Metal Coating Patents (Class 427/217)
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Patent number: 7482059Abstract: A semiconductor nanocrystal complex including a metal layer formed on the outer surface of a semiconductor nanocrystal core after synthesis of the semiconductor nanocrystal core and a method for preparing a nanocrystal complex comprising forming a metal layer on a semiconductor nanocrystal core after synthesis of the semiconductor nanocrystal core. The metal layer may passivate the surface of the semiconductor nanocrystal core and protect the semiconductor nanocrystal core from the effects of oxidation. Also provided is a semiconductor nanocrystal complex with a shell grown onto the metal layer formed on the semiconductor nanocrystal core. In this embodiment, the metal layer may prevent lattice mismatch between the semiconductor shell and the semiconductor nanocrystal core.Type: GrantFiled: May 10, 2005Date of Patent: January 27, 2009Assignee: Evident TechnologiesInventors: Adam Peng, Wei Liu
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Publication number: 20090022994Abstract: A composite powder product suitable for hardmetal cutting tools and wear resistance applications is described. The product comprises a hard particulate phase chosen from a range of metallic carbides, nitrides, carbonitrides and the like, onto which hard phase is deposited a coating of cobalt or nickel, or a mixture of cobalt and nickel. The hard particulate phase has a particle size between 0.1 and 10 ?m, and preferably between 0.1 and 2 ?m.Type: ApplicationFiled: November 29, 2005Publication date: January 22, 2009Inventors: Hossein Aminian, Ding Yuan
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Publication number: 20080305257Abstract: The invention relates a method for the production of stabilised suspensions of nanometric or submicrometric particles, which is a method contained in a continuous flow that includes a step (20) for the placing in suspension, dispersion and/or functionalisation of these particles produced in a gaseous stream containing the particles at the output of a reactor in a stream of at least one liquid. The invention also relates a device that implements this method.Type: ApplicationFiled: December 13, 2005Publication date: December 11, 2008Applicant: COMMISSARIAT A LENERGIE ATOMIQUEInventors: Francois Tenegal, Benoit Guizard
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Publication number: 20080278181Abstract: The present invention is directed toward oxidation-resistant, ligand-capped nanoparticles, each comprising one or more capping ligands on a copper-containing core. Methods of making and using these nanoparticles are also disclosed.Type: ApplicationFiled: March 7, 2008Publication date: November 13, 2008Applicant: Research Foundation of State University of New YorkInventors: Chuan-Jian ZHONG, Derrick MOTT
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Publication number: 20080241543Abstract: The invention relates to a process for producing a material based on silver-carbon, comprising the steps of: (i) providing a suspension of carbon particles; and (ii) supplying a solution of a silver compound and of a reducing agent, such that a silver-containing precipitate is deposited onto the carbon particles, where the carbon particles have a mean diameter of 200 nm or greater. The invention further relates to a material obtainable by this process and to the use of the material in circuit breakers for low-voltage power engineering.Type: ApplicationFiled: August 10, 2006Publication date: October 2, 2008Applicant: UMICORE AG & CO. KGInventors: Bernd Kempf, Roger Wolmer, Carsten Boehme, Werner Roth, Andreas Koffler
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Publication number: 20080226958Abstract: In a method of producing a particulate electrocatalyst composition, a precursor medium comprising at least a first metal precursor, a liquid vehicle, and a substrate precursor to substrate particles is atomized into precursor droplets. The droplets are then heated to a reaction temperature of not greater than 700° C. to form composite particles comprising said first metal at least partly in an oxide form dispersed on said substrate particles. The composite particles are then collected and are heated at a first treatment temperature no greater than 250° C. in the presence of a reducing atmosphere to at least partly convert said oxide form to the metal.Type: ApplicationFiled: March 13, 2007Publication date: September 18, 2008Applicant: CABOT CORPORATIONInventors: Yipeng SUN, Paolina ATANASSOVA, James BREWSTER, Leonard P. PEREZ, Hanwei LEI, Berislav BLIZANAC
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Publication number: 20080190323Abstract: A process for the formation of particles of a target material is disclosed, comprising: (i) introducing the target material into a particle formation vessel, and forming a continuous liquid surface of the target material in the particle formation vessel, and an interface between said liquid surface of the target material and additional gaseous contents of said particle formation vessel; (ii) introducing a stream of cryogenic material including solid particles of cryogenic material into the particle formation vessel and into contact with the target material in a liquid state below the continuous liquid surface; (iii) allowing rapid volumetric expansion of the cryogenic material into a gaseous state while in contact with the target material in a liquid state, and release of the expanded gaseous cryogenic material through the continuous liquid surface, and forming liquid droplet particles of the target material; and (iv) collecting the formed particles of the target material.Type: ApplicationFiled: February 13, 2007Publication date: August 14, 2008Inventors: Rajesh V. Mehta, Robert Link, Michael A. Marcus
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Publication number: 20080187769Abstract: A method of making metal-coated superabrasive material comprises heating components comprising: superabrasive material, a metal-containing compound that comprises a metal capable of forming at least one of a carbide, boride or nitride, and a reducing agent capable of reducing the metal-containing compound. The components are heated in an inert atmosphere to sufficient temperature and for sufficient time to form metal-coated superabrasive material. The metal-coated superabrasive material is useful in the manufacture of various superabrasive tools.Type: ApplicationFiled: March 27, 2007Publication date: August 7, 2008Inventors: Gary M. Huzinec, Richard M. Andrews, Christopher P. Bieniasz
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Publication number: 20080160191Abstract: This invention releases the preparation method and equipment of graphite and catalyst composite for a kind of synthetic diamond. Firstly the clean graphite particle shall be placed into the heating chamber for pre-heating, the lower limit of the heating temperature shall be higher than the boiling point of the coated carbonyl metal complex and the upper limit of the heating temperature shall be set according to the thickness of the coating needed; secondly, the heated graphite particle will be fed into the coating room with vibrator or agitator and the steam of carbonyl metal complex shall be input for coating; finally the coated graphite particle shall be fed into the cooling and passivation room for cooling and passivation of the discharging materials or enter the next round circle of heating and coating.Type: ApplicationFiled: December 28, 2007Publication date: July 3, 2008Applicant: JIANGSU TIANYI MICRO METAL POWDER CO., LTD.Inventors: Weixing Gao, Bin Wang, Zunbin Ke
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Publication number: 20080135407Abstract: In one embodiment, a protective coating for an electrode of a sensor is described, the protective coating comprising an annealed catalyst, said annealed catalyst comprising at least one metal that has been subjected to thermal energy that is at least equivalent to or greater than that received from calcining the at least one metal for 24 hours at a temperature of 930 degrees C. in air. In another embodiment, the annealed catalyst will comprise at least one metal that has been subjected to thermal energy that is equal to or less than that received from calcining the at least one metal for 24 hours at 1030 degrees C. in air. In one exemplary embodiment, the annealed catalyst will comprise at least one metal that has been subjected to thermal energy that is equal to that received from calcining the at least one metal for 24 hours at 980 degrees C. in air.Type: ApplicationFiled: October 10, 2007Publication date: June 12, 2008Inventors: Carlos A. Valdes, Marsha Nottingham, Earl W. Lankheet, Eric P. Clyde
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Patent number: 7361430Abstract: The present invention discloses a carbon nanotube (SWNT)-polymer composite actuator and method to make such actuator. A series of uniform composites was prepared by dispersing purified single wall nanotubes with varying weight percents into a polymer matrix, followed by solution casting. The resulting nanotube-polymer composite was then successfully used to form a nanotube polymer actuator.Type: GrantFiled: April 8, 2004Date of Patent: April 22, 2008Assignee: The United States of America as represented by the United States Department of EnergyInventors: Thomas Gennett, Ryne P. Raffaelle, Brian J. Landi, Michael J. Heben
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Patent number: 7338686Abstract: The present invention provides a low-cost method for producing conductive particles in a short period of time by simplifying pretreatment in electroless plating. The method for producing conductive particles includes the steps of: introducing a solution composed mainly of palladium chloride and hydrochloric acid into an electroless plating bath containing particles of an organic material or an inorganic material while stirring the bath; and simultaneously applying an electroless plating to the surface of the particles and allowing the palladium catalyst to be carried on the surface of the particles to give conductive particles having an electroless plate coating.Type: GrantFiled: April 13, 2004Date of Patent: March 4, 2008Assignee: Kiyokawa Plating Industry Co., Ltd.Inventors: Hajime Kiyokawa, Kiyoto Fukuoka
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Patent number: 7335418Abstract: Disclosed is a semiconductor nanoparticle having excellent chemical durability and high luminescence properties. The chemical durability of the particle is provided by coating the semiconductor nanoparticle having high luminescence properties dispersed in an organic solvent using a surface-active agent, an amphipathic molecule, and a lipid composed of a combination of two or more layers selected from a polar group, a hydrophobic group, a hydrophilic group, and a functional group (herein, the hydrophobic group is a necessary element and the hydrophilic group and the functional group are optional).Type: GrantFiled: November 9, 2005Date of Patent: February 26, 2008Assignee: Hitachi Software Engineering Co., Ltd.Inventors: Keiichi Sato, Susumu Kuwabata
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Patent number: 7306823Abstract: CIGS absorber layers fabricated using coated semiconducting nanoparticles and/or quantum dots are disclosed. Core nanoparticles and/or quantum dots containing one or more elements from group IB and/or IIIA and/or VIA may be coated with one or more layers containing elements group IB, IIIA or VIA. Using nanoparticles with a defined surface area, a layer thickness could be tuned to give the proper stoichiometric ratio, and/or crystal phase, and/or size, and/or shape. The coated nanoparticles could then be placed in a dispersant for use as an ink, paste, or paint. By appropriate coating of the core nanoparticles, the resulting coated nanoparticles can have the desired elements intermixed within the size scale of the nanoparticle, while the phase can be controlled by tuning the stochiometry, and the stoichiometry of the coated nanoparticle may be tuned by controlling the thickness of the coating(s).Type: GrantFiled: September 18, 2004Date of Patent: December 11, 2007Assignee: Nanosolar, Inc.Inventors: Brian M. Sager, Dong Yu, Matthew R. Robinson
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Patent number: 7294289Abstract: Disclosed are conductive powder having a packing density of 68% by volume or more with a relative value preferably comprising 60 to 92% by weight of roughly spherical and silver-plated copper powder part of the surface of which has been coated with 3 to 30% by weight of silver based on an amount of roughly spherical copper powder with exposing at least a surface of a portion of an alloy of copper with silver, and the surface of which is coated with 0.02 to 1.0% by weight of an aliphatic acid based on an amount of the roughly spherical and silver-plated copper powder, and 8 to 40% by weight of silver powder, and a method for preparing the same.Type: GrantFiled: June 16, 2006Date of Patent: November 13, 2007Assignee: Hitachi Chemical Co., Ltd.Inventor: Hideji Kuwajima
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Patent number: 7261752Abstract: A superabrasive particle coated with a solidified coating of a molten braze alloy that is chemically bonded to the superabrasive particle is disclosed and described. In one aspect, the reactive metal alloy may be chemically bonded to at least about 80% of an outer surface of the superabrasive particle. Various methods for making and using such a coated superabrasive particle are additionally disclosed and described.Type: GrantFiled: July 25, 2003Date of Patent: August 28, 2007Inventor: Chien-Min Sung
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Patent number: 7253104Abstract: The invention includes methods of forming particle-containing materials, and also includes semiconductor constructions comprising particle-containing materials. One aspect of the invention includes a method in which a first monolayer is formed across at least a portion of a semiconductor substrate, particles are adhered to the first monolayer, and a second monolayer is formed over the particles. Another aspect of the invention includes a construction containing a semiconductor substrate and a particle-impregnated conductive material over at least a portion of the semiconductor substrate. The particle-impregnated conductive material can include tungsten-containing particles within a layer which includes tantalum or tungsten.Type: GrantFiled: December 1, 2003Date of Patent: August 7, 2007Assignee: Micron Technology, Inc.Inventors: Garo J. Derderian, Gurtej S. Sandhu
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Patent number: 7247259Abstract: A process for making an aerogel-electrolyte-metal composite includes contacting an aerogel with an electrolyte to form an aerogel-electrolyte composite; contacting the aerogel-electrolyte composite with a metal precursor to form an aerogel-electrolyte-precursor composite; and converting the metal precursor of the aerogel-electrolyte-precursor composite to metal crystals to form the aerogel-electrolyte-metal composite. In addition, an aerogel-electrolyte-metal composite is formed by the process, wherein the average longest dimension of the metal crystals is about 1 to about 3 nanometers, and wherein the metal crystals are about 30% to about 100% dispersed.Type: GrantFiled: April 4, 2005Date of Patent: July 24, 2007Assignees: Aerogel Composite, LLC, University of ConnecticutInventors: Can Erkey, Hiroaki S. Hara
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Patent number: 7226636Abstract: A process of preparing gold-coated magnetic nanoparticles is disclosed and includes forming a suspension of magnetic nanoparticles within a suitable liquid, adding an amount of a reducible gold compound and a reducing agent to the suspension, and, maintaining the suspension for time sufficient to form gold-coated magnetic nanoparticles.Type: GrantFiled: July 31, 2003Date of Patent: June 5, 2007Assignee: Los Alamos National Security, LLCInventors: Douglas E. Berning, Robert H. Kraus, Jr., Robert W. Atcher, Jurgen G. Schmidt
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Patent number: 7217318Abstract: In a method for the manufacture of a nacreous pigment, in which a multi-layer film is produced by vacuum evaporation coating on a substrate and, after release from the substrate, the particles thus produced are comminuted to pigment particles of a desired size, vapor deposition of a plurality of layers taking place at separate locations within an evacuable container and the substrate being passed along the sources of evaporation, it is provided that at least a backing (A), in particular a silicon oxide layer, and at least a metal oxide layer (B), in particular a titanium oxide layer, are vapor-deposited on the substrate, in particular a circulating metal belt.Type: GrantFiled: July 28, 2004Date of Patent: May 15, 2007Assignee: Eckart GmbH & Co. KGInventor: Günter Sommer
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Patent number: 7172791Abstract: Methods for synthesizing luminescent nanoparticles and nanoparticles prepared by such methods are provided. The nanoparticles are prepared by a method in which an additive is included in the reaction mixture. The additive may be a Group 2 element, a Group 12 element, a Group 13 element, a Group 14 element, a Group 15 element, or a Group 16 element. In additions, a luminescent nanoparticle is provided that comprises a semiconductive core surrounded by an inorganic shell, an interfacial region and an additive present in the interfacial region or both the interfacial region and the shell.Type: GrantFiled: November 9, 2004Date of Patent: February 6, 2007Assignee: Invitrogen Corp.Inventors: Joseph A. Treadway, Donald A. Zehnder, Marc D. Schrier
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Patent number: 7112369Abstract: A polymer nanoparticle is provided. The nanoparticle includes an inner layer having alkenylbenzene monomer units. The nanoparticle further includes an outer layer having monomer units selected from conjugated dienes, alkylenes, alkenylbenzenes, and mixtures thereof. The nanoparticle has at least one functional group associated with the outer layer. The nanoparticle further has at least one metal complexed with said functional group. The nanoparticles can be used as a templates for preparation of nano-sized metal crystals and polymer-metal nanocomposite.Type: GrantFiled: March 2, 2004Date of Patent: September 26, 2006Assignee: Bridgestone CorporationInventors: Xiaorong Wang, James E. Hall, Georg G. A. Böhm, Chenchy Jeffrey Lin
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Patent number: 7048965Abstract: A surface-covering article and method of installing the same are described. The surface-covering article includes a top layer, a bottom layer, and reinforcing layer. The top layer is made of a first type of resin. The bottom layer is made of a second type of resin. The second type of resin of the bottom layer chemically bonds with the first type of resin of the top layer to join the bottom layer and the top layer. The reinforcing layer is disposed between the top layer and bottom layer and includes a material to distribute a load force throughout the reinforcing layer when the load force is applied to the surface-covering article.Type: GrantFiled: May 28, 2004Date of Patent: May 23, 2006Inventor: Felisa Blazek
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Patent number: 6977097Abstract: A particle forming method includes feeding a first set of precursors to a first energy application zone. Energy is applied to the first set of precursors in the first energy application zone effective to react and form solid particles from the first set of precursors. The application of any effective energy to the solid particles is ceased, and the solid particles and a second set of precursors are fed to a second energy application zone. Energy is applied to the second set of precursors in the second energy application zone effective to react and form solid material about the solid particles from the second set of precursors. At least one precursor is fed to at least one of the first and second energy application zones as a liquid. Other aspects are contemplated.Type: GrantFiled: July 23, 2003Date of Patent: December 20, 2005Assignee: Micron Technology, Inc.Inventor: Trung Tri Doan
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Patent number: 6974601Abstract: Disclosed is a positive active material for a rechargeable lithium battery. The positive active material includes at least one compound represented by formulas 1 to 4: LixNi1-yMnyF2??(1) LixNi1-yMnyS2??(2) LixNi1-y-zMnyMzO2-aFa??(3) LixNi1-y-zMnyMzO2-aSa??(4) where M is selected from the group consisting of Co, Mg, Fe, Sr, Ti, B, Si, Ga, Al, Sc, Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Ac, Th, Pa, U, Np, Pu, Am, Cm, Bk, Cf, Es, Fm, Md, No and Lr, 0.95?x?1.1, 0<y?0.99, 0?z?0.5, and 0?a?0.5; and a metal oxide or composite metal oxide layer formed on the compound.Type: GrantFiled: March 23, 2004Date of Patent: December 13, 2005Assignee: Samsung SDI Co., Ltd.Inventors: Ho-Jin Kweon, Hyun-Sook Jung, Yong-Chul Park, Geun-Bae Kim
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Patent number: 6972134Abstract: A method of preparing for a positive active material for a rechargeable lithium battery is provided. In this method, a lithiated compound to be coated and an organic solution or aqueous solution including a coating-element source are putted into a mixer, the mixture is continuously stirred to mix the contents thoroughly, and a hot dry gas is introduced into the mixer to evaporate the solvent while the powder is continuously agitated. The resulting dry coated powdery compound is heat-treated at an elevated temperature to obtain an oxide coating on the lithiated compound.Type: GrantFiled: September 25, 2001Date of Patent: December 6, 2005Assignee: Samsung SDI Co., Ltd.Inventors: Ho-Jin Kweon, Jun-Won Suh, Won-Il Jung, Jeong-Joon Park
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Patent number: 6958308Abstract: A method for producing dispersed metal particles on a substrate and the compositions produced is disclosed. A method for producing the particles comprises exposing an organometallic and a particulate substrate to supercritical or near supercritical fluid under conditions to form a mixture of the fluid and the organometallic, allowing the mixture to remain in contact with the substrate for a time sufficient to deposit dispersed organometallic onto the substrate, venting the mixture, thereby adsorbing the organometallic onto the substrate, and reducing the dispersed organometallic to dispersed metal particles with a reducing agent.Type: GrantFiled: March 16, 2004Date of Patent: October 25, 2005Assignee: Columbian Chemicals CompanyInventor: Garth Desmond Brown
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Patent number: 6926964Abstract: Disclosed is a fuel tank for a motor vehicle whose inner face is processed with an inorganic coating agent comprising (A) fine particles carrying silver and/or copper and (B) inorganic fine particles, and the tank inhibits oxidation of the fuel such as gasoline or light oil, and further decreases the cluster of gasoline or light oil to make finer the particle size of atomized fuel, thereby improving ignitionability and combustibility, which makes it possible to decrease imperfect combustion and to decrease substantially the consumption of the fuel.Type: GrantFiled: December 12, 2003Date of Patent: August 9, 2005Assignee: Kabushiki Kaisha NippankenkyushoInventor: Yoshio Ichikawa
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Patent number: 6905814Abstract: The invention concerns the use of a film-forming titanium dioxide dispersion for cleaning and disinfecting surfaces exposed to light, by depositing a film of titanium dioxide nanoparticles on said surfaces, the continuous phase of said dispersion comprising water and/or at least an alcohol with boiling point at less than 120° C., said dispersion having, when it comprises water, a pH different by at least 1 unit of the value of the titanium dioxide isoelectric pH in said dispersion. The invention also concerns a film-forming titanium dioxide dispersion further comprises a film-forming polymer. The invention further concerns a method for cleaning and disinfecting surfaces exposed to light which consists in depositing and then drying on said surfaces a titanium oxide film-forming dispersion.Type: GrantFiled: February 15, 2000Date of Patent: June 14, 2005Assignee: Rhodia ChimieInventors: Eric Aubay, Thierry Chopin, Cédric Geffroy, Véronique Guillou, Corinne Lehaut
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Patent number: 6855273Abstract: The present invention concerns electrode materials capable of redox reactions by electrons and alkaline ions exchange with an electrolyte. The applications are in the field of primary (batteries) or secondary electrochemical generators, super capacitors and light modulating system of the super capacitor type.Type: GrantFiled: June 21, 2002Date of Patent: February 15, 2005Assignees: ACEP, Inc., Centre National de la Recherche Scientifique, Universite de MontrealInventors: Nathalie Ravet, Simon Besner, Martin Simoneau, Alain Vallée, Michel Armand, Jean-François Magnan
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Patent number: 6821314Abstract: An electrolyte capacitor containing a niobium anode, a niobium oxide barrier layer, a semiconducting cathode and an electrolyte is described, where the niobium oxide barrier comprises a least one metal from the group consisting of Al, Si, Ti, Zr, Mo, W, Y and Ta.Type: GrantFiled: May 7, 2002Date of Patent: November 23, 2004Assignee: H. C. Starck GmbHInventors: Karlheinz Reichert, Oliver Thomas, Christoph Schnitter
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Patent number: 6803073Abstract: A submicron particle forming method includes feeding a first set of precursors to a first energy application zone. Energy is applied to the first set of precursors in the first energy application zone effective to react and form solid particles having maximum diameter of no greater than 100 nanometers from the first set of precursors. The application of any effective energy to the solid particles is ceased, and the solid particles and a second set of precursors are fed to a second energy application zone. Energy is applied to the second set of precursors in the second energy application zone effective to react and form solid material about the solid particles from the second set of precursors with the solid particles with solid material thereabout having maximum diameter of no greater than 100 nanometers. Other aspects are contemplated.Type: GrantFiled: March 11, 2003Date of Patent: October 12, 2004Assignee: Micron Technology, Inc.Inventor: Trung Tri Doan
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Patent number: 6773763Abstract: A method of manufacturing a permanent magnet by the steps of preparing an admixture of magnetic material and binder material, the admixture material having a particle size of less than 325 mesh. Then heating a carrier gas to a temperature substantially below the melting point of either component of the admixture. The admixture is introduced into the carrier gas and the admixture is sprayed atop a ductile carrier. The admixture adheres to the carrier and forms a solid permanent magnet. An electric field is applied to the sprayed admixture to create a permanent magnetic moment.Type: GrantFiled: July 29, 2002Date of Patent: August 10, 2004Assignee: Ford Global Technologies, LLCInventors: Franco Leonardi, John Matthew Ginder, Robert Corbly McCune
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Patent number: 6761971Abstract: A protective coating for aluminate phosphors is described. The protective coating comprises at least a partial spinel coating having the general formula Mg1-xAl2(1-y)O4-3y-x, where 0≦x<1 and 0≦y<1. The coating is applied by an aqueous solution method which may be compatible with conventional fluorescent lamp manufacturing techniques.Type: GrantFiled: September 26, 2001Date of Patent: July 13, 2004Assignee: Osram Sylvania Inc.Inventors: Madis Raukas, Kailash C. Mishra, Thomas H. Reilly III
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Patent number: 6726964Abstract: A process for depositing metal on microparticulate comprising immersing microparticulate in an autocatalytic plating bath comprising the metal; inducing ultrasonic vibration in the plating bath at a frequency corresponding to resonance frequency of the microparticulate; and inducing a turbulent vibration signal in the plating bath in a direction non-parallel to the ultrasonic vibration. This process results in the autocatalytic plating bath depositing the metal on the microparticulate with uniform thickness. The microparticulate can be spheres, flakes or microfibers, and can be made from a number of materials, such as synthetic polymers (nylon, Kevlar™, Zylon™, and aramid fibers) and biodegradable compounds. A method is disclosed for coating a surface with metallized microparticulate fibers with an orientation perpendicular to the surface.Type: GrantFiled: July 11, 2002Date of Patent: April 27, 2004Inventors: G. Alan Thompson, David E. Marx
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Patent number: 6706330Abstract: The invention relates to a process for coating a surface through graft polymerization, characterized in that before graft polymerization, the surface is modified, in the presence of an amine of formula: wherein R1 is hydrogen or a group R4, R2 and R3 are each independently a group R4, and R4 is [-1,2-C2-C3alkylen-T-]n-H wherein T is O or NH and n is a number from 1 to 3, by a compound having a functional group: wherein R5 to R7 are each C1-C4alkyl. The amount of amine is preferably from 5 to 500 g/m2 of surface of the substrate particle. The amount of the trialkoxysilane compound is preferably from 0.1 to 2 g/m2 of surface of the substrate particle. The process for coating a surface is particularly useful for effect pigments.Type: GrantFiled: May 17, 2002Date of Patent: March 16, 2004Assignee: Ciba Specialty Chemicals CorporationInventors: Ryuichi Takahashi, Adrian Schulthess, Kimiya Takeshita, Fritz Herren, Patrice Bujard
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Patent number: 6685986Abstract: The present invention is for particulate compositions and methods for producing them that can absorb or scatter electromagnetic radiation. The particles are homogeneous in size and are comprised of a nonconducting inner layer that is surrounded by an electrically conducting material. The ratio of the thickness of the nonconducting layer to the thickness of the outer conducting shell is determinative of the wavelength of maximum absorbance or scattering of the particle. Unique solution phase methods for synthesizing the particles involve linking clusters of the conducting atoms, ions, or molecules to the nonconducting inner layer by linear molecules. This step can be followed by growth of the metal onto the clusters to form a coherent conducting shell that encapsulates the core.Type: GrantFiled: January 5, 2001Date of Patent: February 3, 2004Assignee: William Marsh Rice UniversityInventors: Steven J. Oldenburg, Richard D. Averitt, Nancy J. Halas
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Patent number: 6680081Abstract: A conductive powder having an organic silicon polymer layer on the surface of each particle and a metal layer enclosing the silicon polymer layer possesses a stronger bond between the particle base and the metal even at elevated temperature and exhibits a high and stable conductivity and heat resistance.Type: GrantFiled: March 22, 2002Date of Patent: January 20, 2004Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Motoo Fukushima, Kunio Itoh, Shigeru Mori, Masaki Kasashima, Yoshitaka Hamada, Mikio Aramata
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Patent number: 6680128Abstract: Solder compositions, solder pastes and methods of manufacturing thereof having a solder material coated with a coating material by an immersion coating process or an electroless plating process. The solder composition and solder pastes are substantially lead-free and have melting temperatures approaching those of traditional tin-lead solders.Type: GrantFiled: September 27, 2001Date of Patent: January 20, 2004Assignee: Agilent Technologies, Inc.Inventor: Zequn Mei
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Patent number: 6660381Abstract: Metal Nanoshells having partial coverage of a substrate or core particle and methods of making them are provided. A method of making a partial metal nanoshell preferably includes asymmetrically confining a substrate particle and selectively layering a metallic material over the substrate particle according to the asymmetry. Confining the substrate particle may include attaching it to a support defining an exposed portion and a contact portion. The method may include either chemically modifying the substrate particle. The solid angle of coverage of the partial metal nanoshell may be influenced by the nature of the chemical modification, such as alternatives of activating and passivating the exposed portion.Type: GrantFiled: November 5, 2001Date of Patent: December 9, 2003Assignee: William Marsh Rice UniversityInventors: Nancy J. Halas, Robert K. Bradley
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Patent number: 6652968Abstract: A pressure activated electrically conductive polymeric matrix material that is doped with particulate filler material. Electrical conductivity is pressure activated with a change in electrical resistance; specifically, with no pressure applied, the material is at a high resistance and with pressure the resistance is materially lower. Conductive fillers may be spherical or powder substrate, such as glass, graphite, etc., having plated thereon a metal coating which is electrically conductive and which is more thermally conductive than the substrate. The polymeric matrix materials may include polyurethane, silicone, and many other synthetic or natural rubbers.Type: GrantFiled: March 22, 2001Date of Patent: November 25, 2003Inventors: Dorothy H. J. Miller, Brian L. Miller
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Patent number: 6652773Abstract: A polymer dispersion composition obtained by dispersing an electrode active material and a polymer having a gel content of 50% or more in an organic dispersion medium of which boiling point at 760 mmHg is 80° C. or above. The composition is successfully usable as, for instance, a binder composition for batteries, and the battery produced therefrom is high in initial capacity and small in the drop of capacity.Type: GrantFiled: December 3, 2001Date of Patent: November 25, 2003Assignee: Nippon Zeon Co., Ltd.Inventors: Koichiro Maeda, Toshihiro Inoue, Haruhisa Yamamoto, Keiko Imai
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Patent number: 6651871Abstract: A substrate is coated with a conductive layer, which comprises a conductive layer of bonded ultrafine metal particles formed on the top surface thereof. The ultrafine metal particles have a diameter of 1-20 nm, and the substrate is of a flexible high polymer material. Since the conductive layer is formed by bonded layer of the ultrafine metal particles, an extremely thin layer having high conductivity can be formed. This structure enables the formation of a flexible printed circuit board with high-density interconnects or a transparent conductive film provided with both transparency and conductivity. Conventional vacuum equipments and complicated processes are not necessary for forming the conductive layer on the substrate.Type: GrantFiled: November 18, 2002Date of Patent: November 25, 2003Assignee: Ebara CorporationInventor: Naoaki Ogure
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Patent number: 6645625Abstract: The invention relates to a stabilized, pulverulent red phosphorus material composed of phosphorus particles whose particle size is not more than 2 mm, and whose surface has been covered with a thin layer of an oxidation stabilizer, wherein the oxidation stabilizer is silver, and also to the use of the same, and to a process for its preparation.Type: GrantFiled: November 28, 2001Date of Patent: November 11, 2003Assignee: Clariant GmbHInventors: Sebastian Hörold, Jürgen Laubner
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Patent number: 6641918Abstract: Geldhart class C tungsten carbide particles are provided with a discontinuous coating of grain growth inhibitor. Further, the fine tungsten carbide coatings are preferably provided with a continuous coating of another discreet phase material, such as, for example, a continuous coating of cobalt. Compacts produced using such materials are particularly useful as WC—Co hardmetals wherein the compacts are extremely fine grained.Type: GrantFiled: May 30, 2000Date of Patent: November 4, 2003Assignee: Powdermet, Inc.Inventors: Andrew J. Sherman, Animesh Bose
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Publication number: 20030203207Abstract: The invention relates to a method for coating particles and particles thus obtained. According to the inventive method, the particles that are to be coated and at least one organo-metallic complex precursor of the coating material are brought into contact with each other in a liquid containing one or several solvents, whereby said particles are maintained in a dispersion in the liquid which is subjected to temperature conditions and supercritical pressure or slightly sub-critical pressure conditions; the precursor of the coating material is transformed in such a way that it is deposited onto the particles, whereupon the liquid is placed in temperature and pressure conditions so that it can eliminate the solvent in a gaseous state. The invention can be used to coat nanometric particles in particular.Type: ApplicationFiled: April 24, 2003Publication date: October 30, 2003Applicant: Centre National de la Recherche ScientifiqueInventors: Vincent Pessey, Francois Cansell, Bernard Chevalier, Francois Weill, Jean Etourneau
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Patent number: 6599608Abstract: Substantially spherical magneto-plumbite ferrite (barium or strontium ferrite) particles are formed from well-dispersed ultra-fine substantially spherical iron-based oxide and/or hydroxide particles as precursor particles. The precursor particles are mixed with a colloidal barium or strontium carbonate (BaCO3 or SrCO3), and with small amounts of a byproduct, such as sodium or potassium chloride (NaCl or KCl) or hydroxide (NaOH or KOH) or nitrate (NaNO3 or KNO3), functioning as a flux to lower the calcination temperature. The particles are filtered out of the mixture, dried, and calcined for a time sufficiently long and/or at a temperature sufficiently high to form magneto-plumbite ferrite from the precursor particles, and for a time sufficiently short and/or a temperature sufficiently low to maintain the general spherical shape of the precursor particles.Type: GrantFiled: July 8, 2002Date of Patent: July 29, 2003Assignee: Idaho Research Foundation, Inc.Inventors: Yang-Ki Hong, Hong Sik Jung, Patrick R. Taylor
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Patent number: 6596342Abstract: A method of coating of mass-produced bulk goods (5) including loading the bulk goods (5) into a rotatable drum (1) through an opening (4) formed in a side surface of the drum (1), heating a coating material in coating apparatus (8), having a spray gun (6) and provided outside of the rotatable drum (1); and thereafter, applying the heated coating material to the bulk goods (5) with the spray gun (6) through the drum opening (4).Type: GrantFiled: December 21, 2001Date of Patent: July 22, 2003Assignee: Hilti AktiengesellschaftInventors: Rainer Batliner, Gerald Felder, Werner Schörghofer
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Patent number: 6592935Abstract: A method of manufacturing electric machines comprised of geometrically patterned arrays of permanent magnets, soft magnetic materials, and electrical conductors deposited by kinetic spraying methods directly atop a carrier. The magnets and planar coils of the present invention may be integrally formed atop carriers to form electrical machines such as motors, generators, alternators, solenoids, and actuators. The manufacturing techniques used in this invention may produce highly defined articles that do not require additional shaping or attaching steps. Very high-purity permanent and soft magnetic materials, and conductors with low oxidation are produced.Type: GrantFiled: May 30, 2001Date of Patent: July 15, 2003Assignee: Ford Motor CompanyInventors: Franco Leonardi, John Matthew Ginder, Robert Corbly McCune
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Patent number: 6592938Abstract: The invention relates to a method for coating particles thus obtained. According to the inventive method, the particles that are to be coated and at least one organo-metallic complex precursor of the coating material are brought into contact with each other in a liquid containing one or several solvents, whereby said particles are maintained in a dispersion in the liquid which is subjected to temperature conditions and supercritical pressure or slightly sub-critical pressure conditions; the precursor of the coating material is transformed in such a way that it is deposited onto the particles, whereupon the liquid is placed in temperature and pressure conditions so that it can eliminate the solvent in a gaseous state. The invention can be used to coat nanometric particles in paticular.Type: GrantFiled: October 1, 2001Date of Patent: July 15, 2003Assignee: Centre National de la Recherche ScientifiqueInventors: Vincent Pessey, François Cansell, Bernard Chevalier, François Weill, Jean Etourneau