Nitrate Patents (Class 423/395)
  • Patent number: 10957930
    Abstract: A solid alkaline fuel cell has a cathode that is supplied with an oxidant which contains oxygen, an anode that is supplied with a fuel which contains hydrogen atoms, and an inorganic solid electrolyte that is disposed between the anode and the cathode and that exhibits a hydroxide ion conductivity. The inorganic solid electrolyte enables the permeation of water of greater than or equal to 80 ?g/min·cm2 and less than or equal to 5400 ?g/min·cm2 per unit surface area of a cathode-side surface.
    Type: Grant
    Filed: March 7, 2019
    Date of Patent: March 23, 2021
    Inventors: Yukihisa Takeuchi, Hirofumi Kan, Toshiyuki Nakamura, Makoto Ohmori
  • Patent number: 10090523
    Abstract: Provided is a lithium cobalt composite oxide for a lithium secondary battery represented by Formula 1 below and having a polycrystalline state, a method of preparing the same, a positive electrode for a lithium battery including the lithium cobalt composite oxide, and a lithium secondary battery including a positive electrode, which includes the lithium cobalt composite oxide. LiaCobOc??Formula 1 In Formula 1, a is an integer from 0.9 to 1.1, b is an integer from 0.980 to 1.0000, and c is an integer from 1.9 to 2.1. Also included is a method of manufacture therefor.
    Type: Grant
    Filed: April 30, 2015
    Date of Patent: October 2, 2018
    Assignee: Samsung SDI Co., Ltd.
    Inventors: Jihyun Kim, Dohyung Park, Seonyoung Kwon, Juhyeong Han, Jinhwa Kim, Minhan Kim, Kyounghyun Kim
  • Patent number: 10011754
    Abstract: Method of maintaining or widening the long-term operating temperature range of a heat transfer medium and/or heat storage medium comprising a nitrate salt composition selected from the group consisting of alkali metal nitrate and alkaline earth metal nitrate and optionally alkali metal nitrite and alkaline earth metal nitrite, wherein the nitrate salt composition is brought into contact with an additive comprising the components nitric acid and/or nitrous acid and oxygen-comprising gas having an oxygen partial pressure which is equal to or greater than that in air and/or oxygen-generating compounds and optionally nitrogen oxides and/or compounds which generate further nitrogen oxide.
    Type: Grant
    Filed: January 23, 2014
    Date of Patent: July 3, 2018
    Assignee: BASF SE
    Inventors: Jürgen Wortmann, Michael Lutz, Johan ter Maat, Kerstin Schierle-Arndt, Stephan Maurer, Michael Ladenberger, Florian Garlichs, Katharina Kaleta
  • Patent number: 9656877
    Abstract: Provided is a method for manufacturing nanostructured layered double hydroxides (LDHs) having a uniform size distribution with homogenous nano-disc morphology. Disclosed method has three main steps of: pretreatment of metal wires; wire-explosion in a liquid phase; and finally, centrifugation and drying the as-prepared colloidal products to obtain the LDHs nanostructured dried powder.
    Type: Grant
    Filed: September 28, 2015
    Date of Patent: May 23, 2017
    Inventor: Cobra Rahmani Nezhad
  • Publication number: 20150093317
    Abstract: A novel method for making a CO2 capture agent is provided. The capture agent is made of a calcium/iron salt. The capture agent is prevented from degradation at high temperature. The capture agent is fit to be used at various temperatures in high CO2 densities for achieving high CO2 capture capacity, environmental protection and low power consumption.
    Type: Application
    Filed: September 30, 2013
    Publication date: April 2, 2015
    Applicant: Institute of Nuclear Energy Research, Atomic Energy Council, Executive Yuan, R.O.C.
    Inventors: Ching-Tsung Yu, San-Yuan Chen, Wei-Chin Chen, Po-Hsueh Chang
  • Patent number: 8986644
    Abstract: A method for preparing crystalline cobalt nitrate. The method includes: 1) calcining a spent Co/SiO2 catalyst, cooling the calcined material to room temperature, and grinding it to yield a powder; 2) heating the powder in a fluidized bed reactor; 3) adding the heated powder into excess dilute nitric acid solution and filtering to obtain a cobalt nitrate solution; 4) adjusting the pH value of the cobalt nitrate solution to 1.5, adding a preheated oxalic acid solution, adjusting a pH value of the resulting solution to 1.5, immediately filtering the resulting solution to yield a precipitate of cobalt oxalate, washing the precipitate of cobalt oxalate to yield a neutral filtrate; 5) drying the precipitate and calcining to yield cobalt oxide; 6) dissolving the cobalt oxide in nitric acid to yield a second cobalt nitrate solution; and 7) evaporating the second cobalt nitrate solution to obtain crystalline cobalt nitrate.
    Type: Grant
    Filed: September 5, 2014
    Date of Patent: March 24, 2015
    Assignee: Wuhan Kaidi Engineering Technology Research Institute Co., Ltd.
    Inventors: Yiming Han, Qianqian Liu, Bo Lai, Li Xu, Dechen Song
  • Patent number: 8871170
    Abstract: A process for producing KNO3 from polyhalite to is disclosed. In a preferred embodiment, the process comprises steps of (a) contacting polyhalite with HNO3; (b) adding Ca(OH)2 to the solution, thereby precipitating as CaSO4 at least part of the sulfate present in said solution; (c) precipitating as Mg(OH)2 at least part of the Mg2+ remaining in said solution by further addition of Ca(OH)2 to the remaining solution; (d) concentrating the solution, thereby precipitating as a sulfate compound at least part of the sulfate remaining in solution; (e) separating at least part of the NaCl from the solution remaining; and (f) crystallizing as solid KNO3 at least part of the K+ and NO3-contained in the solution. The process enables direct conversion of polyhalite to KNO3 of purity exceeding 98.5% and that is essentially free of magnesium and sulfate impurities.
    Type: Grant
    Filed: June 27, 2010
    Date of Patent: October 28, 2014
    Assignee: IMI TAMI Insitute for Research and Development
    Inventors: Michael Bonan, Eyal Ginzberg, Akiva Mozes, Eyal Barnea, Hugo Keselman, Gideon Friedman, Ron Frim, Cornelis Petrus Langeveld
  • Patent number: 8845993
    Abstract: A method of preparing purified barium nitrate includes precipitating barium nitrate crystals from a solution, and washing the barium nitrate crystals with an aqueous solution including at least 10 wt % nitric acid.
    Type: Grant
    Filed: January 20, 2011
    Date of Patent: September 30, 2014
    Assignee: EEStor, Inc.
    Inventors: Lucas Pettey, Richard D. Weir
  • Publication number: 20140286927
    Abstract: A engineered composition and method of delivery of said composition providing effective therapy for the treatment of ulcerative colitis, and Crohn's disease.
    Type: Application
    Filed: June 19, 2012
    Publication date: September 25, 2014
    Inventor: Peter Edward Smith
  • Patent number: 8753534
    Abstract: Formulations useful for preparing hydrous aluminum oxide gels contain a metal salt including aluminum, an organic base, and a complexing agent. Methods for preparing gels containing hydrous aluminum oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including aluminum, an organic base, and a complexing agent.
    Type: Grant
    Filed: January 7, 2010
    Date of Patent: June 17, 2014
    Inventor: Jack L. Collins
  • Publication number: 20140147367
    Abstract: A reaction-crystallization apparatus for carrying out reaction and/or solvent extraction and/or crystallization of soluble salts has an upper section having a top and a decanter. The decanter has a vertical vessel having a horizontal weir at the top of the upper section. The top of the upper section has an outlet for removing a light phase at the top of the decanter. The apparatus has a lower section, including a crystallizer. The crystallizer includes: a coaxial draft tube; a feed pipe; an agitator inside the draft tube; and at least one outlet at the bottom for crystal slurry removal. The apparatus has an intermediate section sandwiched between the lower section and the upper section such that the sections are in fluid communication and includes at least one coaxial vertical baffle with a gap between the draft tube and the coaxial vertical baffle and is adjustable by moving the baffle.
    Type: Application
    Filed: March 29, 2012
    Publication date: May 29, 2014
    Inventor: Tamar ZIV
  • Publication number: 20130323156
    Abstract: Provided is a method and an apparatus for purifying potassium nitrate from the solid waste produced by a chemical glass-strengthening process. In the method, the solid waste is melted into a liquid waste at first. Potassium nitrate of various purity grades can be obtained by batch processing the liquid waste through stepwise cooling processes of cooling the liquid waste to a first temperature facilitating the potassium nitrate contained in the liquid waste to be crystallized at a first rate and then cooling the liquid waste to a second temperature close to the freezing point of the potassium nitrate at a second rate that is slower than the first rate. The recovered potassium nitrate from the solid waste can be recycled and reused.
    Type: Application
    Filed: January 17, 2013
    Publication date: December 5, 2013
    Applicant: NATIONAL FORMOSA UNIVERSITY
    Inventor: Min-Hui YANG
  • Patent number: 8524114
    Abstract: A method of producing anhydrous calcium nitrate, anhydrous magnesium nitrate or mixture thereof involves removing water from a solution of calcium nitrate, magnesium nitrate or mixture thereof in a pulse combustion drier. The invention also provides a mixture of anhydrous calcium nitrate, anhydrous magnesium nitrate and the individual anhydrous nitrate salts in a sealed container.
    Type: Grant
    Filed: July 27, 2006
    Date of Patent: September 3, 2013
    Assignees: John Arthur Bewsey, Alastair James Forsyth
    Inventor: John Arthur Bewsey
  • Publication number: 20130171053
    Abstract: The present invention relates to a method for converting nitrogen (N2) into nitrate and/or ammonia comprising the steps of compressing air and separating nitrogen (N2) and oxygen (O2) therefrom, and either reacting earth alkaline metal with oxygen to produce earth alkaline metal oxide, using the high temperatures obtained to react N2 and O2 to NO, converting the NO with O2 to NO2, followed by the reaction of NO2 with water to result in HNO3 and NO; or reacting the nitrogen obtained with earth alkaline metal to produce earth alkaline metal nitride and reacting thereof with water to result in earth alkaline metal hydroxide and ammonia.
    Type: Application
    Filed: December 27, 2012
    Publication date: July 4, 2013
    Applicant: KING SAUD UNIVERSITY
    Inventor: KING SAUD UNIVERSITY
  • Publication number: 20130149229
    Abstract: In various embodiments, the present disclosure provides a method of fixing nitrogen. An amount of titania catalyst is provided and contacted with a feed stream that includes nitrogen. The titania catalyst is heated. The heated titania catalyst fixes nitrogen in the feed stream to form nitrogen products, such as nitrates. The nitrogen products are then removed from the titania catalyst. In some examples, the titania catalyst is treated with a base. In further examples, the catalytic process is carried out in the absence of light for photochemically activating the titania catalyst.
    Type: Application
    Filed: May 3, 2012
    Publication date: June 13, 2013
    Inventors: Glenn C. Miller, Ahmed A. Al-Taani
  • Patent number: 8388916
    Abstract: A method for the production of KNO3 from polyhalite is provided. The method comprises steps of decomposing said polyhalite into syngenite, gypsum, and soluble components, treating the solid decomposition products sequentially with HNO3 and Ca basic compound, precipitating the CaSO4 thus formed, and crystallizing the KNO3 from the solution remaining. The method recovers up to 75% of the potassium present in the raw polyhalite as KNO3 and substantially all of the remainder as a potassium magnesium sulfate salt.
    Type: Grant
    Filed: June 27, 2010
    Date of Patent: March 5, 2013
    Assignee: IMI Tami Institute for Research and Development
    Inventors: Michael Bonan, Eyal Ginzberg, Akiva Mozes, Eyal Barnea, Hugo Keselman, Gideon Friedman, Ron Frim, Cornelis Petrus Langeveld
  • Publication number: 20120252999
    Abstract: Systems and methods of producing chemical compounds are disclosed. An example chemical production system includes a combustion chamber having intake ports for entry of a gas mixture. An igniter ignites the gas mixture in the intake chamber to facilitate a reaction at a high temperature and high pressure. A nozzle restricts exit of the ignited gas mixture from the combustion chamber. An expansion chamber cools the ignited gas. The expansion chamber has an exhaust where the cooled gas exits the expansion chamber. A chemical compound product is formed in the expansion chamber.
    Type: Application
    Filed: April 12, 2012
    Publication date: October 4, 2012
    Inventor: Bruce H. Peters
  • Patent number: 8268269
    Abstract: As population density increases, the transportation of hazardous chemicals, including acids and disinfectants, lead to an increased incidence of spills while the consequences of spills become more serious. While solutions of halide acids, hypohalites and halites are safer disinfectants for transportation, handling, storage and use than traditional gaseous chlorine, the manufacturing cost of these disinfectants has here-to-fore limited their use. Economical processes are presented for the manufacture of O2, halogen oxides, halide acids, hypohalites, and halates; as well as polynucleate metal compounds, metal hydroxides and calcium sulfate hydrate (gypsum). The instant invention presents methods and processes that incorporate the use of sulfur. This is while environmental regulators, such as the US EPA, require an increased removal of sulfur from hydrocarbon fuels, thereby creating an abundance of sulfur, such that the refining industry is in need of a way to dispose of said abundance of sulfur.
    Type: Grant
    Filed: July 23, 2007
    Date of Patent: September 18, 2012
    Inventors: Richard Alan Haase, John Smaardyk
  • Publication number: 20120219638
    Abstract: The present invention includes antimicrobial silver-containing compositions that are effective in treating Erwinia species bacteria. These compositions are particularly effective for treating plants susceptible to Erwinia species infections.
    Type: Application
    Filed: November 21, 2011
    Publication date: August 30, 2012
    Inventors: Merle E. Olson, Michael W. Harding
  • Publication number: 20120201737
    Abstract: A method for the production of KNO3 from polyhalite is provided. The method comprises steps of decomposing said polyhalite into syngenite, gypsum, and soluble components, treating the solid decomposition products sequentially with HNO3 and Ca basic compound, precipitating the CaSO4 thus formed, and crystallizing the KNO3 from the solution remaining. The method recovers up to 75% of the potassium present in the raw polyhalite as KNO3 and substantially all of the remainder as a potassium magnesium sulfate salt.
    Type: Application
    Filed: June 27, 2010
    Publication date: August 9, 2012
    Applicant: IMI TAMI Institute for Research and Development
    Inventors: Michael Bonan, Eyal Ginzberg, Akiva Mozes, Eyal Barnea, Hugo Keselman, Gideon Friedman, Ron Frim, Cornelis Petrus Langeveld
  • Publication number: 20120195818
    Abstract: A process for producing KNO3 from polyhalite to is disclosed. In a preferred embodiment, the process comprises steps of (a) contacting polyhalite with HNO3; (b) adding Ca(OH)2 to the solution, thereby precipitating as CaSO4 at least part of the sulfate present in said solution; (c) precipitating as Mg(OH)2 at least part of the Mg2+ remaining in said solution by further addition of Ca(OH)2 to the remaining solution; (d) concentrating the solution, thereby precipitating as a sulfate compound at least part of the sulfate remaining in solution; (e) separating at least part of the NaCl from the solution remaining; and (f) crystallizing as solid KNO3 at least part of the K+ and NO3-contained in the solution. The process enables direct conversion of polyhalite to KNO3 of purity exceeding 98.5% and that is essentially free of magnesium and sulfate impurities.
    Type: Application
    Filed: June 27, 2010
    Publication date: August 2, 2012
    Applicant: IMI TAMI INSTITUTE FOR RESEARCH AND DEVELOPMENT
    Inventors: Michael Bonan, Eyal Ginzberg, Akiva Mozes, Eyal Barnea, Hugo Keselman, Gideon Friedman, Ron Frim, Cornelis Petrus Langeveld
  • Publication number: 20120141745
    Abstract: A chiral liquid crystal precursor composition which comprises at least one salt that changes a position of the selective reflection band exhibited by the composition in a cured state compared to the position of a selective reflection band exhibited by a composition in the cured state that does not contain the at least one salt. This abstract is neither intended to define the invention disclosed in this specification nor intended to limit the scope of the invention in any way.
    Type: Application
    Filed: December 7, 2011
    Publication date: June 7, 2012
    Applicant: SICPA HOLDING SA
    Inventors: Andrea CALLEGARI, Tristan JAUZEIN
  • Patent number: 8178068
    Abstract: A catalyst charge for ammonia oxidation, including the Andrussow process, comprises a first stage ammonia oxidation catalyst capable of oxidizing 20 to 99% of designed ammonia throughput, to produce a first stage product gas comprising unreacted ammonia, oxygen and nitrogen oxides, and a second stage ammonia oxidation catalyst capable of completing the oxidation of unreacted ammonia. Low levels of nitrous oxide are produced an extended campaign lengths may be seen.
    Type: Grant
    Filed: April 27, 2004
    Date of Patent: May 15, 2012
    Assignee: Johnson Matthey PLC
    Inventors: Sean Alexander Axon, Duncan Roy Coupland, Brian Thomas Horner, John Ridland, Ian Carmichael Wishart
  • Publication number: 20120114768
    Abstract: An angiogenesis regulating composition used to treat/prevent an angiogenic disease in a subject, that contains in an effective amount at least one of nitrate, nitrite, and a compound convertible into nitrate or nitrite after the compound is absorbed into the subject, and an angiogenesis regulation method administering to a subject a composition containing as an active ingredient at least one of nitrate. nitrite, and a compound convertible into nitrate or nitrite after the compound is absorbed into the subject, provide a composition effective in treating and preventing angiogenic diseases, that can medically control angiogenic diseases, and medically regulate angiogenesis in ophthalmologic diseases in particular, and allows treatment without inhibiting physiological neovascularization, with a limited side effect and significantly safely, and an angiogenesis regulation method using the same.
    Type: Application
    Filed: July 12, 2010
    Publication date: May 10, 2012
    Inventors: Junya Fujimori, Hidekazu Baba, Toshinori Murata
  • Patent number: 8088349
    Abstract: Disclosed is a clean method for preparing layered double hydroxides (LDHs), in which hydroxides of different metals are used as starting materials for production of LDHs by atom-economical reactions. The atom efficiency of the reaction is 100% in each case because all the atoms of the reactants are converted into the target product since only M2+(OH)2, M3+(OH)3, and CO2 or HnAn? are used, without any NaOH or other materials. Since there is no by-product, filtration or washing process is unnecessary. The consequent reduction in water consumption is also beneficial to the environment.
    Type: Grant
    Filed: September 11, 2007
    Date of Patent: January 3, 2012
    Assignee: Beijing University of Chemical Technology
    Inventors: Xue Duan, Dianqing Li, Zhi Lv, Yanjun Lin, Xiangyu Xu
  • Publication number: 20110275518
    Abstract: The present invention is compositions and methods for improving seed germination rates or speed using a composition comprising at least one high valency silver ion. The compositions and methods of the present invention are effective in treating biofilms.
    Type: Application
    Filed: June 9, 2008
    Publication date: November 10, 2011
    Inventors: Lyriam L. Marques, Merle E. Olson, Michael W. Harding
  • Patent number: 8008225
    Abstract: A substrate, such as a glass, glass ceramic, ceramic or metal substrate, is provided with a thermocatalytically active coating on at least a part of the substrate surface. The thermocatalytic coating contains an inorganic lithium salt or organic lithium-containing compound in an amount that is equivalent to not less than 2 wt. % of lithium ions, based on total coating weight. The thermocatalytic coating has a glass, glass solder or sol-gel matrix in which the lithium salt or organic lithium-containing compound is introduced. Optional barrier and IR-reflecting layers are arranged between the substrate surface and the thermocatalytically active coating.
    Type: Grant
    Filed: August 21, 2009
    Date of Patent: August 30, 2011
    Assignee: SCHOTT AG
    Inventors: Inka Henze, Hrabanus Hack, Gerhard Weber, Hans-Joachim Schmitt, Wolfgang Schmidbauer, Torsten Gabelmann
  • Publication number: 20110206595
    Abstract: A method of preparing purified barium nitrate includes precipitating barium nitrate crystals from a solution, and washing the barium nitrate crystals with an aqueous solution including at least 10 wt % nitric acid.
    Type: Application
    Filed: January 20, 2011
    Publication date: August 25, 2011
    Applicant: EESTOR, INC.
    Inventors: Lucas Pettey, Richard D. Weir
  • Publication number: 20110038809
    Abstract: The present invention provides methods for treating or preventing diseases and disorders caused by iron-dependent pathogenic microorganisms, such as bacteria, fungi, and parasites, by applying a gallium compound to an affected area. In particular, the present invention provides methods for treating or preventing dental caries, vaginal infections, skin infections, and so forth. Gallium compounds can be formulated as toothpaste, mouthwash, cream, ointment, gel, solution, eye drops, suppository, and the like. Furthermore, the invention provides methods for controlling microbial growth on environmental surfaces, including those of toothbrush, denture, dental retainer, contact lens, catheter, food stuff, and so forth. In addition, the present invention provides animal feeds which contain gallium compounds that promote the animal growth and prevent the animals from infections as well as protect consumers from post processing infections.
    Type: Application
    Filed: October 31, 2006
    Publication date: February 17, 2011
    Inventors: Daniel P. Perl, Sharon Moalem
  • Publication number: 20100290974
    Abstract: A titanium dioxide coating method is disclosed. An electrolyte containing Ti3+ and at least one of NO3? and NO2? is provided for an electrodeposition device. A substrate is immersed into the electrolyte and electrically connected to the electrodeposition device. A cathodic current is applied to the substrate via the electrodeposition device for reduction of NO2? or NO3?. A titanium dioxide film is thus formed on the surface of the substrate. The thickness, porosity, and morphology of the titanium dioxide film can be controlled by varying the electroplating parameters, and relatively uniform deposits on complex shapes can be obtained by use of low cost instruments.
    Type: Application
    Filed: July 20, 2009
    Publication date: November 18, 2010
    Inventors: Chi-Chang HU, Ching-Chun HUANG, Kuo-Hsin CHANG
  • Patent number: 7799296
    Abstract: A method for converting nickel into a nickel salt solution. Nickel is dissolved and reacted in an oxygen-enriched acidic solution to produce a nickel salt solution as illustrated in the following chemical equation, wherein X is a conjugate base: Ni+H2X+½O2->NiX+H2O.
    Type: Grant
    Filed: November 8, 2005
    Date of Patent: September 21, 2010
    Assignee: Ovonic Battery Company, Inc.
    Inventors: Michael A. Fetcenko, Cristian Fierro, Avram Zallen, Tim Hicks
  • Publication number: 20100104493
    Abstract: Devices and components that can interact with or modify propagation of electromagnetic waves are provided. The design, fabrication and structures of the devices exploit the properties of reactive composite materials (RCM) and reaction products thereof.
    Type: Application
    Filed: March 11, 2009
    Publication date: April 29, 2010
    Inventors: Roderick A. Hyde, Muriel Y. Ishikawa, Edward K.Y. Jung, Jordin T. Kare, Nathan P. Myhrvold, Thomas J. Nugent, JR., Clarence T. Tegreene, Charles Whitmer, Lowell L. Wood, JR.
  • Publication number: 20100092441
    Abstract: Inorganic anions nitrate and nitrite influence metabolic rate and glucose homeostasis. Infusion of nitrite iv caused an acute drop in resting energy expenditure (oxygen consumption) and nitrate, when given perorally, caused a drop in oxygen consumption during exercise and a depression of the increase in blood glucose observed after an oral glucose tolerance test. The doses of nitrate and nitrite did not cause any detectable change in methemoglobin levels of blood. Also, nitrate and nitrite did not alter lactate levels in blood. This discovery provides useful treatments to regulate the energy expenditure and glucose homeostasis of a mammal by administration of inorganic nitrite and/or nitrate.
    Type: Application
    Filed: February 26, 2008
    Publication date: April 15, 2010
    Inventors: Jon Lundberg, Eddie Weitzberg
  • Publication number: 20100056362
    Abstract: A substrate, such as a glass, glass ceramic, ceramic or metal substrate, is provided with a thermocatalytically active coating on at least a part of the substrate surface. The thermocatalytic coating contains an inorganic lithium salt or organic lithium-containing compound in an amount that is equivalent to not less than 2 wt. % of lithium ions, based on total coating weight. The thermocatalytic coating has a glass, glass solder or sol-gel matrix in which the lithium salt or organic lithium-containing compound is introduced. Optional barrier and IR-reflecting layers are arranged between the substrate surface and the thermocatalytically active coating.
    Type: Application
    Filed: August 21, 2009
    Publication date: March 4, 2010
    Inventors: Inka Henze, Hrabanus Hack, Gerhard Weber, Hans-Joachim Schmitt, Wolfgang Schmidbauer, Torsten Gabelmann
  • Patent number: 7648687
    Abstract: Purification techniques have been developed for ceramic powder precursors, e.g., barium nitrate. These techniques can be performed using one or more of the following operations: (1) removal of impurities by precipitation or coprecipitation and separation using a nonmetallic-ion-containing strong base, e.g., tetraalkylammonium hydroxides; (2) reduction of higher oxidation-state-number oxymetal ions and subsequent precipitation as hydroxides that are separated from the solution; and (3) use of liquid-liquid exchange extraction procedures to separate certain impurities.
    Type: Grant
    Filed: June 15, 2006
    Date of Patent: January 19, 2010
    Assignee: EEStor, Inc.
    Inventors: Richard D. Weir, Carl W. Nelson
  • Patent number: 7635459
    Abstract: Disclosed is a method of removing nitric acid from an aqueous liquid containing various components such as vegetable extract, and nitrate ion is removed selectively without spoiling the taste or other components, by subjecting the aqueous liquid to chromatographic treatment with an amphoteric ion exchanger to separate nitrate ion from other components contained in the aqueous liquid. A nitric acid-reduced drink is produced by preparing a raw drink material comprising an extract or juice of plant tissue; removing nitric acid from the raw drink material with use of the method of removing nitric acid from an aqueous liquid as described above; and preparing a drink using the raw drink material after the removing of nitric acid.
    Type: Grant
    Filed: September 20, 2005
    Date of Patent: December 22, 2009
    Assignee: ITO EN, Ltd.
    Inventors: Takanobu Takihara, Yuji Kubota
  • Publication number: 20090169807
    Abstract: Methods for assembly of monolayers of nanoparticles using the Langmuir-Blodgett technique, as well as monolayers, assemblies, and devices are described. The surface properties of these monolayers are highly reproducible and well-defined as compared to other systems. These monolayers can readily be used for molecular detection in either an air-borne or a solution environment, and sensors using the monolayer could have significant implications in chemical and biological warfare detection, national and global security, as well as in medical detection applications.
    Type: Application
    Filed: December 2, 2008
    Publication date: July 2, 2009
    Applicant: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
    Inventors: Peidong Yang, Franklin Kim, Andrea Tao, Christian Hess
  • Publication number: 20090130016
    Abstract: Provided is a thermionic cathode doped with an increased binding energy hydrogen species and a method of making the doped thermionic cathode.
    Type: Application
    Filed: May 21, 2008
    Publication date: May 21, 2009
    Inventor: Randell L. Mills
  • Patent number: 7517514
    Abstract: A process for treating organic material, separating calcium and recovering phosphorus and to utilization of the obtained products and their use as a soil conditioner and a fertilizer as well as for providing carbon dioxide traps in gas cleaning. In the process, organic ingredients are separated from calcium-phosphate-containing ingredients, the calcium-phosphate-containing ingredients are dissolved in an acid-containing solution and/or the calcium is precipitated as a salt corresponding to the acid, and optionally phosphoric acid formed from a phosphate ion is separated. The invention also relates to a calcium-carbonate-containing product and a phosphoric-acid containing product, which are prepared by the process of the invention.
    Type: Grant
    Filed: June 2, 2003
    Date of Patent: April 14, 2009
    Assignee: Preseco Oy
    Inventor: Jussi Järventie
  • Publication number: 20090028770
    Abstract: The present invention provides a method for advantageously producing an iron oxyhydroxide exhibiting excellent capability of adsorbing harmful substances, such as a phosphrous components and endocrine disrupting chemicals, which are contained in industrial wastewater, exhaust gases, etc., and an adsorbent material comprising the iron oxyhydroxide produced by the method as a main component. Specifically, the present invention provides an adsorbent material produced by a method comprising the steps of: (a) adding a base to an aqueous iron ion-containing solution, adjusting the pH of the resultant mixture to 9 or less, to form a precipitate that contains an iron oxyhydroxide; (b) drying the precipitate at a temperature of 100° C. or lower to obtain an iron oxyhydroxide; (c) contacting the resultant iron oxyhydroxide with water; and (d) subjecting the resultant iron oxyhydroxide to a heat treatment under a gas atmosphere having an inert gas concentration of 80% or greater at a temperature of 100 to 280° C.
    Type: Application
    Filed: February 16, 2006
    Publication date: January 29, 2009
    Applicants: JAPAN SCIENCE AND TECHNOLOGY AGENCY, SHIGA PREFECTURE INDUSTRIAL SUPPORT CENTER, KYOTO UNIVERSITY
    Inventors: Kazuhiro Mae, Taisuke Maki, Atsushi Yamamoto
  • Patent number: 7462342
    Abstract: A process in which a basic metal nitrate is obtained in a high yield is provided. A process for producing a basic metal nitrate, which comprises adding an aqueous solution of a metal nitrate or an aqueous solution of a mixture of a metal nitrate and a water-soluble additive and an alkali solution to a reaction vessel in which a reaction solvent whose pH at 20° C. is adjusted to 6 or less is present, and conducting the reaction with stirring.
    Type: Grant
    Filed: March 27, 2002
    Date of Patent: December 9, 2008
    Assignee: Daicel Chemical Industries, Ltd.
    Inventors: Shogo Tomiyama, Xingxi Zhou
  • Publication number: 20080217894
    Abstract: A gas generant composition used in pressure activated restraint system devices such as micro-gas generator applications such as seat belt pretensioners is provided. The gas generant composition includes a potassium perchlorate gas generant additive in addition to a non-azide nitrogen-containing gas generating fuel, a metal ammine nitrate oxidizer, and a metal oxide burn rate enhancing and slag formation additive. The gas generant composition desirably has improved ignitability as compared to a similar composition without the potassium perchlorate gas generant additive. The gas generant composition also desirably produces or results in effluents having either or both reduced carbon monoxide and NOx contents as compared to the effluent produced or resulting from a similar composition but without the inclusion of the potassium perchlorate gas generant additive.
    Type: Application
    Filed: October 19, 2007
    Publication date: September 11, 2008
    Inventors: Ivan V. Mendenhall, Robert G. Smith
  • Publication number: 20080171392
    Abstract: The present invention relates generally to kits, compositions and methods useful in the qualitative analysis of the presence of chemicals used and produced in the manufacture of illegal drugs. The compositions and methods may be useful for, among other things, qualitatively determining whether items of real or personal property or other chattels have been exposed to the manufacture of illegal drugs or whether such items have been contaminated by illegal drugs.
    Type: Application
    Filed: January 14, 2008
    Publication date: July 17, 2008
    Applicant: BOARD OF TRUSTEES OF THE UNIVERSITY OF ARKANSAS
    Inventor: J. Jennifer Wu
  • Publication number: 20080153735
    Abstract: This invention includes a cleaning composition, the method of use of the cleaning composition, and a new use of a composition. The composition includes an oxidizing agent with a reduction potential of greater than about 0.1 E°(V) at 25° C., and is devoid of an oxidizing agent with a reduction potential of greater than about 1.5 E°(V) at 25° C. The oxidizing agent may be a salt of a nitrate or nitrite. The method includes applying the composition to a textile and working the composition. The composition may be effective in cleaning urine odors from textiles. The composition may remove odors from textiles without bleaching or discoloring the textile, even if the textile includes natural fibers such as wool.
    Type: Application
    Filed: June 19, 2007
    Publication date: June 26, 2008
    Applicant: HARRIS RESEARCH, INC.
    Inventor: Edward E. Durrant
  • Publication number: 20080113102
    Abstract: Agents for surface treatment which can impart excellent corrosion resistance to zinc or zinc alloy products at low cost. The agents for the surface treatment of zinc or zinc alloy products of this invention include at least one water-soluble compound which contains antimony, bismuth, tellurium or tin. Ideally, a nickel salt and/or a manganese salt is also included, and most desirably tannins and/or thioureas are also included. Ideally, the zinc or zinc alloy products which have been immersed and treated in an aqueous solution which contains these agents for surface treatment are immersed in an aqueous solution which includes a sealing treatment agent selected according to the colour of the zinc or zinc alloy product to seal pinholes.
    Type: Application
    Filed: November 13, 2006
    Publication date: May 15, 2008
    Inventors: Takashi Arai, Ro Bo Shin, Takahisa Yamamoto
  • Patent number: 7371357
    Abstract: A process for the removal of pollutants from a combustion process and, more particularly, a process for removing pollutants such as carbon dioxide, mercury, sulphur dioxide, nitrogen compounds and oxygen compounds from a combustion process. The process includes the removal of pollutants from a combustion process that produces an emission comprising: cooling the emission to a temperature of about 200° C.; removing nitrogen, water and oxygen from the emission to produce a gas containing a concentration of pollutants; contacting the gas with an aqueous magnesium chloride solution, wherein a slurry mixture is formed; and cooling the gas and the slurry mixture, wherein hydrochloric acid vapour and a sludge are formed.
    Type: Grant
    Filed: October 28, 2005
    Date of Patent: May 13, 2008
    Assignee: Clean World Strategies Corp.
    Inventors: Lionel Magumbe, Douglas S. Scott
  • Patent number: 7105136
    Abstract: In a method for preparing copper salts from at least one cupriferous and one additional reactant, the reactants are used to prepare micro-emulsions while employing at least one block polymer, the intermediate products obtained this way are mixed and reacted together so as to form a micro-emulsion. The preparation of the starting micro-emulsion as well as the subsequent joint reaction preferably occur either with ultrasound or in a high-pressure homogenizer. The copper salts obtained this way exhibit a particle size of less than 50 nm, preferably 5 to 20 nm and can be adjusted to specific applications through the appropriate doping of foreign ions.
    Type: Grant
    Filed: September 27, 2002
    Date of Patent: September 12, 2006
    Assignee: Spiess-Urania Chemicals GmbH
    Inventors: Hartmut Ploss, Gerhard Goebel, André Simon
  • Patent number: 6949236
    Abstract: Addition of an aminosulfonate product to an inorganic nitrogen-containing salt provides a composition of matter with improved properties. In particular, 2-acrylamido-2-methylpropanesulfonic acid and its derivatives can be added to ammonium nitrate to provide improved prills.
    Type: Grant
    Filed: November 6, 2001
    Date of Patent: September 27, 2005
    Assignee: The Lubrizol Corporation
    Inventors: Kastrui Lal, Alvin E. Haas, Ricardo M. Collins, Jeffrey M. Carey
  • Patent number: 6911188
    Abstract: The invention relates a process for producing an alkali metal nitrate and an alkali metal phosphate in the same process from a phosphate raw material and a nitrate raw material comprising the steps of: a) reacting the phosphate raw material with the nitrate raw material to provide an aqueous nitrophosphate feed, optionally followed by the separation of solid material, b) introducing the aqueous nitrophosphate feed into a first ion exchange step comprising an alkali metal-loaded cationic exchange resin for exchanging cations present in the feed with alkali metal ions present on the resin to obtain a stream enriched in alkali metal ions, c) subjecting the stream from step (b) to a first crystallization under such conditions that an alkali metal nitrate is crystallized and separating the crystallized alkali metal nitrate from the mother liquor, d) introducing the mother liquor from step (c) into a second ion exchange step comprising an alkali metal-loaded cationic exchange resin for exchanging cations present
    Type: Grant
    Filed: December 1, 2000
    Date of Patent: June 28, 2005
    Assignee: Kemira Growhow Oy
    Inventor: Flemming Mathiesen
  • Patent number: 6899858
    Abstract: A method of preparing a hafnium nitrate thin film includes placing phosphorus pentoxide in a first vessel; connecting the first vessel to a second vessel containing hafnium tetrachloride; cooling the second vessel with liquid nitrogen; dropping fuming nitric acid into the first vessel producing N2O5 gas; allowing the N2O5 gas to enter the second vessel; heating the first vessel until the reaction is substantially complete; disconnecting the two vessels; removing the second vessel from the liquid nitrogen bath; heating the second vessel; refluxing the contents of the second vessel; drying the compound in the second vessel by dynamic pumping; purifying the compound in the second vessel by sublimation to form Hf(NO3)4, and heating the Hf(NO3)4 to produce HfO2 for use in an ALCVD process.
    Type: Grant
    Filed: January 23, 2003
    Date of Patent: May 31, 2005
    Assignee: Sharp Laboratories of America, Inc.
    Inventors: Wei-Wei Zhuang, David R. Evans, Sheng Teng Hsu