Aqueous Coating Agent Patents (Class 510/442)
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Patent number: 6136777Abstract: A non-tower process for continuously preparing granular detergent composition having a density of at least about 600 g/l is provided. The process comprises the overall steps of: (a) dispersing a surfactant, and coating the surfactant with fine powder in a mixer, wherein first agglomerates are formed; (b) spraying finely atomized liquid onto the first agglomerates in a mixer, wherein second agglomerates are formed; and (c) granulating the third agglomerates in one or more fluidizing apparatus. The process is improved by further step (b'), by thoroughly mixing the second agglomerates in a mixer, between step (b) and step (c), wherein, in step (b'), choppers are used to reduce the amount of oversized agglomerates.Type: GrantFiled: April 1, 1999Date of Patent: October 24, 2000Assignee: The Procter & Gamble CompanyInventors: Angela Gloria Del Greco, Wayne Edward Beimesch, Manivannan Kandasamy
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Patent number: 6121229Abstract: A non-tower process for continuously preparing granular detergent composition having a density of at least about 600 g/l is provided. The process comprises the overall steps of (a) dispersing a surfactant, and coating the surfactant with fine powder having a diameter from 0.1 to 500 microns, in a mixer, wherein first agglomerates are formed, (b) spraying on finely atomized liquid to the first agglomerates in a mixer, wherein second agglomerates are formed, and (c) the second agglomerates are thoroughly mixed in a mixer to provide rounding and growth.Type: GrantFiled: April 1, 1999Date of Patent: September 19, 2000Assignee: The Procter & Gamble CompanyInventors: Angela Gloria Del Greco, Manivannan Kandasamy
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Patent number: 6087311Abstract: Tablets comprise a core and a coating, the core being formed by compressing a particulate material, the particulate material comprising surfactant and detergent builder, and the coating comprising dicarboxylic acid. The tablets are provided with effervescent agents, in the core or water-swellable desintegrant in the coating which aid in their disintegration in wash liquors. The invention also relates to processes for making the tablets.Type: GrantFiled: June 4, 1999Date of Patent: July 11, 2000Assignee: The Proctor & Gamble CompanyInventor: Paul Irma Albertus Van Dijk
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Patent number: 6054425Abstract: Cleansing bars are formed from compositions containing an oil phase, particulate silica and a cleansing agent. The particulate silica is present in an amount to provide sufficient hardness to the composition to facilitate processing into a bar while maintaining good foaming despite a high oil content.Type: GrantFiled: May 20, 1996Date of Patent: April 25, 2000Assignee: Imaginative Research Associates, Inc.Inventors: Jose E. Ramirez, Mohan Vishnupad
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Patent number: 5998360Abstract: Soluble alkali metal silicates combined with antiredeposition agents can actually have a beneficial effect on bleach stabilisation if said antiredeposition agents are intimately mixed with an alkali metal silicate solution, the resulting product being then dried (spray drying, turbo drying, etc . . . ) into granules.Type: GrantFiled: April 13, 1998Date of Patent: December 7, 1999Assignee: Crosfield LimitedInventors: Keith R Cockett, Theo J Osinga
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Patent number: 5958864Abstract: A process for producing a particulate amorphous alkali metal silicate having a molar ratio of M.sub.2 O to SiO.sub.2 of 1:1.5 to 1:3.3 bya) spray-drying an aqueous mixture of amorphous alkali metal silicate,b) impregnating the spray-dried amorphous alkali metal silicate with an aqueous dispersion or solution of detergent composition components containing at least one organic component, andc) optionally drying the impregnated amorphous alkali metal silicate.Type: GrantFiled: June 24, 1998Date of Patent: September 28, 1999Assignee: Henkel Kommandiggesellschaft auf AktienInventors: Rene-Andres Artiga Gonzalez, Hubert Freese, Manfred Greger, Kathrin Schnepp, Adolf Wiche
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Patent number: 5898024Abstract: The present invention discloses an alkaline cleaning composition for cleaning heavily soiled metal surfaces such as food fryers, baking pans, high temperature pasteurizers, and beer kettles, ceramic surfaces such as restaurant grade ceramic china plates and platters, and plastic surfaces. The cleaning composition is noncaustic and includes a peroxygen compound, a chelate, and a metasilicate and/or sesquisilicate. A preferred cleaning composition further includes a surfactant and hydrated builder.Type: GrantFiled: January 9, 1997Date of Patent: April 27, 1999Assignee: Charvid Limited LiabilityInventor: Charles Bullick Talley
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Patent number: 5891835Abstract: A cleaner impregnated towel comprises a flexible, porous substrate and, impregnated into the substrate, a cleaner formulation comprising d-limonene, dibasic acid ester, N-methyl-2-pyrrolidone, secondary alcohol ethoxylate, sodium lauryl sulfate, polysorbate 80, a salt of a coconut oil fatty acid ester of isethionic acid, glycerine, ethyl alcohol, an antimicrobial preservative, and optionally water.Type: GrantFiled: March 17, 1998Date of Patent: April 6, 1999Assignee: Dotolo Research CorporationInventor: Jack T. Vlasblom
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Patent number: 5792738Abstract: There is provided a granular, silicate-built, phosphate free laundry detergent composition comprising fine alkali metal percarbonate particles having mean particle diameter below 450 .mu.m, preferably below 400 .mu.m, wherein no more than 20%, preferably no more than 10%, of the particles have a diameter above 710 .mu.m, said particles having a coating comprising one or more soluble inorganic salts. The salts may be selected from alkali or alkaline earth metal carbonates, sulphates, chlorides and nitrates. The coated percarbonate particles have improved stability to storage and are capable of dissolving quickly in wash liquor.Type: GrantFiled: January 16, 1996Date of Patent: August 11, 1998Assignee: The Procter & Gamble CompanyInventors: Gerard Marcel Baillely, Anthony Dovey, Graham Alexander Sorrie, David William York
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Patent number: 5789361Abstract: The present invention discloses an alkaline cleaning composition for cleaning heavily soiled metal surfaces such as food fryers, baking pans, high temperature pasteurizers, and beer kettles, ceramic surfaces such as restaurant grade ceramic china plates and platters, and plastic surfaces. The cleaning composition is noncaustic and includes a peroxygen compound, a chelate, and a metasilicate and/or sesquisilicate. A preferred cleaning composition further includes a surfactant and hydrated builder.Type: GrantFiled: March 1, 1996Date of Patent: August 4, 1998Assignee: Charvid Limited Liability Co.Inventor: Charles Bullick Talley
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Patent number: 5756445Abstract: A granular detergent component having a bulk density of less than 400 g/l comprises from 20% to 50%, by weight, of aluminosilicate, optionally up to 50%, by weight, of a co-filler, and 0.05% to 2%, by weight, of anionic surfactant, preferably C14-C20 alkyl sulphate. The low bulk density component is preferably mixed with other components such as percarbonate, silicate, layered silicate, carbonate, bicarbonate, sesquicarbonate, sulphate, citrate and mixtures thereof to provide a granular detergent composition.Type: GrantFiled: July 30, 1996Date of Patent: May 26, 1998Assignee: The Proctor & Gamble CompanyInventors: Andrew Dorset, Robin Gibson Hall
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Patent number: 5756447Abstract: A cleaning composition contains (a) a detersive surfactant and (b) a poly(amino acid) compound or a precursor thereof, the said component (b) being protected from contact with a level of alkalinity as would cause degradation thereof. The component (b) may be stabilized by, for example, coating it with an organic acid compound or with a film-forming polymer; by agglomerating it with a controlled level of alkaline or alkaline-reacting compound (e.g. sodium carbonate); by spray-granulating it in admixture with a nonionic surfactant; by encapsulating it with a silicone-based resin; or by incorporating it in a composition that is non-alkaline. The storage stability of the compositions is thereby improved.Type: GrantFiled: December 19, 1996Date of Patent: May 26, 1998Assignee: The Procter & Gamble CompanyInventor: Robin Gibson Hall
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Patent number: 5700294Abstract: Unique detergent compositions include a calcium precipitate-scavenging amount of an amorphous alkali metal silicoaluminate, advantageously are devoid of phosphate and zeolite values, and typically comprise at least one amorphous alkali metal silicoaluminate, an alkali metal carbonate, and at least one inhibitor of the crystal growth of calcium carbonate, such alkali metal carbonate being present in ionic calcium-removing amounts.Type: GrantFiled: January 11, 1996Date of Patent: December 23, 1997Assignee: Rhone-Poulenc ChimieInventors: Patrick Boittiaux, Virginie Couvret, Daniel Joubert
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Patent number: 5691294Abstract: Detergent components or compositions having a bulk density of at least 700 g/l comprise a nonionic surfactant system including at least one nonionic surfactant which is a liquid at temperatures below 40.degree. C., and from about 0.5% to 15% by weight of the component or compositions of a flow aid which is a premixed powder comprising sodium aluminosilicate and hydrophobic silica in a weight ratio of from 100:1 to 5:1. The detergent components or compositions are made by free dispersion mixing or granulation.Type: GrantFiled: December 11, 1995Date of Patent: November 25, 1997Assignee: The Procter & Gamble CompanyInventors: Paul Amaat Raymond Gerard France, Paul Irma Albertus Van Dijk
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Patent number: 5665427Abstract: The invention relates to a process for stabilizing particulate alkali metal percarbonate by coating by coating it with an aqueous solution, preferably concentrated, of a complex formed from a boric acid or borate and an organic diol, polyol or hydroxycarboxylic acid, to the resulting coated product, and to compositions including the product. The coating can additionally contain an alkali metal neutral salt such as sodium chloride or sodium sulphate.Type: GrantFiled: May 30, 1996Date of Patent: September 9, 1997Assignee: Solvay Interox LimitedInventors: Graham Robert Horne, Alun Pryce James
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Patent number: 5658873Abstract: Sodium percarbonate is often used in the form of coated particles to increase its storage stability in detergents.Sodium percarbonate particles coated in accordance with the invention have a coating containing reaction products from the reaction of a dialkali metal tetraborate or alkali metal pentaborate with aqueous hydrogen peroxide. Preferred coating components are: perborax with the formula Na.sub.2 B.sub.4 O.sub.7 .multidot.H.sub.2 O.sub.2, where n =2 or 4.The coated sodium percarbonate particles are produced by coating the percarbonate particles using a solution containing the reaction products mentioned above.Detergent, bleaching and cleaning compositions containing sodium percarbonate particles coated in accordance with the invention are distinguished by very high stability in storage.Type: GrantFiled: October 2, 1995Date of Patent: August 19, 1997Assignee: Degussa AktiengesellschaftInventors: Birgit Bertsch-Frank, Claas-Juergen Klasen, Thomas Lieser, Klaus Mueller, Martin Bewersdorf
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Patent number: 5556834Abstract: A process for stabilizing percarbonate by coating by means of a coating agent according to which the percarbonate particles are treated with a concentrated aqueous solution containing at least one boron compound selected from meta and ortho boric acids and at least one silicate, following by removal of water to provide coated percarbonate particles. The solution is prepared by adding the boron compound to a solution of the silicate. The coated particles are useful in washing and bleaching compositions.Type: GrantFiled: June 21, 1995Date of Patent: September 17, 1996Assignee: Solvay Interox LimitedInventors: Alun P. James, Graham R. Horne