Including Vaporization, E.g., Distillation, Concentration-evaporation, Etc. Patents (Class 426/492)
  • Patent number: 5637339
    Abstract: A tar-depleted liquid smoke having total water miscibility, and related method for making same. The tar-depleted liquid smoke may be made from commercially existing liquid smoke products, for instance, by treating such a commercial product with a column filtration process using activated carbon particles packed in the column. The resultant tar-depleted liquid smoke typically will have a phenols reduction of about 10% to about 90% compared to the commercial starting product of liquid smoke. In an alternative embodiment, the tar-depleted liquid smoke made from carbon contact is then vacuum concentrated so that it has a phenols content greater than that of the commercial starting product of liquid smoke, but the concentrate will still be totally water miscible.
    Type: Grant
    Filed: April 27, 1995
    Date of Patent: June 10, 1997
    Assignee: Hickory Specialties, Inc.
    Inventor: Patrick W. Moeller
  • Patent number: 5626756
    Abstract: In order to fractionate or/and refine natural lipid materials by extraction with compressed gases, the natural materials are used in a liquid form and they are extracted with a liquid mixture of 50 to 90% by weight propane and 10 to 50% by weight carbon dioxide which is in a subcritical state.
    Type: Grant
    Filed: December 27, 1995
    Date of Patent: May 6, 1997
    Assignee: SKW Trostberg Aktiengesellschaft
    Inventors: Jurgen Heidlas, Georg Huber
  • Patent number: 5620728
    Abstract: The present invention pertains to a method of obtaining oil from grain materials such as rice bran, wheat mill feed, rapeseed, amaranth, and similar grains.
    Type: Grant
    Filed: November 17, 1994
    Date of Patent: April 15, 1997
    Assignee: Food Sciences, Inc.
    Inventors: Charles E. Langley, Stanley Finelt
  • Patent number: 5597602
    Abstract: A process for recovering lecithin from oil- and lecithin-containing mixtures, comprising extracting a lecithin/oil mixture with an extractant selected from the group consisting of a hydrocarbon having 3 carbon atoms, an unbranched hydrocarbon having 4 carbon atoms, a branched hydrocarbon having 4 carbon atoms, and mixtures thereof, at a pressure of from 1 to 8 MPa and a temperature of from 20 to 100.degree. C., which conditions ensure liquid phase extraction with the development of two liquid phases, one of which is an oil enriched liquid hydrocarbon phase and the other of which is a lecithin enriched hydrocarbon phase; separating the two liquid hydrocarbon phases; and recovering substantially lecithin-free oil from the oil-enriched phase and substantially oil-free, pure lecithin from the lecithin-enriched phase.
    Type: Grant
    Filed: April 21, 1995
    Date of Patent: January 28, 1997
    Assignee: Siegfried Peter
    Inventors: Siegfried Peter, Bernd Czech, Eckard Weidner, Zhenfeng Zhang
  • Patent number: 5558893
    Abstract: A process is disclosed for the preparation of citrus oils which are essentially pesticide free. The essentially pesticide-free citrus oil is prepared by gently distilling raw citrus oil in a short-path distillation column whereby the essentially pesticide-free citrus peel oil is collected as the distillant. Suitable citrus oils include citrus peel oils and citrus stripper oils with citrus peel oils being preferred. The essentially pesticide-free citrus peel oil generally contains less than about 1.6 ppm total pesticides, preferably less than about 0.5 ppm total pesticides, more preferably less than 0.1 ppm total pesticides, and most preferably less than 0.05 ppm total pesticides. The distillation residue contains essentially all the pesticides contained in the raw citrus peel oil.
    Type: Grant
    Filed: March 27, 1995
    Date of Patent: September 24, 1996
    Assignee: Cargill, Incorporated
    Inventor: Harapanahalli S. Muraldihara
  • Patent number: 5534274
    Abstract: This invention relates to a novel method and system for recovering water from fruit. Water is evaporated from juice during a concentration process. The water can be bottled and distributed to consumers. Water vapor is condensed and water is collected. Preferably, a distribution cone is used for evaporating the water vapor. The water produced has improved purity characteristics.
    Type: Grant
    Filed: June 1, 1994
    Date of Patent: July 9, 1996
    Inventor: Donald DeStefano
  • Patent number: 5518751
    Abstract: The invention relates to a process for the preparation of milk and milk powders having a long storage life utilizing techniques which are known per se. To that end, a milk liquid is prepared, which is evaporated, and a fat fraction is added to the milk liquid in one or more effects of the evaporator. This process is particularly suitable for the preparation of a milk having a long storage life, in which unsaturated fatty acid chains are present.
    Type: Grant
    Filed: September 8, 1994
    Date of Patent: May 21, 1996
    Assignee: Friesland Brands B.V.
    Inventors: Cor de Boer, Ellert Camminga, Cornelis Glas, Rienk Weerstra
  • Patent number: 5468511
    Abstract: A method for extraction and removal of cholesterol from untreated liquid egg yolk with simultaneous production of cholesterol as a by-product. The removal of cholesterol from the untreated liquid egg yolk is achieved by the extraction of cholesterol into a vegetable oil by ultra high pressure homogenization producing liquid egg yolk having reduced amount of cholesterol. The cholesterol extracted into the vegetable oil is further removed from the oil by steam stripping method, allowing a recycling of the steam stripped extraction oil. Cholesterol is recovered as the extraction by-product from the aqueous steam stripping distillate.
    Type: Grant
    Filed: July 6, 1993
    Date of Patent: November 21, 1995
    Assignee: The Regents of the University of California
    Inventor: Gideon Zeidler
  • Patent number: 5425962
    Abstract: The present invention provides a method for refining peppermint oil containing compositions. Additionally, the present invention provides a method for making chewing gum having a peppermint flavor. To this end, a method for refining a peppermint oil containing composition that includes sulfur compounds to remove at least a portion of the sulfur compounds is provided. The method comprises the step of subjecting the composition to a distillation process that removes at least a portion of the sulfur compounds from the composition, but does not remove more than 3% of the total composition.
    Type: Grant
    Filed: May 13, 1994
    Date of Patent: June 20, 1995
    Assignee: Wm. Wrigley Jr. Company
    Inventors: Sonya S. Johnson, Michael J. Greenberg
  • Patent number: 5405633
    Abstract: A process for the extraction of fats and oils from natural substances using liquid propane as the solvent is described in which the extraction is carried out at a pressure of 10 to 30 bar and a temperature of 10.degree. to 55.degree. C. and the separation of the extracted fats and oils from the solvent is carried out by means of pressure reduction or/and temperature increase to .ltoreq.80.degree. C. High quality products are isolated in this way in a good yield and under mild conditions.
    Type: Grant
    Filed: October 4, 1993
    Date of Patent: April 11, 1995
    Assignee: SKW Trostberg Aktiengesellschaft
    Inventors: Jurgen Heidlas, Jan Cully, Heinz-Rudiger Vollbrecht
  • Patent number: 5356651
    Abstract: A method for treating raw milk to produce treated milk having a lower bacterial content than the raw milk. The milk is homogenized and, within about 5 minutes from the homogenization, subjected to dynamic microfiltration, to yield a filtrate which has a lower bacterial content than the initial raw milk. When the flow rate of milk through the microfilter drops below a predetermined level, the dynamic microfilter is removed from milk filtration service, flushed with water, and returned to milk filtration service, the steps being repeated as necessary until the membrane cannot be rejuvenated to a minimum filtration capacity, at which time the membrane is subjected to chemical cleaning to essentially restore the original filtration capacity of the membrane.
    Type: Grant
    Filed: December 30, 1992
    Date of Patent: October 18, 1994
    Assignee: Pall Corporation
    Inventors: Peter J. Degen, Tony Alex, Joseph W. Dehn, Jr.
  • Patent number: 5356641
    Abstract: A process for obtaining a blending and ageing additive from oak wood which comprises (a) mixing oak wood in subdivided or particulate form with water, alcohol or mixture thereof; (b) enzymatically digesting the mixture at elevated temperature; (c) adding wine or other alcohol to the digestion mixture after the digestion is completed; (d) refluxing the resulting mixture at elevated temperature until the wood changes color and the liquid phase no longer changes color; (e) separating the resulting liquid phase from the wood; and (f) distilling the liquid phase to obtain a clear or water-white distillate and solid extract. The distillate and/or extract may be added to wine or other beverage, or other composition such as vinegar, to improve properties thereof.
    Type: Grant
    Filed: May 10, 1993
    Date of Patent: October 18, 1994
    Assignee: Indopco, Inc., d/b/a Quest International Flavors & Food Ingredients Company
    Inventors: David Bowen, Jan Benning, Chris Bronzert, Alan Ellison
  • Patent number: 5262163
    Abstract: The invention relates to a process for preparing the nonsaponifiable matter of avocado oil from the fruit, wherein the nonsaponifiable matter of avocado oil is separated and its content in one of its fractions termed H is improved by carrying out the heat treatment of the fruit before extracting the oil at a temperature of 80.degree. C. to 120.degree. C. for not less than four hours.It also relates to the nonsaponifiable matter obtained by the process and to medicinal products, cosmetics and food additives containing it.
    Type: Grant
    Filed: September 13, 1991
    Date of Patent: November 16, 1993
    Assignee: Laboratoires Pharmascience
    Inventor: Alain Rancurel
  • Patent number: 5252350
    Abstract: A process for clarifying raw juice in which the proportion of solids in the retentate circuit (2, 3, 4) of an ultrafiltration or microfiltration device (1) is sharply increased during the starting time (FIG. 1). With increasing proportion of solids, the filtration yield falls off sharply and then increases again to a value which is higher than the starting value. On reaching the maximum possible filtration yield value, the proportion of solids and thereby also the filtration yield is maintained constant by regulating the amount of retentate outflow or the amount of fresh juice to be fed in. In this way the filtration yield can be significantly improved.
    Type: Grant
    Filed: June 22, 1989
    Date of Patent: October 12, 1993
    Assignee: Bucher - Guyer AG Maschinenfabrik
    Inventor: Eduard Hartmann
  • Patent number: 5221550
    Abstract: Reduction sauces are prepared by first preheating ingredients of a reduction sauce and then feeding the preheated ingredients to and through a scraped surface heat exchanger operating at substantially atmospheric pressure and having a scraper speed of below 200 RPM which heats the ingredients to a temperature for evaporating at least some of the ingredients for concentrating the ingredients and developing a reduction sauce flavor during the residence time of the ingredients in the heat exchanger. The evaporated vapors are separated and removed from the concentrated heated reduction sauce.
    Type: Grant
    Filed: February 26, 1991
    Date of Patent: June 22, 1993
    Assignee: Nestec S.A.
    Inventor: Nigel B. Freeman
  • Patent number: 5213826
    Abstract: The present invention includes a whey permeate-derived dry sweetener made from a condensed whey permeate and a method of feeding animals the dry whey permeate sweetener. The condensed whey permeate is at least partially caramelized and has a protein level of less than approximately 8% and a lactose level of at least approximately 79% on a dry matter basis.
    Type: Grant
    Filed: December 19, 1990
    Date of Patent: May 25, 1993
    Assignee: Land O'Lakes, Inc.
    Inventors: Bill L. Miller, H. Bruce Perry, Robert DeGregorio
  • Patent number: 5167979
    Abstract: Cooking process and apparatus is provided for cooking food products in a continuous manner whereby the moisture formed during the process of cooking is removed from the cooking oil and the time-temperature profile within the cooker along the cooking path may be adapted to substantially conform to a linear or nonlinear curve. The apparatus provides a novel process for cooking specialty snack foods having harder bite and/or lowered oil content.
    Type: Grant
    Filed: May 15, 1991
    Date of Patent: December 1, 1992
    Assignee: Heat and Control, Inc.
    Inventors: Clark K. Benson, Andrew A. Caridis, Lawrence F. Klein
  • Patent number: 5130157
    Abstract: The present invention relates to a process for obtaining an aroma concentrate that is enriched in lactones. The present invention is particularly concerned with a process for concentrating lactones from a distillate obtained by the distillative deacidification of a fat composition rich in lauric acid residues, said distillate containing at least 0.1 wt. % of lactones having 6-20 carbon atoms, by subjecting the distillate or a fraction thereof to a fractional distillation so as to obtain a fraction containing at least 1 wt. % of lactones having 6-20 carbon atoms.The present invention offers a commercially and technically attractive route for obtaining natural lactones.Other aspects of the present invention are a lactone concentrate obtainable by the above process, the use of such a concentrate for flavoring food products and to food products flavored by such a lactone concentrate.
    Type: Grant
    Filed: January 23, 1991
    Date of Patent: July 14, 1992
    Assignee: Van den Bergh Foods Co., Division of Conopco, Inc.
    Inventors: Franciscus H. Hulsker, Koene de Jong, Hessel Turksma
  • Patent number: 5092964
    Abstract: Butter oil is heated under high vacuum and sparged for up to about 6 hours to remove cholesterol. Walls surrounding a vapor space above the sparged mass preferably are heated to remove cholesterol with reduced loss of desirable low molecular weight components. Alternatively, the temperature of the butter oil is lowered, and the butter oil is sparged with steam for an additional period of up to about 3 hours to partially hydrolyze triglycerides to mono- and di-glycerides and free fatty acids. The low cholesterol butter oil then is cooled before being exposed to air, thus avoiding oxidation which produces off-flavors. The resulting low-cholesterol butter fat and products made therefrom have composition and organoleptic characteristics substantially similar to those of natural butter oil and butter.
    Type: Grant
    Filed: February 3, 1989
    Date of Patent: March 3, 1992
    Assignee: Campbell Soup Company
    Inventors: Joseph A. Conte, Jr., Bobby R. Johnson
  • Patent number: 5023100
    Abstract: An edible fish oil is disclosed which contains EPA and DHA. This oil, with significantly reduced undesirable impurities, is obtained by subjecting fish oil to vacuum steam distillation contacting the oil with an adsorbent and recovering the oil. The oil can be combined with a vegetable oil and/or Rosemary extract antioxidant to improve its oxidative stability.
    Type: Grant
    Filed: October 2, 1989
    Date of Patent: June 11, 1991
    Assignee: Kabi Vitrum AB
    Inventors: Stephen S. Chang, Yongde Bao, Timothy J. Pelura
  • Patent number: 5006348
    Abstract: In accordance with the method of the present invention for manufacture of Swiss cheese from milk, the fat level of milk is standardized to about 3.5%. The milk is subjected to membrane processing by ultrafiltration and diafiltration to provide a retentate with particular characteristics. The retentate is then fermented with a particular blend of a coccus culture and a high level of a rod culture. The usual propionic acid-forming micro-organism, such as Propionibacterium shermannii, is used. The fermentation is desirably carried out at high temperatures to achieve the results of the invention. The fermented retentate is then evaporated to a solids level desired in the finished Swiss cheese, which is generally in the range of 35% to 41% moisture. The fermented and evaporated product is suitable for packing into containers to be cured and to provide Swiss cheese without further manipulation or treatment. The particular conditions are necessary to provide the desired Swiss cheese.
    Type: Grant
    Filed: May 4, 1990
    Date of Patent: April 9, 1991
    Assignee: Kraft General Foods, Inc.
    Inventors: Brent K. Pope, Susan P. Monckton, Kaser R. Nath
  • Patent number: 4996072
    Abstract: Disclosed are physical processes for fats and oils, especially fish oils and dairy oils and fats, involving deodorization and/or cholesterol level reduction. Either freshly refined oils or stored oils that have oxidized (such as reverted fish oil) can be treated. When processing fish oil, the fish oil is preferably deaerated, mixed with steam, heated, flash vaporized, thin-film stripped with countercurrent steam, cooled (all steps being performed under vacuum), and then stored under oxygen free conditions. When processing dairy and various other oils and fats, certain of the above steps such as initial deaeration and final storage under oxygen free conditions may be eliminated. The process provides oils and fats from which all or a substantial portion of the free or non-esterified cholesterol has been removed and which, at least in the case of fish oils, are clean tasting.
    Type: Grant
    Filed: February 13, 1989
    Date of Patent: February 26, 1991
    Assignee: General Mills, Inc.
    Inventors: Steven S. Marschner, Jeffrey B. Fine
  • Patent number: 4995945
    Abstract: A counter-current contacting device which includes a number of features which increase the efficiency and/or increase the pressure differential across the device is disclosed. Systems for reducing the alcohol content of an alcohol containing beverage or wine, for stripping aroma and flavor from a fruit juice and for desulphuring a liquid containing dissolved sulphur dioxide are also disclosed. Each of these systems incorporate a counter-current contact device of the invention.
    Type: Grant
    Filed: March 8, 1988
    Date of Patent: February 26, 1991
    Assignee: Flavourtech Pty. Ltd.
    Inventor: Andrew J. M. Craig
  • Patent number: 4988525
    Abstract: For selective removal of volatile substances from liquids, the initial liquid is fed to a crosscurrent diaphragm separation device (2), in which the permeate consisting of water and volatile substances is separated by increased transdiaphragm pressure and concentration difference. Then, the permeate is fed into a further liquid-volatile separation device (8), in which the alcohol is distilled out. The permeate now only consisting of water, salts, acids and extracts is then fed back into the crosscurrent diaphragm separation device (2), where it flows through the permeate side in countercurrent to the flow of the retenate. Excess permeate can be introduced into the dealcoholized initial liquid. By the process according to the invention the economic efficiency of the unit and the quality of the end product are significantly improved.
    Type: Grant
    Filed: April 26, 1989
    Date of Patent: January 29, 1991
    Assignee: Bucher-Guyer AG Maschinenfabrik
    Inventor: Walter Gresch
  • Patent number: 4976974
    Abstract: In this invention, both a grape juice concentrate and a grape juice drink are produced by first preparing the raw material for a year's production during vintage, transferring grape juice so produced to a vacuum concentrating column before it ferments, heating the grape juice in the column and subjecting it to a low pressure (vacuum) to separate it into a distillate and a first stage grape juice concentrate which has a Baume of about 35, separate storing the first stage grape juice concentrate, remixing some of the stored concentrate with the distillate to produce a low calorie grape juice drink and further concentrating the first stage concentrate to produce a food product having a Baume above 35.
    Type: Grant
    Filed: June 2, 1988
    Date of Patent: December 11, 1990
    Assignee: Chateau Yaldara PTY. Ltd.
    Inventor: Hermann Thumm
  • Patent number: 4971660
    Abstract: A method and apparatus for distilling, especially vacuum refining and deodorizing edible oils and fats utilizing sheets of oil driven downwardly in a distiller with a vacuum source at its top. A nozzle includes pressure equalization chambers, cantilever adjustment screws, and a central drag sheet to produce longer lasting and more uniform thin oil sheets to be driven in the distiller. A continuous process deaerates, dehydrates, degums, bleaches, refines, removes tocopherol, deodorizes, and strips peroxides and hydroperoxides from raw oil in a series of isothermal stages utilizing driven sheet distillers. No stripping steam is used except in the stage which strips peroxides and hydro peroxides. The method produces valuable, pure products such as tocopherol and fractionated fatty acids. It is especially efficient in heat exchange and low in waste and pollution producing products.
    Type: Grant
    Filed: October 11, 1988
    Date of Patent: November 20, 1990
    Inventor: Jacob B. Rivers, Jr.
  • Patent number: 4959234
    Abstract: There is provided a method for concentrating and improving the taste, texture and mouth feel of a liquid dairy product. The liquid dairy product is cooled to a temperature at or below its feezing point. Ice crystals are crystallized from the cooled liquid dairy product to produce a mixture of concentrated product and ice crystals. A portion of the ice crystals is separated from the mixture and heated to form a melt thereof. The mixture is washed with the melt to form a washed mixture of the concentrated product and the ice crystals, and the ice crystals are separated from the washed mixture and the concentrated product is recovered. The amount of ice crystals formed in the crystallizing step is sufficient that the recovered product has a solids content of at least about 20%.
    Type: Grant
    Filed: November 17, 1988
    Date of Patent: September 25, 1990
    Assignee: Electric Power Research Institute
    Inventors: Salah H. Ahmed, Anthony J. Luksas
  • Patent number: 4921709
    Abstract: A process for obtaining banana peel essences and juice from banana peels removed by hand from whole ripe bananas.
    Type: Grant
    Filed: September 7, 1989
    Date of Patent: May 1, 1990
    Assignee: Chiquita Brands, Inc.
    Inventor: Pedro Sole
  • Patent number: 4921717
    Abstract: A process for producing a sterilized, concentrated milk product comprising the steps of(a) partially concentrating milk or a milk product,(b) sterilizing a partially concentrated milk product and(c) further concentrating the sterilized product of step (b) under sterile conditions.
    Type: Grant
    Filed: December 22, 1987
    Date of Patent: May 1, 1990
    Assignee: Milk Marketing Board
    Inventor: Heva M. P. Ranjith
  • Patent number: 4900565
    Abstract: An extract having a bread-like flavor is prepared by baking bread, size reducing the baked bread, mixing water with the size reduced bread for preparing a mash, treating the mash with at least one enzyme capable of liquifying bread for liquifying the bread of the mash, subjecting the aqueous liquified bread to slurry extraction, and then the aqueous slurry extracted liquified bread is subjected to steam distillation. A combined residue and extract and a distillate result from the steam distillation. The residue and extract are separated for obtaining a clarified extract which is then concentrated by evaporation. The distillate is mixed with the concentrated extract, and the mixture is dried. A water-soluble light colored powder with a bread-like flavor is obtained. To improve the yield, the separated residue also may be mixed with water and processed by slurry extraction and each of the subsequent steps of the process for obtaining further product.
    Type: Grant
    Filed: September 21, 1987
    Date of Patent: February 13, 1990
    Assignee: Nestec S.A.
    Inventor: Gerhard Spies
  • Patent number: 4874629
    Abstract: A process of treating oils containing Omega-3 fatty acids, such as fish oils like Menhaden oil, sardine oil, salmon oil and other oils, to produce odorless and flavorless oils which contain only insignificant amounts of undesirable minor constituents, such as thermal and oxidative polymers of unsaturated glycerides, trans-isomers, positional isomers, conjugated dienes and trienes, cholesterols, pesticides, PCBs and heavy metals, and which have reasonably good flavor and oxidative stabilities.
    Type: Grant
    Filed: May 2, 1988
    Date of Patent: October 17, 1989
    Inventors: Stephen S. Chang, Yongde Bao, Timothy J. Pelura
  • Patent number: 4874617
    Abstract: A process for obtaining banana juice, banana essences and/or de-flavored banana juice from whole, ripe bananas is disclosed.
    Type: Grant
    Filed: December 4, 1987
    Date of Patent: October 17, 1989
    Assignee: United Brands Company
    Inventor: Pedro Sole
  • Patent number: 4820530
    Abstract: High solids curd and cheese are produced by fermenting and evaporating a milk retentate. Preferably, moisture is evaporated under vacuum to 55 percent or more solids while the fermented retentate is spread on a drum surface. Curd is formed on the surface under quiescent conditions and is doctored off without substantial breakdown of curd structure. Salts such as sodium chloride may be added to the retentate to prevent coagulation during fermentation. A milk clotting enzyme may be added after fermentation and before evaporation in an amount insufficient to cause coagulation which is avoided prior to curd formation.
    Type: Grant
    Filed: September 11, 1984
    Date of Patent: April 11, 1989
    Assignee: Kraft, Incorporated
    Inventors: James W. Moran, James R. Posdal, Gary W. Trecker
  • Patent number: 4818555
    Abstract: Low viscosity evaporative orange juice concentrates having less cooked off-flavor, as measured by the % retained valencene, are disclosed. These concentrates are preferably obtained by an evaporative concentration process which starts with a feed juice having a relatively low viscosity and sinking pulp level and which heats this feed juice to temperature no higher than about 180.degree. F. to avoid the generation of cooked off-flavor. In addition, the juice, at a critical solids content, is headed under vacuum to temperatures in the range of from about 160.degree. to about 180.degree. F. under conditions of high shear across the heated surface of the evaporator to insure effective deactivation of pectinesterase enzymes initially present in the feed juice.
    Type: Grant
    Filed: May 18, 1987
    Date of Patent: April 4, 1989
    Assignee: The Procter & Gamble Company
    Inventors: Robert D. Piotrowski, George R. Ross, Rudolf G. K. Strobel, Raju V. Thundathil, Chee-Hway Tsai
  • Patent number: 4816275
    Abstract: Green coffee is decaffeinated in a continuous economical process without organic solvent. Caffeine is extracted from a solution of green coffee solubles with supercritical carbon dioxide in a novel extractor under specified conditions.
    Type: Grant
    Filed: December 7, 1987
    Date of Patent: March 28, 1989
    Assignee: Chock Full O'Nuts Corp.
    Inventor: Ismar M. Reich
  • Patent number: 4810330
    Abstract: Deodorizing and/or physical refining of relatively small, varying charges of high-boiling liquids, viz. fatty acids, edible oils, fats, glycerides and other high-boilding esters, is conducted continuously in a single-stage or multi-stage falling-film column (20) through the trickle passages (23) of which stripping steam is passed in counter-current flow. In the supply conduit (15, 15', 15", 15'") leading to the falling-film column and in the discharge conduit (30, 30', 30", 30'") leading away from the bottom (26) of the falling-film column a plug-flow of the liquid is maintained. Upon a change of charge the fresh liquid to be treated is normally introduced into the supply conduit--without any blank charge--directly following the liquid of the preceding charge. Charging of the liquid onto the deflector (22) in the head (21) of the falling-film column is interrupted for a short period of time when the front of the liquid of the fresh charge has reached a check valve (16) disposed adjacent said deflector.
    Type: Grant
    Filed: February 17, 1988
    Date of Patent: March 7, 1989
    Inventor: Hermann Stage
  • Patent number: 4806379
    Abstract: A process for producing a natural flavorant, green leaf essence, containing leaf aldehyde, leaf alcohol and at least 10% cis-3-hexenal is disclosed. The process comprises homogenizing strawberry leaves with or without stems attached thereto in water to form a slurry. Prior to homogenization or concurrently therewith, from 1 to 10 mM of linolenic acid is added. The homogenate is then fed to a scraped or wiped surface evaporator and subsequently fractionated and concentrated to form a green leaf essence. The essence may be added to a food product to impart a fresh green fruity flavor and/or enhance the fresh flavor impact of the food product.
    Type: Grant
    Filed: June 5, 1987
    Date of Patent: February 21, 1989
    Assignee: General Foods Corporation
    Inventors: Steven K. Goers, Parviz Ghossi, John T. Patterson, Cynthia L. Young
  • Patent number: 4804555
    Abstract: Disclosed are physical processes for fats and oils, especially fish oil, involving simultaneous deodorization and cholesterol level reduction. Either freshly refined or stored oils that have oxidized (reverted fish oil) can be treated. In the process the fish oil is deaerated, mixed with steam, heated, flash vaporized, thin-film stripped with countercurrent steam, cooled (all steps being performed under vacuum), and then stored under oxygen free conditions. The process provides fish oils which are clean tasting and from which has been removed substantially all of the free or non-esterified cholesterol.
    Type: Grant
    Filed: March 2, 1987
    Date of Patent: February 14, 1989
    Assignee: General Mills, Inc.
    Inventors: Steven S. Marschner, Jeffrey B. Fine
  • Patent number: 4778688
    Abstract: Low-ethanol wines and other alcoholic beverages are produced by treating ordinary alcoholic beverages with novel membrane extraction methods. Semipermeable membranes and extraction fluids comprised either of a non-toxic, water-immiscible organic solvent or an aqueous solution of a low-molecular-weight but membrane-impermeable solute are used under mild conditions to selectively extract ethanol from alcoholic beverages, while leaving substantially intact the complement of other organic constituents that contribute to the color, aroma, and taste of the beverage. The methods disclosed may be adapted to continuous processing of alcohol-containing beverages, in which an ethanol-rich product is continuously recovered from the organic or aqueous extraction fluid and the latter is continuously regenerated and subsequently recycled to the membrane extraction unit.
    Type: Grant
    Filed: October 11, 1985
    Date of Patent: October 18, 1988
    Assignee: Sepracor, Inc.
    Inventor: Stephen L. Matson
  • Patent number: 4759944
    Abstract: Chlorohydrins are eliminated from liquid hydrolyzates prepared from vegetable proteins hydrolyzed with concentrated hydrochloric acid. The hydrolyzates are subjected to steam distillation under reduced pressure for removing the chlorohydrins while keeping the density of the hydrolyzates at a substantially constant value.
    Type: Grant
    Filed: November 7, 1986
    Date of Patent: July 26, 1988
    Assignee: Nestec S. A.
    Inventors: Roland Fasi, Giancarlo Werner, Ursula Wolfensberger
  • Patent number: 4687671
    Abstract: A method for concentrating aqueous mixtures and particularly mixtures which contain volatile desirable components such as flavor constituents is disclosed. An aqueous feed mixture is cooled sufficiently to produce ice crystals therein. The ice crystals are removed from the chilled mixture to produce a liquid phase from which some of the water has been removed and which is therefore concentrated. The concentrated liquid phase is split into two portions, one of which is collected as a first product, the other being first treated to separate the volatile components, which are recycled to the freezing step in which the ice crystals are formed. The residual liquid after the volatile component separation is then concentrated thermally in a conventional fashion to produce a second concentrated product which can be mixed with the first product to produce a product having a desired solids concentration and containing at least a substantial proportion of the original volatile components present in the feed.
    Type: Grant
    Filed: August 19, 1985
    Date of Patent: August 18, 1987
    Assignee: Chicago Bridge & Iron Company
    Inventors: Matloob Husain, Ban-Yen Lai
  • Patent number: 4666561
    Abstract: Liquids, such as juices, milk, molten metal and the like are concentrated by forming uniformly-sized, small droplets in a precision droplet forming assembly (14) and deploying the droplets in free fall downwardly as a central column within an evacuated tower (12) having cool walls (32). A portion of the solvent evaporates. The vapor flows to the wall (32), condenses, and usually flows down the wall as a film (62) to condensate collector (26) and drain (28). The vertical column of freely-falling droplets enters the splash guard (68). The condensate can be collected, sent to other towers or recycled.
    Type: Grant
    Filed: July 30, 1985
    Date of Patent: May 19, 1987
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventor: Eugene R. DuFresne
  • Patent number: 4647465
    Abstract: The invention relates to a whippable, non-homogenized cream having a fat content of 20 to 30% by weight and a pH of 6.2 to 6.5, which contains0.2 to 0.4% by weight of at least one emulsifying agent consisting of a mixture of distilled monoglycerides in a carrier, wherein the weight ratio of saturated fatty acids to unsaturated fatty acids in the fatty acid ester is between 80:20 and 20:80,0.2 to 0.4% by weight of at least one binder based on starch, as well as0.03 to 0.06% by weight of carragheenate as a stabilizer, and to a method wherein at least one of said emulsifying agent, said binder, said carragheenate and at least one organic and physiologically acceptable acid are dispersed in milk and the amount of non-homogenized cream required to achieve the desired fat content in the final product.
    Type: Grant
    Filed: September 9, 1985
    Date of Patent: March 3, 1987
    Assignee: Melkunie Holland B.V.
    Inventors: Martinus J. M. van de Ven, Zeger Provily
  • Patent number: 4613410
    Abstract: A method and apparatus for distilling, especially vacuum refining and deodorizing edible oils and fats utilizing sheets of oil driven downwardly in a distiller with a vacuum source at its top. A nozzle includes pressure equalization chambers, cantilever adjustment screws, and a central drag sheet to produce longer lasting and more uniform thin oil sheets to be driven in the distiller. A continuous process deaerates, dehydrates, degums, bleaches, refines, removes tocopherol, deodorizes, and strips peroxides and hydroperoxides from raw oil in a series of isothermal stages utilizing driven sheet distillers. No stripping steam is used except in the stage which strips peroxides and hydroperoxides. The method produces valuable, pure products such as tocopherol and fractionated fatty acids. It is especially efficient in heat exchange and low in waste and pollution producing products.
    Type: Grant
    Filed: October 7, 1983
    Date of Patent: September 23, 1986
    Inventor: Jacob B. Rivers, Jr.
  • Patent number: 4601790
    Abstract: Deodorizing and/or physical refining of cocoa butter and cocoa butter substitutes is carried out in accordance with the principle of continuous counter-current falling film stripping steam distillation in at least two different zones, where different flow and current conditions prevail for the liquid film and the vapors, respectively. In the initial zone 10 the vapors pass through trickle passages having a hydraulic equivalent diameter greater than the hydraulic equivalent diameter in the final zone 22.The working pressure in the top of the falling film column 10 is maintained below 2.0 mbar, and in the bottom of the falling film column 22 it is maintained by at most 1.6 mbar in excess of that in the falling film column 10. The accumulation of any significant liquid content in the bottoms of the serially operating zones is avoided. Stripping steam is supplied in an amount of 2 to 10 kg of steam per 100 kg of charged liquid.
    Type: Grant
    Filed: July 18, 1983
    Date of Patent: July 22, 1986
    Inventor: Hermann Stage
  • Patent number: 4599143
    Abstract: The deodorization and/or physical refining of high-boiling organic edible oils, fats and esters is carried out according to the principle of continuous counter-current falling film stripping steam distillation in an internally imposed temperature field in at least two different zones having different flow conditions for the liquid film and the vapors, respectively, prevailing therein. In the initial zone 10 directly adjacent the liquid charge and ensuring at least two separation stages the vapors flow through trickle passages having a hydraulic equivalent diameter of 73 to 150 mm. If necessary, this initial zone may be subdivided, wherein in the first sub-zone the trickle passages are provided with hydraulic equivalent diameters of 120 to 150 mm and in the second sub-zone the trickle passages are provided with hydraulic equivalent diameters of 73 to 120 mm.
    Type: Grant
    Filed: July 18, 1983
    Date of Patent: July 8, 1986
    Inventor: Hermann Stage
  • Patent number: 4597978
    Abstract: A method of concentrating grape juice to a predetermined final degree of concentration comprises the steps of evaporating one part of the water content of the grape juice to obtain an intermediate degree of concentration less than the final degree of concentration, then stabilizing the grape juice for cream of tartar by cooling the grape juice to near freezing temperature; and thereafter resuming evaporation of water of the grape juice for ultimately reaching the final degree of concentration.
    Type: Grant
    Filed: December 27, 1984
    Date of Patent: July 1, 1986
    Assignee: W. Schmidt GmbH & Co. KG
    Inventor: Michael H. Dimitriou
  • Patent number: 4571339
    Abstract: This invention relates to the use of a salt and/or a mild caustic in solution to increase the relative volatility of aromatics contained in an aqueous stream. The increased relative volatility so achieved enables more efficient concentration of the aromas via distillation. The pH of the aroma-containing aqueous stream does not exceed 7.0 through the addition of the salt or caustic to prevent aroma degradation.
    Type: Grant
    Filed: February 7, 1985
    Date of Patent: February 18, 1986
    Assignee: General Foods Corporation
    Inventors: Saul N. Katz, Gerald J. Vogel
  • Patent number: 4562085
    Abstract: To a previously agitated blend of fruit and sugar is added a water solution of pectin to form a premix which is heated to 90.degree.-125.degree. F. during gentle agitation. After adding an acid solution to the premix, it is heated to 135.degree.-145.degree. F. and passed through an evaporation zone at 145.degree.-160.degree. F. under a vacuum of 20-27 inches Hg., all during gentle stirring, to obtain a concentrated product which is then heated to a sterilizing temperature and passed through a holding zone at such a temperature. The resulting product, after cooling, is a fruit preserve concentrated to a desired degree, such as 65.degree. Brix, and in which the fruit has retained its particulate identity and integrity and is well distributed in the preserve.
    Type: Grant
    Filed: October 9, 1984
    Date of Patent: December 31, 1985
    Assignee: Alfa-Laval, Inc.
    Inventor: Frank J. Ruggiero
  • Patent number: RE34237
    Abstract: A process for obtaining banana juice, banana essences and/or de-flavored banana juice from whole, ripe bananas is disclosed.
    Type: Grant
    Filed: October 16, 1991
    Date of Patent: April 27, 1993
    Assignee: Chiquita Brands, Inc.
    Inventor: Pedro Sole