Abstract: This invention discloses an apparatus for extraction of constituents with extraction fluid present in a substance by means of an extraction fluid constituted by a water heated to high temperature known as super-heated water (SHW). According to this invention, in the heater the water is heated to a subcritical point and introduced to the extractor contacting takes place between the substance and the extraction fluid to dissolve the constituents in the fluid. The fluid leaving the extractor is then cooled in a cooler. The process is performed under constant counter pressure given by a Nitrogen tank. Separation of the volatile components is done in one or multistage countercurrent liquid-liquid system with any volatile solvent with proper solubility of the constituents or in a distillation column. distillation column.

Abstract: A plant oil extraction system is disclosed utilizing a novel dual vapor recovery scheme and pressure differentials and valve timing conducive to continuous operation.

Abstract: Dark, red and dark, brown natural cocoa products are disclosed. The cocoa products may be cocoa liquor or cocoa powder. Processes for producing the dark, red and dark, brown natural cocoa products are also disclosed.

Abstract: Increased antigenicity of a membrane-bound polypeptide produced from a plant is provided in a process in which extraction of the polypeptide or other compounds from the plant is such that phospholipids are associated with the polypeptide. Reducing fat by supercritical fluid extraction increases antigenicity of such plant-produced membrane-bound polypeptides. Methods and means of producing such membrane-bound polypeptides are provided. Methods to produce a protective response in animals are provided by administering to the animal the membrane-bound polypeptide. Binding of antibody specific to the membrane-bound polypeptide is increased. The process provides for increased preferred formation of the membrane-bound polypeptide. Stability of the membrane-bound polypeptide is increased when the plant material is defatted.

Abstract: The present disclosure relates to methods and systems for injecting a gas (e.g., air) into a grain oil recovered from a grain process so as to remove an amount of one or more materials (e.g., moisture, unsaponifiables, insolubles, free fatty acids, and the like) from the grain oil.

Abstract: Methods for extracting solute from a source material are shown and described. The methods each include: depositing the source material in a canister, introducing a solvent, exposing the source material to the solvent to create an extract mixture, communicating the extract mixture to one or more extract containers, separating the solute from the extract mixture by heating the extract containers, collecting the recycled solvent in a solvent collection container, and cooling the recycled solvent within the solvent collection container. In some examples, the one or more extract containers are first and second extract containers that are each selectively coupleable to the canister and are selectively removable for storage of the extract mixture. In some other examples, cooling the recycled solvent within the solvent collection container is carried out via a cooling mechanism coupled to the solvent storage container.

Abstract: Disclosed is a method capable of improving the skin regeneration effect of medicinal materials through double boiling using an earthenware pot. The method shows an excellent skin regeneration effect, and the extract of medicinal materials obtained therethrough can be variously applied in the fields of cosmetics, health foods or medicine.

Abstract: A method for preparing a coffee polyol includes: (a) extracting coffee oil from coffee grounds; (b) modifying the coffee oil to obtain an epoxidized coffee oil; and (c) reacting an alcohol with the epoxidized coffee oil to obtain a coffee polyol. A polyurethane dispersive solution is prepared from a prepolymer composition that includes: a coffee polyol prepared from the abovementioned method; an isocyanate; and a solvent. A foam-based material is made from a foaming composition that includes a coffee polyol prepared from the abovementioned method. A polyurethane material is made from a polyurethane composition that includes a coffee polyol prepared from the abovementioned method.

Abstract: The present invention provides a supercritical fluid extraction (SFE) process for extracting oil of kenaf seed (Hibiscus cannabinus L.), wherein the SFE process utilises a supercritical fluid and is conducted in a pressure ranging from 200 to 600 bars with a temperature ranging from 40 to 80° C.

Abstract: The present invention provides a supercritical fluid extraction (SFE) process for extracting oil of kenaf seed (Hibiscus cannabinus L.), wherein the SFE process utilizes a supercritical fluid and is conducted in a pressure ranging from 200 to 600 bars with a temperature ranging from 40 to 80° C.

Abstract: A method of removing a nonpolar solvent from a fluid volume that includes at least one nonpolar compound, such as a fat, an oil or a triglyceride, is provided. The method comprises contacting a fluid volume with an expanding gas to expand the nonpolar solvent and form a gas-expanded solvent. The gas-expanded solvent may have a substantially reduced density in comparison to the at least one nonpolar compound and/or a substantially reduced capacity to solubilize the nonpolar compound, causing the nonpolar compounds to separate from the gas-expanded nonpolar solvent into a separate liquid phase. The liquid phase including the at least one nonpolar compound may be separated from the gas-expanded solvent using conventional techniques. After separation of the liquid phase, at least one of the temperature and pressure may be reduced to separate the nonpolar solvent from the expanding gas such that the nonpolar solvent may be recovered and reused.

Abstract: The present disclosure provides a process for producing 20-carbon fatty acids from a plant seed oil, the process comprising: a) providing a plant seed oil comprising fatty acids, wherein the fatty acids include 18-carbon fatty acids; and b) elongating the fatty acids by two carbon atoms to produce a composition comprising 20-carbon fatty acids.

Abstract: A composition of matter comprises a shelf stable, super critical, CO2 fluid extracted seed oil derived from a cracked biomass of perilla frutescens, the seed oil comprising from about 60 to about 95 percent w/w of PUFAs in a ratio of from about 4:1 to about 6:1 alpha-linolenic acid (ALA) to linoleic acid (LA) and a mixture of selected antioxidants.

Abstract: Generally, a method of pressure regulated supercritical fluid fractionation of oil seed extraction materials which can be utilized to refine oil seed extraction material established in an amount of supercritical fluid. Specifically, a method of pressure regulated supercritical fluid fractionation of corn germ extraction material to produce a refined corn oil extraction material.

Abstract: The present invention reported that SFE is suitable for Nigella sativa seeds oil extraction and fractionation. TQRF that were produced through SFE extractions (600 bars/40° C.) and fractionations (100-200 bars/40-60° C.) possessed high level of TQ and antioxidant activity. SFE fractionation efficiently concentrates the TQ content and antioxidant activity of Nigella sativa seeds oil in short time and low cost manners without using any hazardous organic solvents.

Abstract: Generally, a method of pressure regulated supercritical fluid fractionation of oil seed extraction materials which can be utilized to refine oil seed extraction material established in an amount of supercritical fluid. Specifically, a method of pressure regulated supercritical fluid fractionation of corn germ extraction material to produce a refined corn oil extraction material.

Abstract: Systems and methods for improving dense gas solvent extraction of a solute and recovery of the solvent are provided. A pressure of the solvent/solute mixture obtained from an extraction chamber is increased, e.g. with a pump, thereby providing the mixture above saturation conditions. The increased pressure provides greater solubility of the solute and less solvent being vaporized in a heat exchanger. A buildup of solute in the system is reduced, thus improving system longevity. Also, process conditions of the separation process are isolated from those of the extraction process. Accordingly, the process conditions for the separating process are maintained while the process conditions of the extraction chamber vary with ambient temperature, thus saving cost and energy. This isolation also provides an ability to use, in the gas recovery cycle, a heat pump that can be used for many applications and environmental conditions while still using a conventional refrigerant.

Abstract: The present invention provides a supercritical fluid extraction (SFE) process for extracting oil of kenaf seed (Hibiscus cannabinus L.), wherein the SFE process utilises a supercritical fluid and is conducted in a pressure ranging from 200 to 600 bars with a temperature ranging from 40 to 80° C.

Abstract: Methods of separating oil from oil-containing seeds, involving aerating an aqueous dispersion of germ particles of oil-containing seeds (e.g., corn) to produce bubbles therein, whereby the oil in the aqueous dispersion adheres preferentially to the surfaces of the bubbles and are carried by the bubbles to the upper surface of the aqueous dispersion where a foam of the bubbles is formed; separating the foam from the aqueous dispersion; and recovering the oil from the foam. The aqueous dispersion of germ particles of oil-containing seeds may be produced by mixing corn germ separated from corn kernels with an aqueous acetate buffer followed by heating, grinding, cooling, and optionally agitation; generally cellulase is added after the grinding.

Abstract: Apparatus for the continuous processing and solids handling in first near-critical and supercritical fluids. The present invention also allows for treatment of the starting material with the first near-critical or supercritical fluid. The remaining raffinate is then continuously transferred and may be collected in a second fluid.

Abstract: The present invention provides methods and apparatuses for the continuous processing and solids handling in near-critical and supercritical fluids. The present invention also allows for treatment of the starting material with the near-critical or supercritical fluid. The remaining raffinate is then continuously transferred and may be collected in a barrier fluid.

Abstract: Supercritical carbon dioxide extraction of corn germ oil from corn germ utilizing extraction conditions adapted to a dry corn fractionation ethanol production process.

Abstract: The invention relates to a method for producing a margosa extract, an oil from cores and/or seeds of the neem tree being used and the oil being extracted using a carbon dioxide-containing extracting agent. The invention further relates to a margosa extract as is obtained using the method, its use as an agent for pest control and a composition for pest control which contains this extract.

Abstract: Soybean oil is extracted by a two-stage process in which up to 85%, preferably from about 60 to about 75%, of the soybean oil in soybeans is extracted by mechanical or solvent extraction to produce first extracted oil and oil-containing meal. The first extracted oil is then refined by caustic or physical refining. Substantially all of the oil remaining in the meal is extracted by solvent extraction to produce second extracted oil and substantially oil-free meal. The second extracted oil may be transesterified for use in biodiesel fuel.

Abstract: A solvent extraction free, caustic refining free, process for producing refined vegetable oils, including soybean oil, cottonseed oil, rapeseed oil, and canola oil, is described in which the vegetable seeds, after cleaning, cracking and dehulling, are heated and mechanically pressed to separate oil. Free fatty acids are then removed from the pressed oil through physical refining, instead of previously employed caustic refining, since the low level of nonhydratable phospholipids does not create undesirable flavors during the physical refining process. The resultant oil exhibits a significantly greater frylife than non-hydrogenated vegetable oil produced by solvent extraction and caustic refining.

Abstract: Generally, a method of pressure regulated supercritical fluid fractionation of oil seed extraction materials which can be utilized to refine oil seed extraction material established in an amount of supercritical fluid. Specifically, a method of pressure regulated supercritical fluid fractionation of corn germ extraction material to produce a refined corn oil extraction material.

Abstract: Supercritical carbon dioxide extraction of corn germ oil from corn germ utilizing extraction conditions adapted to a dry corn fractionation ethanol production process.

Abstract: A process for continuously extracting oil from a solid or liquid oil-bearing material comprises (a) removing air from the extraction system, (b) introducing an inert gas into the extraction system at a pressure sufficient to maintain a normally gaseous solvent in liquid state, (c) introducing an oil-bearing material into a silo, (d) passing the oil-bearing material from the to a jet pump mixing device, (e) introducing a liquified normally gaseous solvent into the jet pump mixing device, (f) mixing the oil-bearing material and the solvent in the jet pump mixing device for a time sufficient to permit complete wetting of oil-bearing material by the solvent to form a mixture, (g) heating the mixture to near supercritical conditions; (h) passing the mixture through an extractor having a screw conveyor adapted to rotate at a first rpm range and a centrifugal drum adapted to rotate at a second rpm range, (i) treating the mixture within the extractor in such a manner that supercritical temperature and pressure are at

Abstract: The present invention provides a method for extracting carotenoids from green plant materials using supercritical fluid extraction. A first and second supercritical fluid extraction is performed on the green plant composition at two different pressures to obtain two extracts. The first extract includes substantial amounts of ?-carotene. The second extract may have a controlled concentration of ?-carotene, and includes substantial amounts of lutein.

Abstract: The invention provides methods for separating outer birch bark from inner birch bark. The invention also provides methods for isolating betulin; lupeol; betulinic acid; 9,10-epoxy-18-hydroxyoctadecanoic acid; 9,10,18-trihydroxyoctadecanoic acid; polyphenolic polymers and fatty acids from birch bark.

Abstract: The invention concerns a method for fractionating cooking oil, in particular frying oil, using a solvent with supercritical pressure. The method is characterized in that it comprises steps which consist in: contacting, in a mixer, the cooking oil with the solvent with supercritical pressure; separating the resulting mixture into two phases in a decanter, namely a light phase and a heavy phase; decompressing the light phase and the heavy phase so as to recuperate the solvent, and the treated oil and the treatment residues respectively.

Abstract: The invention provides a kernel oil extracted from plant kernels, comprising triglyceride 90-99.9%, diglyceride 0.01-5%, monoglycerides 0.01-3%, sitosterol 0.1-2.5% and cyclolanosterol 0.01-1%. The invention also provides two methods for the extraction of said kernel oil, the pharmaceutical compositions and the uses thereof.

Abstract: The present invention provides a method for extracting carotenoids from green plant materials using supercritical fluid extraction. A first and second supercritical fluid extraction is performed on the green plant composition at two different pressures to obtain two extracts. The first extract includes substantial amounts of &bgr;-carotene. The second extract is substantially free of &bgr;-carotene, and includes substantial amounts of lutein.

Abstract: Process for high pressure extraction of organic products from vegetable or animal matrices or extracts thereof wherein the process is carried out in the presence of one or more liquid solvents and one or more supercritical fluids wherein the proportion of the supercritical fluid is less than 50% by weight of the total weight of the solvent and the supercritical fluid.

Abstract: A process of treating sesame oil to obtain sesame lignans and flavors contained in the oil in higher purity and yield is provided. In the process, the sesame oil is subjected to a supercritical extraction.

Abstract: A process for removing oil from oil-bearing material at substantially atmospheric pressure and are relatively low temperatures. The preferred temperature is the boiling point of the solvent, particularly a normally gaseous solvent, at about atmospheric pressure. This temperature will typically be below the freezing point of water.

Abstract: A process for separating oil from a lubricant composition containing solid particles. The contaminated lubricant composition is mixed with liquid or supercritical CO.sub.2 before the lubricant composition and CO.sub.2 mixture is filtered through a filter medium. The CO.sub.2 is then evaporated, leaving an oil residue. Mixing the lubricant composition with CO.sub.2 before filtration prevents the filter medium from being blinded by solid particles.

Abstract: A method of extracting from an oil bearing product at below a select temperature. The method includes providing an oil bearing product at a temperature at or below the select temperature. A liquid extraction solvent that is a gas under standard temperature and pressure is provided, with the extraction solvent being maintained at a temperature below its boiling point at ambient pressure and below the select temperature and at substantially ambient pressure. The oil bearing product is contacted with the extraction solvent at ambient pressure for a period sufficient to extract a select amount of the oil from the oil bearing product resulting in a reduced oil content product and an oil bearing extraction solvent.

Abstract: A device for the production of oils by pressing and extracting a raw material containing oleiferous or extractable substances in the presence of a liquid or supercritical extraction agent. The device includes an inlet for said raw material, a substantially cylindrical pressing body having outlets for oils and being connected to said inlet, and a press screw movably provided in said cylindrical pressing body whereby said raw material is transported from said inlet into said pressing body and therefrom to a discharge outlet while being pressed. In addition, the pressing body is proof-sealed against its surroundings by a jacket and the press screw and/or the pressing body include outlets wherethrough a liquid extraction agent may be introduced into said raw material present in said pressing body. At the outlet of said pressing body, a pipe permitting degassing of the press cake discharged from the press by applying a vacuum, thus removing the solvent from it, may be provided.

Abstract: Carrier compounds, compositions, and dosage unit forms therefor which are useful in the delivery of active agents are provided. The present invention provides a compound having the formula: ##STR1## or a salt thereof, wherein the compound may be used in a composition or dosage unit form for delivery of at least one active agent, including a peptide, mucopolysaccharide, carbohydrate, or a lipid. Methods of administration and preparation of the compounds and compositions of the invention are provided as well, including oral administration. Further, the compositions of the invention may be prepared by mixing at least one active agent, at least one carrier compound, and, optionally, a dosing vehicle.

Abstract: An oil extractable from corn fiber contains ferulate esters, in particular sitostanyl ester, which has been shown to have cholesterol-lowering activity. The oil is extracted by a novel process which includes a grinding step carried out before extraction with an effective organic solvent such as hexane. The corn fiber oil may be combined with an ingestible and/or edible carrier for administration as a dietary supplement for cholesterol-lowering purposes.

Abstract: Disclosed is a process for the fractionation of wool wax acid mixtures by dissolving the starting material in a polar organic solvent (mixture). The dissolved wool wax acid mixture is treated at a temperature between -5 and 30.degree. C. and at a pressure between 10 and 70 bar with gaseous carbon dioxide and the hydroxy-fatty acids that accumulate as a solid are separated from the solution.

Abstract: The invention relates to a process for extracting oil from an oil bearing plant material with the use of a solvent suitable for dissolving the oil in the plant material. Grounded plant material is deposited into a reactor vessel, and vacuum is created in the reactor vessel. Liquid solvent is introduced into the reactor vessel and allowed to contact the plant material for a time sufficient to dissolve oil from the plant material, while the temperature in the reactor vessel is maintained at a level which prevents denaturing of constituent components of the plant oil and the plant material. Additional solvent vapors are introduced into the bottom of the reactor to cause mixing of the plant material and the solvent and separate fine particulate matter from heavier particles. Pressurized heated solvent vapors are introduced into the top of the reactor vessel while the liquid solvent and oil combination is being removed from the bottom of the reactor vessel through filters.

Abstract: A process for preparing nuts, particularly peanuts, of reduced calorific value by partially extracting oil from the nut kernels by extraction with supercritical carbon dioxide. The process involves pretreatment of the kernels, including their humidification and optional microwaving. The pretreatment and the extraction steps are optimized with a view to removing maximum amounts of high-calorie substances without losing the organoleptic qualities of the nuts. The process produces virtually unbroken peanut kernels.

Abstract: An extraction process comprising contracting a material to be extracted with an extracting fluid at elevated pressure within a defined space, and separating the extracted fluid and extract as a mass, from the extracted material while reducing the volume of the defined space and while maintaining the elevated pressure within the defined space. Apparatus for carrying out the process is adapted to separate the extracting fluid and the extract, as a mass, from the extracted material, while maintaining elevated pressure and reducing the volume as the point of separation.

Abstract: An improved low temperature process for extracting oil from oil-bearing materials by extracting the oil-bearing material in an extraction zone with a normally gaseous solvent selected from propane, butane, and mixtures thereof. As the resulting solvent/oil mixture is passed through the bed of extracted oil-bearing material, from the extraction zone, and to a separation zone, it is done so under conditions that will maintain the solvent in liquid form. The resulting extracted materials have substantially more of their protein and vitamin value intact when compared with similar materials extracted by more conventional high temperature methods. The present process is also a lower energy consuming process than more conventional, extractive processes.

Abstract: The present invention is directed toward a process for extracting compounds from plant material, comprisinga) contacting hydrolyzed plant material with a supercritical fluid and optionally with a co-solvent and p1 b) recovering the compound from the supercritical fluid.In another embodiment, the present invention is directed toward a process for removing a compound from plant material, comprising contacting the plant material with an acid, a supercritical fluid and a co-solvent, and recovering the compound from the supercritical fluid. The sterols, diosgenin and sarsapogenin, are efficiently extracted from barbasco root and Yucca seed, respectively.

Abstract: A process for the extraction of oils from oil-containing solid vegetable material by means of compressed gases, wherein said vegetable material is extracted with a mixture consisting of a supercritical gas and a subcritical entraining agent selected from the group consisting of propane, butane, pentane, ethanol, ethyl acetate, formaldehydedimethylacetal, CHF.sub.

Abstract: The present invention is drawn to a process for extraction of gossypol for cottonseed using a solvent solution which includes: (a) a water miscible organic solvent; (b) water; and (c) an acid which is strong enough to prevent binding of gossypol to cottonseed protein but which is not so strong as to hydrolyze a substantial portion of the cottonseed protein. The present invention also includes cotton seed meals of reduced gossypol content (and optionally reduced aflatoxin and/or fat content) produced by the aforementioned extraction.