Abstract: A sliding member for which adhesiveness between the surface of a base member and metal coating is enhanced. An undercoat layer having a resin material at the surface thereof is provided, and a solid lubricating portion is formed on the undercoat layer so as to provide a sliding face from at least one kind of material of silver, silver alloy, copper and copper alloy. An intermixture layer in which both the undercoat layer and the solid lubricating portion are intermixed with each other is interposed between the undercoat layer and the solid lubricating portion.

Abstract: A method for making device housing comprises: providing a transparent film; forming a coating on one surface of the film by printing ink containing metal powder on the film and ultrasonically treating the coating; and molding a substrate onto the coating.

Abstract: A long range, periodically ordered array of discrete nano-features (10), such as nano-islands, nano-particles, nano-wires, non-tubes, nano-pores, nano-composition-variations, and nano-device-components, are fabricated by propagation of a self-assembling array or nucleation and growth of periodically aligned nano-features. The propagation may be induced by a laterally or circularly moving heat source, a stationary heat source arranged at an edge of the material to be patterned (12), or a series of sequentially activated heaters or electrodes. Advantageously, the long-range periodic array of nano-features (10) may be utilized as a nano-mask or nano-implant master pattern for nano-fabrication of other nano-structures.

Abstract: Disclosed herein is a method of preventing corrosion degradation in a defective region including an expansion transition region and/or an expansion region of a heat transfer tube of a steam generator in a nuclear power plant by using nickel (Ni) plating or nickel (Ni) alloy plating. The method can prevent various types of corrosion damage, such as pitting corrosion, abrasion, stress corrosion cracking, lead-induced stress corrosion cracking and the like, occurring during the operation of the steam generator, and particularly, pitting corrosion or primary and secondary stress corrosion cracking, so that the life span of the steam generator is increased, maintenance costs are reduced, and the operation rate of a nuclear power plant is increased, with the result that the unit cost of the production of electric power can be decreased, thereby improving economic efficiency.

Abstract: A method of forming conductive features on a substrate, the method comprising: providing two or more solutions, wherein a metal nanoparticle solution contains metal nanoparticles with a stabilizer and a destabilizer solution contains a destabilizer that destabilizes the stabilizer, liquid depositing the metal nanoparticle solution and the destabilizer solution onto the substrate, wherein during deposition or following the deposition of the metal nanoparticle solution onto the substrate, the metal nanoparticle and the destabilizer are combined with each other, destabilizing the stabilizer from the surface of the metal nanoparticles with the destabilizer and removing the stabilizer and destabilizer from the substrate by heating the substrate to a temperature below about 180° C. or by washing with the solvent.

Abstract: Mechanical plating provides a new technique of manufacturing of certain materials containing multiple elements, including amalgams, and novel pellets containing multiple materials. Some embodiments provide new and versatile materials for dosing mercury, metals or other inorganic compounds into lamps. Some embodiments include materials comprising layers of metals or compounds built up on a substrate. One embodiment is a layer of zinc amalgam applied to a glass sphere. Also disclosed is an improved method of manufacture for such particles that will speed production, increase yields, lower costs and reduce exposure to mercury in the workplace.

Abstract: A spangle-free, hot-dip galvanized steel sheet, and a method and device for manufacturing the same. The hot-dip galvanized steel sheet is characterized in that a solidified zinc crystal of hot-dip galvanized layer has an average crystalline texture particle diameter of 10 to 88 ?m and there is no solidification traces of dendrites upon observing under a microscope at a magnification of 100×. The method comprises dipping a steel sheet in a bath of a zinc-coating solution containing 0.13 to 0.3% by weight of aluminum; air-wiping the steel sheet to remove an excess of the coating solution; spraying water or an aqueous solution on the air-wiped steel sheet, using a steel sheet temperature in the range of a hot-dip galvanization temperature to 419 ° C. as a spray initiation temperature and using a steel sheet temperature in the range of 417 ° C. to 415 ° C.

Abstract: An improved protective coating, for parking meters or other equipment that is subject to environmental deterioration and/or vandalism, having thereon at least a three layer coating of a composite thickness sufficiently thick to avoid pinholes and sufficiently thin to avoid crazing and cracking due to variations in the ambient environment. The coating has a conventional lower layer of zinc on or proximate to the equipment surface (in the alternative the substrate may be a zinc part); a second layer of a thermosetting polymer that has been applied by a powder coating electrostatic method, and a third, top, coating of an epoxysiloxane polymer. The total coating thickness should preferably not exceed about 6 mils.

Abstract: A ferrite layer formation process that may be performed at a lower temperature than conventional ferrite formation processes. The formation process may produce highly anisotropic structures. A ferrite layer is deposited on a substrate while the substrate is exposed to a magnetic field. An intermediate layer may be positioned between the substrate and the ferrite to promote bonding of the ferrite to the substrate. The process may be performed at temperatures less than 300° C. Ferrite film anisotropy may be achieved by embodiments of the invention in the range of about 1000 dyn-cm/cm3 to about 2×106 dyn-cm/cm3.

Abstract: A method of electroless plating for processing a plating surface to form a barrier layer being capable of uniformly forming a barrier layer and reducing the consumption of a processing solution, comprising a step of feeding a processing solution used in at least one of the pre-processing steps of the electroless plating and the electroless plating step to the plating surface for puddling treatment, or, using a processing solution at least containing, with respect to one mole of a first metallic material supplying a main ingredient of the barrier layer, three or more moles of a completing agent and three or more moles of reducing agent and having a pH value adjusted to 9 or more and stored in an atmosphere of an inert gas or ammonia gas, and a corresponding electroless plating apparatus.

Abstract: A holder for electroless plating to hold a plurality of ceramic elements for ceramic electronic parts during electroless plating treatment, each surface of said ceramic elements being to be electroless plated, said holder comprising a plurality of cells to house each of said plurality of ceramic elements separately, and each of said cells having such a structure as to permit the flow communication of a plating solution into the cell.

Abstract: A surface treatment method that increases the wear resistance of contact portions of levers of a diaphragm spring in a clutch cover assembly and of a plate member that slides there-against is provided. The surface treatment method is applied to the contact portions of the diaphragm spring of the clutch cover assembly and to the plate member that slides there-against. In this method, the contact portion of the diaphragm spring and the sliding portion of the plate member are designated as treatment surfaces. The treatment surfaces are subjected to an electric discharge coating using a coating material such that the treatment surface is covered with a coating layer of approximately 50 &mgr;m or less and a diffusion layer is formed inside the treatment surface.

Abstract: A single component liquid heat-curable adhesive formulation that is stable at room temperature. The formulation includes from about 5 to about 70 wt % of at least one acrylate monomer, from about 5 to about 94 wt % of an acrylate oligomer, and from about 0.1 to about 10 wt % of a thermal initiator selected from the group consisting of diacyl peroxides, benzoyl peroxides and peroxy esters. A photo initiator may be included thereby rendering the stable liquid formulation to be both heat-curable and UV-curable.

Abstract: A zinc coating directly covers a bare ferrous base of parking meter housing parts. A non-epoxy thermosetting electrically insulating organic non-epoxy powder coating directly covers the zinc coating. The organic coating is directly applied to the zinc coating by electrostatically charging the powder and parts with opposite d.c. voltage polarities and by heating the powder so it adheres to and covers the zinc coating. Alternatively, the base is zinc, directly covered by the organic powder coating.

Abstract: A process for reclaiming aluminum alloy donor from a vapor phase deposition process used to form a diffusion aluminide coating on a component, such as the high-temperature superalloy components of gas turbine engines. The process generally entails recycling a particulate aluminum alloy donor material that, as a result of having been used as the donor material for depositing a diffusion aluminide coating on an article by vapor phase deposition, particles of the donor material comprise an aluminum alloy core encased in an aluminum-depleted shell. The process generally entails tumbling the donor material in a manner that removes the aluminum-depleted shell, followed by sieving the donor material to remove shell fragments and undersized particles.

Abstract: A method for removing contaminants from a semiconductor wafer having a spin on coating of material. Contaminants are removed by applying a cleaning solution to the periphery, and preferably, the exposed backside of the wafer after the edge bead has been dissolved and removed. The cleaning solution is formulated to react chemically with unwanted coating material residue to form a compound that may be ejected from the periphery of the spinning wafer. Any residual solution or precipitate that is not ejected from the wafer may be rinsed away with water, preferably deoinized water. One exemplary use of this method is the removal of metallic contaminants that may be left on the periphery and backside of a wafer after the formation of ferroelectric film coatings. A cleaning solution comprising a mixture of hydrochloric acid HCl and water H2O or ammonium hydroxide NH4OH and water H2O is applied to the periphery of the spinning wafer.

Abstract: An Fe—B—R based permanent magnet and metal pieces are placed into a treating vessel, where they are vibrated and/or agitated, whereby a metal film is formed on the surface of the magnet. A sol solution produced by the hydrolytic reaction and the polymerizing reaction of a metal compound which is a starting material for a metal oxide film is applied to the metal film and subjected to a heat treatment to form a metal oxide film. Therefore, it is possible to form, on the surface of the magnet, a corrosion-resistant film which can be produced easily and at a low cost without carrying-out of a plating treatment or a treatment using hexa-valent chromium and which has an excellent adhesion to the surface of the magnet and can exhibit a stable high magnetic characteristic which cannot be degraded even if the magnet is left to stand for a long period of time under high-temperature and high-humidity conditions of a temperature of 80° C. and a relative humidity of 90%.

Abstract: The present invention provides methods of electrolessly depositing metal onto the surfaces of electronic components using an enclosable single vessel. The methods of the present invention include contacting the electronic components with an activation solution followed by contacting the electronic components with a metal deposition solution. In a preferred embodiment of the present invention, the oxygen levels in the activation solution and metal deposition solution are controlled in a manner for improved processing results. In another preferred embodiment of the present invention, the activation and metal deposition solutions are used one time without reuse.

Abstract: A method for removing contaminants from a semiconductor wafer having a spin on coating of material. Contaminants are removed by applying a cleaning solution to the periphery, and preferably, the exposed backside of the wafer after the edge bead has been dissolved and removed. The cleaning solution is formulated to react chemically with unwanted coating material residue to form a compound that may be ejected from the periphery of the spinning wafer. Any residual solution or precipitate that is not ejected from the wafer may be rinsed away with water, preferably deionized water. One exemplary use of this method is the removal of metallic contaminants that may be left on the periphery and backside of a wafer after the formation of ferroelectric film coatings. A cleaning solution comprising a mixture of hydrochloric acid HCl and water H.sub.2 O or ammonium hydroxide NH.sub.4 OH and water H.sub.2 O is applied to the periphery of the spinning wafer.

Abstract: An automated method and apparatus for galvanizing threaded rods, comprising conveying threaded rods while horizontally oriented through a bath of molten zinc, then simultaneously spinning the threaded rods in horizontal orientation at sufficient rotational velocity to remove excess molten zinc therefrom by centrifugal force and conveying the threaded rods to a cooling bath. The automated apparatus then conveys the zinc coated threaded rods through a cooling bath to solidify the molten zinc coating and then collects cooled zinc coated threaded rods to permit efficient removal thereof from the apparatus. A rotary conveyor mechanism of the automated apparatus conveys the threaded rods through a molten zinc bath and removes excess molten zinc therefrom by rolling the coated threaded rods down an inclined zinc removal platform.

Abstract: An improved process for chromizing commercial quantities of small, industrial, ferrous-based parts, such as but not limited to threaded connectors, pins, bolts, nuts, washers, fasteners, fittings, couplings, studs, etc., uses a retort filled with layers of parts coated with a chromium-containing slurry. The plurality of parts are arranged in layers on sheets of refractory felt paper and are heat treated simultaneously for causing the chromizing reaction between the slurry and the ferrous-based parts.

Abstract: A method of manufacturing a terminated ceramic capacitor comprises forming the capacitor in the configuration of a parallelepiped having end surfaces joining the major base portions which define an acute angle with one base and an obtuse angle with the other. Electrodes of opposite polarities are exposed at the opposite end surfaces. A conductive coating, generally of metal or metal frit is applied to the entire end and base surfaces, the side surfaces being maintained clear of termination material. By removing termination materials from the acute angle junctions of end and base surfaces there is provided a capacitor which may be inserted into a circuit by contact with the opposite bases or the opposite ends. the invention relates also to the unique resultant capacitor.

Abstract: A method is disclosed of forming thin uniform micron range and submicron range aberration-resistant and hole-free high-temperature thermally stable metal oxide coatings upon metal, insulating and other substrates, involving the application of a polymer metal complex precursor solution to the substrate and appropriate firing for oxidation of the metal and the coating while burning off all traces of the polymer.

Abstract: A method of tinning tinnable areas of an electronic component package, the method comprising a first step during which additional metal is applied in the liquid state to said tinnable areas, and a following step during which at least one cycle of oscillations about an equilibrium position is applied to the package while said metal thus applied is still in the liquid state, for the purpose of setting up successive and opposite displacements of masses of said metal along said areas in order to obtain a uniform distribution of said metal over said areas.

Abstract: A method and apparatus for tinning and soldering metal parts of electronic components and assemblies, and removing excess solder therefrom. The metal parts of the electronic components and assemblies are heated to a temperature near that of molten solder. A holding fixture, adapted to hold the heated components, slidably connects to an acceleration means which dips the metal parts of the components into the molten solder. Then acceleration energy is applied to the acceleration means, causing it to rapidly remove the components from the molten solder. Rapidly removing the components from the molten solder leaves excess solder behind, whereby all metal parts of the components are thoroughly tinned and soldered together without leaving unwanted solder bridges therebetween. A vibration means may also be used to prevent solder voids and promote solder wetting in densely packed leads and rails being tinned.

Abstract: A method of infiltrating a porous ceramic compact with a molten metal to form a cermet is disclosed. A solid-phase metal is disposed on a surface of a porous ceramic compact. The surface of the porous ceramic compact is at an angle to the horizontal which is sufficient to allow molten metal formed from the solid-phase metal to rupture an oxide layer at least partially supporting the molten metal. The solid-phase metal is heated to a temperature sufficient to melt the solid-phase metal and to allow the molten metal formed to rupture the oxide layer. The molten metal flows through an opening in the metal oxide layer formed by the rupture and infiltrates the porous ceramic compact. The porous ceramic compact, containing the molten metal, is then cooled to a temperature whereby the molten metal solidifies, thereby forming a cermet.

Abstract: An improved method and an apparatus for the ion implantation of spherical surfaces are disclosed. The method includes the provision of a revised fixture by which a plurality of spherical workpieces are presented to a large area ion beam in a way that their entire respective spherical surfaces are uniformly ion implanted to improve their surface characteristics. The fixture includes a disc mounted for motion about two axes normal to each other, a plurality of holes formed in a the disc loosely to accommodate therein a plurality of spherical workpieces, each of the plurality of holes formed with a spherical bottom and having a cleaning orifice, cooling means disposed on one side of the disc, a thermocouple operatively mounted in association with the disc, and a cover plate mounted on a second side of the disc and provided with a plurality of apertures concentric with the plurality of holes formed in the disc.

Abstract: An electroless metal plating process, particularly for use in plating through-holes in printed circuit substrates, and more particularly for additively depositing copper metal on through-hole surfaces, in which the substrate is at least intermittently subjected to vibrating motion in contact with the electroless depositing bath, and an electroless metal depositing apparatus for carrying out the process.

Abstract: On spray-forming metals onto a substrate from which the sprayed coating is to be detached, unwanted adhesion may occur, even to a smooth substrate. Conversely, if the coating is meant to adhere, it may accidentially delaminate, even from a roughened substrate.By vibrating the substrate, marginally adherent splats will be encouraged to detach themselves while, on the other hand, well adherent splats will not be affected.

Abstract: A method for the manufacture of catalyst electrodes with structurally connected carrier bodies, in which an excess of catalyst suspension is applied to the surface of the carrier body which thereafter is centrifuged off by rotation of the carrier body about an axis disposed perpendicularly to its surface. An aqueous suspension with Raney nickel as catalyst, which is particularly suitable as an example for the use in the coating method, has a dynamic viscosity of 10,000 to 50,000 mPa . s at a temperature of 20.degree. C. as well as a solids content of 55 to 75% by weight. An extraordinarily uniform coating can be acheived with the method of the present invention.

Abstract: A method and apparatus for producing flush solder fill over recessed pins and over passage holes in circuitized substrates. A substrate carrying rack is immersed in a vessel of molten solder after it has been similarly immersed in a flux bath. While in the molten solder, the rack is vigorously agitated. The rack is then withdrawn from the molten solder and is pivoted upwardly while positioned over the molten solder. Simultaneously, an anvil is rotated from a home position to an impact position at precisely the correct moment. With the solder still molten on the substrate surfaces, the rack is then permitted to descend and is positively biased to strike the anvil thereby dislodging any excess molten solder. A unique supporting arrangement for the rack insures that only a minimum of mass actually impacts against the anvil while insuring the effectiveness of the operation.

Abstract: A soldering apparatus includes a solder bath 40 and a component holder 43 positioned to lower an exposed tag of a component to contact solder in the solder bath 40. After removal from the bath the component is deliberately subjected to a mechanical shock when a limb of a bracket 44 strikes a turret plate 42 under the action of a spring 46. The shock causes a short time vibration in the component and spreads solder in tears which naturally form on the exposed tags to remove or substantially reduce those tears.

Abstract: Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

Abstract: During the pre-soldering of printed circuit boards, as a rule, also the drill holes or bores and, in particular, the through-metallized drill holes are filled in an undesirable manner with solder. This solder must be removed before mounting the electrical components or elements upon the printed circuit boards. A simple method is disclosed for this purpose, affording a faultless de-soldering of the drill holes, without deleteriously affecting the properties of the solder material. The printed circuit boards, in a condition where the solder applied during the pre-soldering operation is still molten, are accelerated at least once and thereafter suddenly brought to standstill in such a fashion that the excess solder is knocked or propelled out of the drill holes.

Abstract: A method for electroless nickel plating of silicon-iron which has been heat treated prior to the plating operation and subjected to thermal shock after the plating operation includes the steps of cleaning the surface of the silicon-iron with a fluoride etch salt, forming a thin deposit of palladium on the clean surface of the silicon-iron, hardening the palladium deposit by treatment with a solution of ammonium hydroxide and nickel plating the silicon-iron using an electroless nickel plating solution, followed by baking at about 250.degree. F. for about six hours.

Abstract: An improved galvanizing system is provided having a centrifuge assembly wherein an elongate member positively couples a motor means to a container holding articles to be spun. This positive engagement results in more rapid rotational acceleration and deceleration. A dumping means is provided to automatically remove articles from the container. Further, an automated ejection means is provided for removing the empty container from the centrifuge assembly.

Abstract: Seafood pots made of wire mesh netting are prepared for galvanizing by first passing them through an incineration chamber to burn, melt and loosen foreign material thereon, and then passing them through a high pressure liquid spray to remove residual burned matter and loosened foreign material. The pots are then ready to be passed through the steps of the galvanizing process, which includes dipping the pots into heated preflux before they are dipped into molten zinc. An inverted drying chamber bridges the distance between the preflux tank and the zinc kettle, through which the seafood pots are moved by conveyor means to dry the preflux, with drying heat within the chamber being drawn from the tank and the kettle. The seafood pots are vibrated as they are withdrawn from the molten zinc to effect an even coating of zinc on the wire mesh netting thereof.

Abstract: An article comprising: (1) an interpolymer which comprises crosslinked (meth)acrylate, crosslinked styrene-acrylonitrile, and uncrosslinked styrene-acrylonitrile components; and (2) an adherent metallic coating on said interpolymer. The article is useful as a plated component in motor vehicles, for example, as trim, grille work, wheel covers, and the like, or as plated appliance parts or plumbing components.

Abstract: Articles of almost any imaginable configuration are given a uniform, complete coating over all surfaces by placing them in a spinnable perforate container or basket that is suspended from a reversible spinning assembly which is adapted to spin the perforate container and its articles in both directions during steps of the process of pre-coating, coating, quenching or air drying.A new control system is also employed to provide rapid response in reversing directions of rotation of the perforated container or bringing it to a complete stop.

Abstract: A method of draining parts emerging from hot galvanizing baths using a range of vibration excitation frequencies capable of covering the fundamental frequencies of the parts to be drained. Three different methods are disclosed. According to a first method the vibrations are obtaining by exciting with a narrow band white noise the support for the parts to be drained. According to a second method, the vibrations are produced from a single exciter fed with narrow band white noise and energizing vibrators through the medium of amplifiers. According to a third method, the vibrations are produced by a number of small vibrators each of which furnishes one of the frequencies of the chosen spectrum, whereby said vibrators jointly synthesize the narrow band white noise.

Abstract: A process for removing excess molten aluminum or its alloys from articles following the aluminizing of same in such melt by high speed revolution of said articles while withdrawing from said melt.

Abstract: A method of draining parts emerging from hot galvanizing baths using a range of vibration excitation frequencies capable of covering the fundamental frequencies of the parts to be drained. Three different methods are disclosed. According to a first method the vibrations are obtaining by exciting with a narrow band white noise the support for the parts to be drained. According to a second method, the vibrations are produced from a single exciter fed with narrow band white noise and energizing vibrators through the medium of amplifiers. According to a third method, the vibrations are produced by a number of small vibrators each of which furnishes one of the frequencies of the chosen spectrum, whereby said vibrators jointly synthesize the narrow band white noise.

Abstract: A method for coating a metal wire with a thin layer of a second powdered metal. A metal flake powder having a residual surface lubricant from a prior milling operation is placed in the lubricant holding box of a conventional draw bench. The wire to be coated is passed through the metal flake powder and drawn through a conventional drawing die to provide a green-coat wire having a mechanically adherent metal flake powder coating. The green-coat wire is subsequently sintered to metallurgically bond the coating to the wire surface.

Abstract: A method of producing a refractory lining in a cylinder or tube by initiating an exothermic reduction reaction, such as an aluminothermic reduction reaction, within the cylinder and causing the reaction products to coat the interior of the tube substantially uniformly. The product of the method, a ceramic-or refractory-lined cylinder, is also disclosed.

Abstract: Preparation of thin layers of tungsten or molybdenum on a highly temperature-resistant layer substrate by thermal evaporation in a high vacuum, where WO.sub.3 or MoO.sub.3, respectively, is evaporated and the layer substrate is heated so that the oxides are decomposed and a pure tungsten or molybdenum layer is deposited on the layer substrate.

Abstract: This application discloses "wiping" of a liquid, molten zinc, for example, across the surface of a strip to which it adheres. A wiping fluid, such as steam, is directed from an orifice at the strip. A valve, preferably an elongated relieved bar is positioned adjacent and behind the orifice, and flow of wiping fluid is controlled by rotation of an elongated valve in the form of a relieved bar or cam.

Abstract: A method and apparatus for electroless plating of a metal on a workpiece overcomes the problem of metal plating on solid particles suspended in the solution and on those parts of the plating apparatus in contact with the solution by maintaining a concentration of anticatalytic substance, such as lead ions, between about 10.sup.-.sup.6 and 10.sup..sup.-1 mols per liter and maintaining a relative speed of more than about 0.9 meter per second between the solution and those parts of the apparatus in contact with the solution.