Includes A Chemical Reaction Patents (Class 419/63)
  • Patent number: 9905907
    Abstract: The housing includes a base and an antenna coating layer. The base includes a first surface. The base is made of one of glass and ceramic. The antenna coating layer is formed on the first surface. The antenna coating layer is made of metal power. The metal power is selected from one of copper power, copper alloy power, or copper and nickel mixed power.
    Type: Grant
    Filed: September 1, 2015
    Date of Patent: February 27, 2018
    Assignees: SHENZHEN FUTAIHONG PRECISION INDUSTRY CO., LTD., FIH (HONG KONG) LIMITED
    Inventors: Yu-Tsai Wang, Jing-Hai Zheng
  • Publication number: 20150118095
    Abstract: A method of manufacturing a ferrous alloy article is disclosed and includes the steps of melting a ferrous alloy composition into a liquid, atomizing and solidifying of the liquid into powder particles, outgassing to remove oxygen from the surface of the powder particles, and consolidating the powder particles into a monolithic article.
    Type: Application
    Filed: May 20, 2014
    Publication date: April 30, 2015
    Applicant: CRS HOLDINGS INC.
    Inventors: David E. Wert, Timothy R. Armstrong, David A. Helmick, Michael L. Schmidt
  • Publication number: 20140377121
    Abstract: A component, such as a SOFC interconnect, and methods of making the component are provided using various chromium powders, including powder particles with a chromium core covered with an iron shell, a pre-alloyed Cr—Fe powder or a chromium powder produced by hydrogen reduction with hydrogen.
    Type: Application
    Filed: September 11, 2014
    Publication date: December 25, 2014
    Inventors: Martin Janousek, Shivanand I. Majagi
  • Publication number: 20140334963
    Abstract: A titanium metal or a titanium alloy having submicron titanium boride substantially uniformly dispersed therein and a method of making same is disclosed. Ti power of Ti alloy powder has dispersed within the particles forming the powder titanium boride which is other than whisker-shaped or spherical substantially uniformly dispersed therein.
    Type: Application
    Filed: July 28, 2014
    Publication date: November 13, 2014
    Applicant: Cristal Metals Inc.
    Inventors: Lance Jacobsen, Adam Benish
  • Patent number: 8709335
    Abstract: A method of making a sputtering target includes providing a backing structure, and forming a copper indium gallium sputtering target material on the backing structure by cold spraying. The step of cold spraying includes spraying a powder comprising copper, indium and gallium in a process gas stream, and at least one of an average particle size of the powder is at least 35 ?m, a velocity of the process gas stream is at least 150 m/s, or a process gas pressure is 20 bar or less.
    Type: Grant
    Filed: October 19, 2010
    Date of Patent: April 29, 2014
    Assignee: Hanergy Holding Group Ltd.
    Inventors: Johannes Vlcek, Daniel R. Juliano
  • Publication number: 20140106144
    Abstract: The method for forming a 3-D metal object by 3-D printing or injection molding comprising providing as a feed material metal particles formed by establishing multiple metal components in a primary billet of a ductile material, working the primary billet through a series of reduction steps to form the components into elongated elements, leaching the ductile material from the elongated elements and reducing the length to short uniform lengths.
    Type: Application
    Filed: August 8, 2013
    Publication date: April 17, 2014
    Applicant: COMPOSITE MATERIALS TECHNOLOGY, INC.
    Inventor: James Wong
  • Publication number: 20130315773
    Abstract: The invention relates to energy-saving manufacturing of purified hydrogenated titanium powders or alloying titanium hydride powders, by metallo-thermic reduction of titanium chlorides, including their hydrogenation, vacuum separation of titanium hydride sponge block from magnesium and magnesium chlorides, followed by crushing, grinding, and sintering of said block without need for hydrometallurgical treatment of the produced powders. Methods disclosed contain embodiments of processes for manufacturing high-purity powders and their use in manufacturing near-net shape titanium and titanium-alloy articles by sintering titanium hydride and alloyed titanium hydride powders produced from combined hydrogen-magnesium reduction of titanium chlorides, halides and hydrides of other metals.
    Type: Application
    Filed: May 24, 2012
    Publication date: November 28, 2013
    Applicant: Advance Materials Products, Inc. (ADMA Products, Inc.)
    Inventors: Vladimir S. Moxson, Volodymyr A. Duz, Andrey G. Klevtsov, Viktor D. Sukhoplyuyev, Mihajlo D. Sopka, Yury V. Shuvalov, Mykhailo Matviychuk
  • Publication number: 20130236349
    Abstract: The invention provides an industrial method for producing dispersion-strengthened iron-based materials at low cost and in large-scale. The industrial acid pickling waste solution is treated by spray roasting process after yttrium chloride is added. During the spray roasting process, the solution is atomized into fine droplets, the droplets are contacted with gas and dried into powders, which are heated in air to form metal oxides. The mixed powders of the metal oxides are reduced in hydrogen stream to obtain yttria dispersion-strengthened iron powders. High performance dispersion-strengthened iron materials are obtained by densifying the yttria dispersion-strengthened iron powders. The method has simple process and low cost, and is suitable for large-scale production due to the direct use of acid pickling waste solution from steel factory.
    Type: Application
    Filed: June 30, 2011
    Publication date: September 12, 2013
    Applicant: UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJING
    Inventors: Zhimeng Guo, Weiwei Yang, Ji Luo, Huiqin Cao, Cunguang Chen
  • Publication number: 20120282130
    Abstract: A carbothermic reduction method is provided for reducing a rare earth element-containing oxide including at least one of neodymium (Nd) and praseodymium (Pr) and possibly other rare earth elements (La, Ce, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Sc, and Y) as alloying agents in the presence of carbon and a source of a reactant element including one or more of silicon, germanium, tin, lead, arsenic, antimony and bismuth to form a rare earth element-containing intermediate alloy as a master alloy for making permanent magnet material. The process is a more efficient, lower cost and environmentally friendly technology than current methods of manufacturing rare earth metals. The intermediate material is useful as a master alloy for making a permanent magnet material comprising at least one of neodymium and praseodymium, and possibly other rare earth metals as alloying additives.
    Type: Application
    Filed: April 18, 2012
    Publication date: November 8, 2012
    Inventors: Karl A. Gschneidner, JR., Frederick A. Schmidt, Ralph W. McCallum
  • Publication number: 20120263619
    Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.
    Type: Application
    Filed: June 15, 2012
    Publication date: October 18, 2012
    Applicant: GENERAL ELECTRIC COMPANY
    Inventors: Andrew Philip WOODFIELD, Eric Allen OTT, Clifford Earl SHAMBLEN, Michael Francis Xavier GIGLIOTTI
  • Publication number: 20120237769
    Abstract: The present invention provides a powder for a magnet which can form a rare earth magnet having excellent magnetic characteristics and which has excellent moldability, a method for producing the powder for a magnet, a powder compact, and a rare earth-iron-boron-based alloy material. Magnetic particles constituting a powder for a magnet each include a structure in which a particle of a phase 3 of a hydrogen compound of a rare earth element is dispersed in a phase 2 of an iron-containing material. Since the phase 2 of the iron-containing material is uniformly present in each of the magnetic particles 1, the powder has excellent moldability and easily increases the density of a powder compact 4.
    Type: Application
    Filed: April 13, 2011
    Publication date: September 20, 2012
    Applicant: Sumitomo Electric Industries, Ltd.
    Inventors: Toru Maeda, Asako Watanabe
  • Publication number: 20110162550
    Abstract: In making frangible objects, including lead-free bullets and other projectiles, powdered metal primary and powdered ceramic secondary phases are mixed and densified at an elevated temperature such that the ceramic phase forms a brittle network. Any combination of metal and ceramic phases may be used to achieve desired chemical and physical properties. Any appropriate mixing, forming, and/or thermal processing methods and equipment may be used. Degrees of frangibility, strength, and toughness can be adjusted to suit a given application by precursor selection, degree of mixing, relative amounts of metal and ceramic phases, forming method, and thermal and mechanical processing parameters.
    Type: Application
    Filed: January 6, 2010
    Publication date: July 7, 2011
    Inventors: Mark C. Hash, James Trent Pearson
  • Patent number: 7833472
    Abstract: An article is prepared by furnishing a plurality of powder particle substrates made of a substrate metal, providing a nonmetallic precursor of a metallic coating material, wherein the metallic coating material comprises an alloying element that is thermophysically melt incompatible with the substrate metal, contacting the powder particle substrates with the nonmetallic precursor, chemically reducing the nonmetallic precursor to form coated powder particles comprising the powder particle substrates having a surface-enriched layer of the metallic coating material thereon without melting the powder particle substrates, and processing the coated powder particles to form the article, without melting the powder particle substrates.
    Type: Grant
    Filed: June 1, 2005
    Date of Patent: November 16, 2010
    Assignee: General Electric Company
    Inventors: Eric Allen Ott, Andrew Philip Woodfield, David Paul Mourer, John Frederick Ackerman, Jon Raymond Groh, Robert Edward Schafrik, Kenneth Rees Bain, Michael Francis Xavier Gigliotti, Matthew Bernard Buczek
  • Publication number: 20100222212
    Abstract: A process and apparatus for producing chain agglomerations of nano-scale metal particles includes feeding at least one decomposable moiety selected from the group consisting of organometallic compounds, metal complexes, metal coordination compounds and mixtures thereof into a reactor vessel; exposing the decomposable moiety to a source of energy sufficient to decompose the moiety and produce nano-scale metal particles; and deposit or collection of chain agglomerations of nano-scale metal particles.
    Type: Application
    Filed: May 14, 2010
    Publication date: September 2, 2010
    Inventor: Robert A. Mercuri
  • Patent number: 7666349
    Abstract: The present invention provides a method of gel-casting WC—Co cemented carbide powder, where the resulting gelled body can be of complex shape and has a high green density, a good homogeneity and sufficiently good mechanical properties for the gelled body to be demolded and dried without significant shape-distortions and cracking. The method relates to the forming of a gelled body through the gelling of an aqueous slurry of WC—Co cemented carbide powder with good dispersion characteristics, where the gelling is achieved by the temperature induced polymerization reaction between a monomer and a cross-linker, catalyzed by a free-radical initiator. By further subjecting the body to drying, heating, and sintering, a dense cemented carbide body is obtained.
    Type: Grant
    Filed: January 5, 2007
    Date of Patent: February 23, 2010
    Assignee: Sandvik Intellectual Property AB
    Inventors: Eric Laarz, Karin Andersson
  • Patent number: 7510680
    Abstract: A metallic alloy having at least two metallic constituents is produced by first furnishing at least two non-oxide compounds, wherein the non-oxide compounds collectively comprise each of the metallic constituents, and wherein each of the non-oxide compounds is soluble in a mutual solvent. The method further includes dissolving the non-oxide compounds in the mutual solvent to produce a solution containing the metallic constituents, thereafter heating the solution to remove the mutual solvent and oxidize the metallic constituents to produce a mixed metallic oxide, thereafter cooling the mixed metallic oxide to form a substantially homogeneous mixed metallic oxide solid mass, and thereafter chemically reducing the mixed metallic oxide solid mass to produce a metallic alloy. The metallic alloy may be consolidated or otherwise processed.
    Type: Grant
    Filed: December 13, 2002
    Date of Patent: March 31, 2009
    Assignee: General Electric Company
    Inventors: James Dale Steibel, Andrew Philip Woodfield
  • Publication number: 20080292488
    Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.
    Type: Application
    Filed: August 7, 2008
    Publication date: November 27, 2008
    Applicant: GENERAL ELECTRIC COMPANY
    Inventors: Andrew Philip WOODFIELD, Eric Allen OTT, Clifford Earl SHAMBLEN, Michael Francis Xavier GIGLIOTTI
  • Patent number: 7442338
    Abstract: The present invention develops a manufacture method, via conventional liquid metallurgy, of finished and semi-finished metallic parts as casting, ingot, blooms and slabs in alloys base Fe, base Ni and base Co, microstructurally reinforced with complex molybdenum and titanium carbide particles, by means of their previous elaboration and latter addition to the molten alloy in the melting furnace. Then, when the alloy solidifies, they are inserted and distributed within the grains of the base metallic matrix, enhancing their mechanical properties and behavior at room as well as at high temperatures.
    Type: Grant
    Filed: May 13, 2004
    Date of Patent: October 28, 2008
    Assignee: Fundacion Inasmet
    Inventors: Ignacio Erauskin Lopetegui, Manuel Gutierrez Stampa, Inigo Agote Beloki, Manuel Orbegozo Ibarguren
  • Publication number: 20080175740
    Abstract: A method for manufacturing of iron- respectively micro-alloyed steel powders, starting from fluffy spray roasted iron oxides exhibiting a specific surface area in excess of 2.0 m2/g and residual chloride contents over 440 ppm Cl?, decrease the chloride content in two steps to less than 100 ppm, the specific surface area (BET) of to a pre-selected value of less than 10.0 m2/g, preferably between 0.1 and 2.0 m2/g and reduce the pre-sintered granules exhibiting a bulk density in excess of 1.200 g/dm3.
    Type: Application
    Filed: December 3, 2007
    Publication date: July 24, 2008
    Applicant: Dr. Michael J. Ruthner
    Inventor: Michael J. RUTHNER
  • Patent number: 6849229
    Abstract: A method of preparing an article made of a metallic material having its constituent elements includes the steps of furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively include the constituent elements of the metallic material in their respective constituent-element proportions, and thereafter utilizing the nonmetallic precursor compound to produce a metallic injection molded brown article. The nonmetallic precursor compounds may be processed into the metallic material by first chemically reducing them to the metallic material, and then injection molding the metallic material, or first injection molding the nonmetallic precursor compounds and then chemically reducing them to the metallic material.
    Type: Grant
    Filed: December 23, 2002
    Date of Patent: February 1, 2005
    Assignee: General Electric Company
    Inventors: Eric Allen Ott, Andrew Philip Woodfield, Clifford Earl Shamblen
  • Publication number: 20040211293
    Abstract: A martensitic steel metallic article (20) made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds is chemically reduced to produce a metallic martensitic steel, without melting the metallic martensitic steel. The metallic martensitic steel is consolidated to produce a consolidated metallic article (20), without melting the metallic martensitic steel and without melting the consolidated metallic article (20).
    Type: Application
    Filed: April 25, 2003
    Publication date: October 28, 2004
    Inventors: Clifford Earl Shamblen, Andrew Philip Woodfield, Eric Allen Ott, Michael Francis Xavier Gigliotti
  • Publication number: 20040115085
    Abstract: A metallic alloy having at least two metallic constituents is produced by first furnishing at least two non-oxide compounds, wherein the non-oxide compounds collectively comprise each of the metallic constituents, and wherein each of the non-oxide compounds is soluble in a mutual solvent. The method further includes dissolving the non-oxide compounds in the mutual solvent to produce a solution containing the metallic constituents, thereafter heating the solution to remove the mutual solvent and oxidize the metallic constituents to produce a mixed metallic oxide, thereafter cooling the mixed metallic oxide to form a substantially homogeneous mixed metallic oxide solid mass, and thereafter chemically reducing the mixed metallic oxide solid mass to produce a metallic alloy. The metallic alloy may be consolidated or otherwise processed.
    Type: Application
    Filed: December 13, 2002
    Publication date: June 17, 2004
    Inventors: James Dale Steibel, Andrew Philip Woodfield
  • Patent number: 6403210
    Abstract: The invention relates to a composite material, manufactured by dynamic densification of an amount of granular or powdered relatively brittle material or a mixture of one or more of such materials, wherein a continuous porous product is obtained, whereafter, by infiltration thereof with a second material, the brittle material particles are embedded in a continuous network of the second material. The invention further relates to a composite comprising ceramic particles embedded in a continuous matrix of a second material, obtainable by a method according to the invention, and to products manufactured from such composite.
    Type: Grant
    Filed: October 21, 1999
    Date of Patent: June 11, 2002
    Assignee: Nederlandse Organisatie voor toegepast-natuurwetenschappelijk Onderzoek TNO
    Inventors: Marianne Euphemia Corry Stuivinga, Amanda Margaretha Maas, Erik Peter Carton
  • Patent number: 6340397
    Abstract: A ferromagnetic powder comprising ferromagnetic particles coated with a material that does not degrade at temperatures above 150° C. and permits adjacent particles to strongly bind together after compaction such that parts made from the ferromagnetic powder have a transverse rupture strength of about 8,000 to about 20,000 pounds/square inch before sintering, The coating includes from 2 to 4 parts of an oxide and one part of a chromate, molybdate, oxalate, phosphate, or tungstate. The coating may be substantially free of organic materials. The invention also includes a method of making the ferromagnetic powder, a method of making soft magnetic parts from the ferromagnetic powder, and soft magnetic parts made from the ferromagnetic powder.
    Type: Grant
    Filed: February 11, 1999
    Date of Patent: January 22, 2002
    Assignee: Materials Innovation, Inc.
    Inventors: David S. Lashmore, Glenn L. Beane, Lev Deresh, Zonglu Hua
  • Patent number: 6150048
    Abstract: Disclosed are a metallic interconnection material for solid oxide fuel cells and a preparation method thereof. The metallic interconnection material has two fine microstructural phases in which 5-25% by volume of LaCrO.sub.3 is dispersed at the grain boundaries of Cr particles. It can be prepared by mixing 75-95% by volume of a Cr powder and 5-25% by volume of an LaCrO.sub.3 powder, together with a solvent and a binder, in a mill, molding the mixture into a predetermined shape after drying, and sintering the molded shape at approximately 1,500.degree. C. for 10 hours in an Ar atmosphere with 5 vol % of hydrogen to give an LaCrO.sub.3 -dispersed Cr alloy. The LaCrO.sub.3 -dispersed Cr alloy shows high electric conductivity by virtue of the growth inhibition of Cr particles during sintering and high chemical stability by virtue of the presence of the rare earth metal, La, meeting meet the requirements for the interconnection materials for solid oxide fuel cells.
    Type: Grant
    Filed: July 30, 1999
    Date of Patent: November 21, 2000
    Assignee: Korea Institute of Energy Research
    Inventors: Rak-Hyun Song, Dong-Ryul Shin, Kwangg-Sun Jeon, Yi-Sup Han, Dokiya Masayuki
  • Patent number: 5989489
    Abstract: The invention relates to a method for manufacturing a composite material wherein by dynamic densification of an amount of granular or powdered relatively brittle material or a mixture of one or more of such materials, a continuous porous product is obtained, whereafter, by infiltration thereof with a second material, the brittle material particles are embedded in a continuous network of the second material. The invention further relates to a composite comprising ceramic particles embedded in a continuous matrix of a second material, obtainable by a method according to the invention, and to products manufactured from such composite.
    Type: Grant
    Filed: November 25, 1997
    Date of Patent: November 23, 1999
    Assignee: Nederlandse Organisatie voor toegepast-natuurwetenschappelijk Onderzoek TNO
    Inventors: Marianne Euphemia Corry Stuivinga, Amanda Margaretha Maas, Erik Peter Carton
  • Patent number: 5968428
    Abstract: Disclosed is a molding method for powder particles, which is excellent in molding performance, and which makes it possible to obtain a preliminary molded product excellent in strength by enhancing mutual bonding between particles in the preliminary molded product. A molding apparatus for powder particles includes an outer frame die having a mold space with a lower punch and an upper punch to be slidably fitted thereto. Slight clearances exist between the outer frame die and the lower and upper punches. A mixture is prepared by mixing a powdery raw material with a liquid additive to cause an exothermic reaction therewith.
    Type: Grant
    Filed: June 26, 1997
    Date of Patent: October 19, 1999
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventor: Mitsuo Kuwabara
  • Patent number: 5925463
    Abstract: The object of the invention is a method for the electrochemical preparation of metal colloids with particle sizes of less than 30 nm, characterized in that one or more metals of groups Ib, IIb, III, IV, V, VI, VIIb, VIII, lanthanoides, and/or actinoides of the periodic table are cathodically reduced in the presence of a stabilizer, optionally with a supporting electrolyte being added, in organic solvents or in solvent mixtures of organic solvents and/or water within a temperature range of between -78.degree. C. and +120.degree. C. to form metal colloidal solutions or redispersible metal colloid powders, optionally in the presence of inert substrates and/or soluble metal salts of the respective metals.The invention further relates to soluble or redispersible colloids as well as application on substrates and immobilization thereof, in particular for the preparation of catalysts.
    Type: Grant
    Filed: December 18, 1996
    Date of Patent: July 20, 1999
    Assignee: Studiengesellschaft Kohle mbH
    Inventors: Manfred T. Reetz, Wolfgang Helbig, Stefan Andreas Quaiser
  • Patent number: 5908588
    Abstract: A process of molding inorganic materials into desired shapes comprises mixing the material with a dispersant, milling, molding the mixture, drying the mixture and sintering.
    Type: Grant
    Filed: February 17, 1998
    Date of Patent: June 1, 1999
    Assignee: Eastman Kodak Company
    Inventors: Syamal K. Ghosh, Dilip K. Chatterjee, James S. Reed, Steven R. Arrasmith
  • Patent number: 5852768
    Abstract: In order to produce precious metal powders of uniform particle size and low BET specific surface, appropriate aerosols are introduced into a flame reactor, whereby the aerosols are first freed of solvent as completely as possible by a thermal treatment.
    Type: Grant
    Filed: September 30, 1996
    Date of Patent: December 22, 1998
    Assignee: Degussa Aktiengesellschaft
    Inventors: Hauke Jacobsen, Werner Hartmann, Stipan Katusic, Karl-Anton Starz
  • Patent number: 5785731
    Abstract: To dope ammonium paratungstate with potassium, essentially devoid of silicon and ammonium, an aqueous potassium containing solution, preferably potassium hydroxide is added to an aqueous solution of ammonium paratungstate (APW), in a mol relationship of potassium to ammonium of between 0.1 and 10. A doped ammonium potassium paratungstate (AKPW) is obtained. This ammonium potassium paratungstate is then converted to tungsten blue oxide, which is reduced, preferably in a hydrogen containing atmosphere and a tungsten powder is then obtained which will be doped with 40 to 120 ppm, preferably about 90 ppm of potassium. Lamps equipped with tungsten wire filaments drawn from so doped tungsten have lifetimes at least 10% more than lamps with conventional tungsten filaments.
    Type: Grant
    Filed: February 28, 1996
    Date of Patent: July 28, 1998
    Assignee: Patent-Treuhand-Gesellschaft fur elektrische Gluhlampen mbH
    Inventors: Martin Fait, Joachim Fuchs, Alfred-Georg Gahn, Hans-Joachim Lunk, Michael Salmen, Burkhard Ziemer
  • Patent number: 5718865
    Abstract: A moulded alum composition is formed by mixing crushed solid alum with a polyol plasticiser followed by heating to form a slurry, and then pouring the mixture into a mould. No mechanical cutting and grinding is required and weakening cracks and fissures present in the raw alum are removed.
    Type: Grant
    Filed: December 24, 1996
    Date of Patent: February 17, 1998
    Inventor: Darren John Askew
  • Patent number: 5538684
    Abstract: The present invention provides lubricant compositions for the powder metallurgical field. The lubricant compositions contain a solid phase lubricant such as graphite, molybdenum disulfide, and polytetrafluoroethylene in combination with a liquid phase lubricant that is a binder for the solid phase lubricant. The binder can be chosen from various classes of compounds including polyethylene glycols, polyethylene glycol esters, partial esters of C.sub.3-6 polyhydric alcohols, polyvinyl esters, and polyvinyl pyrrolidones. The binder is solubilized in an organic solvent.
    Type: Grant
    Filed: June 6, 1995
    Date of Patent: July 23, 1996
    Assignee: Hoeganaes Corporation
    Inventors: Sydney Luk, Ann Lawrence
  • Patent number: 5529747
    Abstract: A formable composite magnetic flux concentrator material is composed of about 65% to 90% ferromagnetic material, such as iron powder, and about 35% to 10% binder, the binder being a mixture of an epoxy and one or more catalysts. The concentrator material is provided in a formable state as a putty-like body which can be worked into any desired shape dictated by the configuration of the induction heating coil used in a particular application. In one form, the density of the concentrator material is increased by application of vibration, compression and vacuum to de-air the material and to reduce voids therein. In another form, the iron powder comprises spherical-shaped particles and non-spherical shaped powders chosen in a ratio to maximize the density of material available.
    Type: Grant
    Filed: December 7, 1994
    Date of Patent: June 25, 1996
    Assignee: Learflux, Inc.
    Inventor: Thomas J. Learman
  • Patent number: 5468446
    Abstract: The pelletisation or granulation of a material or mixture of materials the or at least one of which is reactive in a liquid to produce a gas is improved by treating the reactive material prior to final compaction to form a coating thereon of a substance which is less soluble in the liquid than the reactive material. The preferred reactive material is calcium hydride and the preferred coating is calcium carbonate with or without calcium hydroxide.
    Type: Grant
    Filed: February 28, 1994
    Date of Patent: November 21, 1995
    Assignees: British Aerospace PLC, BAeSEMA Ltd.
    Inventors: Peter C. Morgan, Alan D. Hart, Philip D. Morgans
  • Patent number: 5366687
    Abstract: A method is taught for the preparation of ceramic fibers by electrophoretic deposition of metal oxide upon a conductive fiber core, which core may be subsequently removed.
    Type: Grant
    Filed: December 10, 1993
    Date of Patent: November 22, 1994
    Assignee: United Technologies Corporation
    Inventors: William J. Dalzell, Jr., Robert J. Wright, Jarrett L. Spence
  • Patent number: 5360494
    Abstract: A powdered magnesium composition is mixed with lithium dispersed in an inert, non-water absorbent, liquid medium to produce a substantially homogenous admixture that is heated to melt the lithium and vaporize the liquid medium to thereby obtain a decovered powdered alloy comprising aluminum and lithium. The liquid medium has first and second liquid constituents, wherein the first liquid constituent has a boiling point below the melting point of lithium and the second liquid constituent has a boiling point above the melting point of lithium but below the melting point of the alloy being produced.
    Type: Grant
    Filed: July 29, 1993
    Date of Patent: November 1, 1994
    Inventor: Sanford W. Brown
  • Patent number: 5342572
    Abstract: In accordance with this invention, there is provided a process for producing a shaped article in which a reaction mixture containing at least two elemental materials is first charged into a die to form a shaped green body. A uniaxial pressure of from about 500 to about 5,000 pounds per square inch of cross-sectional area of the green body is then uniaxially applied to the green body, and the green body is then ignited; during ignition, the uniaxial pressure of from about 500 to about 5,000 pounds per square inch is maintained at a substantially constant level and continually applied to the reaction mixture.
    Type: Grant
    Filed: September 27, 1993
    Date of Patent: August 30, 1994
    Assignee: Alfred University
    Inventors: Gregory C. Stangle, William C. Williams
  • Patent number: 5340533
    Abstract: A process for producing a dense composite material by combustion synthesis. In the first step of the process, a reaction mixture comprised of an elemental material is provided. The elemental material is charged to a die, a uniaxial pressure of from about 500 to about 5,000 pounds per square inch is applied to the elemental material within the die, and the elemental material within the die is ignited. Prior to, during, and subsequent to the time said elemental material is been ignited, the uniaxial pressure of from about 500 to about 5,000 pounds per square inch is applied to the elemental material within said die.
    Type: Grant
    Filed: April 27, 1993
    Date of Patent: August 23, 1994
    Assignee: Alfred University
    Inventors: Gregory C. Stangle, Scott E. Niedzialek, William C. Williams
  • Patent number: 5340657
    Abstract: This invention relates to pillared micas, which comprise an active metal selected from the group consisting of Pt, Cr, Pd, It, Rh and mixtures thereof, and a first modifier metal selected from the group consisting of Sn, Ga and mixtures thereof. The mica may also be modified with a second modifier metal selected from the group consisting of alkali metals, alkaline earth metals, or rare earth metals and mixtures thereof. This invention further relates to a process for preparing such a catalyst.
    Type: Grant
    Filed: August 26, 1992
    Date of Patent: August 23, 1994
    Assignee: Exxon Research and Engineering Company
    Inventors: Michael C. Kerby, Kenneth L. Riley, Fred M. Long, Jack W. Johnson, John F. Brody
  • Patent number: 5198188
    Abstract: Disclosed is a method of producing dense refractory products, comprising:(a) obtaining a quantity of exoergic material in powder form capable of sustaining a combustion synthesis reaction;(b) removing absorbed water vapor therefrom;(c) cold-pressing said material into a formed body;(d) plasma spraying said formed body with a molten exoergic material to form a coat thereon; and(e) igniting said exoergic coated formed body under an inert gas atmosphere and pressure to produce self-sustained combustion synthesis.Also disclosed are products produced by the method.
    Type: Grant
    Filed: January 16, 1991
    Date of Patent: March 30, 1993
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: J. Birch Holt, Michael Kelly
  • Patent number: 5112572
    Abstract: The invention provides a method for removing the oxide surface from water atomized metal powders containing an oxidizer capable of oxidizing chromium from a trivalent to a soluble hexavalent state, whereby chromium oxides are removed from the metal powder surface. The powder is then treated with a dilute acid solution essentially devoid of hydrofluoric acid to remove other hydrated oxides from the metal powder surface. The powder is then water washed and dried.
    Type: Grant
    Filed: October 1, 1991
    Date of Patent: May 12, 1992
    Assignee: Inco Limited
    Inventors: Thijs Eerkes, James A. E. Bell, Carlos M. Diaz
  • Patent number: 5059387
    Abstract: Shaped parts are formed from a powder having the desired chemistry of the finished part by mixing the powder with a thermosetting condensation resin that acts as a binder. The resin may be partially catalyzed, or additives or surfactants added to improve rheology, mixing properties, or processing time. Upon heating, the inherently low viscosity mixture will solidify without pressure being applied to it. A rigid form is produced which is capable of being ejected from a mold. Pre-sintered shapes or parts are made by injection molding, by using semi-permanent tooling, or by prototyping. Binder removal is accomplished by thermal means and without a separate debinding step, despite the known heat resistance of thermosetting resins. Removal is due to the film forming characteristic of the binder leaving open the part's pores, by providing oxidizing conditions within the part's pores as the part is heated, and by insuring that the evolving resin vapor diffuses through the pores by heating the part in a vacuum.
    Type: Grant
    Filed: June 2, 1989
    Date of Patent: October 22, 1991
    Assignee: Megamet Industries
    Inventor: Gregory M. Brasel
  • Patent number: 4960459
    Abstract: A method for pickling and consolidating water atomized metallic powders to reduce surface oxides. The technique includes introducing the powder into an acid bath--preferably nitric acid and hydrofluoric acid, rinsing the powder, introducing the powder into an alkaline bath, rinsing the powder and then consolidating the powder into a workpiece. Alternatively, the powder can be additionally introduced into a second acid bath and/or placed into a finishing boric acid bath before consolidation.
    Type: Grant
    Filed: September 19, 1988
    Date of Patent: October 2, 1990
    Assignee: Inco Alloys International, Inc.
    Inventors: Jon M. Poole, Lindy J. Curtis
  • Patent number: 4957421
    Abstract: Titanium and titanium alloy surfaces can be diffusion coated, and portions of the surface protected against such coating by localized powdered masking layer of about 43% titanium, aluminum in an amount equal to the aluminum content of the surface masked, as well as other metals in an amount about one-fifth of their content in the surface masked. Diffusion coating can be speeded by high heat input. Diffusion coating packs can be made with chemically reduced metal content of sludges. Diffusion aliminizing followed by caustic leaching to remove much of the diffused-in aluminum, yields catalytically and pyrophorically active porous surface that also accepts top coatings. Mixtures of aluminum powder with nickel and/or iron powders react when heated to form Raney-like product that can be leached to become pyrophoric, and when held on a metal foil or gauze web will adhere to the web so that leached product can be used as pyrophoric foil for decoying heat-seeking missiles.
    Type: Grant
    Filed: April 10, 1989
    Date of Patent: September 18, 1990
    Assignee: Alloy Surfaces Company, Inc.
    Inventor: Alfonso L. Baldi
  • Patent number: 4954169
    Abstract: Earth acid metal powders, such as tantalum or niobium, useful in the production of electrolytic capacitors and other electronic components, are agglomerates of sintered compacts, wherein the mean grain size of the agglomerates is no more than 2.0 .mu.m, determined by the Fisher Sub-Sieve Sizer, and wherein the agglomerates consist of primary individual agglomerated particles of mean grain size of no more than 0.7 .mu.m.
    Type: Grant
    Filed: June 12, 1989
    Date of Patent: September 4, 1990
    Assignee: Bayer Aktiengesellschaft
    Inventor: Dieter Behrens
  • Patent number: 4946643
    Abstract: Dense, finely grained composite materials comprising one or more ceramic phase or phase and one or more metallic and/or intermetallic phase or phases are produced by combustion synthesis. Spherical ceramic grains are homogeneously dispersed within the matrix. Methods are provided, which include the step of applying mechanical pressure during or immediately after ignition, by which the microstructures in the resulting composites can be controllably selected.
    Type: Grant
    Filed: September 26, 1989
    Date of Patent: August 7, 1990
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Stephen D. Dunmead, Joseph B. Holt, Donald D. Kingman, Zuhair A. Munir
  • Patent number: 4933025
    Abstract: A method for treating rare earth permanent magnetic material is disclosed. The treatment includes soaking ribbon rare earth permanent magnetic material consisting essentially of grains of the tetragonal crystal phase RE.sub.2 TM.sub.14 B where RE is neodymium and/or praseodymium or mixtures thereof with other rare earth elements and TM is iron or mixtures of iron and cobalt, cobalt in a soaking solution of either distilled water or phosphoric acid and manganese phosphate solution, draining off the soaking solution, rinsing with distilled water while agitating to separate and remove fine powdered magnetic material, and washing and drying the remaining powder or ribbons. The treated material is taken to substantial dryness before the material is incorporated into a permanent magnet.
    Type: Grant
    Filed: October 2, 1989
    Date of Patent: June 12, 1990
    Assignee: General Motors Corporation
    Inventors: Erwin A. Alson, Thomas H. VanSteenkiste
  • Patent number: 4879262
    Abstract: A self-sustaining combustion synthesis process for producing hard, tough, lightweight B.sub.4 C/TiB.sub.2 composites is based on the thermodynamic dependence of adiabatic temperature and product composition on the stoichiometry of the B.sub.4 C and TiB.sub.2 reactants. For lightweight products the composition must be relatively rich in the B.sub.4 C component. B.sub.4 C-rich composites are obtained by varying the initial temperature of the reactants. The product is hard, porous material whose toughness can be enhanced by filling the pores with aluminum or other metal phases using a liquid metal infiltration process. The process can be extended to the formation of other composites having a low exothermic component.
    Type: Grant
    Filed: July 28, 1988
    Date of Patent: November 7, 1989
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Danny C. Halverson, Beverly Y. Lum, Zuhair A. Munir
  • Patent number: RE33243
    Abstract: The invention relates to a process for the treatment of a metal oxide powder, particularly a UO.sub.2 or PuO.sub.2 powder, with a view to its fritting.This process consists of oxidizing the powder, so as to form on its surface a hydrated oxide layer of the same metal. When the oxide is UO.sub.2 or PuO.sub.2 and mixtures thereof, as well as those prepared with ThO.sub.2, the treated powder can be used for producing nuclear fuel pellets by cold compression, followed by fritting.
    Type: Grant
    Filed: January 13, 1989
    Date of Patent: June 26, 1990
    Assignee: Commissariat a l'Energie Atomique
    Inventors: Camille Braun, Joel Danroc, Bernard Francois, Jean Michel