Abstract: This invention relates to an improved process for the continuous production of 2-phosphonobutane-1,2,4-tricarboxylic acid (PBTC) and alkali metal salts thereof, in which dialkylphosphite, and ethene-1,2-dicarboxylic acid dialkyl ester, are reacted in the presence of a basic catalyst to form phosphonosuccinic acid tetraalkyl ester, the ester thus obtained is directly reacted with alkyl-acrylate, in the presence of an alkaline catalyst and the reaction product thus obtained is directly hydrolyzed to PBTC or alkali metal salts thereof.
Type:
Grant
Filed:
August 16, 1989
Date of Patent:
June 5, 1990
Assignee:
Bayer Aktiengesellschaft
Inventors:
Roland Kleinstuck, Cornelia Lensch, Michael Immenkeppel, Hans-Dieter Block, Herbert Odenbach