Abstract: A metal detergent and a preparation method thereof and a lubricant oil containing the metal detergent. The metal detergent is sulfurized calcium alkyl phenolate, the method for preparing the metal detergent includes the following steps: a) mixing alkyl phenol, a calcium source and base oil to obtain a mixed solution; b) mixing the mixed solution, ethylene glycol and a sulfur source to carry out sulfurization reaction to obtain a sulfurization reaction solution; c) implementing carbonation reaction between the sulfurization reaction solution and CO2 to obtain a carbonation reaction solution; and d) extracting the carbonation reaction solution with a solvent, upon refining, to obtain sulfurized calcium alkyl phenolate; wherein the solvent includes solvent oil, water and oxygenous derivative of hydrocarbon. Experimental results show that the content of free alkyl phenol is below 1.5 wt % in the sulfurized calcium alkyl phenolate prepared using the preparation method provided by the present application.

Abstract: The invention provides a lubricating composition containing an oil of lubricating viscosity and a detergent. The invention further relates to a process to prepare the detergent, and the use of the lubricating composition in a mechanical device such as an internal combustion engine, or a driveline device.

Abstract: The present invention provides overbased detergents as lubricating oil additives effective for the lubrication of mechanical components in land and marine engines, such as, for example, hydraulic systems, transmissions, two-stroke and four-stroke vehicular engines, trunk piston and two-stroke crosshead marine engines. These overbased detergents lead to improved detergency and thermal stability performances versus high overbased sulfonates. Moreover, they are more compatible with commercial phenates than conventional sulfonates.

Abstract: A lubricant composition. The lubricant composition includes (a) a phenate, a sulfonate, or both; and (b) a base composition wherein the base composition is (i) a metal carbonate and a metal sulfate, (ii) a metal sulfate and a metal phosphate; (iii) a metal sulfate and a metal carboxylate; (iv) a metal phosphate and a metal carboxylate; or (v) three-way or four-way combination of a metal sulfate, a metal carboxylate, a metal phosphate, and a metal carbonate; and (c) a lubricating oil or a grease.

Abstract: The invention provides a lubricating composition containing an oil of lubricating viscosity and a detergent. The invention further relates to a process to prepare the detergent, and the use of the lubricating composition in a mechanical device such as an internal combustion engine, or a driveline device.

Abstract: Disclosed in certain embodiments is a method of determining the individual concentration of different antioxidants of the same class in a sample comprising contacting the sample with an effective amount of phenol; and analyzing the sample by voltammetry.

Abstract: Lubricant formulations and methods for producing lubricant formulations are described that provide improved wear protection in engines operated using ethanol-based fuels. The improved wear protection may be provided by an increased amount of overbased calcium detergent present in the formulation.

Abstract: Disclosed in certain embodiments is a method of determining the individual concentration of different antioxidants of the same class in a sample comprising contacting the sample with an effective amount of phenol; and analyzing the sample by voltammetry.

Abstract: A lubricant for use in processing of a metallic material includes a lubricant base and additives added to the lubricant base. The additives include a sulfuric extreme pressure agent, a rust inhibitive agent and a calcium ingredient. Content of sulfur contained in the sulfuric extreme pressure agent is not less than 0.5 wt % of total weight of the lubricant and not greater than 20 wt % of total weight of the lubricant. Content of the rust inhibitive agent is not less than 0.1 wt % of total weight of the lubricant and not greater than 15 wt % of total weight of the lubricant. Further, content of calcium contained in the calcium ingredient is not less than 0.1 wt % of total weight of the lubricant and not greater than 15 wt % of total weight of the lubricant.

Abstract: A method of lubricating a marine diesel 2-stroke engine comprising: (1) monitoring performance characteristics of said engine; (2) selecting a lubricating composition to modify the performance characteristics of the engine, wherein the lubricating composition is prepared by in-situ controlled blending of at least two different fluids, said fluids comprising: (i) a first fluid comprising an additive package with one or more overbased detergents, and optionally other performance additives; (ii) a second fluid comprising an additive package with one or more neutral detergents or overbased detergents, and optionally other performance additives, with the proviso that the first fluid has a ratio of ?(wt % of overbased detergents)/?(wt % of all additives in the fluid) greater than the second fluid; and (iii) a third fluid comprising an oil of lubricating viscosity; and (3) supplying the lubricating composition of step (2) to the engine, with the proviso that the lubricating composition comprises at least one of the

Abstract: Lubricant formulations and methods for producing lubricant formulations are described that provide improved wear protection in engines operated using ethanol-based fuels. The improved wear protection may be provided by an increased amount of overbased calcium detergent present in the formulation.

Abstract: A method for working or forming metals which consists in usings an aqueous lubricant containing as water-soluble extreme pressure additive, methanesulphonic acid or water-soluble methanesulphonic acid salt. The water-soluble methane sulphonic acid salt is an alkali or alkaline-earth, ammonium, alkanol amine or ethoxylated fatty amine salt. The inventive aqueous lubricants have good extreme pressure properties and good properties with respect to corrosion.

Abstract: A method of improving the compatibility of an overbased detergent with other additives in a lubricating oil composition. The method includes the step of adding an oil-soluble, hydrocarbyl sulphonic acid to the detergent.

Abstract: A composition for cleaning bearings in rotating equipment and industrial machinery that contains powdered limestone having a high calcium content dispersed in a calcium sulfonate grease, together with a colorant that readily enables a user to differentiate between contaminated grease, cleaning composition and fresh grease. A method is also disclosed that enables a user to clean and re-lubricate bearings without the need for removing the bearings from service or for shutting down the associated equipment or machinery.

Abstract: The invention relates to a process for preparing an overbased metal detergent in an oil medium comprising the steps of: (1) providing a metal salt selected from the group consisting of a hydrocarbyl-substituted organic acid; a hydrocarbyl-substituted phenol, a phenate, a hydrocarbyl-substituted carboxylate and mixtures thereof; (2) further providing methanol and a mixture of alcohols containing 2 to about 7 carbon atoms, wherein the mole ratio of methanol to the mixture of alcohols is about 2.

Abstract: Colloidal products are described which comprise micelles of alkaline metals or alkaline-earth metals, held in the colloidal state by at least one alkaline metal or alkaline-earth metal alkyl- or alkylarylsulphonate. The products further comprise micelles of a product containing calcium, phosphorus and sulphur resulting from the in situ reaction of calcium oxide or calcium hydroxide with a phosphorus sulphide, in particular tetraphosphorus decasulphide, and water.These colloidal products are used as antiwear and extreme pressure additives for lubricating greases and oils.