or more alloying products in a mould; and pressing and sintering the powders to form the product.
    Type: Application
    Filed: February 24, 2009
    Publication date: September 10, 2009
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventor: Manuel Marya
  • Patent number: 7524355
    Abstract: A method is disclosed for producing an energetic metastable nano-composite material. Under pre-selected milling conditions a mixture of powdered components are reactively milled. These components will spontaneously react at a known duration of the pre-selected milling conditions. The milling is stopped at a time at which the components have been compositionally homogenized to produce nanocomposite powder, but prior to said known duration, and thereby before the spontaneous reaction occurs. The milled powder is recovered as a highly reactive nanostructured composite for subsequent use by controllably initiating destabilization thereof.
    Type: Grant
    Filed: November 12, 2004
    Date of Patent: April 28, 2009
    Assignee: New Jersey Institute of Technology
    Inventors: Edward Leonid Dreizin, Mirko Schoenitz
  • Publication number: 20090068055
    Abstract: A powder metallurgy method of making a chromium base alloy includes blending a first powder comprising a chromium powder and a second powder comprising at least one of titanium, titanium hydride, zirconium or zirconium hydride, annealing the first powder and the second powder in a reducing atmosphere after the step of mixing, compacting a blend of the first and the second powders, and sintering the compacted blend to form a chromium base alloy. The chromium alloy may be used as an interconnect for a solid oxide fuel cell, and includes least one of iron or nickel greater than zero and equal to or less than 7 weight percent, yttria greater than zero and equal to or less than 2 weight percent, at least one of titanium or zirconium greater than zero and equal to or less than 1 weight percent and at least 90 weight percent chromium.
    Type: Application
    Filed: September 7, 2007
    Publication date: March 12, 2009
    Inventors: Sudhakara Sarma Sreedhara, Ranganathan Sundaresan
  • Patent number: 7470393
    Abstract: Methods of fabricating cermet materials and methods of utilizing the same such as in filtering particulate and gaseous pollutants from internal combustion engines having intermetallic and ceramic phases. The cermet material may be made from a transition metal aluminide phase and an alumina phase. The mixture may be pressed to form a green compact body and then heated in a nitrogen-containing atmosphere so as to melt aluminum particles and form the cermet. Filler materials may be added to increase the porosity or tailor the catalytic properties of the cermet material. Additionally, the cermet material may be reinforced with fibers or screens. The cermet material may also be formed so as to pass an electrical current therethrough to heat the material during use.
    Type: Grant
    Filed: February 25, 2005
    Date of Patent: December 30, 2008
    Assignee: Battelle Energy Alliance, LLC
    Inventor: Peter C. Kong
  • Publication number: 20080310989
    Abstract: A method for preparing metal-matrix composites including cold-process isostatic compaction of previously mixed powders and hot-process uniaxial pressing of the resulting compact disclosed. The method enables metal-matrix composites with improved properties to be obtained. A device for implementing isostatic compaction comprising a latex sheath into which mixture of powders is poured, a perforated cylindrical container in which the latex sheath is arranged, and means for sealed insulation of the mixture of powders contained in the sheath is also disclosed.
    Type: Application
    Filed: March 14, 2006
    Publication date: December 18, 2008
    Applicant: FORGES DE BOLOGNE
    Inventor: Jacques Tschofen
  • Patent number: 7449144
    Abstract: A process for manufacturing a sliding contact piece for medium to high current densities including a step of warm premixing of graphite and plastic binder, a step of cold mixing of the resulting premixture with copper, a step of pressing of the resulting main mixture into the sliding contact piece, and finally a step of sintering of it; and so as to improve the operating characteristics of the sliding contact piece, which is free of any environmentally harmful additives, a metal such as zinc, tin, bismuth or an alloy of such metals is added during the premixing of the graphite and plastic binder.
    Type: Grant
    Filed: January 17, 2003
    Date of Patent: November 11, 2008
    Assignee: Deutsche Carbone AG
    Inventors: Wilhelm Latz, Jürgen Spangenberg, Arwed Uecker
  • Publication number: 20080274003
    Abstract: An electrical contact comprising a matrix of an alloy of a high electro-conductive metal and a low melting point metal and particles of a refractory metal dispersed in the matrix. The electrical contact comprises the alloy containing a low melting point metal of at least one of Sn, Te and Be, and the refractory metal is Cr. The alloy comprising the low melting point metal in an amount of 0.5 to 3% by weight and the balance being Cu.
    Type: Application
    Filed: June 25, 2008
    Publication date: November 6, 2008
    Inventors: Shigeru Kikuchi, Masato Kobayashi, Kenji Tsuchiya, Noboru Baba
  • Publication number: 20080260565
    Abstract: A concentric-circular-gradient functional material for biogenic use is produced using first, second, third and forth cylindrical partitions, and a cylindrical dice which are concentrically stood on a supporting stand. Ti powder (A) fills the first cylindrical partition. A first mixed powder including Ti powder (A) and biogenic material powder (B) fills between the first and second cylindrical partitions. A second mixed powder including a smaller amount of Ti powder (A) than the first mixed powder fills between the second and third cylindrical partitions. A third mixed powder including a smaller amount of Ti powder (A) than the second mixed powder fills between the third and fourth cylindrical partitions. The biogenic material powder (B) fills between the fourth cylindrical partition and the dice. The first to fourth partitions are pulled out. The dice is capped using a punch. The powders are sintered using a discharge plasma sintering machine.
    Type: Application
    Filed: June 13, 2008
    Publication date: October 23, 2008
    Applicant: NIHON UNIVERSITY
    Inventors: Michiharu Okano, Hiroshi Izui
  • Publication number: 20080241570
    Abstract: A method of fabricating a medical implant component. The method may comprise producing a substrate from a first material in which the substrate has a bearing portion, and causing particles of a second material to be formed onto at least the bearing portion of the substrate. The second material may be formed from a biocompatible material and a carbide source, in which the carbide source is 6.17% or more of the second material by weight. The particles of the second material may be formed onto at least the bearing portion of the substrate by a predetermined spraying technique, a CVD process, a PVD process, or a carburization process. The biocompatible material may be cobalt chrome and the carbide source may be graphite.
    Type: Application
    Filed: March 26, 2007
    Publication date: October 2, 2008
    Applicant: Howmedica Osteonics Corp.
    Inventors: Daniel E. Lawrynowicz, Aiguo Wang, Zongtao Zhang
  • Patent number: 7422720
    Abstract: High density, nontoxic projectiles and other articles, and their methods of manufacture, are disclosed. More particularly, high density nontoxic W—Cu—Ni—Fe alloy compositions, methods of their manufacture and methods by which they may be used as projectiles such as shots, bullets, and pellets and other products traditionally made of lead alloys will be detailed herein in some embodiments. These products have a density comparable to that of lead while avoiding problems of toxicity associated with the use of lead.
    Type: Grant
    Filed: May 10, 2005
    Date of Patent: September 9, 2008
    Assignee: Spherical Precision, Inc.
    Inventors: Tim T. Wei, Luguang Tian