Includes A Chemical Reaction Patents (Class 419/63)
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Patent number: 9905907Abstract: The housing includes a base and an antenna coating layer. The base includes a first surface. The base is made of one of glass and ceramic. The antenna coating layer is formed on the first surface. The antenna coating layer is made of metal power. The metal power is selected from one of copper power, copper alloy power, or copper and nickel mixed power.Type: GrantFiled: September 1, 2015Date of Patent: February 27, 2018Assignees: SHENZHEN FUTAIHONG PRECISION INDUSTRY CO., LTD., FIH (HONG KONG) LIMITEDInventors: Yu-Tsai Wang, Jing-Hai Zheng
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Publication number: 20150118095Abstract: A method of manufacturing a ferrous alloy article is disclosed and includes the steps of melting a ferrous alloy composition into a liquid, atomizing and solidifying of the liquid into powder particles, outgassing to remove oxygen from the surface of the powder particles, and consolidating the powder particles into a monolithic article.Type: ApplicationFiled: May 20, 2014Publication date: April 30, 2015Applicant: CRS HOLDINGS INC.Inventors: David E. Wert, Timothy R. Armstrong, David A. Helmick, Michael L. Schmidt
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Publication number: 20140377121Abstract: A component, such as a SOFC interconnect, and methods of making the component are provided using various chromium powders, including powder particles with a chromium core covered with an iron shell, a pre-alloyed Cr—Fe powder or a chromium powder produced by hydrogen reduction with hydrogen.Type: ApplicationFiled: September 11, 2014Publication date: December 25, 2014Inventors: Martin Janousek, Shivanand I. Majagi
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Publication number: 20140334963Abstract: A titanium metal or a titanium alloy having submicron titanium boride substantially uniformly dispersed therein and a method of making same is disclosed. Ti power of Ti alloy powder has dispersed within the particles forming the powder titanium boride which is other than whisker-shaped or spherical substantially uniformly dispersed therein.Type: ApplicationFiled: July 28, 2014Publication date: November 13, 2014Applicant: Cristal Metals Inc.Inventors: Lance Jacobsen, Adam Benish
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Patent number: 8709335Abstract: A method of making a sputtering target includes providing a backing structure, and forming a copper indium gallium sputtering target material on the backing structure by cold spraying. The step of cold spraying includes spraying a powder comprising copper, indium and gallium in a process gas stream, and at least one of an average particle size of the powder is at least 35 ?m, a velocity of the process gas stream is at least 150 m/s, or a process gas pressure is 20 bar or less.Type: GrantFiled: October 19, 2010Date of Patent: April 29, 2014Assignee: Hanergy Holding Group Ltd.Inventors: Johannes Vlcek, Daniel R. Juliano
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Publication number: 20140106144Abstract: The method for forming a 3-D metal object by 3-D printing or injection molding comprising providing as a feed material metal particles formed by establishing multiple metal components in a primary billet of a ductile material, working the primary billet through a series of reduction steps to form the components into elongated elements, leaching the ductile material from the elongated elements and reducing the length to short uniform lengths.Type: ApplicationFiled: August 8, 2013Publication date: April 17, 2014Applicant: COMPOSITE MATERIALS TECHNOLOGY, INC.Inventor: James Wong
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Publication number: 20130315773Abstract: The invention relates to energy-saving manufacturing of purified hydrogenated titanium powders or alloying titanium hydride powders, by metallo-thermic reduction of titanium chlorides, including their hydrogenation, vacuum separation of titanium hydride sponge block from magnesium and magnesium chlorides, followed by crushing, grinding, and sintering of said block without need for hydrometallurgical treatment of the produced powders. Methods disclosed contain embodiments of processes for manufacturing high-purity powders and their use in manufacturing near-net shape titanium and titanium-alloy articles by sintering titanium hydride and alloyed titanium hydride powders produced from combined hydrogen-magnesium reduction of titanium chlorides, halides and hydrides of other metals.Type: ApplicationFiled: May 24, 2012Publication date: November 28, 2013Applicant: Advance Materials Products, Inc. (ADMA Products, Inc.)Inventors: Vladimir S. Moxson, Volodymyr A. Duz, Andrey G. Klevtsov, Viktor D. Sukhoplyuyev, Mihajlo D. Sopka, Yury V. Shuvalov, Mykhailo Matviychuk
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Publication number: 20130236349Abstract: The invention provides an industrial method for producing dispersion-strengthened iron-based materials at low cost and in large-scale. The industrial acid pickling waste solution is treated by spray roasting process after yttrium chloride is added. During the spray roasting process, the solution is atomized into fine droplets, the droplets are contacted with gas and dried into powders, which are heated in air to form metal oxides. The mixed powders of the metal oxides are reduced in hydrogen stream to obtain yttria dispersion-strengthened iron powders. High performance dispersion-strengthened iron materials are obtained by densifying the yttria dispersion-strengthened iron powders. The method has simple process and low cost, and is suitable for large-scale production due to the direct use of acid pickling waste solution from steel factory.Type: ApplicationFiled: June 30, 2011Publication date: September 12, 2013Applicant: UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJINGInventors: Zhimeng Guo, Weiwei Yang, Ji Luo, Huiqin Cao, Cunguang Chen
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Publication number: 20120282130Abstract: A carbothermic reduction method is provided for reducing a rare earth element-containing oxide including at least one of neodymium (Nd) and praseodymium (Pr) and possibly other rare earth elements (La, Ce, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Sc, and Y) as alloying agents in the presence of carbon and a source of a reactant element including one or more of silicon, germanium, tin, lead, arsenic, antimony and bismuth to form a rare earth element-containing intermediate alloy as a master alloy for making permanent magnet material. The process is a more efficient, lower cost and environmentally friendly technology than current methods of manufacturing rare earth metals. The intermediate material is useful as a master alloy for making a permanent magnet material comprising at least one of neodymium and praseodymium, and possibly other rare earth metals as alloying additives.Type: ApplicationFiled: April 18, 2012Publication date: November 8, 2012Inventors: Karl A. Gschneidner, JR., Frederick A. Schmidt, Ralph W. McCallum
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Publication number: 20120263619Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.Type: ApplicationFiled: June 15, 2012Publication date: October 18, 2012Applicant: GENERAL ELECTRIC COMPANYInventors: Andrew Philip WOODFIELD, Eric Allen OTT, Clifford Earl SHAMBLEN, Michael Francis Xavier GIGLIOTTI
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Publication number: 20120237769Abstract: The present invention provides a powder for a magnet which can form a rare earth magnet having excellent magnetic characteristics and which has excellent moldability, a method for producing the powder for a magnet, a powder compact, and a rare earth-iron-boron-based alloy material. Magnetic particles constituting a powder for a magnet each include a structure in which a particle of a phase 3 of a hydrogen compound of a rare earth element is dispersed in a phase 2 of an iron-containing material. Since the phase 2 of the iron-containing material is uniformly present in each of the magnetic particles 1, the powder has excellent moldability and easily increases the density of a powder compact 4.Type: ApplicationFiled: April 13, 2011Publication date: September 20, 2012Applicant: Sumitomo Electric Industries, Ltd.Inventors: Toru Maeda, Asako Watanabe
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Publication number: 20110162550Abstract: In making frangible objects, including lead-free bullets and other projectiles, powdered metal primary and powdered ceramic secondary phases are mixed and densified at an elevated temperature such that the ceramic phase forms a brittle network. Any combination of metal and ceramic phases may be used to achieve desired chemical and physical properties. Any appropriate mixing, forming, and/or thermal processing methods and equipment may be used. Degrees of frangibility, strength, and toughness can be adjusted to suit a given application by precursor selection, degree of mixing, relative amounts of metal and ceramic phases, forming method, and thermal and mechanical processing parameters.Type: ApplicationFiled: January 6, 2010Publication date: July 7, 2011Inventors: Mark C. Hash, James Trent Pearson
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Patent number: 7833472Abstract: An article is prepared by furnishing a plurality of powder particle substrates made of a substrate metal, providing a nonmetallic precursor of a metallic coating material, wherein the metallic coating material comprises an alloying element that is thermophysically melt incompatible with the substrate metal, contacting the powder particle substrates with the nonmetallic precursor, chemically reducing the nonmetallic precursor to form coated powder particles comprising the powder particle substrates having a surface-enriched layer of the metallic coating material thereon without melting the powder particle substrates, and processing the coated powder particles to form the article, without melting the powder particle substrates.Type: GrantFiled: June 1, 2005Date of Patent: November 16, 2010Assignee: General Electric CompanyInventors: Eric Allen Ott, Andrew Philip Woodfield, David Paul Mourer, John Frederick Ackerman, Jon Raymond Groh, Robert Edward Schafrik, Kenneth Rees Bain, Michael Francis Xavier Gigliotti, Matthew Bernard Buczek
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Publication number: 20100222212Abstract: A process and apparatus for producing chain agglomerations of nano-scale metal particles includes feeding at least one decomposable moiety selected from the group consisting of organometallic compounds, metal complexes, metal coordination compounds and mixtures thereof into a reactor vessel; exposing the decomposable moiety to a source of energy sufficient to decompose the moiety and produce nano-scale metal particles; and deposit or collection of chain agglomerations of nano-scale metal particles.Type: ApplicationFiled: May 14, 2010Publication date: September 2, 2010Inventor: Robert A. Mercuri
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Patent number: 7666349Abstract: The present invention provides a method of gel-casting WC—Co cemented carbide powder, where the resulting gelled body can be of complex shape and has a high green density, a good homogeneity and sufficiently good mechanical properties for the gelled body to be demolded and dried without significant shape-distortions and cracking. The method relates to the forming of a gelled body through the gelling of an aqueous slurry of WC—Co cemented carbide powder with good dispersion characteristics, where the gelling is achieved by the temperature induced polymerization reaction between a monomer and a cross-linker, catalyzed by a free-radical initiator. By further subjecting the body to drying, heating, and sintering, a dense cemented carbide body is obtained.Type: GrantFiled: January 5, 2007Date of Patent: February 23, 2010Assignee: Sandvik Intellectual Property ABInventors: Eric Laarz, Karin Andersson
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Patent number: 7510680Abstract: A metallic alloy having at least two metallic constituents is produced by first furnishing at least two non-oxide compounds, wherein the non-oxide compounds collectively comprise each of the metallic constituents, and wherein each of the non-oxide compounds is soluble in a mutual solvent. The method further includes dissolving the non-oxide compounds in the mutual solvent to produce a solution containing the metallic constituents, thereafter heating the solution to remove the mutual solvent and oxidize the metallic constituents to produce a mixed metallic oxide, thereafter cooling the mixed metallic oxide to form a substantially homogeneous mixed metallic oxide solid mass, and thereafter chemically reducing the mixed metallic oxide solid mass to produce a metallic alloy. The metallic alloy may be consolidated or otherwise processed.Type: GrantFiled: December 13, 2002Date of Patent: March 31, 2009Assignee: General Electric CompanyInventors: James Dale Steibel, Andrew Philip Woodfield
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Publication number: 20080292488Abstract: A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article.Type: ApplicationFiled: August 7, 2008Publication date: November 27, 2008Applicant: GENERAL ELECTRIC COMPANYInventors: Andrew Philip WOODFIELD, Eric Allen OTT, Clifford Earl SHAMBLEN, Michael Francis Xavier GIGLIOTTI
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Patent number: 7442338Abstract: The present invention develops a manufacture method, via conventional liquid metallurgy, of finished and semi-finished metallic parts as casting, ingot, blooms and slabs in alloys base Fe, base Ni and base Co, microstructurally reinforced with complex molybdenum and titanium carbide particles, by means of their previous elaboration and latter addition to the molten alloy in the melting furnace. Then, when the alloy solidifies, they are inserted and distributed within the grains of the base metallic matrix, enhancing their mechanical properties and behavior at room as well as at high temperatures.Type: GrantFiled: May 13, 2004Date of Patent: October 28, 2008Assignee: Fundacion InasmetInventors: Ignacio Erauskin Lopetegui, Manuel Gutierrez Stampa, Inigo Agote Beloki, Manuel Orbegozo Ibarguren
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Publication number: 20080175740Abstract: A method for manufacturing of iron- respectively micro-alloyed steel powders, starting from fluffy spray roasted iron oxides exhibiting a specific surface area in excess of 2.0 m2/g and residual chloride contents over 440 ppm Cl?, decrease the chloride content in two steps to less than 100 ppm, the specific surface area (BET) of to a pre-selected value of less than 10.0 m2/g, preferably between 0.1 and 2.0 m2/g and reduce the pre-sintered granules exhibiting a bulk density in excess of 1.200 g/dm3.Type: ApplicationFiled: December 3, 2007Publication date: July 24, 2008Applicant: Dr. Michael J. RuthnerInventor: Michael J. RUTHNER
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Patent number: 6849229Abstract: A method of preparing an article made of a metallic material having its constituent elements includes the steps of furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively include the constituent elements of the metallic material in their respective constituent-element proportions, and thereafter utilizing the nonmetallic precursor compound to produce a metallic injection molded brown article. The nonmetallic precursor compounds may be processed into the metallic material by first chemically reducing them to the metallic material, and then injection molding the metallic material, or first injection molding the nonmetallic precursor compounds and then chemically reducing them to the metallic material.Type: GrantFiled: December 23, 2002Date of Patent: February 1, 2005Assignee: General Electric CompanyInventors: Eric Allen Ott, Andrew Philip Woodfield, Clifford Earl Shamblen
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Publication number: 20040211293Abstract: A martensitic steel metallic article (20) made of metallic constituent elements is fabricated from a mixture of nonmetallic precursor compounds of the metallic constituent elements. The mixture of nonmetallic precursor compounds is chemically reduced to produce a metallic martensitic steel, without melting the metallic martensitic steel. The metallic martensitic steel is consolidated to produce a consolidated metallic article (20), without melting the metallic martensitic steel and without melting the consolidated metallic article (20).Type: ApplicationFiled: April 25, 2003Publication date: October 28, 2004Inventors: Clifford Earl Shamblen, Andrew Philip Woodfield, Eric Allen Ott, Michael Francis Xavier Gigliotti
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Publication number: 20040115085Abstract: A metallic alloy having at least two metallic constituents is produced by first furnishing at least two non-oxide compounds, wherein the non-oxide compounds collectively comprise each of the metallic constituents, and wherein each of the non-oxide compounds is soluble in a mutual solvent. The method further includes dissolving the non-oxide compounds in the mutual solvent to produce a solution containing the metallic constituents, thereafter heating the solution to remove the mutual solvent and oxidize the metallic constituents to produce a mixed metallic oxide, thereafter cooling the mixed metallic oxide to form a substantially homogeneous mixed metallic oxide solid mass, and thereafter chemically reducing the mixed metallic oxide solid mass to produce a metallic alloy. The metallic alloy may be consolidated or otherwise processed.Type: ApplicationFiled: December 13, 2002Publication date: June 17, 2004Inventors: James Dale Steibel, Andrew Philip Woodfield
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Patent number: 6403210Abstract: The invention relates to a composite material, manufactured by dynamic densification of an amount of granular or powdered relatively brittle material or a mixture of one or more of such materials, wherein a continuous porous product is obtained, whereafter, by infiltration thereof with a second material, the brittle material particles are embedded in a continuous network of the second material. The invention further relates to a composite comprising ceramic particles embedded in a continuous matrix of a second material, obtainable by a method according to the invention, and to products manufactured from such composite.Type: GrantFiled: October 21, 1999Date of Patent: June 11, 2002Assignee: Nederlandse Organisatie voor toegepast-natuurwetenschappelijk Onderzoek TNOInventors: Marianne Euphemia Corry Stuivinga, Amanda Margaretha Maas, Erik Peter Carton
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Patent number: 6340397Abstract: A ferromagnetic powder comprising ferromagnetic particles coated with a material that does not degrade at temperatures above 150° C. and permits adjacent particles to strongly bind together after compaction such that parts made from the ferromagnetic powder have a transverse rupture strength of about 8,000 to about 20,000 pounds/square inch before sintering, The coating includes from 2 to 4 parts of an oxide and one part of a chromate, molybdate, oxalate, phosphate, or tungstate. The coating may be substantially free of organic materials. The invention also includes a method of making the ferromagnetic powder, a method of making soft magnetic parts from the ferromagnetic powder, and soft magnetic parts made from the ferromagnetic powder.Type: GrantFiled: February 11, 1999Date of Patent: January 22, 2002Assignee: Materials Innovation, Inc.Inventors: David S. Lashmore, Glenn L. Beane, Lev Deresh, Zonglu Hua
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Patent number: 6150048Abstract: Disclosed are a metallic interconnection material for solid oxide fuel cells and a preparation method thereof. The metallic interconnection material has two fine microstructural phases in which 5-25% by volume of LaCrO.sub.3 is dispersed at the grain boundaries of Cr particles. It can be prepared by mixing 75-95% by volume of a Cr powder and 5-25% by volume of an LaCrO.sub.3 powder, together with a solvent and a binder, in a mill, molding the mixture into a predetermined shape after drying, and sintering the molded shape at approximately 1,500.degree. C. for 10 hours in an Ar atmosphere with 5 vol % of hydrogen to give an LaCrO.sub.3 -dispersed Cr alloy. The LaCrO.sub.3 -dispersed Cr alloy shows high electric conductivity by virtue of the growth inhibition of Cr particles during sintering and high chemical stability by virtue of the presence of the rare earth metal, La, meeting meet the requirements for the interconnection materials for solid oxide fuel cells.Type: GrantFiled: July 30, 1999Date of Patent: November 21, 2000Assignee: Korea Institute of Energy ResearchInventors: Rak-Hyun Song, Dong-Ryul Shin, Kwangg-Sun Jeon, Yi-Sup Han, Dokiya Masayuki
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Patent number: 5989489Abstract: The invention relates to a method for manufacturing a composite material wherein by dynamic densification of an amount of granular or powdered relatively brittle material or a mixture of one or more of such materials, a continuous porous product is obtained, whereafter, by infiltration thereof with a second material, the brittle material particles are embedded in a continuous network of the second material. The invention further relates to a composite comprising ceramic particles embedded in a continuous matrix of a second material, obtainable by a method according to the invention, and to products manufactured from such composite.Type: GrantFiled: November 25, 1997Date of Patent: November 23, 1999Assignee: Nederlandse Organisatie voor toegepast-natuurwetenschappelijk Onderzoek TNOInventors: Marianne Euphemia Corry Stuivinga, Amanda Margaretha Maas, Erik Peter Carton
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Patent number: 5968428Abstract: Disclosed is a molding method for powder particles, which is excellent in molding performance, and which makes it possible to obtain a preliminary molded product excellent in strength by enhancing mutual bonding between particles in the preliminary molded product. A molding apparatus for powder particles includes an outer frame die having a mold space with a lower punch and an upper punch to be slidably fitted thereto. Slight clearances exist between the outer frame die and the lower and upper punches. A mixture is prepared by mixing a powdery raw material with a liquid additive to cause an exothermic reaction therewith.Type: GrantFiled: June 26, 1997Date of Patent: October 19, 1999Assignee: Honda Giken Kogyo Kabushiki KaishaInventor: Mitsuo Kuwabara
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Patent number: 5925463Abstract: The object of the invention is a method for the electrochemical preparation of metal colloids with particle sizes of less than 30 nm, characterized in that one or more metals of groups Ib, IIb, III, IV, V, VI, VIIb, VIII, lanthanoides, and/or actinoides of the periodic table are cathodically reduced in the presence of a stabilizer, optionally with a supporting electrolyte being added, in organic solvents or in solvent mixtures of organic solvents and/or water within a temperature range of between -78.degree. C. and +120.degree. C. to form metal colloidal solutions or redispersible metal colloid powders, optionally in the presence of inert substrates and/or soluble metal salts of the respective metals.The invention further relates to soluble or redispersible colloids as well as application on substrates and immobilization thereof, in particular for the preparation of catalysts.Type: GrantFiled: December 18, 1996Date of Patent: July 20, 1999Assignee: Studiengesellschaft Kohle mbHInventors: Manfred T. Reetz, Wolfgang Helbig, Stefan Andreas Quaiser
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Patent number: 5908588Abstract: A process of molding inorganic materials into desired shapes comprises mixing the material with a dispersant, milling, molding the mixture, drying the mixture and sintering.Type: GrantFiled: February 17, 1998Date of Patent: June 1, 1999Assignee: Eastman Kodak CompanyInventors: Syamal K. Ghosh, Dilip K. Chatterjee, James S. Reed, Steven R. Arrasmith
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Patent number: 5852768Abstract: In order to produce precious metal powders of uniform particle size and low BET specific surface, appropriate aerosols are introduced into a flame reactor, whereby the aerosols are first freed of solvent as completely as possible by a thermal treatment.Type: GrantFiled: September 30, 1996Date of Patent: December 22, 1998Assignee: Degussa AktiengesellschaftInventors: Hauke Jacobsen, Werner Hartmann, Stipan Katusic, Karl-Anton Starz
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Patent number: 5785731Abstract: To dope ammonium paratungstate with potassium, essentially devoid of silicon and ammonium, an aqueous potassium containing solution, preferably potassium hydroxide is added to an aqueous solution of ammonium paratungstate (APW), in a mol relationship of potassium to ammonium of between 0.1 and 10. A doped ammonium potassium paratungstate (AKPW) is obtained. This ammonium potassium paratungstate is then converted to tungsten blue oxide, which is reduced, preferably in a hydrogen containing atmosphere and a tungsten powder is then obtained which will be doped with 40 to 120 ppm, preferably about 90 ppm of potassium. Lamps equipped with tungsten wire filaments drawn from so doped tungsten have lifetimes at least 10% more than lamps with conventional tungsten filaments.Type: GrantFiled: February 28, 1996Date of Patent: July 28, 1998Assignee: Patent-Treuhand-Gesellschaft fur elektrische Gluhlampen mbHInventors: Martin Fait, Joachim Fuchs, Alfred-Georg Gahn, Hans-Joachim Lunk, Michael Salmen, Burkhard Ziemer
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Patent number: 5718865Abstract: A moulded alum composition is formed by mixing crushed solid alum with a polyol plasticiser followed by heating to form a slurry, and then pouring the mixture into a mould. No mechanical cutting and grinding is required and weakening cracks and fissures present in the raw alum are removed.Type: GrantFiled: December 24, 1996Date of Patent: February 17, 1998Inventor: Darren John Askew
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Patent number: 5538684Abstract: The present invention provides lubricant compositions for the powder metallurgical field. The lubricant compositions contain a solid phase lubricant such as graphite, molybdenum disulfide, and polytetrafluoroethylene in combination with a liquid phase lubricant that is a binder for the solid phase lubricant. The binder can be chosen from various classes of compounds including polyethylene glycols, polyethylene glycol esters, partial esters of C.sub.3-6 polyhydric alcohols, polyvinyl esters, and polyvinyl pyrrolidones. The binder is solubilized in an organic solvent.Type: GrantFiled: June 6, 1995Date of Patent: July 23, 1996Assignee: Hoeganaes CorporationInventors: Sydney Luk, Ann Lawrence
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Patent number: 5529747Abstract: A formable composite magnetic flux concentrator material is composed of about 65% to 90% ferromagnetic material, such as iron powder, and about 35% to 10% binder, the binder being a mixture of an epoxy and one or more catalysts. The concentrator material is provided in a formable state as a putty-like body which can be worked into any desired shape dictated by the configuration of the induction heating coil used in a particular application. In one form, the density of the concentrator material is increased by application of vibration, compression and vacuum to de-air the material and to reduce voids therein. In another form, the iron powder comprises spherical-shaped particles and non-spherical shaped powders chosen in a ratio to maximize the density of material available.Type: GrantFiled: December 7, 1994Date of Patent: June 25, 1996Assignee: Learflux, Inc.Inventor: Thomas J. Learman
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Patent number: 5468446Abstract: The pelletisation or granulation of a material or mixture of materials the or at least one of which is reactive in a liquid to produce a gas is improved by treating the reactive material prior to final compaction to form a coating thereon of a substance which is less soluble in the liquid than the reactive material. The preferred reactive material is calcium hydride and the preferred coating is calcium carbonate with or without calcium hydroxide.Type: GrantFiled: February 28, 1994Date of Patent: November 21, 1995Assignees: British Aerospace PLC, BAeSEMA Ltd.Inventors: Peter C. Morgan, Alan D. Hart, Philip D. Morgans
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Patent number: 5366687Abstract: A method is taught for the preparation of ceramic fibers by electrophoretic deposition of metal oxide upon a conductive fiber core, which core may be subsequently removed.Type: GrantFiled: December 10, 1993Date of Patent: November 22, 1994Assignee: United Technologies CorporationInventors: William J. Dalzell, Jr., Robert J. Wright, Jarrett L. Spence
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Patent number: 5360494Abstract: A powdered magnesium composition is mixed with lithium dispersed in an inert, non-water absorbent, liquid medium to produce a substantially homogenous admixture that is heated to melt the lithium and vaporize the liquid medium to thereby obtain a decovered powdered alloy comprising aluminum and lithium. The liquid medium has first and second liquid constituents, wherein the first liquid constituent has a boiling point below the melting point of lithium and the second liquid constituent has a boiling point above the melting point of lithium but below the melting point of the alloy being produced.Type: GrantFiled: July 29, 1993Date of Patent: November 1, 1994Inventor: Sanford W. Brown
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Patent number: 5342572Abstract: In accordance with this invention, there is provided a process for producing a shaped article in which a reaction mixture containing at least two elemental materials is first charged into a die to form a shaped green body. A uniaxial pressure of from about 500 to about 5,000 pounds per square inch of cross-sectional area of the green body is then uniaxially applied to the green body, and the green body is then ignited; during ignition, the uniaxial pressure of from about 500 to about 5,000 pounds per square inch is maintained at a substantially constant level and continually applied to the reaction mixture.Type: GrantFiled: September 27, 1993Date of Patent: August 30, 1994Assignee: Alfred UniversityInventors: Gregory C. Stangle, William C. Williams
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Patent number: 5340533Abstract: A process for producing a dense composite material by combustion synthesis. In the first step of the process, a reaction mixture comprised of an elemental material is provided. The elemental material is charged to a die, a uniaxial pressure of from about 500 to about 5,000 pounds per square inch is applied to the elemental material within the die, and the elemental material within the die is ignited. Prior to, during, and subsequent to the time said elemental material is been ignited, the uniaxial pressure of from about 500 to about 5,000 pounds per square inch is applied to the elemental material within said die.Type: GrantFiled: April 27, 1993Date of Patent: August 23, 1994Assignee: Alfred UniversityInventors: Gregory C. Stangle, Scott E. Niedzialek, William C. Williams
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Patent number: 5340657Abstract: This invention relates to pillared micas, which comprise an active metal selected from the group consisting of Pt, Cr, Pd, It, Rh and mixtures thereof, and a first modifier metal selected from the group consisting of Sn, Ga and mixtures thereof. The mica may also be modified with a second modifier metal selected from the group consisting of alkali metals, alkaline earth metals, or rare earth metals and mixtures thereof. This invention further relates to a process for preparing such a catalyst.Type: GrantFiled: August 26, 1992Date of Patent: August 23, 1994Assignee: Exxon Research and Engineering CompanyInventors: Michael C. Kerby, Kenneth L. Riley, Fred M. Long, Jack W. Johnson, John F. Brody
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Patent number: 5198188Abstract: Disclosed is a method of producing dense refractory products, comprising:(a) obtaining a quantity of exoergic material in powder form capable of sustaining a combustion synthesis reaction;(b) removing absorbed water vapor therefrom;(c) cold-pressing said material into a formed body;(d) plasma spraying said formed body with a molten exoergic material to form a coat thereon; and(e) igniting said exoergic coated formed body under an inert gas atmosphere and pressure to produce self-sustained combustion synthesis.Also disclosed are products produced by the method.Type: GrantFiled: January 16, 1991Date of Patent: March 30, 1993Assignee: The United States of America as represented by the United States Department of EnergyInventors: J. Birch Holt, Michael Kelly
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Patent number: 5112572Abstract: The invention provides a method for removing the oxide surface from water atomized metal powders containing an oxidizer capable of oxidizing chromium from a trivalent to a soluble hexavalent state, whereby chromium oxides are removed from the metal powder surface. The powder is then treated with a dilute acid solution essentially devoid of hydrofluoric acid to remove other hydrated oxides from the metal powder surface. The powder is then water washed and dried.Type: GrantFiled: October 1, 1991Date of Patent: May 12, 1992Assignee: Inco LimitedInventors: Thijs Eerkes, James A. E. Bell, Carlos M. Diaz
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Patent number: 5059387Abstract: Shaped parts are formed from a powder having the desired chemistry of the finished part by mixing the powder with a thermosetting condensation resin that acts as a binder. The resin may be partially catalyzed, or additives or surfactants added to improve rheology, mixing properties, or processing time. Upon heating, the inherently low viscosity mixture will solidify without pressure being applied to it. A rigid form is produced which is capable of being ejected from a mold. Pre-sintered shapes or parts are made by injection molding, by using semi-permanent tooling, or by prototyping. Binder removal is accomplished by thermal means and without a separate debinding step, despite the known heat resistance of thermosetting resins. Removal is due to the film forming characteristic of the binder leaving open the part's pores, by providing oxidizing conditions within the part's pores as the part is heated, and by insuring that the evolving resin vapor diffuses through the pores by heating the part in a vacuum.Type: GrantFiled: June 2, 1989Date of Patent: October 22, 1991Assignee: Megamet IndustriesInventor: Gregory M. Brasel
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Patent number: 4960459Abstract: A method for pickling and consolidating water atomized metallic powders to reduce surface oxides. The technique includes introducing the powder into an acid bath--preferably nitric acid and hydrofluoric acid, rinsing the powder, introducing the powder into an alkaline bath, rinsing the powder and then consolidating the powder into a workpiece. Alternatively, the powder can be additionally introduced into a second acid bath and/or placed into a finishing boric acid bath before consolidation.Type: GrantFiled: September 19, 1988Date of Patent: October 2, 1990Assignee: Inco Alloys International, Inc.Inventors: Jon M. Poole, Lindy J. Curtis
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Patent number: 4957421Abstract: Titanium and titanium alloy surfaces can be diffusion coated, and portions of the surface protected against such coating by localized powdered masking layer of about 43% titanium, aluminum in an amount equal to the aluminum content of the surface masked, as well as other metals in an amount about one-fifth of their content in the surface masked. Diffusion coating can be speeded by high heat input. Diffusion coating packs can be made with chemically reduced metal content of sludges. Diffusion aliminizing followed by caustic leaching to remove much of the diffused-in aluminum, yields catalytically and pyrophorically active porous surface that also accepts top coatings. Mixtures of aluminum powder with nickel and/or iron powders react when heated to form Raney-like product that can be leached to become pyrophoric, and when held on a metal foil or gauze web will adhere to the web so that leached product can be used as pyrophoric foil for decoying heat-seeking missiles.Type: GrantFiled: April 10, 1989Date of Patent: September 18, 1990Assignee: Alloy Surfaces Company, Inc.Inventor: Alfonso L. Baldi
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Patent number: 4954169Abstract: Earth acid metal powders, such as tantalum or niobium, useful in the production of electrolytic capacitors and other electronic components, are agglomerates of sintered compacts, wherein the mean grain size of the agglomerates is no more than 2.0 .mu.m, determined by the Fisher Sub-Sieve Sizer, and wherein the agglomerates consist of primary individual agglomerated particles of mean grain size of no more than 0.7 .mu.m.Type: GrantFiled: June 12, 1989Date of Patent: September 4, 1990Assignee: Bayer AktiengesellschaftInventor: Dieter Behrens
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Patent number: 4946643Abstract: Dense, finely grained composite materials comprising one or more ceramic phase or phase and one or more metallic and/or intermetallic phase or phases are produced by combustion synthesis. Spherical ceramic grains are homogeneously dispersed within the matrix. Methods are provided, which include the step of applying mechanical pressure during or immediately after ignition, by which the microstructures in the resulting composites can be controllably selected.Type: GrantFiled: September 26, 1989Date of Patent: August 7, 1990Assignee: The United States of America as represented by the United States Department of EnergyInventors: Stephen D. Dunmead, Joseph B. Holt, Donald D. Kingman, Zuhair A. Munir
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Patent number: 4933025Abstract: A method for treating rare earth permanent magnetic material is disclosed. The treatment includes soaking ribbon rare earth permanent magnetic material consisting essentially of grains of the tetragonal crystal phase RE.sub.2 TM.sub.14 B where RE is neodymium and/or praseodymium or mixtures thereof with other rare earth elements and TM is iron or mixtures of iron and cobalt, cobalt in a soaking solution of either distilled water or phosphoric acid and manganese phosphate solution, draining off the soaking solution, rinsing with distilled water while agitating to separate and remove fine powdered magnetic material, and washing and drying the remaining powder or ribbons. The treated material is taken to substantial dryness before the material is incorporated into a permanent magnet.Type: GrantFiled: October 2, 1989Date of Patent: June 12, 1990Assignee: General Motors CorporationInventors: Erwin A. Alson, Thomas H. VanSteenkiste
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Patent number: 4879262Abstract: A self-sustaining combustion synthesis process for producing hard, tough, lightweight B.sub.4 C/TiB.sub.2 composites is based on the thermodynamic dependence of adiabatic temperature and product composition on the stoichiometry of the B.sub.4 C and TiB.sub.2 reactants. For lightweight products the composition must be relatively rich in the B.sub.4 C component. B.sub.4 C-rich composites are obtained by varying the initial temperature of the reactants. The product is hard, porous material whose toughness can be enhanced by filling the pores with aluminum or other metal phases using a liquid metal infiltration process. The process can be extended to the formation of other composites having a low exothermic component.Type: GrantFiled: July 28, 1988Date of Patent: November 7, 1989Assignee: The United States of America as represented by the United States Department of EnergyInventors: Danny C. Halverson, Beverly Y. Lum, Zuhair A. Munir
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Patent number: RE33243Abstract: The invention relates to a process for the treatment of a metal oxide powder, particularly a UO.sub.2 or PuO.sub.2 powder, with a view to its fritting.This process consists of oxidizing the powder, so as to form on its surface a hydrated oxide layer of the same metal. When the oxide is UO.sub.2 or PuO.sub.2 and mixtures thereof, as well as those prepared with ThO.sub.2, the treated powder can be used for producing nuclear fuel pellets by cold compression, followed by fritting.Type: GrantFiled: January 13, 1989Date of Patent: June 26, 1990Assignee: Commissariat a l'Energie AtomiqueInventors: Camille Braun, Joel Danroc, Bernard Francois, Jean Michel