Glass, Ceramic Or Metal Oxide In Coating Patents (Class 428/384)
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Patent number: 6555222Abstract: A reinforced polypropylene mirror assembly, and process for making the same, are described. The mirror assembly, especially the components thereof, includes a long glass fiber reinforced polypropylene material. Additionally, various additives may also be included in the reinforced polypropylene material, such as a UV stabilizer. Because of the physical properties of the reinforced polypropylene material, it is possible to combined several individual components of a conventional automobile side view mirror assembly into single, integral components, thus reducing part content, vehicle weight, and construction costs.Type: GrantFiled: January 13, 2000Date of Patent: April 29, 2003Assignee: Schefenacker Vision Systems France SAInventors: Bernard Duroux, Gilles Benoit
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Publication number: 20030068487Abstract: A crosslinkable thermal interface material is produced by combining at least one rubber compound, at least one amine resin and at least one thermally conductive filler. This interface material takes on the form of a liquid or “soft gel”. The gel state is brought about through a crosslinking reaction between the at least one rubber compound composition and the at least one amine resin composition. Once the foundation composition that comprises at least one rubber compound, at least one amine resin, and at least one thermally conductive filler has been prepared, the composition must be compared to the needs of the electronic component, vendor, or electronic product to determine if a phase change material and/or at least one solvent is needed to change some of the physical properties of the composition.Type: ApplicationFiled: September 9, 2002Publication date: April 10, 2003Inventors: My Nguyen, Kim-Chi Le
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Patent number: 6534196Abstract: The present invention relates to articles, having an extended useful life, which are used in contact with high temperature molten aluminum or molten zinc baths. One aspect of the invention encompasses articles, such as bearings, bushings, couplings or rollers, used in contact with molten aluminum or molten zinc which is coated with a high density coating consisting of a metal selected from Groups Vb, VIb, or VIIb metals (preferably molybdenum or tungsten), in pure or alloyed form. These coatings generally have a thickness of from about 0.06 to about 0.30 inch. Another aspect of the present invention encompasses a roll for guiding steel strip through a high temperature aluminizing bath, which utilizes a multi-layer structure, the first primer layer being a Group Vb, VIb or VIIb metal, preferably tungsten or molybdenum (in pure or alloyed form), the second layer comprising MCrAlY in which M is either nickel or cobalt, and the third layer comprising a refractory metal oxide of Al, Zr, Si or Cr.Type: GrantFiled: February 26, 2001Date of Patent: March 18, 2003Assignee: Cincinnati Thermal SprayInventor: Robert K. Betts
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Patent number: 6521344Abstract: A member for brakes that has a light weight, shock resistance characteristics, excellent corrosion resistance characteristics etc., high abrasive wear resistance characteristics and is made from fiber-composite material is comprised of an assemblage of yarns in which yarns, containing at least a bundle of carbon fibers and a carbon component other then carbon fiber are three-dimensionally combined and integrally formed so as to avoid separation there between; and matrices made of Si—SiC-based material filling the spaces between said yarns adjacent to each other within said assemblage of yarns.Type: GrantFiled: October 23, 1998Date of Patent: February 18, 2003Assignee: NGK Insulators Ltd.Inventor: Shigeru Hanzawa
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Patent number: 6479144Abstract: Polyurethane elastomer yams (particularly spandex) containing certain silver-based antimicrobial formulations therein are provided. This invention relates to polyurethane elastomer yams (particularly spandex) containing certain silver-based antimicrobial formulations therein. Such formulations comprise antimicrobial compounds, such as, preferably, triclosan and/or silver-containing ion-exchange resins, such as zirconium phosphate, glass, and/or zeolite compounds. The inventive spandex yarns exhibit excellent antimicrobial qualities as well as surprisingly good anti-tack/frictional characteristics. As a result, antimicrobial spandex yams are provided which exhibit ease in processing, particularly in further knitting, weaving, etc., to produce fabrics therefrom. Such fabrics are also encompassed within this invention.Type: GrantFiled: December 4, 2000Date of Patent: November 12, 2002Assignee: Milliken & CompanyInventors: Randy D. Petrea, Robert L. Schuette, Leland G. Close, Jr., Shirley Anne Whiteside
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Publication number: 20020119304Abstract: The present invention relates to metal oxide particles capable of being highly dispersed in organic materials to form transparent colloids and ceramers. The metal oxide particles of the present invention have surfaces attached to a dispersing aid and a degree of crystallinity of greater than 55 percent. The crystallite diameter of the metal oxide particles is greater than about 4 nanometers and less than about 20 nanometers. The present invention also relates to the colloids and ceramers prepared using these metal oxide particles and the methods associated with the preparation of the particles, colloids, and ceramers.Type: ApplicationFiled: November 19, 2001Publication date: August 29, 2002Applicant: 3M Innovative Properties CompanyInventors: David S. Arney, Thomas E. Wood
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Publication number: 20020084103Abstract: The present invention provides a silicon nitride ceramic substrate composed of a silicon nitride sintered body in which maximum size of pore existing in grain boundary phase of the sintered body is 0.3 &mgr;m or less, and having a thermal conductivity of 50 W/mK or more and a three point bending strength of 500 MPa or more, wherein a leak current is 1000 nA or less when an alternative voltage of 1.5 kV-100 Hz is applied to a portion between front and back surfaces of the silicon nitride sintered body under conditions of a temperature of 25° C. and a relative humidity of 70%. According to the above structure of the present invention, there can be provided a silicon nitride ceramic substrate capable of effectively suppressing a leak current generation when the above substrate is assembled into various power modules and circuit boards, and capable of greatly improving insulating property and operative reliability of power modules in which output power and capacity are greatly increased.Type: ApplicationFiled: October 26, 2001Publication date: July 4, 2002Applicant: KABUSHIKI KAISHA TOSHIBAInventors: Michiyasu Komatsu, Haruhiko Yamaguchi, Takayuki Naba, Hideki Yamaguchi
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Patent number: 6406788Abstract: An elastic polyurethane fiber excellent in chlorine resistance, which contains particles of a metal compound selected from oxides and hydroxides of a metal selected from zinc and magnesium, and composite oxides of zinc and magnesium, a treating agent selected from a fatty acid, a styrene/maleic anhydride copolymer or its esterified products and a phosphoric ester adhering to the surface of the particles. The elastic polyurethane fiber is appropriate for an elastic fiber material for swimwear used in a swimming pool. The elastic polyurethane fiber can be produced by spinning a polyurethane spinning dope containing the metal compound particles to which such a specific treating agent as mentioned above adheres. The spinning dope suppresses secondary agglomeration of the metal compound particles and enables stabilized spinning of a modified polyurethane fiber.Type: GrantFiled: February 8, 2001Date of Patent: June 18, 2002Assignee: Asahi Kasei Kabushiki KaishaInventors: Masanori Doi, Akihiko Yoshizato
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Publication number: 20020038680Abstract: Disclosed herein is a cooling roll which can provide bonded a magnet having excellent magnetic properties and having excellent reliability. A melt spinning apparatus is provided with a tube 2 having a nozzle 3 at the bottom thereof, a coil 4 for heating the tube and cooling roll 5 having a circumferential surface 53 in which dimple correcting means is provided. A melt spun ribbon 8 is formed by injecting the molten alloy 6 from the nozzle 3 so as to be collided with the circumferential surface 53 of the cooling roll 5 in an inert gas atmosphere (ambient gas) such as helium gas, so that the molten alloy 6 is cooled and then solidified. In this process, dimples to be produced on a roll contact surface of the melt spun ribbon are divided by the dimple correcting means, thereby preventing formation of huge dimples.Type: ApplicationFiled: May 30, 2001Publication date: April 4, 2002Inventors: Akira Arai, Hiroshi Kato
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Patent number: 6352771Abstract: A conductive roller for use in a laser printer includes a solid, thermoset urethane comprising a metal salt and having a hardness of between 30 Shore A and 50 Shore A on cube and a volume resistivity of 1E6 ohm-cm and 9E8 ohm-cm.Type: GrantFiled: February 24, 1999Date of Patent: March 5, 2002Assignee: Mearthane Products CorporationInventors: Albert C. Chiang, John A. Roderick
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Patent number: 6322889Abstract: A ceramic-matrix composite having a multilayered interfacial coating adapted to protect the reinforcing fibers from long-term oxidation, while allowing these to bridge the wake of advancing cracks in the matrix, is provided by selectively mismatching materials within adjacent layers of the interfacial coating, the materials having different coefficients of thermal expansion so that a low toughness interface region is created to promote crack deflection either within an interior layer of the mismatched interfacial coating or between adjacent layers of the mismatched interfacial coating.Type: GrantFiled: April 22, 1999Date of Patent: November 27, 2001Assignee: The United States of America as represented by the United States Department of EnergyInventors: Edgar Lara-Curzio, Karren L. More, Woo Y. Lee
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Publication number: 20010031596Abstract: A method of manufacturing a bearing material, a bearing material and a bearing having the bearing material on a strong backing are described.Type: ApplicationFiled: April 16, 2001Publication date: October 18, 2001Inventors: Julie Ann McDonald, John Edward Wheatley, Anthony Latkowski, David Geoffrey Hall
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Patent number: 6291067Abstract: A photocatalytic powder for environmental clarification, comprising finely divided titanium dioxide particles having a coating of porous calcium phosphate formed on at least part of the surface of each titanium dioxide particle, wherein an anionic surface active agent is present at least on the interface between said coating of porous calcium phosphate and the titanium dioxide particle. This photocatalytic powder is produced by dispersing finely divided titanium dioxide particles in an aqueous slurry containing an anionic surface active agent, and then forming a coating of porous calcium phosphate on at least part of the surface of each titanium dioxide particle. This photocatalytic powder is used, for example, by supporting it in an organic polymer shaped article.Type: GrantFiled: July 14, 2000Date of Patent: September 18, 2001Assignees: Japan as represented by Director General of the Agency of Industrial Science and Technology, Showa Denko Kabushiki KaishaInventors: Hiroshi Taoda, Toru Nonami, Katsura Ito, Hiroyuki Hagihara
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Patent number: 6113861Abstract: A photocatalytic sheet which has a base made of polymeric organic compound, that is not decomposed by a photocatalytic function, and also hardly loses the photocatalytic function after washing and is capable of providing the photocatalytic function even in an environment without sufficient ultraviolet radiation from outside. Using a fiber, a filament, a yarn made of fibers or filaments, a ribbon, a knitted fabric, a woven fabric, a nonwoven fabric, or a film as the base, a base protective layer is formed on a part of the base, which is made of the polymeric organic compound, and a photocatalytic semiconductor layer is formed on the entire surface of the base including the base protective layer.Type: GrantFiled: February 27, 1998Date of Patent: September 5, 2000Assignee: TAO, Inc.Inventor: Shiro Ogata
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Patent number: 6074750Abstract: A composite comprised of reinforcement fibers having a continuous coating of a metal nitride wherein the metal is from the group consisting of silicon, aluminum, titanium, zirconium, hafnium, niobium, tantalum, and mixtures thereof, and a molten silicon infiltration formed silicon carbide matrix. The reinforcement fibers are fibers from the group consisting of elemental carbon, silicon carbide, and mixtures thereof. A method of forming the composite comprises depositing a continuous coating of the metal nitride on the fibers. A carbonaceous material is admixed with the coated fibers so that at least 5 volume percent of the mixture is the coated fibers. The mixture is formed into a preform having an open porosity ranging from about 25 volume percent to about 90 volume percent of the preform. The preform is heated in an inert atmosphere or partial vacuum, and infiltrated with molten silicon to produce an infiltrated product having the composition of the composite.Type: GrantFiled: March 14, 1995Date of Patent: June 13, 2000Assignee: General Electric CompanyInventors: Milivoj Konstantin Brun, Krishan Lal Luthra, Raj Narain Singh
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Patent number: 6060162Abstract: A pulsed voltage surge resistant magnet wire comprising a conductor, a continuous and concentric and flexible uniform coat of base insulation material superimposed on the conductor. An essentially continuous and concentric and uniform pulsed voltage surge shield overlaying the coat of base insulation material. The shield has therein an effective amount of a particulate material. The shield is superimposed on the coat of base insulation material, and has a continuous and concentric and flexible and uniform top coat of insulation material superimposed thereon.Type: GrantFiled: June 8, 1995Date of Patent: May 9, 2000Assignee: Phelps Dodge Industries, Inc.Inventors: Weijun Yin, Donald J. Barta
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Patent number: 6053970Abstract: Two component, storage stable apatitic cement compositions, as well as methods for their production, are provided. The dry component of subject apatitic cements comprises basic calcium source particles at least partially coated with a partially neutralized acidic calcium phosphate. The dry component of subject compositions is prepared by combining basic calcium source particles with dissolved acidic phosphate in at least a partially aqueous medium, whereby the basic calcium source particles become partially coated with a partially neutralized acidic calcium phosphate. The reaction is terminated prior to completion of the reaction between the acidic phosphate and the basic calcium source by removing the available water from the reaction mixture. In a first mode, the subject cement may be produced by mechanically mixing an acidic phosphate source with basic calcium source particles in the presence of an aqueous solvent and stopping the reaction between the acid and base prior to completion.Type: GrantFiled: June 30, 1999Date of Patent: April 25, 2000Assignee: Norian CorporationInventors: Ira C. Ison, Mark T. Fulmer, Bryan M. Barr, Brent R. Constantz
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Patent number: 6004675Abstract: A coated glass fiber for light transmission consisting of a glass fiber for light transmission and at least one coating layer made of a UV-curing resin, wherein an outermost layer of the coating layer is made of a UV-curing resin having a Young's modulus of at least 100 kg/mm.sup.2 and a change of a cure shrinkage degree of 1% or less after a Young's modulus reaches one tenth of an end Young's modulus, which has good lateral pressure characteristics and low transmission loss.Type: GrantFiled: September 1, 1992Date of Patent: December 21, 1999Assignees: Sumitomo Electric Industries, Ltd., Nippon Telegraph & Telephone Corp.Inventors: Nobuhiro Akasaka, Tatsuya Kakuta, Kohei Kobayashi, Yasuo Matsuda, Shigeru Tomita
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Patent number: 5965245Abstract: A prepreg comprising a semi-cured thermosetting resin and electrically insulating whiskers or short fibers dispersed in said semi-cured thermosetting resin, and if necessary, a carrier film attached or bound to said prepreg is suitable for producing multilayer printed circuit boards of reduced thinness, high wiring density and high connection reliability with high productivity and low production cost.Type: GrantFiled: September 13, 1996Date of Patent: October 12, 1999Assignee: Hitachi Chemical Company, Ltd.Inventors: Norio Okano, Kazuhito Kobayashi, Akishi Nakaso
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Patent number: 5958583Abstract: A coated ceramic has alumina as an amorphous residue from an alumina sol containing alumina powder or and, optionally, a high emittance powder. The alumina powder alters the rheology and wetting characteristics of the sol to aid in forming the residue and increases the alumina concentration (% solids) in the residue. The high emittance powder radiates heat out of the residue and away from the ceramic when the coated ceramic is heated, such as during orbital reentry.Type: GrantFiled: December 20, 1996Date of Patent: September 28, 1999Assignee: The Boeing CompanyInventors: Michael E. Rorabaugh, Charles W. Newquist, Juris Verzemnieks
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Patent number: 5955391Abstract: In fiber composite ceramic containing reaction sintered SiC as a matrix and having BN-coated SiC continuous fibers as composite fibers, the thickness of the BN coating need not be especially made large, and a sliding effect during growing of cracks can be improved, i.e., breakdown energy can be increased. A method of manufacturing fiber composite ceramic in which large number of BN-coated SiC fibers covered with a BN coating are gathered to form yarns, or yarns are woven to form a two-dimensional or three-dimensional fabric, and a preform is formed by the yarns or the fabric, C powder is arranged in a gap portion between fibers of the preform to form a compact, a molten Si is impregnated into the compact to form an SiC matrix between fibers. A region having a high B concentration is formed around the SiC fibers before the preform is impregnated with the molten Si, and B in the region is solid-solved in Si during reaction sintering to suppress B in the BN-coated SiC fibers from being solid-solved in Si.Type: GrantFiled: March 28, 1997Date of Patent: September 21, 1999Assignee: Kabushiki Kaisha ToshibaInventors: Tsuneji Kameda, Shoko Suyama, Akio Sayano, Masahiro Asayama, Yoshinori Hayakawa
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Patent number: 5955194Abstract: An improved fiber reinforced glass composite includes a boron-containing refractory fiber having its surface enriched with boron nitride in a matrix of a black glass ceramic having the empirical formula SiCxOy where x ranges from about 0.5 to about 2.0, preferably 0.9 to 1.6 and y ranges from about 0.5 to 3.0, preferably 0.7 to 1.8. Preferably the black glass ceramic is derived from cyclosiloxane or non-cyclic siloxane monomers containing a vinyl group attached to silicon and/or a hydride-silicon group. The boron nitride-containing fiber is the product of treating the boron-containing fiber with ammonia at a temperature between about 1100.degree. C. and 1250.degree. C. Fibrous failure rather than brittle failure under stress can be obtained.Type: GrantFiled: June 12, 1995Date of Patent: September 21, 1999Assignee: AlliedSignal, Inc.Inventor: Scott Sager Campbell
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Patent number: 5952100Abstract: A fiber-reinforced silicon--silicon carbide matrix composite having improved oxidation resistance at high temperatures in dry or water-containing environments is produced. The invention also provides a method for protecting the reinforcing fibers in the silicon--silicon carbide matrix composites by coating the fibers with a silicon-doped boron nitride coating.Type: GrantFiled: May 21, 1997Date of Patent: September 14, 1999Assignee: General Electric CompanyInventors: Gregory Scot Corman, Krishan Lal Luthra
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Patent number: 5932345Abstract: A novel heat-fusible copolymer possessing a combination of excellent properties, including mechanical strength, resistivity against radioactive rays, chemical resistance, low temperature stability, thermal resistance, processabilty, adhesiveness, thermal fusible adhesive stability, and simultaneously satisfying requirements relating to low hygroscopic characteristic and stable dielectric constant. Also, a powder, film, laminated film, laminated insulating material, and article, such as electronic modules and capacitors, made from a thermoplastic polyimide resin composed mainly of the copolymer and suitable for use as electronic components and materials for electronic circuit components. The copolymer possesses a glass transition temperature of 100.degree. C. to 250.degree. C., a hygroscopic degree of 1 or less, and a dielectric rate of 3 or less, and has the following formula: ##STR1## wherein Ar.sub.1 represents a quadrivalent organic radical, Ar.sub.Type: GrantFiled: September 10, 1996Date of Patent: August 3, 1999Assignee: Kanegafuchi Kagaku Kogyo Kabushiki KaishaInventors: Hiroyuki Furutani, Naoki Hase, Junya Ida, Yoshifumi Okamoto, Hitoshi Nojiri, Shinji Inoue, Hirosaku Nagano
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Patent number: 5916932Abstract: A composite building material is disclosed produced from recycled materials. The composite building material is composed of an extruded mixture of high density polyethylene and a thermoplastic coated fiber material such as fiberglass. The resulting material has increased strength and is useful in high stress applications such as railroad ties.Type: GrantFiled: May 16, 1997Date of Patent: June 29, 1999Assignee: Rutgers, The State UniversityInventors: Thomas Jerome Nosker, Richard William Renfree
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Patent number: 5908812Abstract: A superconducting oxide composite structure including a superconducting oxide member, a metal layer surrounding the superconducting oxide member, and an insulating layer of a complex oxide formed in situ adjacent to the superconducting oxide member and the metal layer is provided together with a method of forming such a superconducting oxide composite structure including encapsulating a superconducting oxide member or precursor within a metal matrix layer from the group of: (i) a reactive metal sheath adjacent to the superconducting oxide member or precursor, the reactive metal sheath surrounded by a second metal layer or (ii) an alloy containing a reactive metal; to form an intermediate product, and, heating the intermediate product at temperatures and for time sufficient to form an insulating layer of a complex oxide in situ, the insulating layer to the superconducting oxide member or precursor and the metal matrix layer.Type: GrantFiled: February 5, 1996Date of Patent: June 1, 1999Assignee: The Regents of the University of CaliforniaInventors: James D. Cotton, Gilbert Neal Riley, Jr.
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Patent number: 5891362Abstract: A sol having dispersed in a liquid medium particles of a hydrated zinc stannate having a primary particle diameter of from 2 to 200 nm and represented by the formula xZnO.ySnO.sub.2.zH.sub.2 O wherein the molar ratio of x:y:z is 1:0.83 to 1.43:1.00 to 5.00.Type: GrantFiled: June 6, 1996Date of Patent: April 6, 1999Assignee: Nissan Chemical Industries, Ltd.Inventors: Yoshitane Watanabe, Keitaro Suzuki, Yoshinari Koyama, Motoko Iijima
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Patent number: 5851668Abstract: A fiber having increased cut resistance is made from a fiber-forming polymer and a hard filler having a Mohs Hardness Value greater than about 3. The filler is included in an amount of about 0.05% to about 20% by weight. In preferred embodiments, the fiber-forming polymer is poly(ethylene terephthalate) or a liquid crystalline polyester comprising monomer units derived from 6-hydroxy-2-naphthoic acid and 4-hydroxybenzoic acid. Preferred fillers include tungsten and alumina.Type: GrantFiled: November 19, 1996Date of Patent: December 22, 1998Assignee: Hoechst Celanese CorpInventors: Robert Bruce Sandor, Michele C. Carter, Gunilla E. Gillberg-LaForce, William F. Clear, John A. Flint, Herman Leslie Lanieve, Scott W. Thompson, Etheridge Odell Oakley, Jr., Edward Ronald Kafchinski, Mohammed Ishaq Haider
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Patent number: 5843591Abstract: A method of treating a metal alkoxide solution to form metal oxide prepolymer molecules therein is characterized by irradiating the solution with light energy having a wavelength selected to break the metal-alkoxy group bond in said metal alkoxide, thereby to form the metal oxide prepolymer molecules in the solution. The prepolymer is converted into polymeric metal oxide gel. The stoichiometry of the oxide is high. A gel of carbon content below 4 atomic % can be achieved by the step of decarbonizing the gel, preferably using light to produce ozone.Type: GrantFiled: May 26, 1995Date of Patent: December 1, 1998Assignee: Hitachi, Ltd.Inventors: Tomoji Oishi, Ken Takahashi, Teteuo Nakazawa, Shigeru Tanaka, Tadahiko Miyoshi
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Patent number: 5840433Abstract: A refractory article of manufacture comprises an article of graphite-alumina refractory material coated with at least one mineral having a sheet structure and a refractory oxide bond. The coating protects the article against thermal shock. A typical mineral having a sheet structure may be talc, a mica, vermiculite, antigorite, kaolinite, montmorillonite, pyrophyllite, or combinations of these materials. A typical refractory oxide bond is formed from alumina gel, silica sol, alumina sol, zirconia sol, or combinations of these materials (such as a combination of alumina gel and cationic silica sol). The coating may also contain a minor proportion of fibrous material and a minor proportion of particulate refractory filler other than the mineral having a sheet structure, and a portion of the mineral content of the mineral forming the sheet structure may include graphite.Type: GrantFiled: March 13, 1996Date of Patent: November 24, 1998Assignee: Foseco International LimitedInventor: Kassum Juma
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Patent number: 5834117Abstract: A heat-resistant combination including a substrate, a first layer, and a second layer. The first layer includes a benzisidazole-based polymer with a first face in contact with the substrate; and the second layer contains a ceramic material and is securely fixed to a second face of said first layer.Type: GrantFiled: November 12, 1996Date of Patent: November 10, 1998Assignee: Sumitomo Wiring Systems, Ltd.Inventor: Yasuhiko Onishi
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Patent number: 5814403Abstract: A computer model calculates a critical aspect ratio for a discontinuous fiber composite having fibers dispersed in a matrix. The critical aspect ratio is a function of the elastic modulus and the cohesive energy of the fiber and the matrix. The composite incorporates physical features such as fiber shape features or additives in the fiber or matrix which adjust the elastic modulus and/or cohesive energy of the fiber, of the matrix or both to a value different than the corresponding value for unmodified fiber material or matrix material. These adjustments are selected so that the critical aspect ratio for the material including the modifications will be less than the corresponding critical aspect ratio for the material without the modifications. The resulting composite provides enhanced load sharing between fiber and matrix.Type: GrantFiled: January 28, 1993Date of Patent: September 29, 1998Assignee: Exxon Research and Engineering CompanyInventors: Michael P. Anderson, Liza M. Monette, John P. Dismukes, Shiun Ling, David J. Srolovitz
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Patent number: 5789477Abstract: A composite building material is disclosed produced from recycled materials. The composite building material is composed of an extruded mixture of high density polyethylene and a thermoplastic coated fiber material such as fiberglass. The resulting material has increased strength and is useful in high stress applications such as railroad ties.Type: GrantFiled: August 30, 1996Date of Patent: August 4, 1998Assignee: Rutgers, The State UniversityInventors: Thomas Jerome Nosker, Richard William Renfree
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Patent number: 5733655Abstract: A thermostructural composite article and a method for making in which the article comprises silicon carbide reinforcing fibers having an oxygen content by weight of not more than about 14% and an average diameter of less than about 20 microns in a refractory matrix at least partially formed by chemical vapor infiltration. The fibers in the composite article of the invention have an end-to-end fiber diameter uniformity ratio of less than about 1.5.Type: GrantFiled: August 25, 1995Date of Patent: March 31, 1998Assignee: Du Pont Lanxide Composites, L.P.Inventors: Susan Lydia Bors, Albert Zaki Fresco, Mark Henry Headinger
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Patent number: 5719234Abstract: An object of the present invention is to provide a heat-curable high solid coating composition capable of forming a coating film which is excellent in both acid resistance and scratch resistance, and a method for forming a topcoat using said composition.The present invention provides a heat-curable high solid coating composition comprising:(A) a carboxyl-containing compound,(B) a vinyl polymer having an epoxy group, a hydroxyl group and a hydrolyzable alkoxysilyl group in one molecule,(C) a reactive organopolysiloxane, and(D) a crosslinked particulate polymer. The present invention also provides a method for forming a topcoat using said composition.Type: GrantFiled: November 12, 1996Date of Patent: February 17, 1998Assignee: Kansai Paint Company, LimitedInventors: Motoshi Yabuta, Masaaki Saika, Satoru Ito, Hiroyuki Okada, Yasumasa Okumura, Hiroshi Igarashi, Satoshi Ikushima
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Patent number: 5714236Abstract: A method of decorating a firable article which includes the step of mixing a metallic salt with a fuel material which can supply oxygen to the salt in a reaction. This mixture causes complex formation of the salt, characterized by raising the pH of the mixture to at least 5. Additives in the mixture promote stability and provide the required viscosity surface tension and conductivity for use in an ink jet printer. When applying a solution of this mixture onto a firable article by ink jet printing, the mixture is such that upon drying, the mixture reacts to form an oxide of the metal to provide a decorative color pigment on the article.Type: GrantFiled: December 5, 1996Date of Patent: February 3, 1998Assignee: British Ceramic Research LimitedInventors: Steven Charles Withington, Sally-Anne Alsop, Philip Robert Jackson
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Patent number: 5679149Abstract: The present invention provides a short carbon fiber reinforced hydraulic composite material making the best use of physical properties of short carbon fibers incorporated as reinforcing material. Microparticles are deposited on the short carbon fibers in an amount of 0.5 to 3 wt. %. These microparticles also have a particle diameter of 5 microns or less.Type: GrantFiled: November 19, 1996Date of Patent: October 21, 1997Assignee: Mitsubishi Chemical CorporationInventors: Mitsuharu Tezuka, Mitsuru Awata, Akira Shiraki
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Patent number: 5654095Abstract: A pulsed voltage surge resistant magnet wire comprising a conductor, a continuous and concentric and flexible uniform coat of base insulation material superimposed on the conductor and an essentially continuous and concentric and uniform pulsed voltage surge shield overlaying the coat of base insulation material.Type: GrantFiled: June 8, 1995Date of Patent: August 5, 1997Assignee: Phelps Dodge Industries, Inc.Inventors: Weijun Yin, Donald J. Barta
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Patent number: 5639549Abstract: Disclosed is a fixing roll, comprising a core metal, a heat resistant elastic layer formed to cover the circumferential outer surface of the core metal, and a surface layer formed to cover the circumferential outer surface of the heat resistant elastic layer, the surface layer being formed of a tetrafluoroethylene-perfluoroalkyl vinyl ether copolymer resin film of a double layer structure consisting of an inner layer having a volume resistivity of 10.sup.11 .OMEGA..cm or less and an outer layer having a thickness falling within a range of between 3 .mu.m and 50 .mu.m, and the entire thickness of the resin film falling within a range of between 20 .mu.m and 500 .mu.m.Type: GrantFiled: May 8, 1992Date of Patent: June 17, 1997Assignee: Kinyosha Co., Ltd.Inventors: Noritomo Fukunaga, Michiyoshi Kurosawa
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Patent number: 5631084Abstract: The invention relates to a refractory thermally-insulating component consisting essentially of refractory ceramic fibers which are mechanically combined with one another, the composition of which comprises at least 97.5% by weight of alumina, silica and zirconia in total, wherein:a) no organic or inorganic binder binds the fibers to one another;b) the fibers have the following chemical composition, as % by weight:Al.sub.2 O.sub.3 : 33-45%SiO.sub.2 : 41-53%ZrO.sub.2 : 5.5-17%MgO: 0.02-2%other oxides:<0.50% with Fe.sub.2 O.sub.3 +TiO.sub.2 .ltoreq.0.20% and Na.sub.2 O+CaO+K.sub.2 O.ltoreq.0.30%;c) the said fibers homogeneously have, throughout the entire body of the component, a degree of crystallinity of not less than 30% and not more than 64%, the crystals present being essentially formed of mullite crystals and of quadratic zirconia; andd) the said component has a linear shrinkage of no more than 3% after being held for 24 hours at 1450.degree. C.Type: GrantFiled: December 21, 1994Date of Patent: May 20, 1997Assignee: Societe Europeenne des Produits RefractairesInventors: Daniel Urffer, Joseph Recasens
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Patent number: 5605868Abstract: This invention is directed to the fabrication of SiC fiber reinforced, ceramic matrix composite articles exhibiting superior high temperature oxidative stability, those articles comprising:(a) a glass-ceramic matrix wherein alkali metal and/or alkaline earth metal aluminosilicate crystals constitute the predominant crystal phase;(b) a fiber reinforcing phase comprising SiC fibers coated with an alkali metal and/or alkaline earth metal sheet silicate entrained within said glass-ceramic matrix; and(c) a borosilicate glass phase dispersed as an intergranular glass within said glass-ceramic matrix, said borosilicate glass phase generally being present in an amount sufficient to provide an intergranular glass phase therein.Type: GrantFiled: December 29, 1994Date of Patent: February 25, 1997Assignee: Corning IncorporatedInventors: Kenneth Chyung, Steven B. Dawes, David C. Larsen, Ronald L. Stewart
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Patent number: 5599624Abstract: Fibers having reduced surface roughness have a continuous coating of a silicone resin that undergoes pyrolysis in hydrogen or helium to form a hard, amorphous solid coat containing silicon, oxygen, and carbon. This silicon oxycarbide glass coating has exceptional high temperature strength and chemical stability compared to even vitreous silica. The coating is resistant to crystallization and oxidation at temperatures above 1000.degree. C.Type: GrantFiled: July 3, 1995Date of Patent: February 4, 1997Assignee: General Electric CompanyInventor: Svante Prochazka
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Patent number: 5585165Abstract: The present invention generally relates to mechanisms for preventing undesirable oxidation (i.e., oxidation protection mechanisms) of reinforcement materials in composite bodies. The oxidation protection mechanisms include getterer materials which are added to the composite body which gather or scavenge undesirable oxidants which may enter the composite body. The getterer materials may be placed into at least a portion of the composite body such that any undesirable oxidant approaching, for example, a fiber reinforcement, would be scavenged by (e.g., reacted with) the getterer. In a preferred embodiment of the present invention, the getterer material(s) form at least one compound (e.g., at least one glassy material) which acts as a crack sealant, thereby further enhancing the oxidation protection of the composite body. One or more ceramic filler materials which serve as reinforcements may have a plurality of superimposed coatings thereon, at least one of which coatings may function as a getterer.Type: GrantFiled: September 30, 1994Date of Patent: December 17, 1996Assignee: Lanxide Technology Company, LPInventors: Christopher R. Kennedy, Birol Sonuparlak, Ali S. Fareed, John E. Garnier, Gerhard H. Schiroky
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Patent number: 5580643Abstract: The present invention generally relates to mechanisms for preventing undesirable oxidation (i.e., oxidation protection mechanisms) of reinforcement materials in composite bodies. In a preferred embodiment of the invention, a coated ceramic filler material adaptable for use as a reinforcing component in a ceramic matrix composite is provided with a plurality of superimposed coatings. The coating system includes a first coating in substantially continuous contact with the ceramic filler material and one or more additional or outer coatings superimposed over the underlying coating and in substantially continuous contact therewith. Zonal junctions are formed between the filler and the first coating, between superimposed coatings, and between the outer coating and the ceramic matrix. The coatings are selected so that the interfacial shear strength of at least one of these several zones is weak relative to the other zones.Type: GrantFiled: June 7, 1995Date of Patent: December 3, 1996Assignee: Lanxide Technology Company, LPInventors: Christopher R. Kennedy, Birol Sonuparlak, Ali S. Fareed, John E. Garnier, Gerhard H. Schiroky
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Patent number: 5571621Abstract: An infrared radiation-interactive article comprising a supported or unsupported oxidizable metal film of an infrared radiation-interactive size and shape, with an oxidation-promoting salt in contact with the metal film, arranged so that in exposure to ambient moisture, the metal film is oxidizable to an infrared radiation non-interactive form. The article of the invention may be employed to carry out a method of generating a transient infrared radiation response, e.g., an infrared radiation reflectance signature, or infrared radiation absorption, at a selected locus receiving infrared radiation incident thereon, by disposing at the locus an infrared radiation interactively-effective amount of such infrared radiation-interactive article.Type: GrantFiled: June 7, 1995Date of Patent: November 5, 1996Assignee: Advanced Technology Materials, Inc.Inventors: Ward C. Stevens, Edward A. Sturm
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Patent number: 5567518Abstract: A ceramic composite material comprising matrix material, reinforcing fibers and an intermediate interface material. The matrix material and reinforcing fibers consist of the same or different ceramic oxides having a melting point above 1600.degree. C. The interface material is applied as a coating on the fibers and consists of at least one ceramic oxide not exhibiting solid solubility, eutecticum below the temperature of manufacture or use or reactivity with any of the matrix or reinforcing materials. The matrix and reinforcing materials are substantially pure, and the combination fiber/interface material/matrix material is selected from the group consisting of: Al.sub.2 O.sub.3 /Al.sub.2 TiO.sub.5 /Al.sub.2 O.sub.3, YAG/Al.sub.2 TiO.sub.5 /Al.sub.2 O.sub.3, Al.sub.2 O.sub.3 /YAG/Al.sub.2 O.sub.3, Al.sub.2 O.sub.3 /SnO.sub.2 /Al.sub.2 O.sub.3, YAG/SnO.sub.2 /Al.sub.2 O.sub.3, Al.sub.2 O.sub.3 /mullite/Al.sub.2 O.sub.3, and mullite/ZrO.sub.2 /mullite.Type: GrantFiled: April 13, 1995Date of Patent: October 22, 1996Assignees: Volvo Aero Corporation, Rolls Royce PLCInventors: Lars Pejryd, Robert Lundberg, Edwin Butler
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Patent number: 5552352Abstract: A composite is comprised of reinforcement fibers having a continuous coating with a first layer of a metal oxide wherein the metal is from the group consisting of aluminum, yttrium, titanium, zirconium, beryllium, silicon, and the rare earths, and a molten silicon infiltration formed silicon carbide matrix. The coating may have a second layer from the group consisting of rhodium, iridium, metal carbide, metal silicide, metal nitride, and metal diboride, on the metal oxide coating. The reinforcement fibers being fibers from the group consisting of elemental carbon, silicon carbide, and mixtures thereof. A process for producing the fiber reinforced composite comprises depositing on the fibers a continuous coating comprised of the first layer of the metal oxide, and the second layer. A carbonaceous material is admixed with the coated fibers so that at least 5 volume percent of the mixture is the fibers.Type: GrantFiled: September 8, 1995Date of Patent: September 3, 1996Assignee: General Electric CompanyInventors: Milivoj K. Brun, Krishan L. Luthra, Raj N. Singh
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Patent number: 5508235Abstract: A Cu-doped/Fe-doped low expansion glass ceramic composition comprising:______________________________________ Wt. % ______________________________________ SiO.sub.2 50-65 Al.sub.2 O.sub.3 18-27 P.sub.2 O.sub.5 0-10 Li.sub.2 O 2-6 Na.sub.2 O 0-2 K.sub.2 O 0-2 B.sub.2 O.sub.3 0-1 MgO 0-4 ZnO 0-5 CaO 0-4 BaO 0-5 TiO.sub.2 1-3 ZrO.sub.2 1-3 As.sub.2 O.sub.3 0-1.5 Sb.sub.2 O.sub.3 0-1.5 CuO 0-3 Fe.sub.2 O.sub.3 0-1 ______________________________________wherein the total amount of SiO.sub.2, Al.sub.2 O.sub.3 and P.sub.2 O.sub.5 is 80-89 wt. %, and said glass ceramic contains as a dopant 0.1-3 wt. % CuO, 0.1-1 wt. % Fe.sub.2 O.sub.3 or a combined CuO+Fe.sub.2 O.sub.3 amount of 0.1-4 wt. %. The glass ceramic composition is suitable for use as a cladding material for solid laser energy storage mediums as well as for use in beam attenuators for measuring laser energy level and beam blocks or beam dumps used for absorbing excess or unused laser energy.Type: GrantFiled: July 6, 1994Date of Patent: April 16, 1996Assignee: Schott Glass Technologies, Inc.Inventor: Alexander J. Marker
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Patent number: 5501907Abstract: A fibrous electrically-conductive filler herein provided comprises fibrous aluminum borate as a core material provided thereon with, in order, an optional titanium oxide intermediate layer and an antimony-free tin oxide layer. The fibrous electrically-conductive filler can be prepared by a method which comprises the steps of optionally forming an intermediate layer of titanium oxide by depositing titanium oxide hydrate on the surface of the core material and then calcining the titanium oxide hydrate layer; then forming a coating layer of tin oxide hydrate on the surface of the titanium oxide-coated fibrous aluminum borate or the fibrous aluminum borate as a core material and then calcining the coating layer at a temperature ranging from 150.degree. to 600.degree. C. in an inert gas atmosphere or a reducing atmosphere to form an antimony-free tin oxide layer.Type: GrantFiled: September 29, 1993Date of Patent: March 26, 1996Assignee: Mitsui Mining & Smelting Co., Ltd.Inventors: Takao Hayashi, Nobuyoshi Kasahara, Norihiro Sato, Kouichi Kawaratani
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Patent number: 5498296Abstract: A metal oxide layer is provided around a thermocouple element. The metal oxide layer is formed by preparing a sol, in which particulates of a metal oxide are dispersed, by a sol-gel method, dipping the thermocouple element in this sol, energizing the thermocouple element as a cathode for bonding the precursor particulates of the metal oxide thereto, and heat treating the same. The thermocouple according to the present invention is compact with a thin insulating layer, excellent in flexibility, and provides no gas adsorption source.Type: GrantFiled: October 7, 1991Date of Patent: March 12, 1996Assignee: Sumitomo Electric Industries, Ltd.Inventors: Kazuo Sawada, Shinji Inazawa, Kouichi Yamada