Utilizing Plural Mixing Operations Of Specified Varying Intensity, E.g., Intensity Of Each Mixing Is Reduced, Etc. Patents (Class 523/346)
  • Patent number: 11731405
    Abstract: A multilayer protective film comprising a polyvinylidene fluoride/acrylate polymer layer and one or more thermoplastic polyurethane layers is provided. The multilayer protective film may possess beneficial and desirable properties useful in protecting surfaces, such as for example, high ultraviolet resistance, optical clarity, durability, and gloss.
    Type: Grant
    Filed: November 16, 2018
    Date of Patent: August 22, 2023
    Inventors: David Collette, Thomas Burke
  • Patent number: 11572445
    Abstract: The modified asphalt provided by the disclosure is prepared from the following raw materials in parts by weight: 100 to 120 parts of asphalt, 6 to 20 parts of a modifier, 3 to 9 parts of a compatibilizer, 0.15 to 0.25 parts of sulfur, 0.4 to 0.6 parts of a non-amine anti-stripping agent and 0.2 to 0.4 parts of a coupling agent; and the modifier comprises a styrene-butadiene-styrene block copolymer, a rubber, and a polyurethane. The modified asphalt provided by the disclosure can simultaneously satisfy an elastic recovery at 25° C. of ?98%, a dynamic viscosity at 60° C. of ?500,000 Pa·s, a composite shear modulus at 60° C. of ?10 Pa, and a critical temperature at G*/Sin?2.2 kPa of ?94° C.
    Type: Grant
    Filed: December 27, 2018
    Date of Patent: February 7, 2023
    Assignee: Central Fortune Creation Technology Group Co., Ltd.
    Inventors: Jiangmiao Yu, Guocheng Su, Guangliang Mo, Fuda Chen, Lijuan Chen, Jianyuan Lu
  • Patent number: 10808139
    Abstract: A colored paint that imparts a superhydrophobic surface on an object is a suspension of hydrophobic particles in a polymeric binder and a plasticizer in a solvent or mixed solvent, wherein at least a portion of the hydrophobic particles are colored particles. Colored particles can be ultramarine, iron oxide, chromium oxide, or any other colored metal oxide. The hydrophobic particles can be metal oxide particles that are surface functionalized with a fluorinated alkyl silane or an alkyl silane. The binder is a mixture of PDVF and PMMA in a ratio of 3:1 to 10:1. The plasticizer is a mixture of triethyl phosphate and perfluoro(butyltetrahydrofuran) or other perfluorinated hydrocarbon. Surfaces coated using this paint display contact angles in excess of 150° and resist abrasion.
    Type: Grant
    Filed: April 11, 2017
    Date of Patent: October 20, 2020
    Assignee: University of Florida Research Foundation, Inc.
    Inventors: Wolfgang M. Sigmund, Yung-Chieh Hung
  • Patent number: 8362113
    Abstract: A self-repairing concrete includes a predetermined amount of concrete, micro-capsules and water being mixed together for a fixed function of micro-cracks, wherein a mass ratio of the concrete, micro capsules, and water is 100:1-15:15-50. The manufacturing method mixing water with micro-capsules until the micro-capsules are fully dispersed into the water; placing a mixture of water and micro-capsules in a stirring container and adding a predetermined amount of cement into the stirring mixture; stirring; and gradually adding filling into the concrete slurry into a mixing container and removing bubbles in the concrete slurry in the mixing container to form the self-repairing concrete.
    Type: Grant
    Filed: February 28, 2012
    Date of Patent: January 29, 2013
    Inventors: Feng Xing, Zhuo Ni
  • Patent number: 8263703
    Abstract: The present invention is related to an one component self-crosslinking reactive siloxane-terminated polypropylene oxide emulsion and a process for preparing the same. In the inventive process, using a reactive siloxane-terminated polypropylene oxide (SPPO) as raw material and a polyether-modified polysiloxane as protection colloid, a waterborne SPPO emulsion with excellent storage stability and freeze-thaw stability was prepared through phase inversion emulsification in the presence of composite emulsifying agent. And this process has some advantages such as low capital investment for equipment, simple procedure, easy operation and low production cost. And the obtained SPPO emulsion can be used as basic raw materials for the production of environmental friendly waterborne products such as paints, binders, sealing agents etc.
    Type: Grant
    Filed: June 28, 2010
    Date of Patent: September 11, 2012
    Assignee: Henkel AG & Co. KGaA
    Inventors: Kan Chengyou, Hou Zhao Sheng, Li Zeping, Xie Wei, Zhao Zhiqing, Yon Zhang, Thomas Fay-Oy Lim
  • Patent number: 8222323
    Abstract: A self-repairing concrete includes polyurethane polymer micro-capsules, in which the polyurethane polymer micro-capsules are mixed for a fixed function of micro-cracks. The quality mixture ratio is: concrete/micro capsules/water=100:1-15:15-50. The manufacturing method is weighing a full amount of water in a container, adding polyurethane polymer micro-capsules, stirring, until fully dispersed microcapsules; pouring the water into the mixing container, adding the corresponding quality of cement; stirring; adding sand and gravel filling materials, conducting worksite watering, ? volume for each time, vibrating, and air exhausting; until the slurry filling mold.
    Type: Grant
    Filed: October 24, 2008
    Date of Patent: July 17, 2012
    Inventors: Feng Xing, Zhuo Ni
  • Publication number: 20120045596
    Abstract: The instant disclosure relates to a method of making a dispersion of polymer binder-encapsulated silica pigments for coating an ink-jet recording substrate. The method includes mixing first components of the dispersion to form a mixture, the first components including binder polymer, treating agents and a vehicle selected from the group consisting of water, a water-miscible organic solvent, and combinations thereof; shear mixing silica pigment into the mixture; and after the silica pigment is added to the mixture, shear mixing the mixture at a higher temperature and an increased grinding rate compared to a temperature and grinding rate of the shear mixing of the silica pigment into the mixture.
    Type: Application
    Filed: April 30, 2009
    Publication date: February 23, 2012
    Inventors: Dheya M. Alfekri, Ronald J. Selensky
  • Publication number: 20120004347
    Abstract: A process for producing a natural rubber nanocomposite containing exfoliated organically modified montmorillonite and maleic anhydride grafted elastomer in a dispersion of natural rubber and reinforcing filler/inert filler wherein the cured nanocomposite has improved mechanical properties compared to conventional rubber compound containing a mixture of the reinforcing filler, carbon black and the inert filler, CaCO3.
    Type: Application
    Filed: June 30, 2011
    Publication date: January 5, 2012
    Applicant: Sri Lanka Institute of Nanotechnology (PVT) Ltd.
    Inventors: Upul Nishantha Ratnayake, Charminda Peiris, Nanda Fernando, Sarathchandra Kularatne, Veranja Karunaratne, Dileepa Prematunga
  • Publication number: 20110054070
    Abstract: A self-repairing concrete includes polyurethane polymer micro-capsules, in which the polyurethane polymer micro-capsules are mixed for a fixed function of micro-cracks. The quality mixture ratio is: concrete/micro capsules/water=100:1-15:15-50. The manufacturing method is weighing a full amount of water in a container, adding polyurethane polymer micro-capsules, stirring, until fully dispersed microcapsules; pouring the water into the mixing container, adding the corresponding quality of cement; stirring; adding sand and gravel filling materials, conducting worksite watering, ? volume for each time, vibrating, and air exhausting; until the slurry filling mold.
    Type: Application
    Filed: October 24, 2008
    Publication date: March 3, 2011
    Inventors: Feng Xing, Zhuo Ni
  • Patent number: 7893134
    Abstract: A process for producing an absorbent polymer including a first mixing event, in which a plurality of absorbent polymer particles (1) are mixed with a liquid (2) and a second mixing event, in which the liquid (2) is homogenized within the interior of the polymer particles. The polymer particles (1) in the first mixing event are mixed with a speed such that the kinetic energy of the individual polymer particles (1) is on average larger than the adhesion energy of the individual polymer particles (1), and the polymer particles (1) in the second mixing event are stirred at a lower speed than in the first mixing event. The different speeds effect a fluidization of the polymer particles (1), which prevents a clumping of the polymer particles (1) during the mixing event. The absorbent polymers thus produced are distinguished by a particularly rapid swelling behavior.
    Type: Grant
    Filed: April 27, 2009
    Date of Patent: February 22, 2011
    Assignee: Evonik Stockhausen GmbH
    Inventors: Armin Reimann, Manfred Van Stiphoudt, Herbert Vorholt
  • Publication number: 20090209683
    Abstract: A process for producing an absorbent polymer including a first mixing event, in which a plurality of absorbent polymer particles (1) are mixed with a liquid (2) and a second mixing event, in which the liquid (2) is homogenized within the interior of the polymer particles. The polymer particles (1) in the first mixing event are mixed with a speed such that the kinetic energy of the individual polymer particles (1) is on average larger than the adhesion energy of the individual polymer particles (1), and the polymer particles (1) in the second mixing event are stirred at a lower speed than in the first mixing event. The different speeds effect a fluidization of the polymer particles (1), which prevents a clumping of the polymer particles (1) during the mixing event. The absorbent polymers thus produced are distinguished by a particularly rapid swelling behavior.
    Type: Application
    Filed: April 27, 2009
    Publication date: August 20, 2009
    Inventors: Armin Reimann, Manfred Van Stiphoudt, Herbert Vorholt
  • Patent number: 7541395
    Abstract: A process for producing an absorbent polymer including a first mixing event, in which a plurality of absorbent polymer particles (1) are mixed with a liquid (2) and a second mixing event, in which the liquid (2) is homogenized within the interior of the polymer particles. The polymer particles (1) in the first mixing event are mixed with a speed such that the kinetic energy of the individual polymer particles (1) is on average larger than the adhesion energy of the individual polymer particles (1), and the polymer particles (1) in the second mixing event are stirred at a lower speed than in the first mixing event. The different speeds effect a fluidization of the polymer particles (1), which prevents a clumping of the polymer particles (1) during the mixing event. The absorbent polymers thus produced are distinguished by a particularly rapid swelling behavior.
    Type: Grant
    Filed: October 24, 2003
    Date of Patent: June 2, 2009
    Assignee: Evonik Stockhausen GmbH
    Inventors: Armin Reimann, Manfred Van Stiphoudt, Herbert Vorholt
  • Patent number: 7501459
    Abstract: A method of producing a carbon fiber composite material includes: a first mixing step of mixing an elastomer and carbon nanofibers at a first temperature; and a second mixing step of mixing a mixture obtained by the first mixing step at a second temperature, and the first temperature is 50 to 100° C. lower than the second temperature.
    Type: Grant
    Filed: May 20, 2005
    Date of Patent: March 10, 2009
    Assignee: Nissin Kogyo Co., Ltd.
    Inventors: Toru Noguchi, Akira Magario
  • Patent number: 7354964
    Abstract: The mixture solvent of dichlorimethane type, the TAC and the plasticizer are supplied into a dissolution tank, and stirred therein with a stirrer to obtain a dispersing solution. The dispersing solution is fed into a storing tank and further stirred therein. Then the dispersing solution is fed by a pump to a heat exchanger for the heating, and thereafter the stirring is made with a static mixer. The temperatures of the dope is measured at many measuring points. On the basis of the temperature distribution, the heat transmission conditions of the heat exchanger are adjusted. Then the dope is fed to a heat exchanger for cooling, to cool to at most the normal boiling point of the dope. Then the mixing is made with a static mixer. Thus the obtained dope is uniform.
    Type: Grant
    Filed: July 29, 2004
    Date of Patent: April 8, 2008
    Assignee: FUJIFILM Corporation
    Inventors: Seiichi Ono, Yuji Suzuki, Hidekazu Yamazaki
  • Patent number: 6794430
    Abstract: The process for manufacturing polymer granules includes the operations of mixing a base polymer and additives, with a specific step of adding shading colorant to the cured polymer mixture followed by a step of carrying out an incomplete homogenization of the colorant with the polymer mixture, the duration of which is fixed according to desired colouring anisotropy characteristics, the process providing granules having such an anisotropy which can be used for the manufacturing of coatings and moulded articles.
    Type: Grant
    Filed: December 10, 2001
    Date of Patent: September 21, 2004
    Assignee: Etablissements Boulenger
    Inventors: Jacques Berlemont, Xavier Poupon
  • Patent number: 6787588
    Abstract: A process for transforming a polymer base, having a shaded appearance of anisotropic coloring, into a finished article, the process including operations of mixing a base polymer and additives, of adding a shading colorant to the polymer mixture, followed by incomplete homogenization of the shading colorant in the polymer mixture to form the polymer base with a shaded appearance of anisotropic coloring, subsequent shaping to an intermediate predetermined shape, and vulcanization and cooling as applicable, and then an operation of breaking up the shaded polymer base into individualized elements and an operation of aggregation of the elements, to obtain the finished article, in any desired arrangement. It also relates to a finished article, having such anisotropy, constituted by an agglomerate of individualized elements, and its application as a surface coating.
    Type: Grant
    Filed: October 23, 2002
    Date of Patent: September 7, 2004
    Assignee: Etablissements Boulenger
    Inventors: Jacques Berlemont, Xavier Poupon
  • Patent number: 6489372
    Abstract: Polymer are removed from organic solvent-polymer mixtures by preparing a liquid-liquid dispersion of finely dispersed solvent droplets containing polymer in water, adding this liquid-liquid dispersion to a stirred vessel containing water or other suitable liquid and rapidly evaporating the solvent to produce a slurry of the polymer in a liquid from which the solid polymer particles are recovered.
    Type: Grant
    Filed: October 17, 2000
    Date of Patent: December 3, 2002
    Assignee: General Electric Company
    Inventors: Qiwei He, Paul Russell Wilson, Paul William Buckley, Allen Wai Yee Ko, Larry Allen Divins, William Lee Gately, Ganesh Kailasam
  • Publication number: 20020128366
    Abstract: A process for coloring vulcanized rubber granules that exhibits improved color durability is provided. Coloring is achieved by mixing low concentrations of aqueous based organic or inorganic pigment dispersions with rubber particles for a short time. Binding colorant onto the colored rubber particles is achieved when elastomer latex is added in a second step. The resulting colored vulcanized rubber particles exhibit outstanding color stability and color abrasion resistance. Optimum color adhesion onto rubber particles is achieved by use of elastomer tailored to the type of colorant used. With organic pigments such as copper phthalocyanine, excellent color abrasion resistance to vulcanized rubber particles results when elastomers such as SBR are used. With inorganic pigments such as iron oxide, excellent color abrasion resistance results when elastomers with very low glass transition temperature (Tg) such as acrylic rubber are used. The process can be readily scaled to large commercial blending equipment.
    Type: Application
    Filed: December 20, 2001
    Publication date: September 12, 2002
    Inventor: Gerald P. Coffey
  • Patent number: 6414054
    Abstract: High levels of treated fumed silica, processing fluid and high molecular weight silicone polymer are continuously compounded into a homogeneous silica filled heat-vulcanizable silicone composition by forming a premix in a continuous annular layer mixer and continuously discharging the premix into a compounding apparatus for compounding to form the filled heat-vulcanizable silicone composition.
    Type: Grant
    Filed: December 21, 1999
    Date of Patent: July 2, 2002
    Assignee: General Electric Company
    Inventors: Jodi Boffard, Navjot Singh, Alan L. Tate, Robert Dean
  • Patent number: 6362271
    Abstract: A weather resistant coating composition comprising a miscible polymer blend of highly crystalline polyvinylidene fluoride polymer and polyalkyl methacrylate, such as PVDF and PMMA. The miscible blend comprises from about 50 weight percent to about 90 weight percent polymer comprising polyvinylidene fluoride and from about 10 weight percent to about 50 weight percent polyalkyl methacrylate. The polyalkyl methacrylate having a molecular weight within the range of about 25,000 grams per mole to about 200,000 grams per mole. The crystallinity of the polyvinylidene fluoride polymer is about 20% to about 70%. The weather resistant coating has excellent and unexpected physical characteristics, including solvent resistance and gloss retention.
    Type: Grant
    Filed: August 27, 1999
    Date of Patent: March 26, 2002
    Assignee: Ausimont USA, Inc.
    Inventors: Shiow-Ching Lin, Craig Kamsler, Karol Argasinski
  • Publication number: 20010031801
    Abstract: Apparatus and method for preparing microparticles. An emulsion is formed by combining two phases in a static mixing assembly. The static mixing assembly preferably includes a preblending static mixer and a manifold. The emulsion flows out of the static mixing assembly into a quench liquid whereby droplets of the emulsion form microparticles. The residence time of the emulsion in the static mixing assembly is controlled to obtain a predetermined particle size distribution of the resulting microparticles.
    Type: Application
    Filed: April 10, 2001
    Publication date: October 18, 2001
    Inventors: Shawn L. Lyons, Steven G. Wright
  • Patent number: 6214892
    Abstract: This invention relates to a method of recovering a polymer from an organic mixture comprising polymer and an organic solvent, the method comprising: a) admixing an aqueous solution and the organic mixture by the application of a combined mechanical and hydraulic shear force, the combined mechanical and shear force being sufficient to form a liquid-liquid dispersion; b) removing the organic solvent from the liquid-liquid dispersion thereby forming a remaining solution; and c) separating the polymer from the remaining solution. In one embodiment the polymer is a polycarbonate prepared by the interfacial method, and the organic solvent is methylene chloride.
    Type: Grant
    Filed: December 23, 1999
    Date of Patent: April 10, 2001
    Assignee: General Electric Company
    Inventors: Qiwei He, Paul Russell Wilson, Paul William Buckley, Allen Wai Yee Ko, Larry Allen Divins
  • Patent number: 6001917
    Abstract: In a first step, basic components including (A) 100 parts by weight of an organopolysiloxane gum, (B) 5-100 parts by weight of a reinforcing silica filler, and (C) 0.1-30 parts by weight of a processing aid are fed batchwise to a closed mixer for mixing them at a temperature of room temperature to 150.degree. C. In a second step, the mixture is fed into a kneader/mixer for heat treating at a temperature of 150-250.degree. C. The first step achieves quick dispersion and cooperates with the second step to form a heat-curable silicone rubber compound in an efficient manner.
    Type: Grant
    Filed: June 27, 1998
    Date of Patent: December 14, 1999
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Masaharu Takahashi, Yutaka Hagiwara, Minoru Igarashi, Keiji Shibata
  • Patent number: 5852076
    Abstract: A process and a high pressure apparatus are disclosed which are useful in preparing magnetic dispersions and other dispersions of hard, non-compliant particulates. The apparatus can be monitored for clogs and wear and allows for relatively quick and inexpensive replacement of orifices. The apparatus includes a high pressure pump and a series of impingement chambers comprising an input manifold where the process stream is split into two or more streams and an output manifold where the streams are recombined after passing through restrictive orifices configured in such a manner that the streams impinge on each other at high velocities. The orifices in each succeeding impingement zone are the same size or smaller than the orifices in the preceding impingement zone, and the orifices in the final impingement zone must be smaller than the orifices in the first impingement zone.
    Type: Grant
    Filed: November 7, 1997
    Date of Patent: December 22, 1998
    Assignee: Minnesota Mining and Manufacturing Company
    Inventors: Mark Serafin, Richard D. Olmsted, Richard M. Fuller, Bhaskar V. Velamakanni, Zvi Rogovin
  • Patent number: 5827909
    Abstract: An improvement in a continuous process for making high internal phase emulsions that are typically polymerized to provide microporous, open-celled polymeric foam materials capable of absorbing aqueous fluids, especially aqueous body fluids such as urine. The improvement involves recirculating a portion (about 50% or less) of the emulsion withdrawn from the dynamic mixing zone of this continuous process. This increases the uniformity of the emulsion ultimately obtained from this continuous process in terms of having the water droplets homogeneously dispersed in the oil phase. This also improves the stability of the HIPE and expands the temperature range for pouring and curing this HIPE during subsequent emulsion polymerization. The improvement also eliminates the need for a static mixer outside the dynamic mixing zone, and allows for processing where relatively low pressure drops are required across the mixing zone.
    Type: Grant
    Filed: September 17, 1996
    Date of Patent: October 27, 1998
    Assignee: The Procter & Gamble Company
    Inventor: Thomas A. DesMarais
  • Patent number: 5614583
    Abstract: This invention relates to a crosslinked N-vinyl lactam polymer in the form of a stable, homogenized flowable hydrogel having microparticles which can be passed through a screen of between about 40 and about 350 mesh size. The invention also concerns the process for the preparation of the homogenized gel and to its use as a hair and skin conditioner or as a carrier for a cosmetically or pharmaceutically active substance.
    Type: Grant
    Filed: September 13, 1995
    Date of Patent: March 25, 1997
    Assignee: ISP Investments Inc.
    Inventors: Susan Y. Tseng, Jui-Chang Chuang, Philip F. Wolf
  • Patent number: 5536613
    Abstract: A process for the preparation of pigmented toner compositions comprising: a) forming at a first temperature, a first melt mixture comprised of a partially crosslinked thermoplastic resin, pigment, optionally a wax, and optional additives, wherein the partially crosslinked thermoplastic resin is comprised of a mixture of crosslinked resin macrogel particles, crosslinked resin microgel particles, and uncrosslinked resin; and b) melt mixing at a second temperature, the first melt mixture to form a second mixture, wherein the macrogel particles are partially converted into microgel particles, and wherein the second temperature is less than or equal to the first temperature.
    Type: Grant
    Filed: February 23, 1995
    Date of Patent: July 16, 1996
    Assignee: Xerox Corporation
    Inventors: Hui Chang, Joo T. Chung, Joseph L. Leonardo, Enno E. Agur, John J. Ianni, Allison G. Thomas, Linda A. Flannery
  • Patent number: 5530039
    Abstract: Process for manufacturing stopping compounds, in particular such as can be used for motor vehicle repair lacquering, in which in a first stage at least 90 wt.-% of the solvents required and 80 to 100 wt.-% of the binding agents required are dispersed together with such a proportion of the pigments and/or extenders as is required in order to ensure that the mixture can be dispersed in a high-speed agitator mill, as well as optionally together with the required additives in a high-speed agitator mill, in particular a bead mill or sand mill, whereupon the dispersed material produced is, in a second stage, mixed with the remaining amounts of pigment and/or extender as well as optionally the remaining amounts of binding agent and solvent and dispersed in a dissolver to the required fineness.
    Type: Grant
    Filed: December 9, 1993
    Date of Patent: June 25, 1996
    Assignee: Herberts GmbH
    Inventor: Otfried Nawotka
  • Patent number: 5498646
    Abstract: Method for preparing adhesive compositions subjecting a mixture of block polymer and other adhesive constituents e.g., resin(s) and oil(s) to shearing and smearing in an emulsifier disperser.
    Type: Grant
    Filed: September 6, 1994
    Date of Patent: March 12, 1996
    Assignee: H. B. Fuller Licensing & Financing, Inc.
    Inventors: Glenn C. Heuer, George F. Bateson
  • Patent number: 5403693
    Abstract: A process for the preparation of toner compositions with controlled particle size comprising:(i) preparing a pigment dispersion in water, which dispersion is comprised of a pigment, an ionic surfactant in amounts of from about 0.
    Type: Grant
    Filed: June 25, 1993
    Date of Patent: April 4, 1995
    Assignee: Xerox Corporation
    Inventors: Raj D. Patel, Grazyna E. Kmiecik-Lawrynowicz, Michael A. Hopper
  • Patent number: 5110846
    Abstract: The method consists of the separate simultaneous extrusion, by means of two or more contiguous extruders or one extruder with two or more separate homogenization chambers, of two or more paints in powder form and the union of the extrusions in the molten state or still hot and then subsequent cooling as a single extrusion.
    Type: Grant
    Filed: December 15, 1989
    Date of Patent: May 5, 1992
    Assignee: Hoechst Sara S.p.A.
    Inventors: Silvestro Farronato, Sergio Gazzea
  • Patent number: 5021463
    Abstract: A batch process for making a resin includes adding at least one portion of colored resin material to a resin base material of another color and mixing the combination including the colored material only sufficiently to incomplete blend the colored material into the base mix so that the colored material is only partially dispersed in the resin base. The multicolored product may be foamed or unfoamed material.
    Type: Grant
    Filed: June 17, 1988
    Date of Patent: June 4, 1991
    Assignee: Packaging Industries Group, Inc.
    Inventor: Matthew L. Kozma
  • Patent number: 4988747
    Abstract: Process for the production of a binder modified with synthetic material for building materials, especially street-building material, in which for the formation of the binder, molten bitumen together with a thermoplast or a thermoplast mixture, preferably an olefin polymer, is subjected to a homogenization treatment. To the mixture containing the bitumen and a thermoplast or a thermoplast mixture, there is supplied in the form of kinetic energy an amount of energy corresponding to the difference between the treatment temperature and the disintegration temperature of the thermoplast or thermoplast mixture to form readily reacting molecular fragments of the thermoplast or thermoplast mixture. Preferably, the mixture containing bitumen and the thermoplast or a thermoplast mixture is driven through a narrow gap between two mixing tools standing opposite to one another and rotating relatively to one another.
    Type: Grant
    Filed: July 5, 1988
    Date of Patent: January 29, 1991
    Assignee: Novophalt Overseas S.A.
    Inventor: Erich Strommer
  • Patent number: 4906428
    Abstract: A method for the manufacture of a physical blend of pigment and a polymer powder whereby polymer powder having a particle size in the range of 250 to 750 microns is fed to a high intensity mixer and then powdered pigment is fed to the mixer at a rate of not more than 0.5 parts of pigment per 100 parts of polymer per minute. The pigment has a particle size that is substantially smaller than that of the polymer powder. The resultant admixture is mixed for a further period of time and then discharged from the mixer. The method is particularly applicable to powdered polyethylene intended for use in a rotational moulding process e.g. for the manufacture of containers and other hollow articles.
    Type: Grant
    Filed: January 23, 1989
    Date of Patent: March 6, 1990
    Assignee: Du Pont Canada Inc.
    Inventor: Peter Y. Kelly
  • Patent number: 4705646
    Abstract: Conductive coating (20) is a thorough mixture of 0.03 parts per weight of carbon black together with 0.003 to 0.01 parts per weight of wetting agent and 20 parts of solvent, and further mixing in by low shearing mixing 1/2 to 1 part per weight of thermosetting resin. This is then sprayed into place on the substrate and thermoset. In this particular case, the substrate is exterior face sheet (12) of honeycomb structure (10) which may serve as part of a spacecraft, to electrically conduct away surface charges.
    Type: Grant
    Filed: December 10, 1984
    Date of Patent: November 10, 1987
    Assignee: Hughes Aircraft Company
    Inventors: Preston S. DuPont, Robert E. Ritter, John P. Stafford
  • Patent number: 4647602
    Abstract: This invention provides a method of dispersing a fluoroplastic in a polymer composition. The method comprises the steps of comminuting the fluoroplastic to a uniform dispersion, admixing with the fluoroplastic a finely divided solid adherent material that will coat at least a portion of said fluoroplastic to form a coated fluoroplastic and combining said coated fluoroplastic with a polymer using intensive mixing means.
    Type: Grant
    Filed: May 1, 1985
    Date of Patent: March 3, 1987
    Assignee: General Electric Company
    Inventors: Boguslaw G. Wilczak, Edward V. Wilkus, Alexander F. Wu
  • Patent number: 4619967
    Abstract: Multi-modal emulsions comprise a continuous oil phase and a discontinuous aqueous phase having two or more droplet size distributions and comprising a water-soluble polymer. Such emulsions are prepared by subjecting portions of the emulsion to varying rates of shear during emulsion formation. The multi-modal emulsions can have high polymer solids, reduced oil content, low bulk viscosity and high stability.
    Type: Grant
    Filed: November 2, 1984
    Date of Patent: October 28, 1986
    Assignee: The Dow Chemical Company
    Inventors: Richard R. Emerson, Do I. Lee, James P. Easterly
  • Patent number: 4565836
    Abstract: Multi-modal emulsions comprise a continuous oil phase and a discontinuous aqueous phase having two or more droplet size distributions and comprising a water-soluble polymer. Such emulsions are prepared by subjecting portions of the emulsion to varying rates of shear during emulsion formation. The multi-modal emulsions can have high polymer solids, reduced oil content, low bulk viscosity and high stability.
    Type: Grant
    Filed: May 26, 1983
    Date of Patent: January 21, 1986
    Assignee: The Dow Chemical Company
    Inventors: Richard R. Emerson, Do I. Lee, James P. Easterly
  • Patent number: 4521552
    Abstract: What is disclosed is a method for making a water-in-oil emulsion of a water soluble polymer of high molecular weight of polymerization of an aqueous monomer solution emulsified in an oil, even in large batches or continuously, comprising not moving the emulsion in a turbulent flow pattern at the start of polymerization and not mixing the emulsion at the start of polymerization with portions of emulsion which have been exposed to polymerization conditions for less time. Once polymerization has started, it is continued by the action of an initiator which decomposes to yield free radicals.
    Type: Grant
    Filed: February 11, 1983
    Date of Patent: June 4, 1985
    Assignee: Rohm GmbH
    Inventors: Reiner Schnee, Jurgen Masanek
  • Patent number: 4510271
    Abstract: Thermoplastic granules are finished by blending thermoplastic granules with additive material to form a masterblend; intensively mixing the masterblend with additional thermoplastic granules under conditions (1) to increase the temperature of the thermoplastic to its softening temperature and (2) to increase the bulk density of the granules; and withdrawing and cooling the mixture to form free flowing granules containing additives thereon or therein.
    Type: Grant
    Filed: October 27, 1982
    Date of Patent: April 9, 1985
    Assignee: Exxon Research & Engineering Co.
    Inventors: Mike E. Muhle, Richard J. Stolz, Cecil W. Wright
  • Patent number: 4508859
    Abstract: Rotational mold grade resin is made by subjecting polyolefin to the following process: (1) polyolefin granules are blended with additives to form a masterblend; (2) the masterblend is intensively mixed with additional resin granules to shape the granules, reduce particle size and disperse additives; (3) the intermixed material is cooled and (4) large particles are removed and recycled.
    Type: Grant
    Filed: December 22, 1982
    Date of Patent: April 2, 1985
    Assignee: Exxon Research & Engineering Co.
    Inventors: Mike E. Muhle, Richard J. Stolz, Cecil W. Wright
  • Patent number: 4340516
    Abstract: A method of rapidly compounding melt forming resin, mica and chlorinated hydrocarbon wherein the mica has a coating comprising the chlorinated hydrocarbon, which method comprises providing a molten mass of the resin, contacting the molten mass with the coated mica and kneading the so contacted mica and resin to provide mixing thereof. The compounding is rapid and at optimal temperature.
    Type: Grant
    Filed: December 13, 1979
    Date of Patent: July 20, 1982
    Assignee: Ford Motor Company
    Inventor: Allen J. Keeney