Abstract: A system and method for argon and nitrogen extraction and liquefaction from a low-pressure tail gas of an ammonia production plant is provided. The preferred tail gas of the ammonia production plant comprises methane, nitrogen, argon, and hydrogen. The disclosed system and method provides for the methane rejection via rectification and hydrogen rejection by way of a side stripper column or phase separator. The resulting nitrogen and argon containing stream is separated and liquefied in a double column distillation system.

Abstract: The present invention relates to a method for liquefying hydrogen, the method comprises the steps of: cooling a feed gas stream comprising hydrogen with a pressure of at least 15 bar(a) to a temperature below the critical temperature of hydrogen in a first cooling step yielding a liquid product stream. According to the invention, the feed gas stream is cooled by a closed first cooling cycle with a high pressure first refrigerant stream comprising hydrogen, wherein the high pressure first refrigerant stream is separated into at least two partial streams, a first partial stream is expanded to low pressure, thereby producing cold to cool the precooled feed gas below the critical pressure of hydrogen, and compressed to a medium pressure, and wherein a second partial stream is expanded at least close to the medium pressure and guided into the medium pressure first partial stream.

Abstract: A process for recovery of C2 and C3 components in an on-purpose propylene production system includes utilizing a packed rectifier with a countercurrent stream to strip C2 and C3 components from a combined de-ethanizer overhead lights vapor and cracked gas vapor stream.

Abstract: A system and method for removing nitrogen from an intermediate stream in a gas subcooled process operation that processes natural gas into a sales gas stream and a natural gas liquids stream. The system and method of the invention are particularly suitable for use with gas subcooled process operations where the sales gas stream exceeds pipeline nitrogen specifications by up to about 3%, such as for reducing the nitrogen content of sales gas streams to levels permissible for pipeline transport.

Abstract: Helium can be recovered from nitrogen-rich natural gas at high pressure with low helium loss by cryogenic distillation of the natural gas after pre-treatment of the gas to remove incompatible impurities and then recovery of natural gas liquid (NGL) from the pre-treated gas by distillation. Overall power consumption may be reduced, particularly if the feed to the helium recovery column system is at least substantially condensed by indirect heat exchange against a first portion of nitrogen-enriched bottoms liquid at first pressure, and a second portion of nitrogen-enriched bottoms liquid at a second pressure that is different from the first pressure.

Abstract: A cryocooler-based gas scrubber, or cryocooler-based gas purifier, utilizes the cooling power of a cryocooler to cool and condense cryogen gas forming coalesced impurities which are then filtered through a filter matrix, such as for example a fiberglass filter matrix. The scrubber may further comprise a counter-flow heat exchanger for warming the purified gas prior to dispensing at an outlet for storage or consumption.

Abstract: A system and method for removing nitrogen from an intermediate stream in a gas subcooled process operation that processes natural gas into a sales gas stream and a natural gas liquids stream. The system and method of the invention are particularly suitable for use with gas subcooled process operations where the sales gas stream exceeds pipeline nitrogen specifications by up to about 3%, such as for reducing the nitrogen content of sales gas streams to levels permissible for pipeline transport.

Abstract: A method for producing liquid natural gas (LNG) includes the following steps. Compressor stations forming part of existing natural-gas distribution network are identified. Compressor stations that are geographically suited for localized distribution of LNG are selected. Natural gas flowing through the selected compressor stations is diverted to provide a high pressure first natural gas stream and a high pressure second natural gas stream. A pressure of the first natural gas stream is lowered to produce cold temperatures through pressure let-down gas expansion and then the first natural gas stream is consumed as a fuel gas for an engine driving a compressor at the compressor station. The second natural gas stream is first cooled with the cold temperatures generated by the first natural gas stream, and then expanded to a lower pressure, thus producing LNG.

Abstract: A system and method for removing nitrogen from an intermediate stream in a gas subcooled process operation that processes natural gas into a sales gas stream and a natural gas liquids stream. The system and method of the invention are particularly suitable for use with gas subcooled process operations where the sales gas stream exceeds pipeline nitrogen specifications by up to about 3%, such as for reducing the nitrogen content of sales gas streams to levels permissible for pipeline transport.

Abstract: The invention relates to a method and an installation for producing liquid helium, said installation comprising a cooling/liquefaction device comprising a working circuit that subjects a helium-enriched working fluid to a thermodynamic cycle in order to produce liquid helium, said circuit comprising at least one working fluid compression body and a plurality of heat exchangers. The installation also comprises a plurality of fluid recovery lines having respective upstream ends to be selectively connected to respective reservoirs, and a first collection line having an upstream end connected to the recovery lines and a downstream end connected to a receiving body that can supply the working circuit with a working fluid.

Abstract: A helium recovery plant adapted to filter, compress, and purify helium gas collected from one or more helium-using instruments, as well as to liquefy and redistribute the purified gas within a closed system. The recovery plant is adapted to match the purification and liquefaction rate of the system with the consumption rate of the coupled instruments. Additionally, the recovery plant is adapted to match the liquefaction rate of a liquefaction module with a boil-off rate of liquid helium within a Dewar thereof. The recovery plant is further adapted to recycle helium therein in an effort to achieve zero loss.

Abstract: A vertical support rigidly mounted to a planar base positions and supports a cryocooler expander unit off axis and away from a sample to be examined. The sample support is likewise rigidly mounted to the planar base with a rigidly mounted sample housing therein. The cryocooler expander unit is suspended in the vertical support by spring dampening bearings. A pair of opposing flexible vacuum bellows connects the cryocooler expander unit to the sample housing and vertical support. This configuration isolates the sample from vibration. Flexible thermal links associated with an predictive electronic closed loop control sequence maintains sample temperature.

Abstract: A method is described for separating off trace components from a fraction (1) containing at least nitrogen and helium, wherein this fraction is partially condensed (E) before enrichment of the helium. The partially condensed fraction (2) is fed at least in part to at least one separation column (T) and separated therein into a helium-rich gas fraction (6) and a nitrogen-rich liquid fraction which also contains the unwanted trace components (5).

Abstract: A system and method for recovering helium-3 from helium. A distillation column having a top section that is smaller in diameter than a main section is provided. The column also includes an intermediate condenser that condenses vapor from the main section and above a helium feed stream. Reflux to the column can be provided by liquid helium-3 from a conduit or from an overhead condenser. In a preferred cycle, the distillation column is operated at a subatmospheric pressure, and in a temperature range between 2.3 K and 4.3 K.

Abstract: A system and method for recovering helium-3 from helium. A distillation column having a top section that is smaller in diameter than a main section is provided. The column also includes an intermediate condenser located in the main section and above a helium feed stream. Reflux to the column can be provided by liquid helium-3 from a conduit or from an overhead condenser. In a preferred cycle, the distillation column is operated at a subatmospheric pressure, and in a temperature range between 2.3 K and 4.3 K.

Abstract: A process is described for producing a clean gas, which is provided, in particular, for testing a pressurized construction component (100) for leaks, which process includes the steps of providing a liquefied gas mixture (1) which contains the clean gas (2) and at least one foreign gas (3) in a gas separation unit (20), enriching the clean gas (2), wherein the at least one foreign gas (3) is transferred to a surface region of the liquefied gas mixture (1), and taking off the enriched clean gas (2), wherein the enriched clean gas (2) flows out of a volume region of the gas separation unit (20) via a guide unit (22), and wherein a foreign gas barrier (23) is formed at the guide unit (22), using which the foreign gas (3) in the liquefied gas mixture (1) is passed out from an opening in the guide unit (22). A device for producing a clean gas, a noble-gas-free gas composition and a process for testing a construction component pressurized with a test gas for leaks are also described.

Abstract: Systems and methods are provided for recovering helium from a feed comprising helium, carbon dioxide, and at least one intermediate component having a volatility between those of helium and carbon dioxide. In particular, processes of the present invention comprise separating the carbon dioxide and the components of intermediate volatility from the helium at a temperature greater than ?82.7° C. to form a helium-rich product stream, wherein the concentration of at least one of the intermediate components in the helium-rich product stream is lower than its concentration in the feed stream, and wherein at least part of the separation is effected by contacting a vapor with a liquid.

Abstract: A system and method for recovering helium-3 from helium. A distillation column having a top section that is smaller in diameter than a main section is provided. The column also includes an intermediate condenser that condenses vapor from the main section and above a helium feed stream. Reflux to the column can be provided by liquid helium-3 from a conduit or from an overhead condenser. In a preferred cycle, the distillation column is operated at a subatmospheric pressure, and in a temperature range between 2.3 K and 4.3 K.

Abstract: Methods of reducing the concentration of low boiling point components in liquefied natural gas are disclosed. The methods involve dynamic decompression of the liquefied natural gas and one or more pre-fractionation vessels. Particular embodiments are suited for recovering helium and/or nitrogen enriched streams from a liquefied natural gas stream.

Abstract: A process for simultaneous recovery of a pure helium and a pure nitrogen fraction from a feed stream containing at least methane, nitrogen and helium, is disclosed. The feed stream is partially condensed and separated into a helium-rich gas fraction and a nitrogen- and methane-rich liquid fraction. The helium-rich gas fraction is conveyed to a purification stage in which a pure helium fraction is recovered by adsorption, permeation and/or rectification. At least one partial stream of the nitrogen- and methane-rich liquid fraction is taken to a rectification process for recovery of a pure nitrogen fraction.

Abstract: A method of separating one or more first light components from a carbon dioxide containing gaseous mixture that contains at least 30 mole percent carbon dioxide. In accordance with the method, a feed stream composed of the carbon dioxide is cooled to effect at least in part, liquefaction of the carbon dioxide containing gaseous mixture. The feed stream and a stripping gas stream are introduced into a liquid-vapor contact column to initiate counter-current vapor liquid mass transfer and the formation of a gaseous column overhead stream and a liquid column bottoms stream. The stripping gas stream contains one or more second light components having boiling point lower than that of carbon dioxide and higher than that of the first light component(s) to enrich the gaseous column overhead stream with the first light component(s).

Abstract: The present invention relates to a process and apparatus for producing crude helium, liquefied natural gas product, and synthesis gas from natural gas. A natural gas comprising helium and methane is cooled to produce cooled natural gas. At least a portion of the helium and methane from the cooled natural gas is separated into a vapor comprising helium, from which crude helium is derived, and a liquid comprising methane. At least a portion of the methane from this liquid is separated into a vapor, which is reacted to produce synthesis gas, and a liquid, from which liquefied natural gas is derived. Additional heat exchange and separation steps may be included.

Abstract: A cryogenic flow valve system for controlling the flow of a cryogenic fluid is disclosed. The system has a valve and an adsorption pump. The valve includes a flow chamber and a moveable member. The cryogenic fluid flows the flow chamber, and the moveable member is in contact with a control fluid. The position of the moveable member controls the flow in the flow chamber. The pressure of the control fluid controls the position of the moveable member. The adsorption pump includes a chamber and a heater. The chamber is in contact with the moveable member and contains an adsorption material for retaining control fluid. The heater heats the adsorption material to control the pressure of the control fluid.

Abstract: A method of separating one or more light components, such as helium, from a carbon dioxide containing stream. A two-phase stream is obtained, at least in part, by cooling a pressurized feed stream to at least partially condense such stream. The stream that is subsequently degassed to produce a first vapor stream enriched in the light component(s) and a first liquid stream containing an entrained fraction of the light component(s). The first liquid stream is expanded to create another two-phase stream that is degasified to produce a second vapor stream that is also enriched in the light component(s) and a second liquid stream having an enriched carbon dioxide content. The second liquid stream is repressurized and vaporized. In case of a supercritical feed, the pressurized feed stream is expanded after having been cooled. Thereafter, the feed is degassed to produce the light component enriched vapor stream and a liquid stream enriched in the carbon dioxide.

Abstract: This invention is directed to a three-stage process for recovering and purifying a helium gas, and a system for using the three-stage process. The steps comprise a) introducing a gas from a cold spray forming chamber to a particulate removing apparatus to form a particulate-free helium gas, and recycling a first portion of the particulate-free helium gas back to the chamber; b) passing a second portion of the particulate-free helium gas to a first compressor prior to passing a helium gas purification membrane to form a purified helium gas and an exhaust gas, and passing the purified helium gas to mix with the first portion of particulate-free helium gas to the chamber; and c) passing a third portion of the particulate-free helium gas to a liquid separator apparatus to remove water and a receiver to dampen any pulsations to form a liquid-free helium gas, and recycling the liquid-free helium gas to said cold spray forming chamber.

Abstract: An improved method for loading propellants into separate tanks on a reusable launch vehicle (RLV) uses three innovative methods. The liquid loading provides three liquid transfer methods, integrated and coordinated to provide less complicated loading and unloading operations, transfers, and cools and controls the liquids to provide a safe, cost effective solution to reusable vehicle tanking and de-tanking under commercial conditions. To insure the density of the propellant is maximized by cooling in a quick liquid loading environment, pre-cooling may be used.

Abstract: The invention concerns a method which consists in cooling the feed mixture, and introducing it in the vessel of a distillation column (3), partly condensing (in 4) the column head gas, cooling (in 5) the resulting gas phase so as to condense it partly, and recuperating as impure helium the gas phase resulting from that second condensation. Additionally at least a liquid is produced through a closed refrigerating cycle (8) with variable flow-rate. The invention is useful for producing helium and liquid nitrogen from a natural gas liquefying residue gas.

Abstract: The invention concerns a method and an installation for purifying impure helium. Said method consists in subjecting the helium to at least two successive steps: (a) cryogenic refrigeration of impure helium so as to eliminate by condensation at least part of the main impurities it contains and recuperating helium with intermediate purity containing residual impurities; and (b) permeation of at least part of the helium with intermediate purity derived form step (a) so as to eliminate at least part of said residual impurities and recuperating helium with final purity higher than said intermediate purity. Said method and said installation are useful for purifying impure helium recuperated at the output of an optical fibre cooling chamber, prior to the reintroduction of the resulting purified helium into said chamber so as to recycle the helium.

Abstract: Methods and apparatus for cooling an object using a heat transfer fluid are presented. One of the methods comprises the steps of contacting the object with a heat transfer fluid comprising helium as a major component, the object traversing through a heat exchange unit having an object inlet end and an object outlet end; preventing ingress of contaminants into the heat exchange unit inlet end and outlet end using a seal gas, the seal gas exiting with the heat transfer fluid to form an exit gas; compressing the exit gas to form a compressed recycle gas; routing the compressed recycle gas to a gas-liquid separator, thus forming a helium enriched gas which function as the heat transfer fluid and an enriched liquid; and heating the enriched liquid to form the seal gas.

Abstract: A method of producing high-purity helium, which contains the step of: producing high-purity helium of 99.99 mol % or higher, by a process in which crude helium having a helium concentration of 40 to 90 mol % is, at least, permeated through a separation membrane module composed of a plurality of glass hollow fiber membrane.

Abstract: A method and apparatus for the recovery of Helium3 (He-3) from ilmenite ore (iron titanate or FeTiO3), including recovery from the surface and near surface of a satellite such as the Moon, and extraction using solar energy and the natural rotational cycles of the satellite for the purpose of obtaining the He-3 for use in nuclear reactors for generation of pollution-free electrical power for commercial or industrial uses, as a fuel to propel space vehicles, and for other purposes, such as medical use.

Abstract: The present invention relates to a quantitative measuring method of argon impurity contained in high purity oxygen by means of triple point and &ggr;-&bgr; phase transition of oxygen, and also to a cryostat employed in quantitative measuring of argon impurity contained in high purity oxygen.

Abstract: Helium recycling for optical fiber manufacturing in which consolidation process helium is recycled either directly for use in consolidation at high purity or recycled at lower purity adequate for usage in draw or other processes having a lower helium parity. Integrated processes for recycling helium from two or more helium using processes in the optical manufacturing process are also described. Substantial helium and cost savings are recognized.

Abstract: A process is disclosed to remove a high-volatility component, such as nitrogen, from a feed stream rich in methane to produce a product substantially free of the high-volatility component. The feed stream is expanded and fed to a phase separator which produces a vapor stream and a liquid stream. The vapor stream is enriched in the volatile component. The liquid stream, which is lean in the volatile component and rich in methane, is pumped to a higher pressure and heated to produce a pressurized liquefied product stream having a pressure sufficient for the product stream to be at or below its bubble point and having a temperature above about −112° C. (−170° F.).

Abstract: Plant for supplying helium to a plurality of production lines, comprising a helium source of at least 7000 liters; a network of secondary ducts, feeding production lines using helium gas; and a main duct for conveying helium, connected upstream to the helium source and downstream to the network of secondary ducts. Such a plant is useful in a filling operation for diving gas cylinders, dirigible airship gas bags or safety airbag inflation containers, for quenching metal articles, or for fabricating electronic products or optical fibers.

Abstract: A process and a system for producing helium from a helium-bearing feed gas that is purified in a cryogenic processing unit to produce cryogenic crude helium containing at least 10% helium. The cryogenic crude helium is directly introduced into a thermal swing helium refinery where it is refined. Refrigeration is supplied to the refinery by the cryogenic crude helium from the cryogenic processing unit.

Abstract: The production of higher purity helium wherein a feed comprising helium, nitrogen and hydrocarbons is processed in a system comprising two columns operating at different pressure levels, with the product helium produced in the higher pressure column and nitrogen and hydrocarbons cycled to the lower pressure column.

Abstract: An apparatus and method for the cryogenic purification of gaseous mixtures is provided. The apparatus comprises a heat-insulated hermetically sealed vessel which contains liquid hydrogen. Immersed within the liquid hydrogen are a number of serially connected cartridges which contain chips of a thermally conductive mixture. A mixture of neon and helium is input into the apparatus. The neon freezes, while the helium passes through the apparatus in a gaseous state. The resulting neon is allowed to thaw into a liquid or gaseous form and is highly pure.