Distiller's Or Brewer's Residue Patents (Class 426/624)
  • Patent number: 5328707
    Abstract: A process for recovering waste liquid from the distillation of fermented rice liquor. After filtration of the waste liquid, the residue can be recovered as dry feed, and the filtrate which contains about 4-5% crude protein, 1% starch and 92 wt. % water is first concentrated to lower the water content to about 70-80 wt. %. The filtrate is then dried with a spray dryer to produce nutritious dry feed while a suitable chelating agent such as magnesium hydroxide is used to prevent the clinging of the product on the wall of the dryer.
    Type: Grant
    Filed: July 1, 1992
    Date of Patent: July 12, 1994
    Assignee: Industrial Technology Research Institute
    Inventors: Rey-Chein Chang, Jyh-Feng Hwang
  • Patent number: 5316782
    Abstract: A process for manufacturing flavors from the spent mash of a fermentation mixture is provided wherein the spent mash of the fermentation mixture after distillation is separated into two constituent portions, the thin stillage and the wet distillers' grains. The thin stillage portion is then combined with a base to adjust pH thereof to between about 7 and about 11. The pH-adjusted thin stillage portion is then cooked at a temperature between about 130.degree. F. and about 210.degree. F. for a period of about 4 to about 14 hours. The cooked solution is concentrated in an evaporator until about 30% wt. solids level is obtained. The product is then dried to about 5-about 10% wt. moisture content. The product obtained has different flavors, depending on the base added and the pH of the cooking step. If the base is sodium hydroxide, the product has a bland, sweet or yeasty flavor if the pH is 8.5, maple or caramel flavor if the pH is 9.5, and a cracker or nutty flavor if the pH is 10.5.
    Type: Grant
    Filed: October 21, 1992
    Date of Patent: May 31, 1994
    Assignee: Brown-Forman Beverage Company
    Inventor: Joseph A. Zimlich, III
  • Patent number: 5260089
    Abstract: A livestock feed supplement providing high by-pass protein, being substantially free of urea and molasses, and providing good palatability. The supplement is formulated using byproducts of grain alcohol fermentation, namely distillers dried grains obtained from the stillage of fermented, dry-milled whole grain, and condensed distillers solubles from such stillage. Standard amounts of other nutritional supplements, including vitamins and minerals, are added to the composition to form the block. The supplement may be compressed and cured into a substantially hard block for free-choice feeding, or packaged in its granular, somewhat moist form for subsequent mixing in livestock feed. The byproducts of the fermentation include natural flavors that provide good palatability without the addition of sweeteners such as molasses.
    Type: Grant
    Filed: January 30, 1992
    Date of Patent: November 9, 1993
    Assignee: Harvest Fuel, Inc.
    Inventor: Robert Thornberg
  • Patent number: 5225228
    Abstract: The invention is a method for preparing a bran from wet distiller's grain (WDG) or distiller's dried grain with solubles (DDGS). In the method sodium bicarbonate, amino acid and potato starch are added to the wet, solid residue from the fermentation of grain. Then, the residue-additive mix is blended and dried to produce a bran which may be utilized on a 50-50 weight basis with wheat flour, for example, in the manufacture of noodles and baked goods.
    Type: Grant
    Filed: October 9, 1991
    Date of Patent: July 6, 1993
    Inventors: James A. Reddy, Roger Stoker
  • Patent number: 5156877
    Abstract: A protein-rich composition of brewer's spent grain origin is disclosed, which includes products separated from the husks of BSG and which contains 40 to 60% by weight of proteins, 12 to 18% by weight of lipids, 2 to 6% by weight of fibrous materials, and 1 to 4% by weight of ashes based on dry weight.
    Type: Grant
    Filed: February 19, 1991
    Date of Patent: October 20, 1992
    Assignees: Kirin Beer Kabushiki Kaisha, Chiyoda Corporation
    Inventors: Sohtaroh Kishi, Takashi Kimura, Takeshi Minami, Haruto Kobayashi
  • Patent number: 5135765
    Abstract: A process for producing a protein-rich product and/or a fibrous product is disclosed which includes the steps of pressing brewer's spent grain (BSG) in a wet state, and sieving the resulting pressed BSG in the presence of water to thereby separate it into a protein-containing fraction and a fibrous fraction.
    Type: Grant
    Filed: November 16, 1989
    Date of Patent: August 4, 1992
    Assignees: Kirin Beer Kabushiki Kaisha, Chiyoda Corporation
    Inventors: Sohtaroh Kishi, Takashi Kimura, Takeshi Minami, Haruto Kobayashi
  • Patent number: 5064665
    Abstract: To increase the efficiency of utilizing protein in feed by ruminants, feed containing a protein and a reducing sugar are mixed in quantities suitable for the Maillard reaction. The mixture is heated at a temperature, pH and time sufficient to cause early Maillard reactions but not advanced Maillard reactions.
    Type: Grant
    Filed: January 26, 1990
    Date of Patent: November 12, 1991
    Assignee: The Board of Regents of The University of Nebraska
    Inventors: Terry J. Klopfenstein, Lowell D. Satterlee, Robert A. Britton, Ralph N. Cleale
  • Patent number: 5023091
    Abstract: To increase the efficiency of utilizing protein in feed by ruminants, feed containing a protein and a reducing sugar are mixed. The mixture is heated at a temperature, pH and time sufficient to reduce degradability of the feed protein by rumen microorganisms and provide significant protein digestibility in the post rumen tract. Preferably, the sugar is xylose obtained by mixing sulfite liquor with the feed.
    Type: Grant
    Filed: February 2, 1990
    Date of Patent: June 11, 1991
    Assignee: The Board of Regents of the University of Nebraska
    Inventor: Thomas S. Winowiski
  • Patent number: 4957748
    Abstract: To increase the efficiency of utilizing protein in feed by ruminants, feed containing a protein and a reducing sugar are mixed in quantities suitable for the Maillard reaction. The mixture is heated at a temperature, pH and time sufficient to cause early Maillard reactions but not advanced Maillard reactions. Preferably, the sugar is xylose obtained by mixing sulfite liquor with the feed.
    Type: Grant
    Filed: March 23, 1987
    Date of Patent: September 18, 1990
    Assignee: The Board of Regents of the University of Nebraska
    Inventor: Thomas S. Winowiski
  • Patent number: 4938986
    Abstract: An energy-efficient method of recovering roughage from brewery residues (draff), including adding water to the draff and mixing to form a mixture of a soft protein fraction and a hard roughage fraction, separating the soft protein fraction from the hard roughage fraction, and removing water from the separated roughage fraction. After separating water the roughage fraction may be dried, and comminuted. In contrast to other methods, the separation into roughage and protein fractions is performed before the drying step and only the roughage fraction of interest is dried.
    Type: Grant
    Filed: December 29, 1987
    Date of Patent: July 3, 1990
    Assignee: Binding-Brauerei AG
    Inventors: Christian Zurcher, Rudiger Gruss
  • Patent number: 4812324
    Abstract: Pre-heated mash is pelleted. The resulting warm pellets are cooled by the ambient air and the ambient air is heated by the warm pellets. The heated ambient air is used to pre-heat the mash.
    Type: Grant
    Filed: March 23, 1987
    Date of Patent: March 14, 1989
    Assignee: California Pellet Mill Company
    Inventor: Henry Pierik
  • Patent number: 4552775
    Abstract: A high quality animal feed stuff is produced by thermal dewatering of liquid stillage obtained from fermentation of grain raw material and distillation of the fermentation product. The liquid stillage is mixed with particles of already dewatered product and the mixture is granulated in a granulation device to form essentially spherical granules with a dry substance content of 50-70% by weight, the major part of the granules having a particle diameter in the range of 2-6 mm, whereafter the granules are dried by being conveyed as a porous bed in a controlled path in contact with hot gas of a temperature less than 100.degree. C., and whereafter a part of the dried granules with a desired particle size are discharged and the remaining part of the granules after possible disintegration are recirculated to the granulation step.
    Type: Grant
    Filed: February 28, 1983
    Date of Patent: November 12, 1985
    Assignees: Alfa-Laval AB, Svenska Lantmannens Riksforbund, Forening u.p.a
    Inventors: Peter Baeling, Lars Ehnstrom
  • Patent number: 4479978
    Abstract: A description is given of the use of agricultural waste in the form of chemically treated cereal straw or fruit plant prunings together with the liquid residue from sugarbeet molasses in the production of balanced feedingstuffs suitable for feeding polygastric animals. The final useful mixture contains the agricultural waste as its main component and up to 60% of sugarbeet pulp, the remainder consisting of conventional additives.
    Type: Grant
    Filed: January 28, 1982
    Date of Patent: October 30, 1984
    Assignee: E.N.I. Ente Nazionale Idrocarburi
    Inventors: Andrea Robertiello, Leonello Angelini, Ludwig Degen
  • Patent number: 4315038
    Abstract: Trub obtained from the wort kettle of a brewing system is rich in protein and thus can be used in human foods. The trub is processed to yield a trub flour by extraction with an azeotropic mixture of isopropanol and water, and drying to remove the solvent in a roller drum drier, the latter yielding the trub flour in dry flake form.
    Type: Grant
    Filed: August 20, 1980
    Date of Patent: February 9, 1982
    Assignee: The Molson Companies Limited
    Inventors: Phillip M. Townsley, Robert L. Weaver
  • Patent number: 4309254
    Abstract: A process for the production of alcohol from a fermented feed wherein insoluble organic matter is separated prior to entry into a first distillation column. The insoluble organic matter is dried under pressure to produce dried distillers grain and wherein excess vapor is removed from the drying zone to provide heat to the distillation system. The present process also includes removing excess water vapor from the evaporation zone, obtained from supplemental heating supplied by the overhead from said first distillation column, compressing said water vapor, and recycling it to the distillation columns and the evaporation zone.
    Type: Grant
    Filed: April 17, 1980
    Date of Patent: January 5, 1982
    Assignee: Stone and Webster Eng. Corp.
    Inventors: Rodney A. Dahlstrom, Jacob N. Rubin
  • Patent number: 4278699
    Abstract: Distillers solubles are purified by a centrifugal separation to a degree above 50,000, which is the product of g.times.minute, or a filtration with addition of a filter aid. The clarified matter is purified by a molecular sieve treatment, ultrafiltration, reverse osmosis or an organic solvent precipitation. The clarified matter or purified matter thus obtained is pulverized by spray drying, lyophilic drying or air drying.Said clarified matter, purified matter or pulverized matter is added to a fermentation medium or a feed as an available component.
    Type: Grant
    Filed: January 26, 1977
    Date of Patent: July 14, 1981
    Assignees: National Tax Administration Agency, Kibun Company Limited
    Inventors: Kiyoshi Yoshizawa, Kikuo Nojiro, Masamitsu Itoh, Hiroshi Kiuchi, Kazuo Horii
  • Patent number: 4273659
    Abstract: For removing potassium salts from distiller's wash, an acid the potassium salts of which are poorly soluble and an organic solvent are added to the wash, whereafter the precipitated salts are collected on a filter and the solvent is recovered by distillation.
    Type: Grant
    Filed: September 12, 1979
    Date of Patent: June 16, 1981
    Assignee: E.N.I. Ente Nazionale Idrocarburi
    Inventors: Andrea Robertiello, Ludwig Degen
  • Patent number: 4197321
    Abstract: In the brewing of beer, spent grain at about 90% moisture from a straining tank having no internal rotating rake is collected and pumped to a centrifuge which reduces the moisture of the spent grain to about 70% and provides spent grain liquor of about 2.0 to 4.5% or more of total solids. The spent grain liquor is stored in a tank at 165.degree. F. to 170.degree. F. and held until it is used up to 50% of the sparge liquid for a subsequent brew in the straining tank. The spent grains at about 70% moisture are directed to a large holding tank. Nutritious brewery waste streams are added thereby increasing the nutritional value.
    Type: Grant
    Filed: April 3, 1978
    Date of Patent: April 8, 1980
    Assignee: Anheuser-Busch, Incorporated
    Inventors: Gustav W. Chyba, John H. Dokos
  • Patent number: 4109019
    Abstract: An improved two step method for producing feeds for ruminant animals whereby carbamides, particularly urea and biuret, are reacted with fermented proteinaceous agricultural products and wastes with the aid of an aliphatic dicarboxylic acid catalyst to produce a highly palatable nutritive feed which releases protein and protein equivalent nitrogen in a slow and controlled manner in the rumen.First stage of the method mechanically destroys the cellular structure of the fermented agricultural products and wastes, removes unpalatable acids, aldehydes and amines by stripping with hot gas, and partially completes the adduct-forming reaction between proteinaceous sugars, fats, and cellulose in the fermented material and the carbamides in a homogeneous liquid phase at temperatures of between 80.degree. and 100.degree. C. In the second stage, adduct reaction and drying is completed in a hot gas fluidized reactor at temperatures between 100.degree. and 150.degree. C.
    Type: Grant
    Filed: February 8, 1977
    Date of Patent: August 22, 1978
    Inventor: William Percy Moore
  • Patent number: 3962478
    Abstract: Mash is separated into draff and clarified beer wort using a cylindrical upright vessel having an upper portion with a circumferential wall, a lower portion conically converging toward an apertured support forming the bottom of the vessel, and a suction chamber connected to the vessel bottom having a lower conical portion with an outlet for wort and having a conduit leading from the side for applying a vacuum.
    Type: Grant
    Filed: June 5, 1974
    Date of Patent: June 8, 1976
    Inventors: Gerhard Hohlbein, Heinrich Huppmann