Abstract: A light-control membrane (11) is joined to a first surface (10a) of an electrolyte membrane (10), and hydrogen gas is supplied to a second surface (10b) side of the electrolyte membrane (10). If the electrolyte membrane (10) has a defect (10c), such as a crack or a pinhole, the hydrogen gas leaks through the defect (10c) to the first surface (10a) of the electrolyte membrane (10). In result, the light-membrane (11) is hydrogenated by the leaked hydrogen gas, and the reflectance of the light-control membrane (11) is locally changed. This makes it possible to visually spot the presence of the defect (10c).

Abstract: Methods and apparatus are disclosed for leak testing the ventilation system of an environmental enclosure using a gas that is naturally present in ambient air, such as nitrogen, oxygen, argon, or carbon dioxide, as a tracer gas. In one embodiment, a gas filter capable of filtering all of the tracer gas from the air flowing through the filter is installed in the ventilation system. Testing is performed by operating the ventilation system to cause outside air to flow through the filter and into the enclosure so as to establish positive pressurization inside the enclosure. A gas monitor placed inside the enclosure is used to detect for the presence of leaks in the ventilation system by monitoring the concentration of the tracer gas inside the enclosure.

Abstract: Composition, which includes a dye that changes color when contacted with a suitable amount of an organic substance, in conjunction with a matrix, paste, support or web, can indicate visually or photometrically the presence of the organic substance. An organic spill absorbing material may be present. For instance, the dye may be selected from the class of anthracene, azo, anthraquinone, pyrazolone, and quinone dyes, and be hydrophobic and organic oleophilic. For an example, the dye may be Oil Red “A.” The matrix, paste, support or web may include a microfiber cloth, which may be coated with an adhesive for attachment of the dye, and/or include a water-dissolving paper which may envelope the dye. A device for ascertaining whether an organic substance is present includes the dye or composition with the dye at a certain locale, and a light-transmissive pathway in communication with the location and a detection site external the location.

Abstract: In order to check the hermeticity of a closed cavity of at least one micrometric component, said component includes a structure made over or in one portion of a substrate, a cap fixed to one zone of the substrate to protect the structure, and an indicator element whose optical or electrical properties change in the presence of a reactive fluid. The indicator element may be a copper layer for an optical check or a palladium resistor for an electrical check. The micrometric component is placed in a container which is then hermetically closed. This container is filled with a reactive fluid under pressure, which is oxygen for the optical check and hydrogen for the electrical check. The component in the container is subjected to a reactive fluid pressure higher than 10 bars for a determined time period, and to thermal (T>100° C.) or optical (?<500 nm) activation. After this time period, an optical or electrical check of the indicator element determines the hermeticity of said cavity.

Abstract: The present invention relates to a porous adaptive membrane structure that has movable membranes. The structure can be made to change its gas, liquid or particulate permeability in response to surrounding environmental conditions. The application of this invention is includes protective apparel that is comfortable to wear wherein the level of protection provided is based on conditions in the environment. Hence, the protective apparel is highly breathable and comfortable in a non-hazardous environment but impermeable or only semipermeable in a hazardous environment.

Abstract: An apparatus and method for testing the integrity of a filter under humid conditions is provided. The apparatus includes an injection assembly which is located on a first side of the filter and a detection assembly which is spaced from the injection assembly and located on a second side of the filter. The injection assembly injects a mixture of an air stream and a hydrophilic test chemical vapor of a known concentration through the filter. The injection assembly includes a sealed vaporizer which generates the mixture of the air stream and the hydrophilic test chemical vapor. The vaporizer includes a contact bed having an inert packing media for vaporizing the hydrophilic test chemical. The detection assembly detects a concentration peak of the hydrophilic test chemical vapor exiting the filter. The detection assembly includes a chemical sampling member, a chemical enriching member and a chemical detector.

Abstract: The invention relates to a method of determining the cleanness of an apparatus comprising the steps of treating the interior of the apparatus with a solution comprising permanganate so as to cause the permanganate to react with contaminants, if any, being present within the apparatus, rinsing the interior of the apparatus to remove non-reacted permanganate, contacting the interior of the apparatus with a solution comprising peroxide and detecting a splitting, if any, of peroxide into oxygen and water. The invention also relates to a method of detecting a leakage in an apparatus and to a use of the method for determining the cleanness of an apparatus and for detecting a leakage in an apparatus.

Abstract: The present invention relates to a process for detecting a leak in a package. The process comprises preparing a package by covering at least a portion of an O2-sensitive product with a multilayer film comprising (i) a leak-indicator layer in which a O2-sensitive indicator is present throughout the leak-indicator layer; and (ii) an O2-barrier layer outward of the leak-indicator layer. A low O2-environment is provided within the package. The leak-indicator layer is then illuminated with light containing a wavelength absorbed by the O2-sensitive indicator, so that the O2-sensitive indicator produces an emission of radiation in an amount inversely proportional to a level of O2 present with the O2-sensitive indicator. Then the multilayer film is scanned while the O2-sensitive indicator is emitting radiation, the scanning being carried out by sensing and comparing the amount of radiation emitted from at least two different regions of the multilayer film.

Abstract: The present invention is to detect leakage of fluid from a channel in a microreactor certainly at an early stage. A chemical reactor has a microreactor with a pump for sending first, second solutions, and a channel for mixing and reacting the first, second solutions. The solution sending amount of the first, second solutions to be supplied to the microreactor is controlled by a pump controlling device. The microreactor has a first substrate with a channel and a second substrate to be bonded airtightly with the first substrate. A leak detecting channel is formed in the vicinity of the channel in the first substrate.

Abstract: A method of detecting oxygen leakage. Firstly, a detection wafer with a first color positioned on the substrate is provided. Then, the detection wafer is loaded into a reaction tube from a loading chamber, and subsequently, the detection wafer is unloaded from the reaction tube. Finally, the detection wafer is observed to obtain a second color, wherein if oxygen leaks into the loading chamber, the second color is different from the first color.

Abstract: A chemical storage and dispensing vessel having associated therewith a colorimetric member that is effective to change color in exposure to leakage of a gas contained in the vessel. The colorimetric member may be constituted by a film, e.g., of a shrink-wrap character, that contains or is otherwise associated with a colorimetric agent undergoing color change in exposure to fluid leaking from the vessel. Such shrink-wrap film may be applied to a portion of the vessel susceptible to leakage, or alternatively to the entire vessel, so that the film is colorimetric effective to indicate the occurrence of a leakage event by visually perceptible change of color.

Abstract: An improved device for the detection of leakage is achieved when the device includes at least two components, of which at least one is capable of migrating with the liquid within the carrier, and forming a distinct color or other detectable signal with the first component. Such device is not sensitive to normal, ambient humidity and the color signal formed is resistant to being diluted or rinsed away in cases of abundant or repeated leakage.

Abstract: An apparatus for dispensing an odorant to a fluid in a vessel having an interior volume containing the fluid includes at least one odorant material and an odorant-permeable material. The at least one odorant material is disposed in the interior volume, the odorant material having at least one detectable odor. The odorant-permeable material encapsulates the odorant material.

Abstract: A metal co-ordinated complex in a medium, e.g. a palladium-fluorophore, may be used to detect food spoilage products by the release of a detectable component by preferential binding of the metal to, for example, sulphur compounds or amines. It can be easy to detect food spoilage in sealed packs.

Abstract: Systems and methods providing for the introduction of a dye, particularly a xanthene dye, and more particularly a rhodamine dye, to liquid anhydrous ammonia to discourage theft of the anhydrous ammonia and provide for leak detection in storage vessels. The dye will stain objects which come into contact with the liquid anhydrous ammonia allowing for the detection of such contact. Generally, the staining will be visible to the naked eye, but may also fluoresce when exposed to a particular light source such as ultra violet (UV) light.

Abstract: A library of material samples is screened for properties such as permeability. A library of material samples is provided. A stimulus such as an exposure to a permeate fluid is provided to each member of the library. A response of each of the material samples due to the stimulus is measured and the response, the stimulus or both are recorded and related to provide data. Thereafter, the data is analyzed to reach conclusions regarding the properties of the material samples.

Abstract: A method for evaluating the integrity of the closure on a hot-filled container in which the hot-filled container is subjected to a pressurized spray of cooling medium, including the step of providing a cooling medium having an effective amount of a fluorescing dye contained therein, is provided. The sealed container then is sprayed with the cooling liquid. After the container has exited the cooling portion of the filling and sealing operation, the container is subjected to ultraviolet light to activate any fluorescing dye which may have migrated past the closure into the interior of the container. The container is then viewed to determine the presence or absence of activated dye.

Abstract: An apparatus is provided for testing equipment located in a local environment by presenting a detectable indicator gas therein. The apparatus has a container portion, a chemical substance stored in the container portion, a pump operable to draw air into the container portion and in contact with the chemical substance to generate a detectable indicator gas, and an outlet to the container for directing the indicator gas into the local environment. Further, the pump is integrally formed as one piece with the container portion. Preferably, the pump is a manually squeezable polymeric bulb that is joined (e.g., by molding) seamlessly with the container portion.

Abstract: A cartridge for holding a test specimen with an extremely small volume. The cartridge has a test chamber and a vestibule through which the test fluids are inserted into the test chamber. The cartridge has a stopper having a pair of seals, the first of which seals the test chamber inlet between the vestibule and the test chamber, and the second of which seals the mouth of the vestibule so that when the stopper is in place, the test chamber is closed to the admission of air or other contaminants and the vestibule is similarly closed against escape of the overflow from the test chamber.

Abstract: An apparatus for detecting a leak of a fluid from a system for storing and/or transporting a volume of the fluid includes an odorant material. The system includes at least one vessel and at least one sealant having an outer surface. The odorant material is encapsulated or sorbed on the sealant, at least a portion of the odorant material having at least one detectable odor.

Abstract: Use of fluorescent dyes based on pyrromethene difluoroborate complexes is disclosed for use in fluorescent marking of lubricants and fro the determination of leakages in lubricant systems and a corresponding fluorescent dye concentrate.

Abstract: Methods and systems of facilitating detection of fuel leaks in a fuel cell system include adding organic molecules to a fuel cell fuel supply to odorize the fuel supply.

Abstract: An apparatus for dispensing an odorant to a hydrogen gas includes at least one container, each container having an interior volume. At least one odorant material is disposed in the interior volume of a first container, the odorant material having at least one detectable odor. At least one hydrogen storage material is disposed in the interior volume of the first container or the interior volume of a second container.

Abstract: An apparatus for dispensing an odorant to a hydrogen gas includes at least one container, each container having an interior volume. At least one odorant material is disposed in the interior volume of a first container, the odorant material having at least one detectable odor. At least one hydrogen storage material is disposed in the interior volume of the first container or the interior volume of a second container.

Abstract: An apparatus for detecting a leak of a fluid from a vessel having an inner wall and an outer wall includes at least one chemical material layer adjacent the outer wall. At least a portion of the chemical material layer is adapted to undergo a chemical reaction with a portion of the fluid leaking through the outer wall. The apparatus may also include at least one semi-permeable material layer adjacent the chemical material layer. The fluid may be a pressurized gas, such as hydrogen or another gas that will react with the chemical material layer to produce a detectable odor and/or a detectable discoloration of the chemical material layer.

Abstract: An apparatus for detecting a leak of a fluid from a vessel having an inner wall and an outer wall includes: at least one odorant layer adjacent the inner wall or the outer wall; and at least one semi-permeable material layer adjacent the odorant layer.

Abstract: This invention discloses a method for detecting a leak from a sealed optical device. The method includes steps of: A) injecting a target gas with no performance interference to the sealed optical device for leak detection followed by sealing the sealed optical device. B) placing the sealed device in a leak testing chamber and measuring a background level of the target gas in the leak testing chamber. C) heating the sealed device to a gas-expelling temperature for expelling the target gas from the leak in the sealed optical device. And, D) detecting the target gas in a one-part-per million (PPM) range in the leak-detecting chamber for an comparing with the background level of the target gas for determining the leak in the sealed optical device.

Abstract: The present invention relates to new color compositions which are especially suitable to be used in oxygen indicators. The compositions comprise iron(II), an agent containing pyrogallol entities and an organic acid.

Abstract: A weathering test method comprising making active oxygen and light simultaneously act on a test piece, a weathering test method comprising successive and/or alternate steps of making active oxygen and light simultaneously act on a test piece and making at least one of light, oxygen, and water to act on the test piece, and apparatus for carrying out the methods are disclosed. In evaluating weatherability of organic materials, articles made of organic materials or articles coated with organic materials, the methods and apparatus achieve acceleration of deterioration of test pieces to greatly reduce the testing time.

Abstract: An insulating glass pane (1) has at least two glass plates (10, 12) which are spaced apart from one another, and an edge joining strip (14) which surrounds and joins together the glass plates (10, 12) in the region of their edges. The edge joining strip (14) seals and delimits an insulating cavity (16) which is located between the glass plates (10, 12) and which is filled with a fill gas which is not air. A sensor (18) is provided in the insulating cavity (16) of the insulating glass pane (1), which sensor reacts and gives a signal if the composition of the fill gas changes.

Abstract: A method and device for detecting water leaks is disclosed. The method and device comprise an odorant in a water soluble barrier. The odorant and water soluble barrier can be contained in a housing and placed in a location where water leakage can occur. In the method and device described herein, leaking water dissolves the barrier and releases the odorant into the atmosphere thereby alerting persons to the presence of water as a result of a leak.

Abstract: A test kit for testing acidity of a lubricant in a climate control system containing a naphthalimide dye contains an aqueous solution having a salt and a known amount of hydroxide and an organic solution containing an alcohol and an organic solvent having a flash point of at least 130° F. When a lubricant is added to a combination of the aqueous solution and the organic solution, the color of the bottom layer indicates the acid content of the lubricant.

Abstract: Detection of an evolving or diffusing gaseous substance emanating from an irradiated or thermolyzed layer of polymeric composition in semiconductor processing or similar processes is disclosed. The evolving or diffusing gaseous substance is detected by spatially disposing from the irradiated or thermolyzed layer a detector layer that includes a compound having leaving groups that are sensitive to the gaseous substance being detected.

Abstract: A method and apparatus suitable for use in high volume production for determining leakage from a nominally sealed product container, e.g., a battery case. The method and apparatus first functions to analytically test for leakage of a particular component of interest, e.g., a liquid electrolyte comprising a mixture of ethylene carbonate (EC) and methyl-ethyl carbonate (MEC) in a lithium-ion battery. A second gas leakage test can then be performed.

Abstract: The present invention relates to new color compositions which are especially suitable to be used in oxygen indicators. The compositions comprise iron(II), an agent containing pyrogallol entities and an organic acid.

Abstract: A sterilant challenge device, for use in testing the efficiency of the removal stage of a sterilization cycle in a sterilizer. In a preferred embodiment, the device includes a tube that is closed at one end and open at the other for the entry of sterilant, a plurality of thermally-conductive masses the tube, and at least one temperature sensor. When the challenge device is located in a sterilizer, the penetration of sterilant along the bore of the tube during a sterilization cycle, is inhibited by the accumulation of air and/or non-condensable gas within the bore resulting from the condensation of moisture on the walls of the bore. By measuring the temperature inside the device adjacent the closed end of the tube, the efficiency of the sterilization cycle can be determined.

Abstract: An additive is introduced into a fluid system and dissolved in a carrier fluid which is immiscible or slightly miscible in the fluid system, wherein the carrier fluid is subsequently removed from the fluid system. This method can be used to detect leaks, wherein an on-off UV light source, such as xenon light, can be used to detect the leak visually.

Abstract: The present invention relates to new color compositions which are especially suitable to be used in oxygen indicators. The compositions comprise iron(II), an agent containing pyrogallol entities and an organic acid.

Abstract: A method and device for detecting water leaks is disclosed. The method and device comprise an odorant in a water soluble barrier. The odorant and water soluble barrier can be contained in a housing and placed in a location where water leakage can occur. In the method and device described herein, leaking water dissolves the barrier and releases the odorant into the atmosphere thereby alerting persons to the presence of water as a result of a leak.

Abstract: The present invention provides for an improved method for monitoring the concentration of molecules and chemical treatment agents in ceramic slurries and powders.

Abstract: A test device and method is described for directly determining the liquid phase water content of organic solvents and indirectly the liquid phase water content of solids. The device and method utilize a reagent composition consisting basically the dried residue of a mixture of a colorimetric indicator material, preferably a cobaltous or cuprous salt, and a polymeric water barrier material, such mixture incorporated into a matrix which is contacted with or immersed into the liquid test sample, removed therefrom and the color change of the test composition correlated with a standard color chart to give a quantitative result of the amount of water in the test sample. When the method is applied to solids, the water must first be extracted from the solid using a substantially anhydrous extracting fluid such as reagent alcohol.

Abstract: A detection device for testing gloves or other protective clothing or equipment for breakthrough by a contaminant includes a pad carrying a reagent which is responsive to the contaminant for producing a color change. A barrier layer covers the reverse side of the pad to prevent escape of chemicals therefrom and an adhesive strip is secured to the barrier layer for attachment of the pad either to the skin of the user or to the inside of the glove or other clothing so that the obverse side of the pad is adjacent to the inside of the glove. In one embodiment the pad is impregnated with the reagent which directly reacts with the contaminant to produce a color change. In another embodiment, plural reagents are carried respectively in separate regions of the pad and, after exposure to the contaminant, a carrier solvent is applied to the pad which brings the reagents into intimate contact for cooperation to produce the color change.

Abstract: An apparatus and method for detecting a leak by mixing an amount of odorant ith the contents of a sealed container. An amount of odorant having a detectable odor is mixed with the contents of a sealed container. The sealed container with the odorant is placed within a detection zone which is monitored to detect the presence of the odorant which would indicate leakage of the container's contents. The detection zone defines an area within which leakage of the contents will produce a detectable quantity of the odorant. The odorant may be a gas. Preferred odorants are selected from the group consisting of sulfides, cyclic sulfides and mercaptans. In a sealed light source device having radioactive tritium gas, the preferred odorant is hydrogen sulfide which is detectable by individuals in concentrations of at least 5 parts-per-billion (ppb). Individuals, which may be part of a scheduled roving sentry or a patrol, monitor for the presence of the odorant in the detection zone.

Abstract: Leakage in a heat exchanger between two liquids which are in indirect heat exchange relationship is detected by marking one of the two liquids with a colorless chemical marker and detecting it in the second liquid by extraction and conversion to a colored material. The heat exchanger liquids are preferably organic liquids which are immiscible with water. The marker is detected in a heat exchanger liquid by extraction of the marker followed by chemical conversion of the marker to a colored material that can be detected visually. Aminoalkylnaphthalenes are suitable markers which can be extracted by an acidic aqueous solution and converted to a colored material by reaction with a diazotized aromatic amine. Phenylazoalkylphenol derivatives are also suitable markers which can be extracted and simultaneously converted to a colored material with a detection reagent which is comprised of water and a water-soluble amine.

Abstract: Methods for labeling a material are disclosed. The methods comprise combining with the material (a) a photosensitizer capable upon irradiation of generating singlet oxygen and (b) a chemiluminescent compound capable of being activated by singlet oxygen wherein the photosensitizer and the chemiluminescent compound are incorporated in a particulate matrix or a non-particulate solid matrix. The particulate matrix can be solid or fluid. The methods allow for generating delayed luminescence, which can be realized upon irradiation of the matrix. The methods have application to the determination of an analyte in a medium suspected of containing the analyte.

Abstract: The invention is a method of monitoring for the presence of certain constituents of food processing streams by measurement of fluorescence. The constituent monitored can be a fluorescing impurity of a food product, or the food product itself if such naturally fluoresces. Moreover, losses of the constituent to be monitored may be determined by concurrent measurement of fluorescence of a fluorescent material added to the food process stream. The method is applicable to the following food processing streams among others: meat, vegetable oil, sugar beet, sugar cane, grain, poultry, fruit and soybean processing streams. Upon determination of a variation of the fluorescing constituent to be measured, the food process can be adjusted accordingly.

Abstract: A method for determining the sensitivity of at least one nonparaffinophilic microorganism from a specimen obtained from a patient to different antimicrobial agent, and predetermined quantities thereof. The method includes providing at least one receptacle containing an aqueous solution and adjusting the solution to mimic the in vivo clinical conditions of said patient. The method further includes inoculating the solution with the specimen and placing into the receptacle (i) a slide coated with a carbon source and (ii) a predetermined quantity of an antimicrobial agent to be tested. By observing the nonparaffinophilic microorganism growth or lack thereof on the slide, it can be determined whether the predetermined quantity of the antimicrobial agent is effective in inhibiting growth of the nonparaffinophilic microorganism on the slide. An associated apparatus is also disclosed.

Abstract: A method of testing an elastomeric personal barrier which involves positioning the barrier over a mold in the shape of the barrier, the mold being translucent or of a contrasting color to the barrier, exposing the personal barrier to a non-corrosive solvent so that the solvent comes into contact with the exterior of the personal barrier only except where a flaw exists in the barrier, removing the personal barrier from contact with the solvent, and inspecting the exterior of the personal barrier for the appearance of one or more stains which indicate the presence of a flaw in the structural integrity of the barrier.

Abstract: The operation of a steam sterilizer is monitored by a test unit and a controller which together comprise a system which can be operated in two principal method schemes: (1) the testing for completeness of air removal from a sterilizer chamber, and (2) the testing for effective sterilization conditions. These methods each have two principal modes of operation: (a) the performance of a Bowie and Dick type test, as is usually done on a once-a-day basis; and (b) monitoring the sterilizer during load conditions. In a preferred embodiment a test unit including temperature and pressure sensors, a moisture sensor and a heat sink are positioned within the chamber of a steam sterilizer and transmit by radio the conditions therein to an external controller. The test unit can employ a replaceable cartridge to assure effective operation even after a large number of cycles of operation.

Abstract: An Automated data collection system for fugitive emission sources includes a handheld data terminal formed as a single portable package or integral unit. The data terminal is connected to an organic vapor analyzer (OVA) and an emissions receiving probe. The data terminal includes a display, a keypad, a microprocessor, a memory, a barcode reader and an analog to digital (A/D) converter for converting the emissions signal received from the OVA to a digital representation. The data terminal facilitates immediate on-site repair by providing repair guidance or repair options to the inspector during the inspections process. Front and rear magnets detachably mount the probe to the data terminal. The probe's rear magnet is recessed to matingly receive the unit's projecting rear magnet.